#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219602.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219602_Fobs loop_ _publ_author_name 'Ma, Qi' 'Lu, Li-Ping' 'Zhu, Miao-Li' _publ_section_title ; 1,2-Bis(2-furylmethylene)hydrazine ; _journal_coeditor_code HB2802 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2026 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8773 _cell_length_b 8.9956 _cell_length_c 15.1714 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file hb2802Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MQ172-61 in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 132.38 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2323.53 2489.99 35.15 o 4 0 0 743.31 730.38 21.82 o 6 0 0 0.01 0.30 1.09 o 8 0 0 7.24 9.55 2.33 o 2 1 0 495.59 481.78 6.68 o 4 1 0 126.87 144.28 2.45 o 6 1 0 16.29 16.31 1.48 o 8 1 0 0.85 1.23 1.33 o 2 2 0 0.18 0.53 0.31 o 4 2 0 490.69 559.80 18.10 o 6 2 0 2.07 1.65 0.96 o 8 2 0 0.72 1.00 1.55 o 2 3 0 371.22 362.90 5.55 o 4 3 0 333.32 307.51 10.90 o 6 3 0 12.77 11.02 1.51 o 0 4 0 286.28 266.61 6.44 o 2 4 0 424.53 442.02 10.65 o 4 4 0 165.96 182.37 4.01 o 6 4 0 3.74 2.89 1.11 o 2 5 0 199.96 205.90 8.28 o 4 5 0 117.74 124.33 3.54 o 6 5 0 27.76 26.86 2.27 o 0 6 0 69.07 77.34 4.41 o 2 6 0 4.04 5.73 0.96 o 4 6 0 61.32 59.52 3.95 o 6 6 0 0.80 0.00 1.16 o 2 7 0 308.13 294.88 18.61 o 4 7 0 35.20 35.18 2.37 o 6 7 0 20.56 19.70 2.85 o 0 8 0 146.56 167.80 7.72 o 2 8 0 114.06 121.80 6.88 o 4 8 0 18.79 19.67 2.02 o 2 9 0 42.24 40.41 3.12 o 4 9 0 4.87 6.99 2.16 o 0 10 0 13.18 13.52 3.19 o 2 10 0 21.21 22.69 2.87 o 1 1 1 1085.48 1030.75 9.62 o 2 1 1 92.87 82.02 1.25 o 3 1 1 50.20 52.02 0.87 o 4 1 1 82.35 92.83 1.33 o 5 1 1 58.61 63.16 1.42 o 6 1 1 93.62 98.53 2.07 o 7 1 1 148.15 170.85 3.18 o 8 1 1 3.09 3.43 1.07 o 0 2 1 591.53 614.66 6.38 o 1 2 1 8.52 6.50 0.31 o 2 2 1 140.35 144.51 2.22 o 3 2 1 776.74 868.95 8.64 o 4 2 1 212.95 209.97 2.81 o 5 2 1 0.87 1.07 0.41 o 6 2 1 26.28 26.32 1.22 o 7 2 1 6.12 6.57 1.08 o 8 2 1 1.05 1.27 1.03 o 1 3 1 1138.81 1179.07 16.64 o 2 3 1 205.05 206.17 3.56 o 3 3 1 263.19 285.21 2.33 o 4 3 1 22.75 21.84 0.95 o 5 3 1 0.32 0.77 0.45 o 6 3 1 30.29 31.86 1.59 o 7 3 1 30.45 30.17 1.93 o 0 4 1 178.49 195.92 2.79 o 1 4 1 86.77 99.15 1.67 o 2 4 1 73.30 69.44 1.27 o 3 4 1 315.76 325.58 5.21 o 4 4 1 0.79 0.14 0.37 o 5 4 1 23.22 24.03 1.20 o 6 4 1 8.60 7.64 1.02 o 7 4 1 0.48 0.79 0.86 o 1 5 1 538.92 591.99 5.32 o 2 5 1 144.00 143.88 3.77 o 3 5 1 134.68 138.30 4.56 o 4 5 1 19.34 14.06 1.04 o 5 5 1 10.98 12.17 1.10 o 6 5 1 67.08 67.38 2.51 o 7 5 1 1.72 1.91 1.00 o 0 6 1 706.87 750.56 26.12 o 1 6 1 155.70 165.64 5.56 o 2 6 1 11.45 11.75 0.85 