#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/96/2219609.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219609_Fobs loop_ _publ_author_name 'Wang, Mei-Ling' 'Zang, Hong-Jun' 'Cheng, Bo-Wen' _publ_section_title ; 4-Allyl-4-ethylmorpholinium chloride ; _journal_coeditor_code HK2524 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2013 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.032 _cell_angle_gamma 90.000 _cell_length_a 8.5414 _cell_length_b 9.0391 _cell_length_c 13.1237 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.8404 _[local]_cod_data_source_file hk2524Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R80301F in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 109.91 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1527.60 1495.48 17.62 o 4 0 0 3614.06 3464.10 41.20 o 6 0 0 536.25 446.94 15.23 o 8 0 0 369.15 340.85 16.85 o 10 0 0 127.31 142.42 15.04 o 1 1 0 1021.44 975.09 25.55 o 2 1 0 198.33 180.28 4.32 o 3 1 0 898.09 880.85 9.33 o 4 1 0 588.86 599.42 13.02 o 5 1 0 59.46 69.11 2.95 o 6 1 0 14.00 20.80 6.94 o 7 1 0 0.33 1.37 2.46 o 8 1 0 450.14 437.66 18.86 o 9 1 0 6.83 4.73 3.67 o 10 1 0 0.05 0.74 2.06 o 1 2 0 559.16 637.46 7.57 o 2 2 0 371.95 358.72 3.34 o 3 2 0 7216.29 7618.17 69.39 o 4 2 0 2823.47 2851.32 44.06 o 5 2 0 246.04 217.42 8.70 o 6 2 0 93.15 94.06 2.64 o 7 2 0 1334.29 1432.98 45.48 o 8 2 0 408.00 396.26 9.84 o 9 2 0 110.76 123.99 8.78 o 1 3 0 1516.68 1516.93 16.30 o 2 3 0 48.47 48.00 1.08 o 3 3 0 135.86 142.84 3.87 o 4 3 0 521.63 582.41 6.58 o 5 3 0 164.48 185.82 2.45 o 6 3 0 26.15 30.17 0.76 o 7 3 0 43.44 39.40 2.27 o 8 3 0 18.51 31.44 7.63 o 9 3 0 36.50 31.28 7.83 o 0 4 0 482.73 578.81 9.60 o 1 4 0 1509.11 1420.34 26.49 o 2 4 0 89.60 100.67 1.63 o 3 4 0 2281.32 2299.53 28.97 o 4 4 0 6.95 7.57 1.76 o 5 4 0 1196.34 1154.37 12.58 o 6 4 0 121.67 118.02 2.21 o 7 4 0 355.80 402.97 10.78 o 8 4 0 109.67 104.09 6.46 o 9 4 0 577.99 600.89 25.74 o 1 5 0 798.55 868.67 7.44 o 2 5 0 2.48 1.10 0.47 o 3 5 0 336.66 380.03 4.33 o 4 5 0 19.55 22.49 1.27 o 5 5 0 87.32 93.52 1.99 o 6 5 0 7.23 10.40 1.97 o 7 5 0 3.19 2.35 1.28 o 8 5 0 93.07 74.02 4.53 o 0 6 0 117.61 170.89 2.92 o 1 6 0 