#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:53:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181115 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/95/2219512.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219512_Fobs loop_ _publ_author_name 'Wardell, James L.' 'Harrison, William T. A.' _publ_section_title ; Diaquatetrachloridotin(IV)--diglyme (1/2) ; _journal_coeditor_code BT2792 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1297 _journal_volume 64 _journal_year 2008 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4023 _cell_length_b 17.1528 _cell_length_c 15.9612 _exptl_crystal_F_000 1144.00 _reflns_d_resolution_high 0.7684 _cod_data_source_file bt2792Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JIM 1640 SOTON DATA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 347.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10675.31 9657.46 133.80 o 4 0 0 33200.94 33548.96 484.02 o 6 0 0 15663.63 16296.68 279.78 o 8 0 0 4900.92 5077.28 183.05 o 10 0 0 1879.86 2071.78 115.11 o 3 1 0 26851.43 26663.03 244.11 o 5 1 0 13304.88 13617.35 154.95 o 7 1 0 1249.31 1311.01 50.03 o 9 1 0 11.86 65.38 26.81 o 2 2 0 1510.84 1802.98 24.08 o 4 2 0 15891.02 16277.83 179.44 o 6 2 0 4286.70 4472.81 74.75 o 8 2 0 2137.15 2211.64 116.24 o 10 2 0 2460.76 2562.80 135.38 o 1 3 0 32591.73 30356.36 773.76 o 3 3 0 23440.94 23250.55 226.33 o 5 3 0 8759.81 9163.39 123.53 o 7 3 0 15460.93 15883.19 318.77 o 9 3 0 509.63 402.02 40.96 o 0 4 0 27838.88 27228.83 910.12 o 2 4 0 216.47 190.75 7.75 o 4 4 0 1074.27 937.39 24.31 o 6 4 0 2767.42 2793.48 50.42 o 8 4 0 1628.09 1550.80 70.82 o 10 4 0 631.15 699.96 63.03 o 1 5 0 351.44 360.18 11.31 o 3 5 0 247.52 224.11 10.34 o 5 5 0 35.55 31.92 10.42 o 7 5 0 9088.45 9267.17 158.64 o 9 5 0 277.26 210.41 36.49 o 2 6 0 45.75 20.67 4.45 o 4 6 0 18250.71 17928.36 190.94 o 6 6 0 6530.61 6431.80 151.02 o 8 6 0 7898.55 7934.25 174.11 o 10 6 0 4764.27 5062.63 146.24 o 1 7 0 1326.99 1215.07 16.45 o 3 7 0 1011.22 968.01 22.35 o 5 7 0 64.29 74.62 9.96 o 7 7 0 7256.40 7613.06 133.21 o 9 7 0 1917.00 1891.80 74.93 o 0 8 0 24979.25 23981.80 682.02 o 2 8 0 2967.54 2973.82 35.43 o 4 8 0 9621.73 9285.75 103.52 o 6 8 0 59.22 66.57 13.03 o 8 8 0 1702.52 1710.94 64.01 o 10 8 0 131.35 103.51 40.80 o 1 9 0 41414.84 41731.32 778.24 o 3 9 0 32402.24 32419.04 313.16 o 5 9 0 2599.54 2654.67 52.58 o 7 9 0 19519.57 20175.60 322.82 o 9 9 0 181.87 158.91 29.86 o 0 10 0 2763.38 2447.40 111.42 o 2 10 0 11069.66 11381.69 140.94 o 4 10 0 9982.79 10354.03 116.69 o 6 10 0 3398.04 3586.52 68.97 o 8 10 0 863.68 855.80 63.92 o 1 11 0 5177.50 5170.90 112.17 o 3 11 0 14414.77 14738.09 198.76 o 5 11 0 425.04 435.64 18.15 o 7 11 0 3727.91 3633.93 97.37 o 9 11 0 144.89 204.22 50.59 o 0 12 0 44417.48 44704.47 1466.02 o 2 12 0 11895.91 11771.76 197.81 o 4 12 0 29089.25 29678.02 373.70 o 6 12 0 2725.00 2663.76 71.89 o 8 12 0 3895.04 4083.36 127.84 o 1 13 0 19820.48 19505.64 522.51 o 3 13 0 1702.75 1767.74 46.51 o 5 13 0 3864.43 4030.70 79.72 o 7 13 0 1077.95 1112.46 60.51 o 0 14 0 11161.12 11140.04 401.31 o 2 14 0 911.25 910.63 27.33 o 4 14 0 1217.68 1171.02 47.11 o 6 14 0 785.41 725.79 57.54 o 8 14 0 2143.03 1986.66 94.90 o 1 15 0 444.60 456.35 42.51 o 3 15 0 2815.79 2956.80 105.40 o 5 15 0 5344.00 5504.74 180.32 o 7 15 0 6026.67 6379.70 228.47 o 0 16 0 2674.07 2719.27 126.01 o 2 16 0 1216.74 1189.05 62.19 