o 3 6 1 19.75 18.01 1.09 o 4 6 1 143.18 143.32 3.71 o 5 6 1 69.23 65.35 2.14 o 6 6 1 0.16 0.62 0.82 o 1 7 1 24.77 20.46 1.23 o 2 7 1 3.02 2.33 0.58 o 3 7 1 46.14 43.66 1.69 o 4 7 1 1.24 2.47 0.74 o 5 7 1 11.68 14.31 1.45 o 6 7 1 0.16 0.07 0.92 o 0 8 1 119.46 132.81 4.86 o 1 8 1 9.01 7.45 1.12 o 2 8 1 2.89 2.45 0.75 o 3 8 1 0.61 0.65 0.66 o 4 8 1 61.47 61.01 2.15 o 5 8 1 23.34 25.80 1.90 o 1 9 1 102.25 100.04 3.28 o 2 9 1 5.96 6.50 1.22 o 3 9 1 5.72 5.23 1.22 o 4 9 1 7.65 8.24 1.72 o 0 10 1 0.00 0.95 1.25 o 1 10 1 11.89 13.46 1.65 o 2 10 1 0.03 0.26 0.96 o 0 0 2 663.56 707.50 6.03 o 1 0 2 2849.76 2699.69 56.34 o 2 0 2 256.31 268.12 3.90 o 3 0 2 68.42 70.46 1.44 o 4 0 2 19.98 16.78 0.91 o 5 0 2 254.00 266.09 5.38 o 6 0 2 16.46 16.97 1.51 o 7 0 2 46.40 50.45 2.46 o 8 0 2 13.63 15.93 2.73 o 1 1 2 62.05 63.56 1.18 o 2 1 2 19.18 15.20 0.45 o 3 1 2 407.65 434.02 4.77 o 4 1 2 3.05 2.09 0.35 o 5 1 2 51.64 52.06 1.36 o 6 1 2 21.91 22.72 1.15 o 7 1 2 3.24 3.79 0.92 o 8 1 2 0.03 0.00 0.93 o 0 2 2 1404.12 1453.47 12.89 o 1 2 2 550.71 519.99 11.86 o 2 2 2 52.89 68.09 0.92 o 3 2 2 59.94 63.59 1.27 o 4 2 2 5.56 7.53 0.51 o 5 2 2 0.90 1.13 0.43 o 6 2 2 15.27 15.33 1.01 o 7 2 2 0.37 0.57 0.73 o 1 3 2 23.39 16.75 0.55 o 2 3 2 65.04 68.00 1.11 o 3 3 2 267.92 273.75 3.50 o 4 3 2 69.00 69.97 1.58 o 5 3 2 20.53 20.66 1.10 o 6 3 2 48.02 46.69 1.81 o 7 3 2 13.54 12.69 1.46 o 0 4 2 666.69 672.77 4.86 o 1 4 2 128.06 126.56 1.79 o 2 4 2 339.55 334.05 5.58 o 3 4 2 0.16 0.33 0.28 o 4 4 2 0.91 0.53 0.40 o 5 4 2 123.86 114.53 2.32 o 6 4 2 7.26 7.86 1.01 o 7 4 2 29.69 30.37 2.01 o 1 5 2 378.98 390.96 5.44 o 2 5 2 132.19 129.07 3.35 o 3 5 2 68.92 64.48 2.15 o 4 5 2 135.44 131.72 3.31 o 5 5 2 85.26 75.46 2.20 o 6 5 2 4.38 3.88 0.97 o 7 5 2 7.59 7.77 1.37 o 0 6 2 2.84 8.21 3.57 o 1 6 2 32.91 34.25 1.91 o 2 6 2 72.22 74.83 2.25 o 3 6 2 7.12 6.09 0.71 o 4 6 2 2.34 2.73 0.63 o 5 6 2 15.80 13.56 1.36 o 6 6 2 3.49 3.87 1.03 o 1 7 2 252.26 264.58 9.36 o 2 7 2 83.51 86.06 2.59 o 3 7 2 171.45 170.40 6.74 o 4 7 2 67.99 61.01 2.25 o 5 7 2 105.21 98.99 5.00 o 6 7 2 0.24 1.28 0.98 o 0 8 2 95.39 90.40 4.06 o 1 8 2 0.60 0.14 0.64 o 2 8 2 3.13 3.21 0.80 o 3 8 2 11.90 14.23 1.45 o 4 8 2 2.32 2.97 1.08 o 5 8 2 12.93 15.14 1.58 o 1 9 2 30.27 33.06 2.04 o 2 9 2 46.80 49.68 2.45 o 3 9 2 21.13 20.29 3.24 o 4 9 2 3.76 3.61 1.23 o 0 10 2 38.82 38.26 3.26 o 1 10 2 0.59 0.80 0.91 o 2 10 2 0.00 0.00 0.96 o 1 1 3 17523.31 11510.51 1775.85 o 2 1 3 600.76 606.17 5.40 o 3 1 3 324.91 336.60 4.04 o 4 1 3 1.54 1.45 0.32 o 5 1 3 54.61 55.82 1.40 o 6 1 3 199.15 206.66 3.24 o 7 1 3 0.37 0.75 0.78 o 8 1 3 2.76 3.42 1.34 o 0 2 3 758.19 702.74 21.39 o 1 2 3 1131.90 1115.32 11.65 o 2 2 