#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219560_Fobs loop_ _publ_author_name 'Krokidis, Marios' 'Papaioannou, Dionissios' 'Nastopoulos, Vassilios' _publ_section_title ; (Z)-tert-Butyl 2-(4-amino-9H-fluoren-9-ylidene)acetate ; _journal_coeditor_code DN2370 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1978 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.0820 _cell_length_b 13.7330 _cell_length_c 24.5682 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file dn2370Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ======TS1 in Pbca (No 61)======' _shelx_refln_list_code 4 _shelx_F_calc_maximum 248.14 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55274.30 44962.15 385.18 o 4 0 0 2563.52 2474.18 45.26 o 6 0 0 7921.98 7749.09 210.66 o 8 0 0 122.58 79.92 66.18 o 10 0 0 953.31 1133.20 99.77 o 2 1 0 1736.43 1532.80 35.85 o 4 1 0 9911.15 8314.95 70.54 o 6 1 0 17.59 27.97 24.04 o 8 1 0 675.65 756.43 54.86 o 10 1 0 4.33 46.45 55.95 o 2 2 0 41105.37 36279.91 159.76 o 4 2 0 16.16 7.44 18.36 o 6 2 0 64.97 70.21 22.60 o 8 2 0 533.64 608.00 53.92 o 10 2 0 103.31 98.44 58.12 o 2 3 0 46472.51 43885.02 377.61 o 4 3 0 580.35 578.85 22.87 o 6 3 0 278.73 236.38 24.73 o 8 3 0 126.25 161.81 48.90 o 10 3 0 294.16 420.45 62.78 o 0 4 0 6790.30 6753.99 129.27 o 2 4 0 12834.19 12959.10 202.05 o 4 4 0 2051.19 1971.91 42.01 o 6 4 0 5.22 7.96 30.54 o 8 4 0 147.97 152.91 42.76 o 10 4 0 9.17 61.01 67.72 o 2 5 0 1686.30 1818.84 39.51 o 4 5 0 529.26 510.48 27.39 o 6 5 0 129.32 106.67 35.66 o 8 5 0 526.98 654.59 55.88 o 10 5 0 42.28 72.92 86.66 o 0 6 0 3712.39 4005.97 86.25 o 2 6 0 124.80 170.20 29.93 o 4 6 0 3835.84 3484.56 48.91 o 6 6 0 29.52 41.46 41.61 o 8 6 0 19.44 85.26 60.22 o 10 6 0 187.57 202.05 94.86 o 2 7 0 2841.00 2953.73 50.71 o 4 7 0 2854.90 2667.57 56.78 o 6 7 0 2379.72 2144.52 62.58 o 8 7 0 9.25 32.25 61.92 o 0 8 0 1.12 3.03 32.73 o 2 8 0 741.30 856.51 40.15 o 4 8 0 1182.23 1137.93 49.17 o 6 8 0 1869.17 1890.96 90.45 o 8 8 0 55.14 83.06 65.25 o 2 9 0 266.45 280.49 37.92 o 4 9 0 493.15 459.47 44.92 o 6 9 0 128.57 144.79 58.67 o 8 9 0 751.85 808.64 78.33 o 0 10 0 93.86 106.43 40.89 o 2 10 0 2431.11 2403.56 91.53 o 4 10 0 3586.38 3332.11 118.56 o 6 10 0 548.45 541.70 67.26 o 8 10 0 2087.44 1963.25 95.27 o 2 11 0 15.40 4.65 40.55 o 4 11 0 118.58 72.79 44.17 o 6 11 0 701.36 670.54 71.03 o 0 12 0 5.76 -29.73 57.87 o 2 12 0 24.80 29.11 47.91 o 4 12 0 571.63 539.17 52.88 o 6 12 0 28.49 46.60 64.65 o 2 13 0 93.18 59.86 52.53 o 4 13 0 1.39 4.00 67.97 o 6 13 0 438.75 496.28 74.56 o 0 14 0 34.98 11.87 64.90 o 2 14 0 268.00 256.22 50.05 o 4 14 0 136.74 160.64 122.88 o 2 15 0 24.41 72.94 76.51 o 4 15 0 0.72 2.77 122.63 o 0 16 0 51.28 47.71 114.00 o 2 16 0 232.87 231.55 132.11 o 2 1 1 646.05 646.24 20.03 o 3 1 1 1165.70 1063.90 60.18 o 4 1 1 1088.80 1002.89 39.70 o 5 1 1 1245.33 1324.34 89.26 o 6 1 1 1768.01 2336.98 115.16 o 7 1 1 1146.48 1350.88 103.81 o 9 1 1 195.43 315.45 49.06 o 10 1 1 29.21 62.83 39.80 o 1 2 1 6777.19 6914.49 65.77 o 2 2 1 61573.18 56506.69 507.71 o 3 2 1 215.27 161.48 14.12 o 4 2 1 2387.39 2302.23 83.37 o 5 2 1 258.32 230.43 14.82 o 6 2 1 433.10 396.58 17.76 o 7 2 1 540.77 548.81 27.72 o 8 2 1 519.52 690.74 55.03 o 9 2 1 4.79 38.14 36.37 o 10 2 1 8.09 43.51 40.36 o 1 3 1 481.64 547.01 16.23 o 2 3 1 24789.99 23718.55 111.26 o 3 3 1 2474.73 2272.87 82.03 o 4 3 1 110.34 171.57 26.25 o 5 3 1 122.16 146.29 19.84 o 6 3 1 277.03 380.29 43.04 o 7 3 1 600.43 630.73 26.89 o 8 