1235.52 1307.87 10.54 o 2 6 0 683.26 709.72 12.96 o 3 6 0 312.17 310.63 4.09 o 4 6 0 36.03 31.95 1.76 o 5 6 0 434.02 423.27 7.77 o 6 6 0 1241.79 1224.48 10.37 o 7 6 0 52.93 52.22 2.16 o 8 6 0 261.59 267.67 8.76 o 1 7 0 5.29 7.06 1.02 o 2 7 0 601.35 610.23 7.45 o 3 7 0 253.80 258.45 4.24 o 4 7 0 7.96 9.10 2.00 o 5 7 0 37.80 30.97 1.87 o 6 7 0 100.51 98.02 3.03 o 7 7 0 62.07 60.95 2.46 o 0 8 0 150.18 144.10 3.84 o 1 8 0 439.43 459.39 7.91 o 2 8 0 799.35 781.18 13.11 o 3 8 0 86.28 84.61 2.18 o 4 8 0 193.18 199.72 4.14 o 5 8 0 5.86 4.69 1.02 o 6 8 0 484.30 478.53 16.50 o 1 9 0 0.05 1.53 1.00 o 2 9 0 11.74 13.32 3.95 o 3 9 0 54.20 51.87 2.17 o 4 9 0 26.27 25.33 3.38 o 5 9 0 30.66 28.35 1.91 o 0 10 0 91.89 76.59 6.25 o 1 10 0 235.98 216.26 7.54 o 2 10 0 19.12 19.50 8.64 o 3 10 0 173.56 160.99 7.13 o -9 0 1 21.68 17.92 8.85 o -7 0 1 448.00 487.20 17.27 o -5 0 1 51.47 58.17 4.56 o -3 0 1 5181.69 5023.96 52.39 o -1 0 1 939.44 899.80 10.44 o 3 0 1 361.64 363.82 7.63 o 5 0 1 114.15 139.51 7.11 o 7 0 1 2625.71 2515.43 28.37 o 9 0 1 281.31 294.13 10.57 o -10 1 1 65.67 63.34 4.93 o -9 1 1 236.06 243.57 16.45 o -8 1 1 2.19 0.90 2.33 o -7 1 1 13.95 22.17 5.84 o -6 1 1 146.98 149.07 2.61 o -5 1 1 538.17 504.56 7.78 o -4 1 1 8.62 14.22 0.70 o -3 1 1 206.17 179.19 4.53 o -2 1 1 17.42 36.89 1.05 o -1 1 1 2312.57 2052.37 33.01 o 0 1 1 133.25 115.64 1.22 o 1 1 1 636.81 503.87 5.46 o 2 1 1 1451.72 1420.51 11.58 o 3 1 1 44.97 34.85 1.15 o 4 1 1 2.98 3.80 0.82 o 5 1 1 1287.09 1247.38 16.48 o 6 1 1 1.26 2.63 1.98 o 7 1 1 221.37 226.74 7.71 o 8 1 1 288.62 265.09 13.46 o 9 1 1 627.24 652.95 12.79 o 10 1 1 75.34 78.06 5.42 o -9 2 1 121.53 119.26 7.15 o -8 2 1 21.98 24.16 7.00 o -7 2 1 22.33 28.44 6.08 o -6 2 1 191.03 163.46 9.48 o -5 2 1 426.34 429.15 6.92 o -4 2 1 22.05 13.44 0.93 o -3 2 1 1818.11 1790.94 17.58 o -2 2 1 135.27 135.00 2.48 o -1 2 1 1103.95 1061.71 12.15 o 1 2 1 27.89 33.98 0.67 o 2 2 1 314.63 302.22 2.58 o 3 2 1 4.18 7.17 1.70 o 4 2 1 2966.68 3199.62 49.35 o 5 2 1 0.04 0.59 0.90 o 6 2 1 108.35 102.09 3.62 o 7 2 1 83.88 85.19 5.75 o 8 2 1 12.22 12.30 3.15 o 9 2 1 63.33 59.31 5.76 o -9 3 1 7.51 7.12 3.67 o -8 3 1 231.72 235.26 10.11 o -7 3 1 22.47 20.19 