o 4 16 0 318.39 330.24 35.38 o 6 16 0 412.14 467.31 37.68 o 1 17 0 2088.95 2163.17 104.34 o 3 17 0 1255.01 1298.78 65.20 o 5 17 0 2.24 10.22 20.32 o 7 17 0 2205.23 2192.32 131.64 o 0 18 0 7333.00 7726.94 370.13 o 2 18 0 262.67 318.12 41.62 o 4 18 0 4651.96 4668.75 249.62 o 6 18 0 5636.96 5855.51 300.22 o 1 19 0 584.53 456.38 48.78 o 3 19 0 1838.10 2001.20 156.48 o 5 19 0 2253.36 2158.02 231.54 o 0 20 0 7558.31 7826.97 637.42 o 2 20 0 635.83 512.24 80.97 o 4 20 0 5312.67 5724.99 483.92 o 1 21 0 13146.92 13181.15 577.07 o 3 21 0 6725.10 7438.71 455.14 o 0 22 0 1819.87 1742.83 156.01 o 2 1 1 3158.39 3015.09 25.51 o 3 1 1 66840.41 67666.15 448.86 o 4 1 1 9269.24 9653.39 70.12 o 5 1 1 2651.81 2609.71 34.35 o 6 1 1 145.57 128.82 10.75 o 7 1 1 19226.45 19100.50 212.04 o 8 1 1 0.54 -3.41 16.47 o 9 1 1 294.47 307.63 24.63 o 10 1 1 173.57 98.34 29.66 o 1 2 1 2802.53 2662.62 66.89 o 2 2 1 27079.93 26869.00 195.80 o 3 2 1 2750.42 2717.67 27.37 o 4 2 1 53930.51 55843.34 366.01 o 5 2 1 31.31 28.68 8.80 o 6 2 1 1889.68 1773.28 33.32 o 7 2 1 993.87 937.70 30.63 o 8 2 1 5198.99 5324.34 98.25 o 9 2 1 373.02 373.32 32.70 o 10 2 1 2258.77 2264.29 70.75 o 1 3 1 10419.21 10566.15 84.25 o 2 3 1 4983.28 5083.28 41.85 o 3 3 1 406.18 427.35 10.61 o 4 3 1 2018.14 2178.76 29.14 o 5 3 1 89.94 103.16 8.90 o 6 3 1 407.16 338.14 12.70 o 7 3 1 19.38 23.60 15.96 o 8 3 1 27.19 -2.52 20.09 o 9 3 1 60.25 53.05 23.05 o 10 3 1 1.94 14.17 24.67 o 1 4 1 974.13 962.47 9.90 o 2 4 1 437.43 459.23 6.97 o 3 4 1 7.22 14.34 4.26 o 4 4 1 11339.59 11216.15 86.02 o 5 4 1 613.18 570.63 16.16 o 6 4 1 3397.24 3531.97 41.98 o 7 4 1 2052.19 2007.40 46.40 o 8 4 1 9795.73 10263.69 166.91 o 9 4 1 71.38 56.15 20.06 o 10 4 1 4392.21 4598.60 101.80 o 1 5 1 21.77 21.20 2.80 o 2 5 1 730.29 711.49 9.28 o 3 5 1 9619.29 9433.17 66.74 o 4 5 1 4490.46 4382.82 43.53 o 5 5 1 3490.98 3430.10 39.14 o 6 5 1 486.89 493.39 16.88 o 7 5 1 11658.69 11790.62 139.68 o 8 5 1 1617.70 1564.43 45.43 o 9 5 1 2136.63 2331.22 55.28 o 10 5 1 8.68 -19.45 35.12 o 0 6 1 3153.52 3084.24 54.38 o 1 6 1 67.31 67.29 3.07 o 2 6 1 2160.39 2084.91 18.98 o 3 6 1 1555.66 1666.27 17.10 o 4 6 1 12.91 32.23 6.57 o 5 6 1 18.44 14.99 7.97 o 6 6 1 46.67 37.13 10.40 o 7 6 1 455.43 458.24 26.11 o 8 6 1 29.56 50.29 18.91 o 9 6 1 138.49 160.49 22.96 o 10 6 1 32.58 37.61 24.71 o 1 7 1 6561.05 6364.12 55.35 o 2 7 1 2776.13 3095.58 24.90 o 3 7 1 18657.70 18639.68 121.40 o 4 7 1 548.33 574.41 10.86 o 5 7 1 3308.96 3319.41 34.37 o 6 7 1 1159.21 1157.56 24.22 o 7 7 1 8913.73 9153.89 122.17 o 8 7 1 280.23 272.56 23.76 o 9 7 1 628.23 648.70 45.43 o 10 7 1 35.79 29.64 25.91 o 0 8 1 36505.32 36342.40 718.64 o 1 8 1 665.59 719.35 12.79 o 2 8 1 990.65 898.70 11.41 o 3 8 1 342.55 394.03 10.90 o 4 8 1 15000.74 15266.73 107.79 o 5 8 1 135.98 113.28 8.26 o 6 8 1 6259.44 6470.21 72.08 o 7 8 1 1114.25 1048.51 23.43 o 8 8 1 5638.53 5995.50 103.73 o 9 8 1 150.71 150.00 23.64 o 10 8 1 3927.59 3962.84 118.13 o 1 9 1 2.30 12.55 3.13 o 2 9 1 254.41 261.26 6.59 o 3 9 1 164.47 144.01 7.67 o 4 9 1 501.97 496.44 12.16 o 5 9 1 383.51 409.81 11.10 o 6 9 1 26.65 37.67 9.50 o 7 9 1 11.58 19.19 12.94 o 8 9 1 13.82 24.62 19.58 o 9 9 1 883.03 874.76 43.41 o 0 10 1 87909.21 89231.37 1825.99 o 1 10 1 157.22 140.94 3.96 o 2 10 1 8000.48 8007.61 68.36 o 3 10 1 1037.77 1004.60 15.27 o 4 10 1 22684.37 23575.29 199.88 o 5 10 1 2027.87 2153.70 33.16 o 6 10 1 4646.60 