3 1 257.57 290.86 47.50 o 9 3 1 238.42 341.60 39.64 o 10 3 1 34.02 126.75 41.02 o 0 4 1 17345.17 17749.47 308.84 o 1 4 1 87.62 117.55 17.72 o 3 4 1 2205.63 2032.05 78.13 o 4 4 1 6682.31 6098.31 51.51 o 5 4 1 702.51 660.15 18.95 o 6 4 1 453.47 427.23 34.49 o 7 4 1 121.27 130.88 25.91 o 8 4 1 43.44 104.76 30.45 o 9 4 1 145.97 195.39 41.75 o 10 4 1 53.00 38.83 47.30 o 1 5 1 1545.75 1746.54 25.66 o 2 5 1 497.52 588.87 47.72 o 3 5 1 2907.89 2737.43 28.49 o 4 5 1 17642.41 16436.25 260.72 o 5 5 1 90.73 95.26 19.17 o 6 5 1 317.53 322.97 37.69 o 7 5 1 194.98 225.65 30.69 o 8 5 1 377.55 511.86 63.64 o 9 5 1 213.63 195.89 46.67 o 10 5 1 91.44 171.42 81.20 o 0 6 1 5549.84 5975.70 58.28 o 1 6 1 3401.29 3770.35 40.56 o 2 6 1 1029.18 1203.96 26.69 o 3 6 1 862.46 795.93 37.48 o 4 6 1 6515.42 5687.16 103.55 o 5 6 1 989.40 939.54 23.55 o 6 6 1 1234.49 1081.99 68.00 o 7 6 1 1194.87 1326.80 54.68 o 8 6 1 192.67 179.91 43.90 o 9 6 1 20.67 20.30 46.80 o 10 6 1 1.31 88.35 57.44 o 1 7 1 393.21 419.55 26.58 o 2 7 1 14.41 23.23 21.17 o 3 7 1 261.16 242.16 24.46 o 4 7 1 254.95 241.29 23.33 o 5 7 1 220.90 192.04 25.57 o 6 7 1 301.40 296.52 29.55 o 7 7 1 42.01 105.18 40.87 o 8 7 1 20.84 13.19 43.91 o 9 7 1 12.77 69.69 52.34 o 0 8 1 571.54 644.19 27.63 o 1 8 1 2159.70 2439.90 30.63 o 2 8 1 213.19 232.67 24.30 o 3 8 1 652.83 646.99 37.04 o 4 8 1 1032.86 954.90 86.67 o 5 8 1 0.12 24.93 27.06 o 6 8 1 5947.83 5301.31 230.86 o 7 8 1 5.13 26.27 44.73 o 8 8 1 33.29 76.13 45.68 o 9 8 1 38.49 33.79 49.47 o 1 9 1 420.32 461.30 24.48 o 2 9 1 21.49 20.27 24.99 o 3 9 1 273.66 278.86 28.31 o 4 9 1 302.18 303.49 30.25 o 5 9 1 234.63 251.38 30.29 o 6 9 1 1837.33 1730.34 198.56 o 7 9 1 175.09 138.74 45.10 o 9 9 1 21.45 64.51 50.99 o 0 10 1 123.38 152.07 33.00 o 1 10 1 894.19 866.43 31.59 o 2 10 1 1022.38 1129.03 34.15 o 3 10 1 2719.71 2747.75 82.50 o 4 10 1 0.37 -10.92 29.81 o 5 10 1 774.19 820.35 57.91 o 6 10 1 155.57 133.39 43.39 o 7 10 1 1.72 2.51 48.48 o 8 10 1 66.08 339.25 87.89 o 1 11 1 22.53 40.48 26.09 o 2 11 1 69.94 91.48 29.03 o 3 11 1 112.70 102.75 30.97 o 4 11 1 11.67 29.31 31.36 o 5 11 1 8.63 2.99 36.52 o 6 11 1 52.15 86.87 44.46 o 7 11 1 36.02 55.04 47.45 o 0 12 1 1286.90 1308.85 54.36 o 1 12 1 329.73 351.61 32.15 o 2 12 1 17.15 119.32 34.82 o 3 12 1 225.58 170.14 34.76 o 4 12 1 326.84 330.46 38.30 o 5 12 1 290.76 264.99 44.32 o 6 12 1 204.86 190.90 48.06 o 7 12 1 1.01 32.95 49.41 o 1 13 1 247.93 300.30 33.39 o 2 13 1 155.53 151.83 37.63 o 3 13 1 344.89 348.49 40.55 o 4 13 1 219.51 225.99 46.30 o 5 13 1 458.41 396.13 47.46 o 6 13 1 432.22 471.92 59.11 o 0 14 1 208.08 202.79 57.55 o 1 14 1 154.84 152.10 40.10 o 2 14 1 40.72 65.34 40.23 o 3 14 1 65.38 97.23 50.84 o 4 14 1 0.05 40.60 62.04 o 5 14 1 2.87 -12.62 64.06 o 1 15 1 2.26 121.10 46.89 o 2 15 1 9.49 58.76 54.86 o 3 15 1 51.24 123.39 87.03 o 4 15 1 2.84 65.12 127.54 o 0 16 1 630.99 565.68 94.12 o 1 16 1 435.39 472.78 61.65 o 2 16 1 100.64 132.46 67.92 o 2 0 2 9898.57 8288.31 117.79 o 3 0 2 4301.16 4773.48 75.42 o 4 0 2 445.36 410.56 34.65 o 5 0 2 10583.36 10182.55 330.95 o 6 0 2 0.12 -6.75 23.90 o 7 0 2 1059.55 1037.46 42.51 o 8 0 2 482.05 658.98 103.34 o 9 0 2 320.11 354.38 54.96 o 10 0 2 105.22 142.33 58.24 o 1 1 2 250.82 259.88 17.81 o 2 1 2 344.85 294.85 34.47 o 3 1 2 233.64 212.88 23.81 o 4 1 2 2008.31 1634.20 31.11 o 5 1 2 696.97 608.43 33.43 o 6 1 2 1627.58 1485.28 29.78 o 7 1 2 707.75 798.69 31.13 o 9 1 2 424.72 568.16 40.77 o 10 1 2 51.44 139.07 40.74 o 1 2 2 