3 38.80 36.22 0.61 o 3 2 3 17.86 21.18 0.66 o 4 2 3 268.29 288.60 3.53 o 5 2 3 139.72 129.06 2.57 o 6 2 3 24.17 24.15 1.29 o 7 2 3 10.50 10.84 1.34 o 1 3 3 23.06 21.63 0.59 o 2 3 3 0.04 0.58 0.21 o 3 3 3 221.77 247.05 3.16 o 4 3 3 33.02 36.50 1.10 o 5 3 3 34.53 35.70 1.45 o 6 3 3 24.76 27.66 1.52 o 7 3 3 1.23 0.75 0.72 o 0 4 3 149.29 176.06 2.17 o 1 4 3 145.38 135.01 1.67 o 2 4 3 102.38 117.01 1.63 o 3 4 3 94.03 86.83 1.50 o 4 4 3 5.65 5.44 0.65 o 5 4 3 31.16 28.72 1.40 o 6 4 3 11.06 11.38 1.17 o 7 4 3 0.15 1.21 0.78 o 1 5 3 247.43 270.71 4.08 o 2 5 3 2.36 2.66 0.40 o 3 5 3 46.85 49.23 1.54 o 4 5 3 42.33 45.31 1.65 o 5 5 3 10.77 9.92 1.07 o 6 5 3 0.00 0.45 0.66 o 7 5 3 0.04 0.44 0.95 o 0 6 3 79.67 99.37 2.82 o 1 6 3 25.99 22.88 1.17 o 2 6 3 159.05 161.46 2.36 o 3 6 3 136.70 135.61 3.11 o 4 6 3 102.81 91.88 2.38 o 5 6 3 1.20 0.50 0.63 o 6 6 3 0.38 0.83 0.82 o 1 7 3 35.19 33.88 1.71 o 2 7 3 41.36 36.91 1.47 o 3 7 3 0.02 0.80 0.57 o 4 7 3 17.20 19.62 1.50 o 5 7 3 4.98 5.32 1.11 o 6 7 3 0.18 0.28 0.92 o 0 8 3 0.22 0.93 0.98 o 1 8 3 15.92 14.30 1.38 o 2 8 3 30.38 27.41 1.59 o 3 8 3 31.15 32.13 2.09 o 4 8 3 37.24 34.54 2.20 o 5 8 3 1.28 2.04 1.16 o 1 9 3 72.89 80.78 4.52 o 2 9 3 26.44 22.03 2.14 o 3 9 3 2.47 4.12 1.20 o 4 9 3 3.64 2.43 1.13 o 0 10 3 1.20 3.15 1.61 o 1 10 3 1.03 1.06 0.95 o 2 10 3 1.49 2.82 1.37 o 0 0 4 4336.50 4263.65 77.54 o 1 0 4 6599.62 6139.58 159.99 o 2 0 4 543.33 531.82 4.79 o 3 0 4 590.88 656.40 10.85 o 4 0 4 282.50 320.79 10.43 o 5 0 4 26.51 30.40 1.49 o 6 0 4 59.99 62.57 7.46 o 7 0 4 8.63 10.73 2.07 o 1 1 4 639.33 655.46 6.75 o 2 1 4 562.13 541.91 5.13 o 3 1 4 77.29 83.33 1.14 o 4 1 4 83.53 89.18 1.43 o 5 1 4 19.11 19.30 0.87 o 6 1 4 4.99 4.02 0.80 o 7 1 4 0.02 0.00 0.83 o 0 2 4 11.54 13.80 2.58 o 1 2 4 2808.32 2910.43 36.37 o 2 2 4 41.18 38.03 0.69 o 3 2 4 277.96 293.46 2.43 o 4 2 4 109.17 112.42 2.09 o 5 2 4 5.95 6.06 0.72 o 6 2 4 26.79 25.16 1.31 o 7 2 4 0.00 0.00 0.82 o 1 3 4 476.31 491.50 4.59 o 2 3 4 407.39 433.92 5.59 o 3 3 4 150.26 148.74 2.47 o 4 3 4 148.11 160.76 2.86 o 5 3 4 59.57 57.89 1.85 o 6 3 4 1.70 2.25 0.74 o 7 3 4 0.05 0.34 0.81 o 0 4 4 1470.67 1554.82 62.56 o 1 4 4 397.55 453.92 6.80 o 2 4 4 436.08 494.68 8.25 o 3 4 4 89.72 89.99 2.41 o 4 4 4 0.01 0.18 0.42 o 5 4 4 99.92 98.26 2.44 o 6 4 4 4.52 3.70 0.84 o 7 4 4 10.16 12.48 1.34 o 1 5 4 0.06 0.62 0.31 o 2 5 4 54.13 56.22 1.33 o 3 5 4 40.04 38.34 1.26 o 4 5 4 60.10 55.96 1.80 o 5 5 4 29.65 27.35 1.54 o 6 5 4 14.51 12.10 1.27 o 7 5 4 0.00 0.12 0.82 o 0 6 4 58.28 94.47 15.93 o 1 6 4 5.33 6.22 0.68 o 2 6 4 72.89 77.45 1.59 o 3 6 4 50.25 44.14 1.61 o 4 6 4 0.02 0.36 0.53 o 5 6 4 26.98 27.78 1.63 o 6 6 4 2.47 3.21 0.95 o 1 7 4 