4690.85 59.94 o 7 10 1 1273.65 1249.42 30.59 o 8 10 1 1819.31 1767.60 48.33 o 9 10 1 72.94 76.24 26.86 o 1 11 1 21179.84 20930.04 244.73 o 2 11 1 489.32 518.65 9.04 o 3 11 1 25604.29 26422.65 223.52 o 4 11 1 681.82 727.38 17.96 o 5 11 1 7943.45 8014.75 85.96 o 6 11 1 241.76 293.15 14.62 o 7 11 1 5516.67 5579.71 106.10 o 8 11 1 239.18 214.09 21.66 o 9 11 1 952.75 1044.33 78.13 o 0 12 1 389.36 399.36 61.62 o 1 12 1 7.01 2.26 5.71 o 2 12 1 3048.56 2994.70 40.46 o 3 12 1 493.41 467.80 13.09 o 4 12 1 341.00 309.74 13.95 o 5 12 1 1017.24 994.13 22.77 o 6 12 1 346.52 340.25 17.99 o 7 12 1 11.79 3.35 19.21 o 8 12 1 12.14 41.90 22.21 o 9 12 1 51.12 29.48 32.61 o 1 13 1 9855.05 9648.12 183.49 o 2 13 1 215.09 221.60 9.00 o 3 13 1 9664.72 9793.00 97.18 o 4 13 1 240.18 232.54 11.89 o 5 13 1 1197.83 1212.55 25.00 o 6 13 1 126.68 117.34 16.46 o 7 13 1 9179.69 9568.47 172.33 o 8 13 1 126.81 116.55 28.31 o 0 14 1 8530.87 8384.09 225.57 o 1 14 1 3803.56 3945.12 162.34 o 2 14 1 4614.57 4651.64 74.33 o 3 14 1 2.67 5.29 8.27 o 4 14 1 6613.88 6856.78 106.70 o 5 14 1 94.06 44.77 13.78 o 6 14 1 4328.29 4815.69 97.34 o 7 14 1 0.79 -1.31 18.72 o 8 14 1 2514.72 2592.13 75.51 o 1 15 1 361.87 349.68 25.29 o 2 15 1 353.31 354.68 13.33 o 3 15 1 107.61 94.09 9.61 o 4 15 1 467.75 429.80 17.66 o 5 15 1 459.90 466.57 29.99 o 6 15 1 78.25 78.19 19.60 o 7 15 1 832.20 845.76 54.25 o 8 15 1 223.44 175.01 51.08 o 0 16 1 1372.34 1531.72 63.37 o 1 16 1 721.79 736.69 35.69 o 2 16 1 172.42 147.43 13.49 o 3 16 1 145.52 145.16 11.53 o 4 16 1 7891.23 7913.08 174.29 o 5 16 1 678.94 600.43 34.02 o 6 16 1 692.13 682.52 32.73 o 7 16 1 453.80 454.40 32.57 o 1 17 1 2481.76 2462.39 71.56 o 2 17 1 585.19 565.76 34.65 o 3 17 1 1312.10 1345.32 50.16 o 4 17 1 11.86 -6.96 60.16 o 5 17 1 1437.27 1373.92 48.52 o 6 17 1 803.49 754.72 42.46 o 7 17 1 5242.56 5230.84 156.07 o 0 18 1 2117.32 2367.77 172.92 o 1 18 1 0.43 -16.87 16.87 o 2 18 1 91.68 90.94 31.34 o 3 18 1 300.16 268.22 34.46 o 4 18 1 136.56 151.45 27.54 o 5 18 1 338.92 307.42 40.68 o 6 18 1 528.52 519.87 42.17 o 1 19 1 3533.94 3573.96 117.13 o 2 19 1 0.14 -8.63 23.26 o 3 19 1 7186.94 7953.23 349.67 o 4 19 1 28.37 36.34 31.55 o 5 19 1 1374.19 1290.16 77.87 o 0 20 1 7238.93 7546.33 296.21 o 1 20 1 123.58 139.23 47.82 o 2 20 1 6549.42 6407.96 238.01 o 3 20 1 10.28 45.27 51.68 o 4 20 1 5144.56 5434.09 283.61 o 1 21 1 29.78 58.69 41.89 o 2 21 1 56.74 63.22 48.75 o 3 21 1 184.68 142.62 50.72 o 0 22 1 7867.93 7246.95 466.40 o 1 22 1 4.09 58.22 50.95 o 1 0 2 2470.53 2312.18 47.88 o 2 0 2 21702.92 21001.37 219.27 o 3 0 2 15445.05 15098.32 146.59 o 4 0 2 45060.63 44737.59 402.16 o 5 0 2 11816.96 12535.96 136.79 o 6 0 2 9871.81 10064.73 142.92 o 7 0 2 2740.54 2717.25 75.19 o 8 0 2 6767.75 7097.37 140.19 o 9 0 2 292.37 219.16 30.58 o 10 0 2 2694.93 2656.72 87.19 o 1 1 2 14448.06 13686.29 181.12 o 2 1 2 3004.51 2990.56 24.99 o 3 1 2 14425.17 14550.52 97.60 o 4 1 2 84.73 118.51 8.36 o 5 1 2 313.69 307.85 11.36 o 6 1 2 1929.51 1933.27 30.55 o 7 1 2 4361.24 4392.00 69.02 o 8 1 2 609.73 643.93 45.12 o 9 1 2 366.79 333.99 28.18 o 10 1 2 406.00 438.61 38.88 o 0 2 2 11519.80 10586.13 369.58 o 1 2 2 1172.62 1101.44 13.86 o 2 2 2 4567.22 4394.19 41.81 o 3 2 2 449.53 457.99 9.65 o 4 2 2 14320.43 14344.76 114.51 o 5 2 2 4639.92 4575.33 48.25 o 6 2 2 423.98 386.80 14.46 o 7 2 2 19.85 27.16 12.78 o 8 2 2 2699.49 2573.77 51.14 o 9 2 2 27.26 0.98 