2486.31 2583.65 28.06 o 2 2 2 22766.46 19916.84 253.84 o 3 2 2 165.48 193.64 24.42 o 4 2 2 927.40 1127.43 76.32 o 5 2 2 484.62 486.40 49.67 o 6 2 2 90.42 92.19 18.95 o 7 2 2 5.09 31.66 26.55 o 8 2 2 428.06 501.31 47.87 o 9 2 2 155.59 183.77 37.88 o 10 2 2 59.07 73.57 40.30 o 1 3 2 208.54 232.38 14.98 o 2 3 2 22512.67 21583.47 133.02 o 3 3 2 728.00 672.16 26.37 o 4 3 2 28.87 28.38 13.58 o 5 3 2 1.89 6.98 13.87 o 6 3 2 26.04 42.43 20.31 o 7 3 2 1151.98 1141.32 80.35 o 8 3 2 1.79 17.56 30.91 o 9 3 2 441.88 535.11 41.21 o 10 3 2 62.83 41.84 40.67 o 0 4 2 1845.46 1990.35 34.32 o 1 4 2 693.00 699.69 21.12 o 2 4 2 889.91 861.06 19.66 o 3 4 2 693.90 576.40 19.54 o 4 4 2 382.67 361.79 32.18 o 5 4 2 625.53 518.44 18.69 o 6 4 2 334.47 288.55 23.06 o 7 4 2 40.69 57.17 27.39 o 8 4 2 378.51 401.21 33.65 o 10 4 2 1.65 25.05 50.97 o 1 5 2 88.08 72.14 17.59 o 2 5 2 1521.04 1665.85 25.82 o 3 5 2 155.77 179.69 16.87 o 4 5 2 244.94 263.21 19.02 o 5 5 2 138.71 123.62 19.31 o 6 5 2 111.18 77.72 23.24 o 7 5 2 0.07 38.35 29.07 o 8 5 2 0.25 36.49 30.15 o 10 5 2 77.06 206.02 64.07 o 0 6 2 487.32 503.47 24.86 o 1 6 2 1645.02 2114.40 108.82 o 2 6 2 1118.69 1233.84 67.40 o 3 6 2 910.78 1011.63 119.76 o 4 6 2 201.89 183.87 18.68 o 5 6 2 1285.04 1112.36 24.22 o 6 6 2 322.85 297.45 26.17 o 7 6 2 141.91 166.72 33.49 o 8 6 2 22.86 49.54 35.74 o 9 6 2 0.10 6.30 46.01 o 10 6 2 52.34 29.65 56.46 o 1 7 2 630.93 752.85 29.75 o 2 7 2 1921.24 1993.06 36.70 o 3 7 2 89.47 84.76 23.08 o 4 7 2 350.77 340.52 21.50 o 5 7 2 241.30 234.39 21.80 o 6 7 2 1184.08 1022.62 42.82 o 7 7 2 191.67 259.60 42.73 o 8 7 2 3.41 70.79 44.54 o 9 7 2 38.83 39.19 48.98 o 0 8 2 4786.06 5146.86 47.36 o 1 8 2 105.70 115.63 18.67 o 2 8 2 442.89 482.74 26.25 o 3 8 2 244.07 206.57 25.95 o 4 8 2 93.68 81.68 27.25 o 5 8 2 1714.88 1612.47 108.24 o 6 8 2 819.05 924.82 57.24 o 7 8 2 210.91 189.33 38.66 o 8 8 2 51.91 142.95 46.83 o 9 8 2 46.14 46.59 49.68 o 1 9 2 290.99 312.84 25.85 o 2 9 2 1.02 6.37 24.99 o 3 9 2 737.77 731.13 47.12 o 4 9 2 95.26 69.93 28.80 o 5 9 2 551.13 533.81 34.64 o 6 9 2 207.91 189.46 37.76 o 7 9 2 93.46 73.47 43.99 o 8 9 2 563.14 548.49 52.95 o 0 10 2 972.06 972.13 39.18 o 1 10 2 418.90 472.80 28.91 o 2 10 2 3.10 25.99 26.57 o 3 10 2 9.24 8.63 27.91 o 4 10 2 2.69 6.21 29.75 o 5 10 2 233.88 209.86 33.27 o 6 10 2 232.39 219.48 40.24 o 7 10 2 183.51 129.25 46.44 o 8 10 2 584.43 570.73 57.57 o 1 11 2 175.76 135.37 26.69 o 2 11 2 0.04 22.67 28.60 o 3 11 2 5200.90 5073.92 148.79 o 4 11 2 340.15 330.13 36.50 o 5 11 2 1483.07 1437.23 44.44 o 6 11 2 10.77 19.91 58.61 o 7 11 2 0.29 -1.27 47.59 o 0 12 2 0.23 -6.65 41.48 o 1 12 2 1947.76 2012.18 42.95 o 2 12 2 650.57 708.96 37.30 o 3 12 2 1218.60 1145.62 43.06 o 4 12 2 156.90 116.93 36.67 o 5 12 2 290.56 292.67 40.89 o 6 12 2 102.25 58.76 46.17 o 7 12 2 35.68 66.34 63.38 o 1 13 2 699.34 714.77 39.50 o 2 13 2 115.27 101.96 37.68 o 3 13 2 1129.87 1014.44 68.96 o 4 13 2 38.01 -1.01 47.23 o 5 13 2 116.69 90.95 55.87 o 6 13 2 19.89 62.16 54.02 o 0 14 2 125.09 143.06 57.05 o 1 14 2 1921.33 2026.91 56.85 o 2 14 2 197.99 173.47 41.25 o 3 14 2 1400.02 1385.92 68.28 o 4 14 2 357.25 289.78 67.35 o 5 14 2 11.57 8.44 66.23 o 1 15 2 108.37 110.79 42.94 o 2 15 2 9.34 -5.24 47.24 o 3 15 2 20.62 52.62 61.62 o 4 15 2 49.58 53.26 88.91 o 0 16 2 66.31 95.06 80.17 o 1 16 2 49.93 155.44 67.72 o 2 16 2 30.09 107.38 69.94 o 1 1 3 11.34 10.33 12.07 o 2 1 3 4571.06 4435.06 85.46 o 3 1 3 2678.03 2252.20 81.48 o 4 1 3 1321.25 1371.42 