8.95 10.26 1.01 o 2 7 4 132.21 126.72 2.62 o 3 7 4 4.35 4.74 0.93 o 4 7 4 8.57 8.50 1.07 o 5 7 4 2.28 1.54 0.80 o 0 8 4 233.63 218.37 10.47 o 1 8 4 13.59 14.52 1.40 o 2 8 4 2.96 3.85 0.94 o 3 8 4 21.52 23.48 2.01 o 4 8 4 2.29 1.77 1.00 o 5 8 4 0.22 0.23 1.03 o 1 9 4 7.82 9.46 1.37 o 2 9 4 1.38 0.83 0.86 o 3 9 4 0.07 0.00 0.84 o 4 9 4 1.54 2.98 1.26 o 0 10 4 54.59 44.70 3.48 o 1 10 4 6.51 6.47 1.56 o 2 10 4 3.27 3.12 1.36 o 1 1 5 783.77 847.90 9.47 o 2 1 5 952.67 995.85 7.06 o 3 1 5 30.67 35.68 0.79 o 4 1 5 3.35 3.95 0.47 o 5 1 5 10.59 9.20 0.79 o 6 1 5 2.10 2.74 0.79 o 7 1 5 0.11 0.75 0.95 o 0 2 5 974.58 1011.42 13.70 o 1 2 5 52.99 49.82 0.85 o 2 2 5 522.79 590.82 5.51 o 3 2 5 91.16 91.07 1.46 o 4 2 5 169.45 168.06 2.96 o 5 2 5 45.78 44.87 1.47 o 6 2 5 5.32 6.45 1.13 o 7 2 5 8.08 8.57 1.70 o 1 3 5 91.48 88.65 1.50 o 2 3 5 7.93 9.02 0.44 o 3 3 5 2.50 1.57 0.39 o 4 3 5 64.26 61.88 1.55 o 5 3 5 3.86 3.57 0.75 o 6 3 5 71.49 71.64 2.24 o 7 3 5 3.82 4.54 1.07 o 0 4 5 56.40 60.33 1.87 o 1 4 5 168.04 185.49 2.87 o 2 4 5 287.29 298.94 5.11 o 3 4 5 56.51 49.98 1.35 o 4 4 5 0.04 0.33 0.46 o 5 4 5 18.85 16.61 1.23 o 6 4 5 0.60 2.00 0.76 o 7 4 5 4.39 4.04 1.10 o 1 5 5 2.09 2.91 0.40 o 2 5 5 104.41 109.09 1.85 o 3 5 5 2.16 1.96 0.49 o 4 5 5 81.02 80.42 2.25 o 5 5 5 0.89 1.09 0.64 o 6 5 5 34.62 32.91 1.79 o 0 6 5 183.79 164.49 5.44 o 1 6 5 277.92 295.82 6.58 o 2 6 5 52.18 55.28 1.83 o 3 6 5 254.79 240.20 3.58 o 4 6 5 122.67 117.06 2.72 o 5 6 5 0.38 0.42 0.63 o 6 6 5 16.10 16.00 1.50 o 1 7 5 0.80 1.66 0.55 o 2 7 5 5.28 4.75 0.97 o 3 7 5 2.78 2.23 0.80 o 4 7 5 17.03 18.80 1.55 o 5 7 5 1.74 2.63 0.90 o 0 8 5 79.75 78.59 3.83 o 1 8 5 98.44 99.01 3.07 o 2 8 5 1.78 2.81 0.83 o 3 8 5 103.65 97.84 2.97 o 4 8 5 24.72 23.47 1.79 o 1 9 5 0.12 0.00 0.81 o 2 9 5 0.02 0.23 0.77 o 3 9 5 0.03 0.41 0.90 o 0 10 5 12.88 16.42 3.66 o 1 10 5 12.70 12.82 1.94 o 0 0 6 2085.89 2094.23 37.60 o 1 0 6 100.91 94.44 2.52 o 2 0 6 355.47 300.54 3.30 o 3 0 6 360.84 380.33 4.63 o 4 0 6 28.89 28.91 1.35 o 5 0 6 267.37 262.70 7.42 o 6 0 6 8.06 6.25 1.63 o 7 0 6 38.81 42.96 4.87 o 1 1 6 123.79 123.19 1.89 o 2 1 6 21.59 10.13 0.56 o 3 1 6 169.38 176.81 1.95 o 4 1 6 33.37 28.58 1.05 o 5 1 6 121.78 127.60 4.07 o 6 1 6 22.00 20.50 1.48 o 7 1 6 0.11 0.00 0.93 o 0 2 6 221.31 202.15 3.36 o 1 2 6 0.91 0.83 0.22 o 2 2 6 79.97 75.43 1.27 o 3 2 6 6.54 5.80 0.48 o 4 2 6 12.26 13.45 0.83 o 5 2 6 110.32 115.13 3.15 o 6 2 6 7.49 6.64 1.16 o 7 2 6 9.65 11.66 1.86 o 1 3 6 5.26 4.26 0.41 o 2 3 6 44.11 43.05 1.17 o 3 3 6 70.14 60.23 1.56 o 4 3 6 46.36 43.15 1.46 o 5 3 6 227.97 227.62 3.93 o 6 3 6 49.97 44.05 2.26 o 7 3 6 0.23 0.85 0.87 o 0 4 6 188.27 184.47 3.96 o 1 4 6 50.76 45.58 