17.21 o 10 2 2 1196.78 1061.33 56.88 o 1 3 2 21142.39 20398.44 170.87 o 2 3 2 183.88 146.15 6.44 o 3 3 2 35984.21 35990.36 225.32 o 4 3 2 584.93 567.66 13.57 o 5 3 2 2976.19 2902.34 34.94 o 6 3 2 1048.73 1052.84 20.98 o 7 3 2 19196.98 19607.75 224.99 o 8 3 2 272.33 257.13 21.07 o 9 3 2 1760.94 1815.31 79.37 o 10 3 2 6.18 -7.25 20.47 o 0 4 2 18494.15 17908.17 316.47 o 1 4 2 3676.56 3585.89 29.92 o 2 4 2 274.31 257.65 6.15 o 3 4 2 147.67 161.85 6.58 o 4 4 2 5321.61 5206.37 48.52 o 5 4 2 4.98 7.02 6.79 o 6 4 2 4285.86 4443.08 50.03 o 7 4 2 1107.31 1088.23 28.27 o 8 4 2 1025.28 1014.21 30.01 o 9 4 2 3.95 18.81 17.51 o 10 4 2 804.99 762.99 43.76 o 1 5 2 1565.91 1518.74 17.82 o 2 5 2 704.95 742.63 10.54 o 3 5 2 7618.37 7348.56 59.19 o 4 5 2 3441.65 3305.19 33.48 o 5 5 2 527.24 549.32 18.20 o 6 5 2 731.73 748.20 19.34 o 7 5 2 6950.17 6973.03 92.36 o 8 5 2 2194.20 2174.68 53.58 o 9 5 2 126.26 119.70 22.91 o 10 5 2 33.88 45.98 27.20 o 0 6 2 41830.95 39953.54 521.68 o 1 6 2 8301.83 8438.54 63.98 o 2 6 2 1774.19 1635.42 19.15 o 3 6 2 668.06 634.92 11.57 o 4 6 2 29640.20 29828.51 208.00 o 5 6 2 8135.86 8134.05 67.43 o 6 6 2 1790.43 1855.33 31.92 o 7 6 2 544.65 605.99 20.65 o 8 6 2 9016.06 9089.84 127.51 o 9 6 2 268.50 261.61 32.53 o 10 6 2 6145.04 6097.91 129.22 o 1 7 2 2445.16 2200.68 22.39 o 2 7 2 1613.16 1536.43 15.79 o 3 7 2 5207.62 5176.22 49.76 o 4 7 2 560.08 532.49 12.46 o 5 7 2 5396.10 5537.26 53.28 o 6 7 2 3720.39 3773.26 48.03 o 7 7 2 1575.91 1656.40 30.38 o 8 7 2 587.23 579.31 26.82 o 9 7 2 1098.28 1037.06 43.55 o 10 7 2 33.80 2.54 26.60 o 0 8 2 4494.24 4290.43 97.20 o 1 8 2 77.83 78.15 3.46 o 2 8 2 959.73 929.22 12.26 o 3 8 2 2217.12 2249.03 27.94 o 4 8 2 11499.47 11741.07 99.95 o 5 8 2 0.42 -7.70 7.70 o 6 8 2 4.08 21.58 10.18 o 7 8 2 1147.03 1197.50 31.10 o 8 8 2 1575.68 1549.98 48.77 o 9 8 2 120.46 99.66 24.79 o 10 8 2 1146.05 1012.49 58.53 o 1 9 2 16782.58 16489.09 156.50 o 2 9 2 872.48 834.67 15.22 o 3 9 2 23890.61 24103.16 178.17 o 4 9 2 2044.22 2062.59 25.80 o 5 9 2 6624.85 6686.91 68.86 o 6 9 2 424.40 443.82 16.35 o 7 9 2 12095.65 12144.96 159.80 o 8 9 2 15.87 10.85 19.86 o 9 9 2 1242.30 1196.99 43.32 o 0 10 2 9298.84 9276.58 195.15 o 1 10 2 88.41 94.75 4.99 o 2 10 2 6816.78 6894.85 59.88 o 3 10 2 24.28 43.19 5.10 o 4 10 2 3586.63 3561.07 40.63 o 5 10 2 249.48 251.22 12.70 o 6 10 2 911.01 924.07 22.97 o 7 10 2 1408.81 1423.57 38.28 o 8 10 2 2625.95 2665.38 61.51 o 9 10 2 52.88 63.02 26.10 o 1 11 2 4231.74 4382.71 47.30 o 2 11 2 8.95 27.83 3.71 o 3 11 2 5870.40 5910.33 55.28 o 4 11 2 408.72 379.48 12.23 o 5 11 2 7.70 10.66 9.14 o 6 11 2 2191.27 2236.05 40.57 o 7 11 2 3755.68 3804.63 76.39 o 8 11 2 117.37 111.25 22.83 o 9 11 2 45.29 41.19 28.59 o 0 12 2 19099.20 19345.37 528.81 o 1 12 2 991.85 984.27 18.93 o 2 12 2 10249.37 10545.32 102.35 o 3 12 2 2283.86 2232.31 32.69 o 4 12 2 18414.12 18657.66 186.83 o 5 12 2 137.78 166.55 12.95 o 6 12 2 3499.78 3653.65 72.83 o 7 12 2 707.13 687.69 33.22 o 8 12 2 5482.58 5550.19 136.32 o 9 12 2 249.81 236.81 50.72 o 1 13 2 3102.15 3110.49 53.90 o 2 13 2 443.71 406.45 10.27 o 3 13 2 4432.41 4392.27 56.96 o 4 13 2 695.61 719.56 23.06 o 5 13 2 1305.58 1406.91 27.49 o 6 13 2 2672.08 2737.38 63.90 o 7 13 2 1562.46 1596.19 52.48 o 8 13 2 136.51 167.55 30.69 o 0 14 2 6945.15 6740.49 204.12 o 1 14 2 1772.62 1761.69 37.08 o 2 14 2 3.64 20.51 7.97 o 3 14 2 101.38 98.23 4.87 o 4 14 