1.49 o -6 3 1 240.51 233.25 4.86 o -5 3 1 68.24 90.92 4.47 o -4 3 1 6.52 2.41 1.81 o -3 3 1 206.34 222.41 5.00 o -2 3 1 1618.70 1554.64 16.41 o -1 3 1 36.84 47.33 1.09 o 0 3 1 2726.63 2615.35 24.58 o 1 3 1 305.02 317.60 2.97 o 2 3 1 1186.23 1119.07 8.24 o 3 3 1 26.99 30.68 0.85 o 4 3 1 53.05 31.38 1.44 o 5 3 1 139.06 154.25 3.32 o 6 3 1 523.53 530.00 7.30 o 7 3 1 84.05 78.56 1.89 o 8 3 1 66.57 62.25 2.52 o 9 3 1 20.10 22.64 2.90 o -9 4 1 16.16 13.63 4.75 o -8 4 1 704.15 706.21 18.01 o -7 4 1 37.86 29.50 2.43 o -6 4 1 295.12 303.49 6.37 o -5 4 1 55.72 58.97 1.34 o -4 4 1 1062.01 1046.51 14.68 o -3 4 1 666.94 643.90 18.87 o -2 4 1 1244.10 1269.22 35.47 o -1 4 1 213.92 241.20 3.12 o 0 4 1 73.11 108.03 1.89 o 1 4 1 316.98 364.25 3.16 o 2 4 1 43.50 42.11 1.43 o 3 4 1 442.77 461.47 5.98 o 4 4 1 513.50 531.44 6.10 o 5 4 1 37.62 36.33 1.60 o 6 4 1 231.58 232.08 3.14 o 7 4 1 18.31 23.08 1.69 o 8 4 1 11.58 14.39 3.32 o 9 4 1 1.27 1.59 1.53 o -8 5 1 85.39 76.02 4.65 o -7 5 1 309.49 287.64 4.42 o -6 5 1 209.51 219.62 4.63 o -5 5 1 318.67 324.81 5.42 o -4 5 1 90.08 88.33 1.98 o -3 5 1 649.29 671.40 10.61 o -2 5 1 243.10 272.65 3.84 o -1 5 1 4208.67 4347.21 100.47 o 0 5 1 286.83 296.55 3.38 o 1 5 1 1190.89 1193.17 20.04 o 2 5 1 227.46 207.43 4.71 o 3 5 1 900.82 912.14 18.81 o 4 5 1 180.58 169.05 3.50 o 5 5 1 162.43 161.22 2.36 o 6 5 1 426.48 412.35 7.66 o 7 5 1 28.68 29.31 1.66 o 8 5 1 21.59 26.28 6.94 o -8 6 1 257.61 269.34 8.28 o -7 6 1 40.52 36.09 2.75 o -6 6 1 17.79 18.90 1.57 o -5 6 1 481.58 450.19 11.91 o -4 6 1 14.91 12.23 1.86 o -3 6 1 56.05 55.19 2.26 o -2 6 1 151.95 163.65 2.20 o -1 6 1 500.20 511.48 4.71 o 0 6 1 14.84 15.69 0.97 o 1 6 1 431.33 379.37 4.74 o 2 6 1 362.64 390.09 5.94 o 3 6 1 536.06 526.35 7.53 o 4 6 1 215.37 228.00 5.55 o 5 6 1 154.65 141.44 3.33 o 6 6 1 80.05 72.80 2.15 o 7 6 1 7.41 14.73 3.47 o 8 6 1 111.24 104.28 7.35 o -7 7 1 51.58 47.14 2.10 o -6 7 1 3.97 4.07 1.43 o -5 7 1 350.16 347.99 4.54 o -4 7 1 1030.83 1020.19 23.05 o -3 7 1 579.47 560.49 7.62 o -2 7 1 129.92 122.76 2.82 o -1 7 1 758.55 747.01 7.46 o 0 7 1 33.05 33.75 1.04 o 1 7 1 336.21 342.68 5.12 o 2 7 1 135.98 135.36 3.18 o 3 7 1 1751.69 1734.14 18.99 o 