81.64 o 5 1 3 941.40 782.90 49.32 o 6 1 3 819.12 844.87 24.88 o 7 1 3 0.71 68.89 24.07 o 8 1 3 1634.67 1775.69 45.83 o 9 1 3 12.91 135.32 48.80 o 10 1 3 218.88 317.66 59.01 o 0 2 3 42177.96 45499.07 1400.11 o 1 2 3 9556.64 9811.35 113.40 o 2 2 3 52.02 55.54 14.09 o 3 2 3 13978.53 12344.30 139.41 o 4 2 3 760.91 784.56 62.27 o 5 2 3 132.68 120.42 12.70 o 6 2 3 1173.58 1090.62 65.70 o 7 2 3 25.36 44.93 22.56 o 8 2 3 57.55 87.92 33.46 o 9 2 3 31.67 40.43 38.42 o 10 2 3 1.80 13.04 40.30 o 1 3 3 1967.49 2231.58 29.74 o 2 3 3 1692.48 1760.98 20.92 o 3 3 3 2336.59 2188.44 29.46 o 4 3 3 145.71 169.41 20.93 o 5 3 3 380.53 416.04 53.48 o 6 3 3 250.29 256.74 21.39 o 7 3 3 55.37 117.98 26.97 o 8 3 3 0.19 34.91 28.65 o 10 3 3 106.50 113.75 44.50 o 0 4 3 1649.80 1876.71 46.43 o 1 4 3 152.89 124.71 16.35 o 3 4 3 6.95 18.38 14.74 o 4 4 3 2704.99 2475.13 41.77 o 5 4 3 95.88 91.83 15.18 o 6 4 3 23.72 14.36 21.65 o 7 4 3 49.61 69.45 27.51 o 8 4 3 6.28 24.08 31.00 o 9 4 3 237.86 322.78 39.49 o 10 4 3 14.02 18.44 54.10 o 1 5 3 3517.48 4013.51 78.49 o 2 5 3 1010.85 1012.29 22.63 o 3 5 3 1995.10 1886.38 29.65 o 4 5 3 3956.76 3610.20 98.06 o 5 5 3 161.70 149.59 18.29 o 6 5 3 147.33 205.57 38.91 o 7 5 3 142.56 124.50 28.58 o 8 5 3 16.90 61.99 33.35 o 9 5 3 891.31 1099.34 93.19 o 10 5 3 244.82 381.12 66.24 o 0 6 3 1500.73 1636.60 30.28 o 1 6 3 8260.23 9565.31 110.25 o 2 6 3 2539.89 2806.68 44.23 o 3 6 3 1562.17 1402.14 40.20 o 4 6 3 1600.04 1633.77 96.78 o 5 6 3 304.32 293.42 20.19 o 6 6 3 3.36 30.53 24.29 o 7 6 3 547.60 594.88 38.68 o 8 6 3 31.89 18.82 35.26 o 9 6 3 6.80 45.09 50.02 o 1 7 3 122.31 127.41 14.01 o 2 7 3 50.05 26.91 21.21 o 3 7 3 6.71 2.75 21.47 o 4 7 3 755.13 734.84 38.50 o 5 7 3 119.52 105.50 23.03 o 6 7 3 817.01 980.63 93.75 o 7 7 3 1263.85 1234.43 55.42 o 8 7 3 505.35 532.17 45.26 o 9 7 3 145.03 149.79 48.88 o 0 8 3 0.24 1.31 25.05 o 1 8 3 1.14 16.43 15.90 o 2 8 3 362.05 415.15 44.61 o 3 8 3 518.60 497.59 47.58 o 4 8 3 874.37 890.57 88.70 o 5 8 3 2982.58 2802.88 81.53 o 6 8 3 348.74 279.16 33.09 o 7 8 3 330.08 340.05 40.23 o 8 8 3 164.15 165.82 47.52 o 9 8 3 15.41 31.84 49.93 o 1 9 3 949.65 1074.63 30.37 o 2 9 3 312.46 295.19 26.58 o 3 9 3 30.78 31.91 26.42 o 4 9 3 75.26 74.20 28.77 o 5 9 3 7.46 -7.08 30.68 o 6 9 3 142.06 117.50 37.33 o 7 9 3 440.57 441.07 48.78 o 8 9 3 236.26 283.15 51.52 o 0 10 3 4512.19 4988.23 62.35 o 1 10 3 60.50 71.97 25.85 o 2 10 3 1604.01 1671.55 57.93 o 3 10 3 6.04 29.42 27.94 o 4 10 3 1098.02 1068.59 40.96 o 5 10 3 71.20 57.34 32.43 o 6 10 3 344.82 353.50 41.28 o 7 10 3 12.96 22.91 46.32 o 8 10 3 151.37 290.43 52.80 o 1 11 3 103.04 102.51 26.99 o 2 11 3 25.99 45.94 30.48 o 3 11 3 1.65 38.02 32.87 o 4 11 3 70.98 70.10 34.11 o 5 11 3 265.47 286.81 36.42 o 6 11 3 27.03 42.48 44.53 o 7 11 3 142.91 136.20 48.81 o 0 12 3 3408.15 3527.74 112.23 o 1 12 3 541.14 561.64 33.04 o 2 12 3 1877.28 2000.37 133.01 o 3 12 3 73.13 94.34 43.51 o 4 12 3 657.69 563.20 49.38 o 5 12 3 182.47 160.22 40.75 o 6 12 3 213.13 240.35 54.19 o 7 12 3 26.07 61.30 57.17 o 1 13 3 742.37 746.88 44.40 o 2 13 3 168.73 191.60 43.92 o 3 13 3 39.59 37.01 49.19 o 4 13 3 13.93 43.12 47.23 o 5 13 3 480.05 424.50 58.15 o 6 13 3 10.33 70.16 54.21 o 0 14 3 444.53 438.45 62.23 o 1 14 3 1195.45 1242.75 51.20 o 2 14 3 597.52 575.10 51.50 o 3 14 3 45.74 58.63 53.71 o 4 14 3 3.27 16.80 54.77 o 5 14 3 154.80 131.19 60.92 o 1 15 3 38.84 58.01 47.64 o 2 15 3 5.30 64.52 48.73 o 3 15 3 158.67 170.91 57.30 o 4 15 3 17.24 -47.05 81.37 