2 3846.59 3958.64 59.69 o 5 14 2 244.90 251.84 21.11 o 6 14 2 556.43 531.50 26.77 o 7 14 2 316.10 338.53 29.57 o 8 14 2 1159.89 1088.15 46.22 o 1 15 2 4267.64 4288.58 102.28 o 2 15 2 20.35 16.47 9.05 o 3 15 2 13784.71 14013.78 199.52 o 4 15 2 5033.27 4982.18 101.20 o 5 15 2 1337.33 1371.60 40.70 o 6 15 2 804.80 809.62 38.95 o 7 15 2 6500.15 6658.40 157.23 o 0 16 2 18.50 39.60 28.16 o 1 16 2 534.98 461.54 44.42 o 2 16 2 3679.81 3780.40 94.66 o 3 16 2 223.89 219.21 16.16 o 4 16 2 1106.53 1118.61 54.71 o 5 16 2 64.15 52.17 16.96 o 6 16 2 1618.22 1666.06 56.60 o 7 16 2 91.82 85.10 32.35 o 1 17 2 150.81 173.22 26.15 o 2 17 2 382.96 311.07 26.01 o 3 17 2 3133.87 3246.04 102.46 o 4 17 2 90.23 68.79 10.06 o 5 17 2 196.74 202.97 26.15 o 6 17 2 3.13 -13.73 23.84 o 0 18 2 10730.80 11227.98 454.93 o 1 18 2 633.22 614.41 37.01 o 2 18 2 2969.44 2853.16 88.83 o 3 18 2 422.92 285.39 24.87 o 4 18 2 5801.93 6486.98 230.84 o 5 18 2 396.16 339.99 56.16 o 6 18 2 2460.55 2386.99 129.29 o 1 19 2 1814.04 1891.00 99.41 o 2 19 2 11.65 30.80 21.87 o 3 19 2 1642.36 1797.44 91.05 o 4 19 2 163.21 159.59 33.91 o 5 19 2 1762.18 1759.69 93.07 o 0 20 2 4335.20 4165.91 162.80 o 1 20 2 6.40 15.27 22.50 o 2 20 2 80.48 99.24 32.21 o 3 20 2 814.58 700.79 84.38 o 4 20 2 1613.75 1768.03 113.36 o 1 21 2 4716.04 4650.01 215.76 o 2 21 2 329.40 317.00 84.65 o 3 21 2 6533.76 6923.35 350.05 o 0 22 2 2144.52 2042.42 160.53 o 1 22 2 4.24 10.41 50.22 o 1 1 3 15603.15 15082.04 159.64 o 2 1 3 7391.03 7011.93 55.00 o 3 1 3 10829.75 10604.89 77.81 o 4 1 3 10.70 12.08 6.07 o 5 1 3 9694.22 9794.30 82.41 o 6 1 3 5886.97 6032.89 59.71 o 7 1 3 12232.83 12414.44 144.64 o 8 1 3 9.70 18.82 15.31 o 9 1 3 1094.85 1200.00 37.68 o 10 1 3 528.14 460.32 27.54 o 0 2 3 72439.05 69804.82 1399.44 o 1 2 3 9979.74 9913.74 103.36 o 2 2 3 1117.22 1007.46 12.36 o 3 2 3 5587.41 5811.38 48.54 o 4 2 3 19876.03 19853.24 137.40 o 5 2 3 442.68 505.91 14.08 o 6 2 3 2442.52 2432.22 33.64 o 7 2 3 2424.04 2277.30 39.96 o 8 2 3 7744.59 7724.51 112.55 o 9 2 3 147.04 152.04 19.66 o 10 2 3 4952.11 5103.06 102.27 o 1 3 3 15443.97 15356.73 142.74 o 2 3 3 555.35 536.53 9.27 o 3 3 3 298.38 309.04 8.11 o 4 3 3 1665.99 1619.54 21.82 o 5 3 3 255.23 274.40 13.10 o 6 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300.24 17.10 o 9 6 3 10.68 16.85 23.50 o 10 6 3 0.19 4.57 24.19 o 1 7 3 13948.32 13968.96 118.32 o 2 7 3 1825.96 1894.40 20.55 o 3 7 3 19691.56 19563.18 138.07 o 4 7 3 2224.70 2299.63 34.31 o 5 7 3 742.13 727.86 16.72 o 6 7 3 4.55 -10.25 11.76 o 7 7 3 14287.49 14516.47 180.44 o 8 7 3 142.17 145.88 23.00 o 9 7 3 559.40 519.63 30.96 o 10 7 3 1.22 7.61 26.47 o 0 8 3 22286.29 21517.60 324.41 o 1 8 3 1683.28 1596.79 18.86 o 2 8 3 18759.18 19836.37 146.32 o 3 8 3 2.20 2.58 5.65 o 4 8 3 15397.81 15439.92 126.70 o 5 8 3 1375.70 1432.46 22.60 o 6 8 3 6676.69 6710.45 84.01 o 7 8 3 24.23 26.05 12.00 o 8 8 3 3857.37 3979.85 87.14 o 9 8 3 28.26 18.64 22.00 o 10 8 3 816.76 827.48 82.37 o 1 9 3 535.06 531.36 12.67 o 2 9 3 303.36 339.78 7.85 o 3 9 3 118.01 121.17 6.31 o 4 9 3 26.84 31.04 7.16 o 5 9 3 147.93 174.13 11.34 o 6 9 3 423.38 438.92 15.89 o 7 9 3 362.34 336.49 17.36 o 8 9 3 1.33 23.92 18.50 o 9 9 3 141.04 145.25 24.56 o 0 10 3 12073.22 11575.82 216.44 o 1 10 3 475.20 456.03 9.89 o 2 10 3 656.97 693.73 11.41 o 3 10 3 5500.94 5726.78 57.45 o 4 10 3 10400.60 10629.53 100.78 o 5 10 3 2346.17 2275.97 34.54 o 6 