1.11 o 2 4 6 19.52 19.60 1.14 o 3 4 6 149.67 146.45 3.80 o 4 4 6 0.00 0.45 0.45 o 5 4 6 12.05 13.80 1.16 o 6 4 6 1.65 0.81 0.72 o 7 4 6 0.41 1.32 1.03 o 1 5 6 15.63 12.91 0.75 o 2 5 6 12.45 12.51 0.87 o 3 5 6 191.80 185.53 2.74 o 4 5 6 1.98 2.92 0.69 o 5 5 6 3.12 3.21 0.80 o 6 5 6 6.95 5.69 1.06 o 0 6 6 2.33 2.82 0.78 o 1 6 6 14.58 13.73 0.87 o 2 6 6 2.59 3.71 0.72 o 3 6 6 37.38 39.74 1.79 o 4 6 6 1.80 2.57 0.73 o 5 6 6 2.33 4.07 0.89 o 6 6 6 0.11 0.00 0.80 o 1 7 6 31.71 31.84 1.51 o 2 7 6 8.68 7.75 0.98 o 3 7 6 191.68 183.92 3.83 o 4 7 6 0.48 1.13 0.76 o 5 7 6 8.54 9.82 1.40 o 0 8 6 45.27 50.57 3.24 o 1 8 6 84.62 84.57 2.80 o 2 8 6 2.33 3.08 0.99 o 3 8 6 0.37 0.10 0.69 o 4 8 6 0.14 0.49 0.78 o 1 9 6 10.85 9.74 1.65 o 2 9 6 9.68 10.60 1.32 o 3 9 6 0.94 0.17 0.85 o 0 10 6 7.62 7.89 3.25 o 1 10 6 15.43 16.19 2.69 o 1 1 7 142.44 144.16 2.61 o 2 1 7 3298.57 3410.19 21.07 o 3 1 7 14.65 17.02 0.70 o 4 1 7 9.25 8.99 0.79 o 5 1 7 10.28 8.25 0.90 o 6 1 7 2.80 3.22 0.93 o 7 1 7 2.02 4.27 1.37 o 0 2 7 232.71 244.84 3.74 o 1 2 7 527.46 539.31 9.27 o 2 2 7 854.94 872.78 13.44 o 3 2 7 238.26 238.22 7.01 o 4 2 7 33.37 31.09 1.43 o 5 2 7 0.60 0.69 0.64 o 6 2 7 0.02 0.27 0.67 o 7 2 7 0.01 0.43 0.88 o 1 3 7 278.12 297.95 2.97 o 2 3 7 691.25 740.38 11.53 o 3 3 7 2.83 3.75 0.64 o 4 3 7 0.44 0.00 0.38 o 5 3 7 16.47 12.00 1.38 o 6 3 7 12.84 12.84 1.51 o 7 3 7 2.42 4.06 1.24 o 0 4 7 47.16 53.23 1.64 o 1 4 7 122.18 138.03 2.19 o 2 4 7 249.20 239.96 5.33 o 3 4 7 22.68 21.86 1.24 o 4 4 7 9.76 8.30 0.98 o 5 4 7 0.89 1.18 0.76 o 6 4 7 4.40 4.63 1.15 o 1 5 7 277.70 305.37 4.00 o 2 5 7 65.51 63.75 1.92 o 3 5 7 21.44 20.16 1.18 o 4 5 7 0.52 0.14 0.55 o 5 5 7 4.93 5.55 1.05 o 6 5 7 15.59 17.19 1.84 o 0 6 7 0.73 0.36 0.53 o 1 6 7 4.71 3.01 0.67 o 2 6 7 3.10 2.51 0.65 o 3 6 7 15.76 16.86 1.35 o 4 6 7 63.47 61.28 2.33 o 5 6 7 1.47 1.99 0.82 o 1 7 7 1.70 1.64 0.65 o 2 7 7 19.73 17.40 1.36 o 3 7 7 3.92 5.99 1.07 o 4 7 7 9.21 10.31 1.29 o 5 7 7 1.11 0.55 0.89 o 0 8 7 13.65 11.45 1.91 o 1 8 7 3.39 3.97 0.90 o 2 8 7 0.10 0.06 0.68 o 3 8 7 3.25 4.02 1.04 o 4 8 7 10.68 10.59 1.46 o 1 9 7 25.68 25.79 2.04 o 2 9 7 0.46 1.37 0.85 o 3 9 7 0.03 0.11 0.89 o 0 0 8 44.39 43.91 1.78 o 1 0 8 264.42 270.22 7.74 o 2 0 8 217.81 213.34 3.76 o 3 0 8 14.98 13.19 1.05 o 4 0 8 16.01 13.22 1.14 o 5 0 8 77.01 80.47 3.03 o 6 0 8 0.07 0.25 0.84 o 7 0 8 0.33 1.28 1.80 o 1 1 8 22.00 21.45 1.05 o 2 1 8 129.45 128.51 2.02 o 3 1 8 65.62 72.98 1.67 o 4 1 8 62.23 58.80 1.56 o 5 1 8 0.06 0.11 0.52 o 6 1 8 0.68 0.76 0.76 o 7 1 8 0.07 0.51 1.14 o 0 2 8 104.49 101.16 4.14 o 1 2 8 5.26 5.00 0.50 o 2 2 8 51.96 51.93 1.25 o 3 2 8 1.06 1.09 0.45 o 4 2 8 0.12 0.16 0.50 o 5 2 8 99.44 92.02 