o 0 16 3 30.09 -11.78 65.18 o 1 16 3 2240.82 2240.74 72.69 o 1 0 4 22025.70 22098.84 173.48 o 2 0 4 13512.33 12651.18 139.99 o 3 0 4 3251.34 3879.19 62.44 o 4 0 4 2486.28 2230.65 65.74 o 5 0 4 425.88 387.14 130.66 o 6 0 4 758.42 655.75 36.41 o 7 0 4 2.46 -32.04 34.21 o 8 0 4 233.49 162.11 49.83 o 9 0 4 219.76 318.21 99.69 o 10 0 4 123.70 216.82 60.23 o 1 1 4 335.95 337.31 18.55 o 2 1 4 785.33 730.21 14.52 o 3 1 4 1051.92 859.01 22.60 o 4 1 4 778.77 857.20 58.53 o 5 1 4 206.59 211.99 22.54 o 6 1 4 45.84 61.39 20.51 o 7 1 4 32.26 16.48 24.00 o 9 1 4 3.60 42.09 36.91 o 0 2 4 10231.81 10663.42 157.31 o 1 2 4 625.41 678.07 56.59 o 2 2 4 4445.88 4040.66 138.83 o 3 2 4 1406.29 1236.09 79.19 o 4 2 4 677.21 767.49 99.89 o 5 2 4 1272.18 1106.41 24.36 o 6 2 4 80.95 143.96 21.68 o 7 2 4 259.96 240.79 24.65 o 8 2 4 27.80 41.16 29.97 o 9 2 4 0.74 32.76 38.45 o 10 2 4 4.85 23.78 47.44 o 1 3 4 65.38 54.49 13.54 o 2 3 4 29.90 19.03 12.46 o 3 3 4 0.33 -3.23 15.61 o 4 3 4 4083.20 3837.34 60.57 o 5 3 4 2.29 -1.30 18.80 o 6 3 4 431.55 424.02 24.71 o 7 3 4 251.38 293.30 26.39 o 9 3 4 254.09 417.75 42.83 o 0 4 4 794.14 807.00 30.55 o 2 4 4 1777.73 1936.80 33.66 o 3 4 4 232.59 330.49 51.94 o 4 4 4 1105.79 1108.76 26.83 o 5 4 4 237.14 248.32 22.95 o 6 4 4 212.93 222.84 25.02 o 7 4 4 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8 20.84 22.16 26.16 o 5 6 8 1156.46 979.20 53.07 o 6 6 8 41.25 70.83 27.66 o 7 6 8 10.05 16.17 31.95 o 8 6 8 20.40 33.80 36.29 o 9 6 8 21.00 82.25 39.80 o 1 7 8 670.89 676.36 26.38 o 2 7 8 447.96 430.07 21.62 o 3 7 8 58.80 60.57 23.80 o 4 7 8 157.16 170.80 35.35 o 5 7 8 1110.72 1005.12 76.10 o 6 7 8 198.62 153.47 30.01 o 7 7 8 247.04 261.65 33.73 o 8 7 8 82.81 120.11 41.74 o 9 7 8 131.57 196.88 49.51 o 0 8 8 464.28 522.06 27.55 o 1 8 8 1861.32 2178.46 39.76 o 2 8 8 26.05 48.76 21.79 o 3 8 8 1698.77 1604.99 38.15 o 4 8 8 9.51 35.16 27.40 o 5 8 8 992.95 873.71 35.60 o 6 8 8 91.07 144.76 31.57 o 7 8 8 4.33 24.84 31.06 o 8 8 8 0.03 70.67 46.13 o 1 9 8 183.75 191.90 32.32 o 2 9 8 52.51 86.35 30.91 o 3 9 8 34.95 63.07 30.78 o 4 9 8 131.22 92.79 32.84 o 5 9 8 5.14 16.79 39.55 o 6 9 8 7.58 -1.88 38.17 o 7 9 8 63.30 76.23 45.69 o 8 9 8 81.45 69.31 49.95 o 0 10 8 334.38 360.06 50.76 o 1 10 8 62.06 73.25 31.64 o 2 10 8 57.27 125.84 37.73 o 3 10 8 3054.15 2829.85 60.18 o 4 10 8 317.06 239.35 35.38 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1656.07 44.07 o 2 5 9 11.83 19.39 11.27 o 3 5 9 289.42 265.98 22.11 o 4 5 9 6.11 66.15 19.70 o 5 5 9 980.51 913.18 34.76 o 6 5 9 259.30 241.49 28.63 o 7 5 9 1049.98 1289.30 94.28 o 8 5 9 25.26 34.23 35.25 o 9 5 9 68.98 93.65 39.43 o 0 6 9 933.69 908.44 30.95 o 1 6 9 1872.06 2160.04 58.95 o 2 6 9 72.55 69.89 11.95 o 3 6 9 209.74 232.78 23.34 o 4 6 9 119.70 89.89 25.15 o 5 6 9 117.60 120.53 25.21 o 6 6 9 323.19 325.05 29.92 o 7 6 9 293.00 257.64 32.23 o 8 6 9 1.91 -22.27 37.64 o 9 6 9 259.62 261.25 42.04 o 1 7 9 665.91 793.32 53.28 o 2 7 9 56.13 83.43 22.16 o 3 7 9 35.21 48.18 23.57 o 4 7 9 4.67 20.99 27.68 o 5 7 9 12.63 8.98 28.24 o 6 7 9 7.80 43.73 29.88 o 7 7 9 1.90 33.46 33.90 o 8 7 9 7.40 46.77 41.69 o 9 7 9 10.28 72.61 45.42 o 0 8 9 1231.97 1385.74 48.01 o 1 8 9 704.97 739.81 34.51 o 2 8 9 69.55 93.83 28.25 o 3 8 9 578.15 556.36 33.59 o 4 8 9 69.30 41.29 31.46 o 5 8 9 474.10 372.57 35.25 o 6 8 9 13.08 51.74 36.09 o 7 8 9 6.92 36.13 36.51 o 8 8 9 16.29 17.61 47.42 o 1 9 9 139.45 160.70 32.20 o 2 9 9 1.33 28.93 31.08 o 3 9 9 103.47 125.52 32.08 o 