4 7 1 45.74 47.48 1.67 o 5 7 1 24.90 19.39 1.77 o 6 7 1 0.45 0.44 0.65 o 7 7 1 268.87 277.20 6.37 o -6 8 1 29.39 27.94 2.35 o -5 8 1 253.98 266.66 5.01 o -4 8 1 19.82 16.77 2.81 o -3 8 1 15.69 15.04 2.90 o -2 8 1 90.78 86.99 2.19 o -1 8 1 261.43 241.21 4.53 o 0 8 1 60.32 64.34 2.15 o 1 8 1 465.46 481.90 8.18 o 2 8 1 172.23 180.71 4.20 o 3 8 1 361.69 354.06 7.58 o 4 8 1 234.24 216.33 5.01 o 5 8 1 287.81 291.25 6.24 o 6 8 1 139.13 125.13 5.02 o -5 9 1 56.81 52.86 2.71 o -4 9 1 582.40 618.63 11.66 o -3 9 1 147.84 163.31 4.07 o -2 9 1 107.78 110.88 3.15 o -1 9 1 100.30 100.07 3.21 o 0 9 1 243.81 234.01 6.06 o 1 9 1 77.71 96.39 4.17 o 2 9 1 83.90 97.94 3.23 o 3 9 1 151.25 157.29 4.87 o 4 9 1 416.25 443.61 9.98 o 5 9 1 18.80 21.49 2.71 o -3 10 1 27.09 31.97 3.46 o -2 10 1 465.16 446.53 14.90 o -1 10 1 0.01 1.41 1.66 o 0 10 1 45.77 52.58 3.57 o 1 10 1 2.33 1.71 1.53 o 2 10 1 94.36 97.66 4.12 o 3 10 1 7.04 7.28 2.41 o -10 0 2 74.86 54.96 23.54 o -8 0 2 633.93 569.96 25.05 o -6 0 2 164.98 185.02 9.31 o -4 0 2 667.71 640.25 16.68 o -2 0 2 12079.67 11545.99 216.91 o 0 0 2 3663.58 3341.88 33.05 o 2 0 2 978.11 1033.17 8.30 o 4 0 2 112.41 101.19 3.00 o 6 0 2 202.46 197.71 5.00 o 8 0 2 279.92 267.93 11.87 o 10 0 2 44.05 43.29 4.29 o -10 1 2 242.41 229.13 15.11 o -9 1 2 151.67 155.79 9.60 o -8 1 2 168.02 170.16 8.86 o -7 1 2 14.23 18.07 4.29 o -6 1 2 952.50 949.33 19.49 o -5 1 2 1730.08 1814.29 35.55 o -4 1 2 36.20 22.14 0.82 o -3 1 2 106.22 90.48 3.20 o -1 1 2 7.44 2.46 0.46 o 0 1 2 2020.77 1779.26 9.17 o 1 1 2 8.37 3.50 0.33 o 3 1 2 37.93 40.16 1.12 o 4 1 2 448.01 420.39 5.69 o 5 1 2 455.09 422.17 6.35 o 6 1 2 628.88 632.70 8.32 o 7 1 2 13.25 19.16 4.00 o 8 1 2 7.23 9.51 1.69 o 9 1 2 226.82 229.57 7.03 o 10 1 2 32.98 29.55 4.19 o -9 2 2 46.30 42.47 10.89 o -8 2 2 61.20 61.17 5.60 o -7 2 2 2.56 3.11 2.59 o -6 2 2 822.68 874.69 12.27 o -5 2 2 643.18 669.98 14.27 o -4 2 2 3.39 7.86 3.04 o -3 2 2 90.40 96.10 2.59 o -2 2 2 33.53 35.32 1.10 o -1 2 2 332.01 368.37 4.98 o 0 2 2 1513.38 1462.17 11.73 o 1 2 2 731.80 737.26 4.01 o 2 2 2 1131.90 1161.85 19.18 o 3 2 2 302.92 296.88 4.84 o 4 2 2 360.01 363.97 4.42 o 5 2 2 206.50 202.72 3.17 o 6 2 2 10.48 10.13 