2.59 o 6 2 8 1.25 2.26 0.94 o 7 2 8 1.41 2.69 1.12 o 1 3 8 16.36 16.95 0.79 o 2 3 8 34.81 34.60 1.10 o 3 3 8 187.87 187.95 3.11 o 4 3 8 112.83 110.05 2.69 o 5 3 8 0.20 1.50 0.80 o 6 3 8 1.19 1.65 0.87 o 0 4 8 263.66 287.31 3.81 o 1 4 8 73.34 73.71 2.97 o 2 4 8 2.05 1.90 0.55 o 3 4 8 0.16 0.08 0.47 o 4 4 8 23.75 21.43 1.30 o 5 4 8 83.45 81.84 3.01 o 6 4 8 5.60 6.68 1.33 o 1 5 8 9.58 9.79 0.77 o 2 5 8 191.94 182.30 3.25 o 3 5 8 45.10 47.24 1.81 o 4 5 8 2.38 1.75 0.71 o 5 5 8 11.72 13.98 1.62 o 6 5 8 0.42 0.45 0.90 o 0 6 8 5.79 4.96 1.01 o 1 6 8 55.96 51.11 1.83 o 2 6 8 18.27 15.47 1.23 o 3 6 8 0.37 0.53 0.68 o 4 6 8 4.00 5.20 1.01 o 5 6 8 10.14 11.33 1.56 o 1 7 8 15.41 15.05 1.41 o 2 7 8 192.54 200.48 3.86 o 3 7 8 7.09 7.30 1.15 o 4 7 8 10.91 10.55 1.36 o 5 7 8 8.51 8.76 1.49 o 0 8 8 38.84 39.73 2.99 o 1 8 8 11.88 9.38 1.30 o 2 8 8 3.20 3.66 1.07 o 3 8 8 2.17 2.31 0.95 o 4 8 8 0.02 0.55 0.87 o 1 9 8 1.10 2.07 1.19 o 2 9 8 9.17 8.31 1.74 o 1 1 9 95.27 106.29 1.67 o 2 1 9 0.98 1.04 0.42 o 3 1 9 15.40 14.08 0.85 o 4 1 9 1.03 1.24 0.51 o 5 1 9 18.89 15.26 1.29 o 6 1 9 31.36 37.08 2.15 o 7 1 9 0.00 0.63 1.21 o 0 2 9 10.40 9.45 0.78 o 1 2 9 53.49 56.88 1.31 o 2 2 9 45.10 43.31 1.70 o 3 2 9 0.91 1.09 0.52 o 4 2 9 291.39 295.15 3.95 o 5 2 9 30.95 25.00 1.41 o 6 2 9 11.03 9.63 1.42 o 1 3 9 1.94 1.80 0.42 o 2 3 9 183.21 191.19 2.82 o 3 3 9 7.75 7.76 0.90 o 4 3 9 22.88 22.48 1.44 o 5 3 9 0.98 0.00 0.66 o 6 3 9 0.91 2.02 0.96 o 0 4 9 90.77 89.85 2.99 o 1 4 9 15.45 14.75 0.86 o 2 4 9 11.51 10.63 0.87 o 3 4 9 28.70 23.57 1.37 o 4 4 9 63.77 58.93 2.15 o 5 4 9 14.73 13.08 1.54 o 6 4 9 2.75 3.63 1.20 o 1 5 9 1.39 1.05 0.49 o 2 5 9 127.72 125.87 3.26 o 3 5 9 0.43 0.06 0.55 o 4 5 9 20.48 20.37 1.71 o 5 5 9 6.48 8.50 1.42 o 0 6 9 97.58 105.93 3.41 o 1 6 9 6.48 5.76 0.86 o 2 6 9 103.67 103.55 2.69 o 3 6 9 60.81 52.10 2.08 o 4 6 9 7.37 8.33 1.23 o 5 6 9 0.85 1.07 0.99 o 1 7 9 2.91 3.21 0.78 o 2 7 9 1.50 2.39 0.84 o 3 7 9 1.75 2.38 0.91 o 4 7 9 2.98 3.88 1.10 o 0 8 9 67.25 75.28 4.16 o 1 8 9 15.80 16.27 1.47 o 2 8 9 18.90 17.01 2.00 o 3 8 9 10.68 8.34 1.36 o 1 9 9 0.00 0.09 0.88 o 0 0 10 5.20 6.43 0.99 o 1 0 10 547.21 600.20 19.45 o 2 0 10 51.14 55.53 2.20 o 3 0 10 338.04 332.04 8.61 o 4 0 10 29.54 24.95 1.93 o 5 0 10 0.60 2.85 1.00 o 6 0 10 0.16 0.40 1.16 o 1 1 10 47.56 49.33 1.40 o 2 1 10 77.30 81.62 3.10 o 3 1 10 120.79 116.24 2.13 o 4 1 10 1.38 1.87 0.63 o 5 1 10 10.79 11.68 1.20 o 6 1 10 0.01 0.62 0.87 o 0 2 10 8.81 10.68 1.10 o 1 2 10 171.82 180.07 5.60 o 2 2 10 6.39 7.23 0.75 o 3 2 10 133.76 124.29 2.76 o 4 2 10 58.39 55.07 1.84 o 5 2 10 0.04 0.69 0.66 o 6 2 10 0.48 1.17 0.91 o 1 3 10 91.14 90.54 2.45 o 2 3 10 186.08 201.41 4.77 o 