4 9 9 846.29 733.58 37.92 o 5 9 9 391.83 340.50 36.74 o 6 9 9 4.39 16.67 39.84 o 7 9 9 59.92 93.46 38.29 o 8 9 9 6.90 78.17 49.73 o 0 10 9 33.16 6.38 47.69 o 1 10 9 84.62 104.44 36.77 o 2 10 9 0.08 15.85 36.67 o 3 10 9 41.09 75.76 32.57 o 4 10 9 266.61 249.31 36.09 o 5 10 9 2.34 9.71 37.29 o 6 10 9 13.96 45.03 37.67 o 7 10 9 2.53 60.73 48.43 o 1 11 9 34.66 34.34 37.99 o 2 11 9 269.45 353.19 45.43 o 3 11 9 0.63 21.19 37.36 o 4 11 9 9.82 -1.88 38.95 o 5 11 9 71.26 32.39 37.61 o 6 11 9 58.70 49.37 40.38 o 7 11 9 72.37 118.16 47.13 o 0 12 9 944.76 922.53 86.64 o 1 12 9 31.89 128.74 41.03 o 2 12 9 128.53 128.05 45.54 o 3 12 9 1085.87 964.51 51.83 o 4 12 9 143.96 141.45 45.13 o 5 12 9 11.89 52.62 49.93 o 6 12 9 69.10 87.40 47.57 o 1 13 9 115.28 120.91 43.65 o 2 13 9 153.88 124.67 44.86 o 3 13 9 0.02 53.54 49.76 o 4 13 9 26.36 54.21 49.73 o 5 13 9 20.32 24.00 47.47 o 0 14 9 231.85 312.85 83.41 o 1 14 9 85.95 129.28 59.06 o 2 14 9 0.37 18.00 50.42 o 3 14 9 122.15 110.08 52.42 o 4 14 9 5.70 43.41 48.62 o 1 15 9 216.07 244.32 62.68 o 2 15 9 7.03 -8.86 59.38 o 0 0 10 14611.00 14956.43 259.66 o 1 0 10 651.55 659.23 85.95 o 2 0 10 7190.78 7450.52 140.67 o 3 0 10 1081.09 1056.47 27.22 o 4 0 10 2220.48 2516.30 53.69 o 5 0 10 104.25 113.79 28.93 o 6 0 10 0.63 48.89 39.43 o 7 0 10 35.32 54.69 48.06 o 8 0 10 461.04 442.42 51.34 o 9 0 10 862.12 935.90 121.38 o 10 0 10 70.51 177.04 71.44 o 1 1 10 538.38 621.93 28.46 o 2 1 10 1447.53 1589.70 26.53 o 3 1 10 554.51 608.08 36.26 o 4 1 10 66.07 68.86 19.88 o 5 1 10 210.72 189.73 20.40 o 6 1 10 6.79 38.36 24.96 o 7 1 10 209.27 211.39 31.70 o 8 1 10 249.92 293.38 35.52 o 9 1 10 104.85 210.95 41.78 o 10 1 10 133.45 215.73 51.10 o 0 2 10 15291.87 16550.04 223.20 o 1 2 10 71.96 60.10 16.12 o 2 2 10 4687.75 4965.72 131.62 o 3 2 10 1157.33 1197.53 21.01 o 4 2 10 194.63 133.45 20.16 o 5 2 10 522.79 496.22 25.22 o 6 2 10 658.58 685.17 35.10 o 7 2 10 105.76 116.91 27.10 o 8 2 10 24.91 32.79 31.44 o 10 2 10 12.50 6.90 58.69 o 1 3 10 1684.99 1848.27 29.27 o 2 3 10 10.68 29.46 17.60 o 3 3 10 24.25 28.91 16.70 o 4 3 10 232.63 225.76 24.90 o 5 3 10 2.36 -3.63 22.43 o 6 3 10 26.76 38.05 24.75 o 7 3 10 404.76 375.05 29.22 o 8 3 10 0.14 74.24 31.86 o 9 3 10 155.82 187.28 42.66 o 0 4 10 341.33 354.91 33.51 o 1 4 10 39.39 61.82 13.00 o 2 4 10 377.17 409.53 20.59 o 3 4 10 131.93 199.46 31.25 o 4 4 10 287.11 273.94 24.65 o 5 4 10 199.10 199.57 43.10 o 6 4 10 0.81 16.31 25.79 o 7 4 10 22.23 65.42 29.15 o 8 4 10 0.00 32.64 31.40 o 9 4 10 93.32 79.05 42.06 o 1 5 10 892.94 1041.85 27.21 o 2 5 10 9.97 11.58 16.66 o 3 5 10 5.85 16.20 16.39 o 4 5 10 17.14 22.39 20.93 o 5 5 10 0.02 5.03 24.70 o 6 5 10 55.89 69.14 27.69 o 7 5 10 354.74 397.66 32.67 o 8 5 10 155.65 169.92 36.91 o 9 5 10 2.21 8.85 42.02 o 0 6 10 876.07 1031.84 32.44 o 1 6 10 37.19 44.07 19.52 o 2 6 10 272.20 260.56 27.62 o 3 6 10 4.34 28.80 22.20 o 4 6 10 593.83 543.12 26.11 o 5 6 10 905.52 768.07 29.64 o 6 6 10 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397.25 387.26 41.45 o 7 10 10 28.53 95.39 45.52 o 1 11 10 5.99 35.89 38.65 o 2 11 10 1.93 37.22 38.80 o 3 11 10 392.80 404.79 40.91 o 4 11 10 297.16 215.54 41.34 o 5 11 10 20.01 35.93 40.05 o 6 11 10 49.35 45.18 40.35 o 7 11 10 6.31 10.94 47.29 o 0 12 10 33.94 -15.74 74.20 o 1 12 10 18.15 51.83 40.86 o 2 12 10 3.44 65.91 50.21 o 3 12 10 209.90 236.54 45.06 o 4 12 10 2.46 17.05 52.85 o 5 12 10 351.75 296.86 45.72 o 6 12 10 28.53 16.11 48.47 o 1 13 10 577.97 618.39 55.62 o 