10 3 2520.08 2605.38 42.71 o 7 10 3 1733.19 1826.17 42.31 o 8 10 3 5832.68 5984.13 110.22 o 9 10 3 336.54 350.61 28.98 o 1 11 3 6589.00 6672.17 72.75 o 2 11 3 2490.40 2491.64 28.13 o 3 11 3 8437.09 8658.48 106.11 o 4 11 3 597.16 613.76 14.65 o 5 11 3 4303.61 4309.00 67.32 o 6 11 3 1566.21 1607.16 32.06 o 7 11 3 5628.48 5796.23 100.77 o 8 11 3 791.20 778.73 42.48 o 9 11 3 1754.61 1652.57 61.84 o 0 12 3 984.27 942.79 24.23 o 1 12 3 8.75 6.39 3.74 o 2 12 3 73.67 87.69 4.63 o 3 12 3 3.37 8.36 4.92 o 4 12 3 282.03 298.60 13.00 o 5 12 3 1442.57 1502.66 32.41 o 6 12 3 951.20 923.25 27.30 o 7 12 3 61.14 72.93 17.71 o 8 12 3 7.12 18.19 24.88 o 9 12 3 24.64 13.57 32.30 o 1 13 3 4411.11 4314.51 68.08 o 2 13 3 12.58 11.85 5.21 o 3 13 3 9868.93 10136.28 118.40 o 4 13 3 349.50 359.34 14.03 o 5 13 3 4183.32 4188.66 68.71 o 6 13 3 691.50 641.05 29.82 o 7 13 3 6785.37 7206.27 172.58 o 8 13 3 232.81 215.45 48.67 o 0 14 3 24227.62 24376.61 545.94 o 1 14 3 11.04 17.08 6.10 o 2 14 3 2614.16 2628.64 37.22 o 3 14 3 6.99 0.63 5.33 o 4 14 3 6808.92 7131.87 118.24 o 5 14 3 24.69 8.07 12.37 o 6 14 3 3505.08 3647.76 100.50 o 7 14 3 77.98 59.46 38.07 o 8 14 3 3078.41 3158.73 112.00 o 1 15 3 1.04 16.68 9.06 o 2 15 3 171.01 151.18 9.72 o 3 15 3 606.62 517.61 19.44 o 4 15 3 456.04 468.75 19.60 o 5 15 3 1116.67 1103.51 37.03 o 6 15 3 18.72 -6.04 15.07 o 7 15 3 154.80 159.47 24.44 o 0 16 3 22628.97 22281.01 700.80 o 1 16 3 1.17 4.07 4.49 o 2 16 3 2587.59 2574.34 75.23 o 3 16 3 55.68 11.87 13.86 o 4 16 3 7210.86 7433.25 205.74 o 5 16 3 4568.08 4927.75 167.55 o 6 16 3 2018.51 1968.23 66.74 o 7 16 3 173.13 150.31 22.49 o 1 17 3 7459.22 7428.20 173.49 o 2 17 3 1155.63 1126.45 42.55 o 3 17 3 7149.24 7354.06 206.42 o 4 17 3 983.72 940.24 50.72 o 5 17 3 6874.94 6948.31 185.11 o 6 17 3 166.32 149.52 24.48 o 0 18 3 340.18 85.35 118.95 o 1 18 3 126.06 111.20 23.27 o 2 18 3 1862.13 1699.94 61.66 o 3 18 3 465.11 415.69 40.62 o 4 18 3 103.25 87.78 38.04 o 5 18 3 107.90 112.90 37.83 o 6 18 3 84.08 139.45 53.60 o 1 19 3 3712.81 3698.36 116.64 o 2 19 3 359.25 324.07 41.00 o 3 19 3 3179.07 3006.56 114.48 o 4 19 3 1.17 50.09 55.02 o 5 19 3 704.68 607.13 62.11 o 0 20 3 1423.40 1107.70 85.12 o 1 20 3 104.49 149.37 35.75 o 2 20 3 3766.02 3708.05 174.49 o 3 20 3 85.63 -10.05 90.97 o 4 20 3 3248.29 3283.10 175.15 o 1 21 3 551.10 565.78 46.73 o 2 21 3 133.72 152.77 52.98 o 3 21 3 11.67 7.94 67.33 o 0 22 3 3869.99 3686.87 285.38 o 0 0 4 3216.55 2967.10 95.65 o 1 0 4 79563.95 82416.28 1239.53 o 2 0 4 2359.65 2426.33 37.52 o 3 0 4 4639.45 4621.79 58.37 o 4 0 4 21628.77 21770.29 205.19 o 5 0 4 2770.94 2986.51 61.77 o 6 0 4 6915.49 6749.23 119.51 o 7 0 4 887.55 888.20 36.99 o 8 0 4 8813.54 8937.03 189.31 o 9 0 4 255.97 250.84 33.52 o 10 0 4 6734.09 7201.99 172.14 o 1 1 4 5739.17 5316.00 64.59 o 2 1 4 4476.88 4547.23 42.03 o 3 1 4 150.92 127.20 6.49 o 4 1 4 1523.75 1644.58 21.19 o 5 1 4 694.23 730.81 15.37 o 6 1 4 24.55 15.57 9.91 o 7 1 4 5543.62 5715.78 76.50 o 8 1 4 13.64 10.95 12.88 o 9 1 4 1001.48 1035.29 35.32 o 10 1 4 291.87 231.96 32.49 o 0 2 4 56284.98 54100.61 883.79 o 1 2 4 4227.97 4195.60 51.26 o 2 2 4 6836.52 6700.47 60.34 o 3 2 4 2309.12 2401.18 24.51 o 4 2 4 5562.82 5383.76 48.25 o 5 2 4 3.69 6.16 8.00 o 6 2 4 1209.01 1162.83 21.97 o 7 2 4 1.59 -1.56 12.72 o 8 2 4 1182.59 1165.67 32.82 o 9 2 4 54.70 51.65 18.24 o 10 2 4 132.46 112.30 24.32 o 1 3 4 20660.42 20177.68 