3 3 10 154.89 150.84 3.12 o 4 3 10 10.51 11.12 1.06 o 5 3 10 5.94 4.08 0.97 o 6 3 10 0.48 1.00 0.99 o 0 4 10 133.42 147.87 3.72 o 1 4 10 0.78 1.37 0.49 o 2 4 10 8.89 8.35 0.84 o 3 4 10 1.79 2.97 0.74 o 4 4 10 64.25 66.47 2.12 o 5 4 10 0.00 0.64 0.78 o 6 4 10 0.89 2.74 1.22 o 1 5 10 5.62 5.73 0.78 o 2 5 10 25.59 23.99 1.29 o 3 5 10 0.38 0.74 0.59 o 4 5 10 20.10 20.12 1.79 o 5 5 10 13.99 17.05 1.83 o 0 6 10 57.65 63.17 2.78 o 1 6 10 1.47 1.31 0.63 o 2 6 10 27.08 27.38 1.61 o 3 6 10 3.41 3.72 1.03 o 4 6 10 8.35 10.73 1.49 o 5 6 10 0.04 0.26 1.05 o 1 7 10 0.19 0.14 0.61 o 2 7 10 0.08 0.65 0.63 o 3 7 10 8.87 9.47 1.73 o 4 7 10 10.54 10.47 1.68 o 0 8 10 4.65 4.03 1.54 o 1 8 10 4.57 5.57 1.10 o 2 8 10 10.02 10.42 1.55 o 1 1 11 79.48 78.80 1.82 o 2 1 11 3.47 4.61 0.69 o 3 1 11 100.10 101.55 2.29 o 4 1 11 50.72 50.45 1.80 o 5 1 11 0.77 0.84 0.67 o 6 1 11 14.50 18.22 1.90 o 0 2 11 7.77 8.34 1.06 o 1 2 11 15.66 15.83 1.11 o 2 2 11 0.02 0.00 0.41 o 3 2 11 180.54 175.00 3.37 o 4 2 11 0.19 0.61 0.57 o 5 2 11 2.29 2.41 0.81 o 6 2 11 2.88 3.87 1.23 o 1 3 11 205.58 207.42 5.11 o 2 3 11 0.14 0.49 0.46 o 3 3 11 86.97 77.28 2.37 o 4 3 11 23.51 21.15 1.39 o 5 3 11 2.79 3.18 0.89 o 6 3 11 3.18 2.41 1.20 o 0 4 11 0.53 0.83 0.69 o 1 4 11 7.07 6.48 0.78 o 2 4 11 4.62 6.03 1.04 o 3 4 11 61.13 60.75 2.19 o 4 4 11 2.16 2.33 0.75 o 5 4 11 0.49 0.43 0.78 o 1 5 11 93.31 92.85 3.20 o 2 5 11 1.81 1.92 0.71 o 3 5 11 15.90 17.28 1.43 o 4 5 11 2.29 2.24 0.82 o 5 5 11 7.32 9.73 1.41 o 0 6 11 5.22 6.71 1.25 o 1 6 11 37.53 39.44 1.84 o 2 6 11 10.92 12.38 1.26 o 3 6 11 2.72 4.31 1.06 o 4 6 11 4.15 4.53 1.11 o 1 7 11 0.38 0.12 0.63 o 2 7 11 2.96 2.90 0.90 o 3 7 11 1.00 0.99 1.14 o 0 8 11 1.45 1.06 1.29 o 1 8 11 0.47 1.04 0.87 o 2 8 11 5.49 5.28 1.21 o 0 0 12 424.06 426.05 11.31 o 1 0 12 7.25 8.44 1.53 o 2 0 12 18.16 17.89 1.56 o 3 0 12 0.94 0.25 0.75 o 4 0 12 29.61 26.83 2.20 o 5 0 12 0.09 0.00 0.96 o 6 0 12 0.04 0.46 1.34 o 1 1 12 3.75 3.37 0.73 o 2 1 12 29.72 29.25 1.32 o 3 1 12 32.04 31.73 1.43 o 4 1 12 0.07 0.00 0.54 o 5 1 12 5.86 5.53 1.05 o 6 1 12 0.63 0.54 0.97 o 0 2 12 46.61 42.96 2.75 o 1 2 12 2.18 2.43 0.64 o 2 2 12 0.54 0.33 0.53 o 3 2 12 21.63 21.77 1.45 o 4 2 12 16.34 13.46 1.20 o 5 2 12 0.38 0.87 0.76 o 1 3 12 32.53 32.08 1.52 o 2 3 12 47.67 46.99 2.10 o 3 3 12 73.91 76.86 2.43 o 4 3 12 3.16 4.55 0.88 o 5 3 12 10.44 11.42 1.40 o 0 4 12 63.04 68.36 4.05 o 1 4 12 42.98 41.95 1.79 o 2 4 12 2.67 3.14 0.89 o 3 4 12 48.65 53.88 2.42 o 4 4 12 0.86 0.86 0.66 o 5 4 12 0.40 0.58 0.86 o 1 5 12 82.40 78.11 2.76 o 2 5 12 0.42 0.10 0.63 o 3 5 12 4.57 4.03 1.04 o 4 5 12 22.00 20.81 1.73 o 0 6 12 48.67 47.53 3.28 o 1 6 12 17.54 16.01 1.40 o 2 6 12 0.92 