2 13 10 85.03 64.17 43.63 o 3 13 10 32.54 51.55 45.57 o 4 13 10 4.81 48.85 46.70 o 5 13 10 1.17 9.24 58.85 o 0 14 10 26.24 72.71 80.35 o 1 14 10 54.59 46.32 58.93 o 2 14 10 99.88 119.54 50.99 o 3 14 10 14.97 17.96 48.38 o 4 14 10 105.26 98.52 50.01 o 1 15 10 39.36 72.42 62.54 o 2 15 10 0.32 14.16 84.44 o 1 1 11 80.76 110.80 20.26 o 3 1 11 2840.94 2869.39 48.78 o 4 1 11 85.53 68.72 13.62 o 5 1 11 217.81 255.60 46.68 o 6 1 11 781.45 810.28 77.40 o 7 1 11 21.53 92.64 31.56 o 8 1 11 95.38 159.96 35.23 o 9 1 11 399.60 516.47 46.01 o 0 2 11 15322.13 15754.79 113.20 o 1 2 11 861.63 930.52 35.41 o 2 2 11 1412.94 1611.70 77.08 o 3 2 11 91.45 97.09 17.29 o 4 2 11 13.47 1.10 20.66 o 5 2 11 365.73 378.53 26.59 o 6 2 11 1216.44 1150.25 41.27 o 7 2 11 13.39 21.31 31.57 o 8 2 11 0.59 17.81 34.08 o 9 2 11 419.36 503.78 45.88 o 1 3 11 993.53 1106.57 21.62 o 2 3 11 77.42 98.81 18.54 o 3 3 11 101.73 127.28 17.56 o 4 3 11 226.15 270.50 34.56 o 5 3 11 758.19 762.16 51.43 o 6 3 11 15.88 9.76 25.44 o 8 3 11 111.74 134.23 39.26 o 9 3 11 35.21 58.63 41.80 o 0 4 11 3.42 27.67 30.96 o 1 4 11 46.05 6.92 12.72 o 2 4 11 883.39 895.49 22.94 o 3 4 11 53.74 54.03 19.32 o 4 4 11 1310.96 1155.43 48.84 o 5 4 11 843.68 779.23 41.85 o 6 4 11 33.30 33.84 26.57 o 7 4 11 336.96 269.47 35.65 o 8 4 11 162.98 192.26 35.87 o 9 4 11 19.57 52.39 44.33 o 1 5 11 440.97 496.43 30.91 o 2 5 11 1377.50 1391.39 35.75 o 3 5 11 87.27 79.73 17.60 o 4 5 11 154.59 123.98 22.05 o 5 5 11 146.75 106.04 25.66 o 6 5 11 63.79 128.84 28.88 o 7 5 11 732.94 692.65 35.61 o 8 5 11 53.98 50.02 32.54 o 9 5 11 4.21 4.80 50.43 o 0 6 11 419.54 401.58 31.00 o 1 6 11 380.11 405.44 22.18 o 2 6 11 1.23 9.31 25.66 o 3 6 11 178.22 174.26 25.34 o 4 6 11 891.14 810.06 29.53 o 5 6 11 1.30 16.74 26.69 o 6 6 11 401.69 289.43 30.40 o 7 6 11 56.54 80.55 31.49 o 8 6 11 0.65 13.24 42.83 o 9 6 11 77.58 94.24 49.04 o 1 7 11 99.69 135.50 22.48 o 2 7 11 477.46 519.05 29.43 o 3 7 11 40.91 56.82 28.68 o 4 7 11 293.25 243.62 32.07 o 5 7 11 138.06 185.35 39.37 o 6 7 11 25.46 22.52 38.45 o 7 7 11 135.52 126.95 39.70 o 8 7 11 77.85 137.27 48.56 o 0 8 11 7.12 -3.55 36.12 o 1 8 11 97.16 111.08 27.10 o 2 8 11 1190.38 1172.88 35.79 o 3 8 11 1754.52 1644.35 53.16 o 4 8 11 1082.23 889.65 38.63 o 5 8 11 138.93 147.51 37.31 o 6 8 11 657.97 550.16 42.49 o 7 8 11 19.01 38.35 39.97 o 8 8 11 150.19 163.29 50.39 o 1 9 11 2.00 43.95 31.61 o 2 9 11 15.04 38.53 36.95 o 3 9 11 4.51 41.89 32.37 o 4 9 11 131.89 113.58 34.41 o 5 9 11 593.55 489.50 39.25 o 6 9 11 128.79 128.22 37.86 o 7 9 11 79.42 95.30 42.48 o 8 9 11 9.48 87.03 51.33 o 0 10 11 4.33 -24.61 52.77 o 1 10 11 36.16 30.34 36.29 o 2 10 11 513.91 528.11 39.77 o 3 10 11 6.36 34.49 39.05 o 4 10 11 253.69 248.21 36.60 o 5 10 11 97.64 50.81 39.41 o 6 10 11 0.95 42.60 38.59 o 7 10 11 119.91 145.72 41.45 o 1 11 11 407.05 396.12 42.31 o 2 11 11 0.10 37.96 42.46 o 3 11 11 34.88 86.93 38.42 o 4 11 11 106.02 68.23 40.17 o 5 11 11 138.34 62.26 41.86 o 6 11 11 12.16 29.53 40.75 o 0 12 11 22.52 88.42 77.31 o 1 12 11 1079.54 1102.74 63.72 o 2 12 11 620.95 540.62 44.22 o 3 12 11 92.03 117.56 41.05 o 4 12 11 334.49 293.36 44.25 o 5 12 11 186.71 130.44 44.69 o 6 12 11 0.52 32.41 48.50 o 1 13 11 7.67 19.52 49.35 o 2 13 11 17.99 74.46 48.81 o 3 13 11 39.26 76.50 46.33 o 4 13 11 11.25 17.87 50.96 o 5 13 11 142.49 146.47 50.37 o 0 14 11 936.15 1002.50 99.48 o 1 14 11 198.88 256.17 60.98 o 2 14 11 16.95 36.22 53.80 o 3 14 11 4.17 48.42 48.15 o 1 15 11 226.22 224.33 64.27 