206.15 o 2 3 4 597.29 550.18 11.66 o 3 3 4 29711.19 29036.12 202.48 o 4 3 4 417.16 403.44 10.20 o 5 3 4 9147.31 9332.10 81.33 o 6 3 4 15.62 8.87 8.72 o 7 3 4 15735.29 15807.30 170.50 o 8 3 4 904.89 918.41 41.43 o 9 3 4 927.67 916.22 32.04 o 10 3 4 724.54 623.43 40.07 o 0 4 4 29576.73 28201.47 461.45 o 1 4 4 7995.06 8087.94 81.96 o 2 4 4 3476.53 3365.89 32.83 o 3 4 4 353.39 393.68 10.56 o 4 4 4 7605.18 7824.87 71.36 o 5 4 4 184.75 160.41 8.99 o 6 4 4 2938.87 3002.80 41.85 o 7 4 4 10.04 10.58 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9.03 29.17 o 0 8 4 8415.69 8489.51 181.09 o 1 8 4 3.94 12.23 5.40 o 2 8 4 516.30 569.55 10.25 o 3 8 4 410.83 335.79 10.82 o 4 8 4 3817.17 3792.22 45.26 o 5 8 4 529.33 506.91 16.93 o 6 8 4 1508.35 1526.50 30.66 o 7 8 4 682.84 591.78 21.49 o 8 8 4 1976.27 1893.30 50.69 o 9 8 4 79.44 50.98 20.49 o 1 9 4 9603.69 9936.64 120.99 o 2 9 4 11.24 23.12 5.68 o 3 9 4 7834.59 7667.52 66.57 o 4 9 4 377.80 376.79 12.05 o 5 9 4 4640.95 4600.58 60.81 o 6 9 4 5107.75 5144.55 69.43 o 7 9 4 11647.71 11930.47 165.62 o 8 9 4 635.66 581.32 34.28 o 9 9 4 1724.33 1753.08 61.42 o 0 10 4 1505.76 1490.02 43.90 o 1 10 4 3118.96 3203.06 37.44 o 2 10 4 1720.26 1678.97 20.07 o 3 10 4 1085.85 1106.49 20.52 o 4 10 4 2319.04 2374.87 32.02 o 5 10 4 55.58 55.35 10.78 o 6 10 4 1780.09 1832.81 36.72 o 7 10 4 3.50 -16.77 17.37 o 8 10 4 829.64 875.31 46.91 o 9 10 4 162.93 128.59 28.17 o 1 11 4 93.35 93.81 6.07 o 2 11 4 3505.58 3644.47 35.40 o 3 11 4 1618.23 1586.02 24.46 o 4 11 4 193.31 228.57 12.61 o 5 11 4 633.94 659.84 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105.35 140.64 13.57 o 5 15 4 4333.71 4516.92 124.07 o 6 15 4 418.25 320.26 24.32 o 7 15 4 6363.25 6579.27 173.11 o 0 16 4 2294.61 2145.87 59.43 o 1 16 4 199.91 126.03 16.40 o 2 16 4 4650.31 4711.69 93.06 o 3 16 4 296.00 250.81 18.92 o 4 16 4 3001.89 3018.15 150.50 o 5 16 4 235.17 258.79 37.92 o 6 16 4 2245.80 2241.63 127.15 o 7 16 4 0.08 -12.43 20.74 o 1 17 4 832.46 839.26 60.76 o 2 17 4 184.67 178.85 23.20 o 3 17 4 1463.32 1356.75 65.23 o 4 17 4 367.62 337.56 23.45 o 5 17 4 227.85 214.31 41.81 o 6 17 4 156.63 136.14 25.42 o 0 18 4 14864.84 14855.06 773.61 o 1 18 4 660.55 553.27 39.09 o 2 18 4 7430.55 7594.47 211.17 o 3 18 4 133.44 121.11 51.65 o 4 18 4 8162.44 8263.03 284.90 o 5 18 4 1.43 -23.10 23.10 o 6 18 4 2522.88 2680.41 135.76 o 1 19 4 3895.60 3881.08 138.04 o 2 19 4 63.94 61.34 43.05 o 3 19 4 1252.03 1200.81 67.79 o 4 19 4 12.89 -2.00 30.34 o 5 19 4 2073.22 2140.79 144.09 o 0 20 4 326.75 278.28 53.55 o 1 20 4 140.79 131.86 40.35 o 2 20 4 332.98 261.97 37.81 o 3 20 4 1112.73 1215.05 150.36 o 4 20 4 467.72 338.93 80.25 o 1 21 4 1152.28 1015.92 95.91 o 2 21 4 1.06 18.71 30.70 o 1 1 5 21.33 25.24 4.89 o 2 1 5 202.54 182.47 7.64 o 3 1 5 20433.09 20037.50 172.33 o 4 1 5 2757.33 2632.49 28.07 o 5 1 5 570.89 491.45 12.71 o 6 1 5 2647.16 2589.97 34.99 o 7 1 5 9507.14 9528.69 124.67 o 8 1 5 1646.72 1618.17 39.49 o 9 1 5 2306.82 2273.80 51.07 o 10 1 5 623.58 531.38 33.90 o 0 2 5 11631.35 10748.80 182.70 o 1 2 5 72.24 75.51 7.20 o 2 2 5 3016.12 2820.23 28.98 o 3 2 5 1322.34 1370.41 18.47 o 4 2 5 9525.46 9157.00 69.98 o 5 2 5 2866.40 2892.93 34.39 o 6 2 5 9143.63 9114.65 94.38 o 7 2 5 73.88 77.32 15.02 o 8 2 5 7157.27 7408.29 109.70 o 9 2 5 81.74 94.37 19.84 o 10 2 5 2850.85 2794.21 71.96 o 1 3 5 565.93 620.84 12.37 o 2 3 5 2960.80 3064.58 33.24 o 3 3 