2.24 o 7 2 2 0.02 0.78 0.78 o 8 2 2 2.08 3.84 1.28 o 9 2 2 14.53 13.41 3.72 o -9 3 2 176.45 183.17 8.31 o -8 3 2 105.17 109.93 8.85 o -7 3 2 355.60 361.51 18.97 o -6 3 2 194.60 191.86 4.69 o -5 3 2 1137.98 1176.98 12.83 o -4 3 2 18.78 21.78 1.34 o -3 3 2 144.43 130.44 2.58 o -2 3 2 312.12 329.23 3.09 o -1 3 2 4951.29 5018.40 49.96 o 0 3 2 38.72 45.77 1.77 o 1 3 2 5120.53 4867.70 35.46 o 2 3 2 13.60 17.69 0.63 o 3 3 2 176.76 149.29 2.47 o 4 3 2 171.01 170.12 3.08 o 5 3 2 1106.57 1061.05 9.08 o 6 3 2 520.05 513.53 6.33 o 7 3 2 429.79 421.89 7.35 o 8 3 2 123.57 113.80 4.10 o 9 3 2 186.57 180.96 6.53 o -9 4 2 0.03 2.48 2.23 o -8 4 2 0.54 1.48 1.99 o -7 4 2 5.24 6.23 1.99 o -6 4 2 139.03 145.70 3.83 o -5 4 2 3.39 4.85 1.18 o -4 4 2 0.85 1.46 0.78 o -3 4 2 1393.96 1309.28 24.02 o -2 4 2 4.40 5.07 1.02 o -1 4 2 118.38 139.90 2.36 o 0 4 2 722.30 784.59 9.49 o 1 4 2 1457.71 1481.34 35.83 o 2 4 2 5.84 9.93 1.23 o 3 4 2 9.38 8.75 0.95 o 4 4 2 324.99 353.95 4.93 o 5 4 2 70.60 81.76 2.06 o 6 4 2 0.28 0.14 0.74 o 7 4 2 247.67 259.10 5.57 o 8 4 2 202.55 200.21 7.87 o 9 4 2 334.51 354.80 12.15 o -8 5 2 460.50 481.80 16.71 o -7 5 2 67.42 53.11 4.12 o -6 5 2 0.09 0.60 0.52 o -5 5 2 44.21 46.78 1.68 o -4 5 2 680.28 660.09 18.36 o -3 5 2 559.81 540.79 6.44 o -2 5 2 231.80 220.32 3.73 o -1 5 2 493.73 459.46 5.86 o 0 5 2 2170.65 2295.69 46.74 o 1 5 2 1693.81 1626.49 22.76 o 2 5 2 386.17 413.64 11.97 o 3 5 2 1022.41 1050.28 9.76 o 4 5 2 474.63 458.39 6.12 o 5 5 2 10.13 10.23 2.13 o 6 5 2 199.58 186.41 4.98 o 7 5 2 198.87 180.31 4.40 o 8 5 2 600.27 592.15 19.75 o -8 6 2 0.40 -0.11 2.05 o -7 6 2 21.24 19.65 3.28 o -6 6 2 4.07 4.85 2.94 o -5 6 2 16.90 22.08 1.69 o -4 6 2 217.82 196.84 3.94 o -3 6 2 2740.72 2742.72 24.65 o -2 6 2 15.61 14.12 2.56 o -1 6 2 52.72 48.42 1.45 o 0 6 2 0.03 0.45 0.43 o 1 6 2 239.76 250.85 3.70 o 2 6 2 77.83 77.69 2.96 o 3 6 2 3.16 4.10 1.15 o 4 6 2 579.77 574.11 8.03 o 5 6 2 16.23 19.85 2.02 o 6 6 2 25.83 31.52 2.01 o 7 6 2 0.13 1.59 0.75 o 8 6 2 156.14 145.30 5.94 o -7 7 2 15.14 15.17 2.48 o -6 7 2 377.76 408.09 15.98 o -5 7 2 0.08 1.25 0.71 o -4 7 2 1898.76 1937.77 31.63 o -3 7 2 37.90 34.99 2.36 o -2 7 2 148.86 152.15 3.35 o -1 7 2 