o 0 0 12 5783.86 7138.88 115.87 o 1 0 12 8070.51 7803.34 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24 92.25 140.45 47.03 o 1 4 24 136.90 111.12 33.27 o 2 4 24 17.75 42.56 38.37 o 3 4 24 29.45 27.61 58.52 o 4 4 24 227.03 239.91 57.22 o 5 4 24 7.29 63.66 59.02 o 1 5 24 0.37 7.21 33.67 o 2 5 24 0.00 4.98 39.69 o 3 5 24 3.97 12.39 54.48 o 4 5 24 7.08 34.80 56.21 o 5 5 24 0.48 21.74 53.38 o 0 6 24 36.31 92.24 56.93 o 1 6 24 19.66 1.62 35.51 o 2 6 24 110.76 128.93 39.74 o 3 6 24 298.13 364.40 46.99 o 4 6 24 123.81 142.00 58.85 o 1 7 24 28.21 35.31 40.47 o 2 7 24 19.11 45.58 44.16 o 3 7 24 3.16 35.35 49.85 o 4 7 24 20.80 10.79 60.98 o 0 8 24 245.62 309.21 57.14 o 1 8 24 3.49 19.51 42.55 o 2 8 24 119.22 101.57 43.42 o 3 8 24 1.90 2.17 50.60 o 1 9 24 27.44 53.87 44.21 o 1 1 25 0.53 71.36 40.37 o 2 1 25 1.49 38.23 46.21 o 3 1 25 0.00 57.59 70.89 o 4 1 25 18.01 7.42 75.02 o 5 1 25 48.34 96.20 58.82 o 0 2 25 0.03 49.00 52.55 o 1 2 25 7.43 9.00 40.46 o 2 2 25 11.48 69.35 64.46 o 3 2 25 30.16 75.31 59.54 o 4 2 25 39.03 40.10 77.55 o 5 2 25 15.27 22.72 68.89 o 1 3 25 6.64 5.86 37.73 o 2 3 25 5.91 14.33 42.86 o 3 3 25 37.33 78.82 59.12 o 4 3 25 9.77 105.50 61.06 o 5 3 25 2.56 76.60 58.31 o 0 4 25 23.81 23.33 57.02 o 1 4 25 184.98 203.50 35.47 o 2 4 25 96.13 92.91 41.82 o 3 4 25 79.70 115.68 48.78 o 4 4 25 106.47 95.08 55.81 o 1 5 25 23.34 42.30 39.57 o 2 5 25 12.84 40.27 46.55 o 3 5 25 107.67 166.95 49.89 o 4 5 25 93.23 123.77 57.95 o 0 6 25 28.38 20.27 51.54 o 1 6 25 274.42 390.43 42.86 o 2 6 25 23.32 29.96 40.80 o 3 6 25 26.13 60.67 44.51 o 1 7 25 15.95 29.47 45.41 o 2 7 25 3.19 55.62 62.23 o 3 7 25 0.59 50.52 46.55 o 0 8 25 173.89 189.18 57.39 o 1 8 25 71.34 101.35 47.51 o 0 0 26 280.87 297.01 96.49 o 1 0 26 7.28 68.51 64.90 o 2 0 26 7.80 32.46 68.92 o 3 0 26 23.95 13.78 101.82 o 4 0 26 46.08 49.47 110.47 o 1 1 26 9.05 53.62 41.02 o 2 1 26 0.00 50.62 46.96 o 3 1 26 2.52 14.50 76.92 o 4 1 26 85.52 158.01 76.89 o 0 2 26 218.91 294.25 89.29 o 1 2 26 58.85 -7.92 42.03 o 2 2 26 93.70 164.05 50.02 o 3 2 26 104.56 157.87 65.19 o 4 2 26 27.89 35.75 75.16 o 1 3 26 0.02 30.01 43.49 o 2 3 26 6.68 -8.77 50.44 o 3 3 26 16.84 30.39 63.71 o 4 3 26 3.31 104.05 66.79 o 0 4 26 239.44 272.94 54.20 o 1 4 26 38.96 59.51 38.08 o 2 4 26 79.15 78.36 51.99 o 3 4 26 7.87 55.03 54.82 o 4 4 26 10.99 42.74 57.48 o 1 5 26 0.81 22.20 40.22 o 2 5 26 10.80 26.90 43.56 o 3 5 26 0.26 57.12 67.01 o 0 6 26 180.46 160.39 53.99 o 1 6 26 15.14 57.41 41.29 o 2 6 26 35.21 55.79 45.03 o 1 7 26 22.16 71.16 43.00 o 1 1 27 5.42 -2.90 47.54 o 2 1 27 0.30 18.69 60.43 o 3 1 27 5.60 15.07 63.01 o 4 1 27 28.48 47.31 82.79 o 0 2 27 8.82 26.52 67.37 o 1 2 27 45.33 16.73 43.05 o 2 2 27 89.39 131.45 52.00 o 3 2 27 15.49 153.34 80.49 o 1 3 27 0.26 -3.31 56.34 o 2 3 27 19.22 20.39 52.35 o 3 3 27 103.81 165.97 66.99 o 0 4 27 8.26 34.76 73.14 o 1 4 27 64.68 33.54 52.53 o 2 4 27 0.00 15.90 53.88 o 3 4 27 2.17 43.88 66.05 o 1 5 27 77.92 121.40 45.25 o 2 5 27 0.36 36.71 48.13 o 0 6 27 47.12 132.31 56.21 o 1 6 27 39.06 76.76 43.27 o 0 0 28 190.31 203.98 99.63 o 1 0 28 18.12 -15.00 69.53 o 2 0 28 359.68 349.72 120.54 o 3 0 28 0.87 8.39 109.45 o 1 1 28 0.11 13.05 49.11 o 2 1 28 43.29 113.83 62.14 o 3 1 28 1.59 50.25 66.97 o 0 2 28 0.06 26.42 69.53 o 1 2 28 1.31 29.24 49.88 o 2 2 28 0.87 101.41 63.36 o 1 3 28 8.08 22.21 53.56 o 2 3 28 5.63 7.11 65.92 o 0 4 28 46.38 19.75 75.19 o 1 4 28 15.88 45.17 55.52 o 1 1 29 37.09 86.49 51.52 o 0 2 29 0.42 164.19 104.58 o