5 736.83 685.01 13.26 o 4 3 5 406.93 396.78 11.69 o 5 3 5 107.79 129.84 11.14 o 6 3 5 688.34 623.41 20.78 o 7 3 5 69.35 89.20 12.35 o 8 3 5 66.16 55.56 18.33 o 9 3 5 904.44 853.92 34.69 o 10 3 5 128.39 66.86 23.82 o 0 4 5 88629.94 87251.38 1200.96 o 1 4 5 6209.54 5993.58 65.60 o 2 4 5 22690.77 22072.87 184.59 o 3 4 5 1562.47 1447.74 20.28 o 4 4 5 28384.17 28497.41 241.44 o 5 4 5 295.89 281.86 15.05 o 6 4 5 2590.66 2592.33 39.39 o 7 4 5 298.55 292.66 19.71 o 8 4 5 4542.10 4409.45 76.46 o 9 4 5 0.11 -8.79 20.31 o 10 4 5 1612.84 1442.44 49.12 o 1 5 5 53857.30 54854.83 535.01 o 2 5 5 200.48 276.58 8.41 o 3 5 5 35735.19 36392.20 278.73 o 4 5 5 127.95 135.83 9.82 o 5 5 5 9576.11 9545.44 88.98 o 6 5 5 977.10 937.90 23.99 o 7 5 5 6710.60 6923.58 90.26 o 8 5 5 429.85 391.62 20.40 o 9 5 5 1398.68 1283.81 43.10 o 10 5 5 276.91 254.46 29.52 o 0 6 5 533.66 530.35 17.18 o 1 6 5 2840.50 2760.61 33.47 o 2 6 5 2.27 -4.67 4.78 o 3 6 5 24.11 37.50 6.75 o 4 6 5 276.62 287.60 13.29 o 5 6 5 322.00 355.19 14.41 o 6 6 5 548.71 523.40 19.50 o 7 6 5 20.19 42.28 13.39 o 8 6 5 298.42 289.34 28.81 o 9 6 5 52.49 70.03 25.48 o 10 6 5 31.86 34.25 29.14 o 1 7 5 10350.25 10249.59 90.69 o 2 7 5 535.35 560.46 13.36 o 3 7 5 21091.88 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37.51 o 1 7 13 4218.15 4259.89 110.61 o 2 7 13 21.71 50.02 19.15 o 3 7 13 5488.14 5391.91 115.56 o 4 7 13 1808.91 1710.49 57.83 o 5 7 13 3402.61 3452.64 104.95 o 6 7 13 283.48 286.19 35.23 o 7 7 13 723.39 649.31 40.73 o 0 8 13 6213.69 6496.16 233.83 o 1 8 13 13.58 12.84 22.66 o 2 8 13 12954.26 13224.88 253.88 o 3 8 13 250.08 214.99 23.51 o 4 8 13 2781.89 2755.41 90.02 o 5 8 13 144.21 120.59 21.46 o 6 8 13 4822.91 4908.06 132.94 o 7 8 13 53.51 67.13 44.42 o 1 9 13 1255.31 1236.80 46.34 o 2 9 13 575.19 496.95 23.62 o 3 9 13 1736.06 1736.84 56.70 o 4 9 13 4.99 4.37 23.98 o 5 9 13 1.63 1.90 24.18 o 6 9 13 338.32 326.46 37.38 o 7 9 13 16.49 8.33 38.95 o 0 10 13 228.84 250.13 36.45 o 1 10 13 23.29 20.35 17.94 o 2 10 13 3437.51 3361.36 115.77 o 3 10 13 455.43 408.14 33.61 o 4 10 13 986.46 896.44 46.65 o 5 10 13 96.89 98.16 23.18 o 6 10 13 3336.05 3486.18 114.04 o 1 11 13 1042.93 984.98 61.07 o 2 11 13 230.28 230.49 24.41 o 3 11 13 3524.07 3513.19 123.12 o 4 11 13 135.23 112.06 28.53 o 5 11 13 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14 1040.18 1074.91 51.31 o 4 9 14 28.42 14.42 24.34 o 5 9 14 7168.95 7367.11 207.10 o 6 9 14 339.07 342.48 35.33 o 0 10 14 1550.44 1748.39 99.42 o 1 10 14 434.83 357.16 39.66 o 2 10 14 1700.99 1581.06 65.25 o 3 10 14 87.28 88.27 31.69 o 4 10 14 958.76 944.59 69.39 o 5 10 14 3.44 -26.20 36.87 o 6 10 14 319.56 291.47 65.36 o 1 11 14 1234.80 1162.88 117.25 o 2 11 14 89.27 50.33 29.42 o 3 11 14 155.04 162.56 37.29 o 4 11 14 24.74 23.98 43.06 o 5 11 14 1351.43 1338.52 63.30 o 0 12 14 167.42 149.21 55.69 o 1 12 14 460.40 430.76 60.74 o 2 12 14 3955.63 4275.67 151.70 o 3 12 14 181.28 204.03 37.93 o 4 12 14 1525.80 1383.71 82.05 o 5 12 14 124.60 130.63 35.68 o 1 13 14 104.48 26.93 54.12 o 2 13 14 15.99 32.93 69.21 o 3 13 14 192.60 157.50 75.42 o 4 13 14 149.15 149.69 51.10 o 0 14 14 2359.40 2170.15 176.54 o 1 14 14 67.27 61.29 71.64 o 2 14 14 4830.83 5092.19 219.45 o 3 14 14 383.09 333.73 46.69 o 4 14 14 611.22 592.07 61.98 o 1 15 14 6691.27 6610.70 276.27 o 2 15 14 10.94 7.24 32.43 o 3 15 14 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