2.76 0.91 o 3 6 12 6.47 7.18 1.32 o 4 6 12 0.74 0.49 1.00 o 1 7 12 46.30 48.61 2.30 o 2 7 12 8.01 7.60 1.22 o 1 1 13 11.46 10.34 1.22 o 2 1 13 20.13 18.08 1.33 o 3 1 13 5.15 5.05 0.92 o 4 1 13 30.72 23.78 1.64 o 5 1 13 4.31 5.78 1.16 o 0 2 13 7.47 6.12 1.48 o 1 2 13 15.71 18.50 1.32 o 2 2 13 21.57 22.81 1.46 o 3 2 13 3.44 2.90 0.82 o 4 2 13 61.27 60.89 2.15 o 5 2 13 0.10 0.10 0.75 o 1 3 13 7.07 6.36 0.94 o 2 3 13 7.10 7.87 1.16 o 3 3 13 16.38 19.27 1.69 o 4 3 13 5.53 4.89 0.95 o 5 3 13 5.30 4.59 1.17 o 0 4 13 4.38 3.87 1.08 o 1 4 13 16.06 15.49 1.30 o 2 4 13 0.06 0.38 0.69 o 3 4 13 6.75 9.01 1.35 o 4 4 13 15.27 12.98 1.46 o 1 5 13 10.33 8.85 1.27 o 2 5 13 7.62 6.90 1.23 o 3 5 13 31.66 37.55 2.62 o 4 5 13 0.01 0.74 0.96 o 0 6 13 0.94 0.00 0.82 o 1 6 13 1.59 0.79 0.79 o 2 6 13 6.14 6.39 1.26 o 3 6 13 6.78 7.50 1.39 o 1 7 13 0.29 0.94 0.86 o 0 0 14 228.32 223.15 9.05 o 1 0 14 0.24 0.38 0.94 o 2 0 14 0.19 0.00 0.89 o 3 0 14 42.94 53.10 2.71 o 4 0 14 7.88 9.18 2.01 o 5 0 14 2.26 4.80 1.80 o 1 1 14 0.19 0.00 0.61 o 2 1 14 11.34 11.02 1.35 o 3 1 14 9.52 9.94 1.31 o 4 1 14 5.13 5.92 1.11 o 5 1 14 0.96 0.56 0.98 o 0 2 14 198.25 192.48 6.07 o 1 2 14 1.04 1.35 0.75 o 2 2 14 0.01 0.00 0.59 o 3 2 14 30.88 32.80 2.06 o 4 2 14 19.64 20.98 1.52 o 1 3 14 5.22 5.43 1.10 o 2 3 14 25.30 23.37 1.93 o 3 3 14 22.02 21.10 1.82 o 4 3 14 16.58 16.31 1.59 o 0 4 14 101.07 102.75 4.63 o 1 4 14 9.66 12.19 1.29 o 2 4 14 0.01 0.20 0.70 o 3 4 14 5.51 5.40 1.22 o 4 4 14 27.26 32.15 2.10 o 1 5 14 10.97 12.70 1.51 o 2 5 14 0.34 0.80 0.80 o 3 5 14 2.11 1.50 0.98 o 0 6 14 11.52 12.59 3.25 o 1 6 14 6.86 8.41 1.41 o 2 6 14 0.85 1.39 0.99 o 1 1 15 25.58 28.97 2.00 o 2 1 15 23.15 24.09 1.89 o 3 1 15 23.65 21.60 2.16 o 4 1 15 5.62 6.85 1.57 o 0 2 15 27.79 28.96 2.83 o 1 2 15 19.81 19.42 1.72 o 2 2 15 4.63 5.09 1.16 o 3 2 15 3.89 3.35 1.05 o 4 2 15 0.16 0.87 0.89 o 1 3 15 7.43 8.78 1.33 o 2 3 15 0.45 0.00 0.81 o 3 3 15 8.92 8.85 1.42 o 0 4 15 52.92 52.09 4.41 o 1 4 15 8.58 9.37 2.32 o 2 4 15 3.18 3.59 1.11 o 3 4 15 0.08 0.05 0.81 o 1 5 15 21.14 22.92 2.31 o 2 5 15 3.46 4.78 1.24 o 0 0 16 2.86 3.37 2.03 o 1 0 16 4.35 3.49 1.48 o 2 0 16 11.65 9.58 1.97 o 3 0 16 15.32 9.86 3.13 o 1 1 16 0.00 0.00 0.72 o 2 1 16 2.82 2.91 1.05 o 3 1 16 0.90 1.34 1.21 o 0 2 16 8.81 8.05 1.92 o 1 2 16 7.26 7.34 1.34 o 2 2 16 0.09 0.10 0.96 o 3 2 16 2.29 1.45 1.16 o 1 3 16 0.01 0.37 0.86 o 2 3 16 10.47 10.43 1.80 o 3 3 16 0.18 0.65 1.11 o 0 4 16 54.38 56.33 5.48 o 1 4 16 3.29 3.66 1.36 o 2 4 16 16.30 18.19 2.24 o 1 1 17 19.20 17.60 1.84 o 2 1 17 5.83 7.03 1.44 o 0 2 17 15.85 18.44 4.38 o 1 2 17 1.60 2.18 1.03 o 2 2 17 6.36 5.85 1.57 o 1 3 17 2.60 2.68 1.19 o 0 0 18 4.54 5.74 2.67 o