44.91 47.46 1.38 o 0 7 2 772.63 797.82 8.73 o 1 7 2 31.23 25.83 1.87 o 2 7 2 7.42 8.52 1.73 o 3 7 2 304.11 292.87 8.82 o 4 7 2 957.78 961.14 20.72 o 5 7 2 206.14 207.50 3.53 o 6 7 2 129.75 133.09 4.40 o 7 7 2 11.82 9.82 2.96 o -6 8 2 130.01 130.38 4.64 o -5 8 2 5.81 5.10 1.25 o -4 8 2 0.31 1.06 0.74 o -3 8 2 14.16 12.79 2.46 o -2 8 2 0.81 1.44 0.99 o -1 8 2 3.65 6.60 1.60 o 0 8 2 224.48 202.80 5.43 o 1 8 2 35.06 42.99 2.85 o 2 8 2 2.78 2.94 1.18 o 3 8 2 2.46 3.23 1.50 o 4 8 2 113.75 104.06 4.15 o 5 8 2 1.49 1.55 0.95 o 6 8 2 39.92 34.79 3.24 o -5 9 2 187.75 190.01 4.83 o -4 9 2 9.31 7.36 1.93 o -3 9 2 495.43 520.28 9.11 o -2 9 2 295.25 328.70 8.54 o -1 9 2 168.93 164.94 5.26 o 0 9 2 178.89 200.26 5.40 o 1 9 2 89.63 85.97 3.28 o 2 9 2 1.30 2.11 1.44 o 3 9 2 426.52 425.09 10.01 o 4 9 2 135.45 126.15 3.68 o 5 9 2 91.84 91.32 3.38 o -3 10 2 108.90 117.48 6.67 o -2 10 2 38.80 40.06 3.48 o -1 10 2 0.02 1.04 1.40 o 0 10 2 3.55 2.85 1.76 o 1 10 2 0.38 0.86 0.97 o 2 10 2 1.68 2.39 1.78 o 3 10 2 179.38 188.92 10.14 o -9 0 3 311.67 334.48 30.78 o -7 0 3 1126.81 1074.11 33.51 o -5 0 3 1172.42 1153.02 33.16 o -3 0 3 245.07 247.44 8.44 o -1 0 3 6166.86 6129.44 96.39 o 1 0 3 3118.97 3194.86 32.71 o 3 0 3 4421.01 4102.36 44.80 o 5 0 3 1543.32 1531.65 49.23 o 7 0 3 1958.21 1946.47 48.36 o 9 0 3 90.69 87.76 7.77 o -9 1 3 83.83 87.75 7.15 o -8 1 3 151.42 148.75 7.73 o -7 1 3 588.20 592.61 18.05 o -6 1 3 8.13 7.16 2.78 o -5 1 3 2304.99 2358.58 63.69 o -4 1 3 356.73 376.34 30.99 o -3 1 3 440.66 447.87 9.33 o -2 1 3 1404.32 1440.65 22.84 o -1 1 3 4031.74 4084.07 27.08 o 0 1 3 865.97 855.61 12.85 o 1 1 3 311.67 350.51 3.72 o 2 1 3 3358.69 3450.72 26.69 o 3 1 3 152.74 172.55 5.41 o 4 1 3 0.04 0.72 0.69 o 5 1 3 1301.06 1348.86 17.32 o 6 1 3 22.09 20.45 1.40 o 7 1 3 302.69 307.17 5.99 o 8 1 3 5.56 4.92 1.73 o 9 1 3 36.05 38.53 3.74 o -9 2 3 196.55 213.70 10.25 o -8 2 3 370.20 381.33 11.20 o -7 2 3 416.02 427.80 12.57 o -6 2 3 0.13 2.33 2.08 o -5 2 3 870.26 932.99 27.89 o -4 2 3 1615.06 1661.01 53.91 o -3 2 3 131.55 113.56 2.61 o -2 2 3 4221.51 4187.00 50.38 o -1 2 3 69.75 59.27 1.46 o 0 2 3 2652.40 2644.01 21.78 o 1 2 3 2428.80 2436.18 15.28 o 2 2 3 1051.41 1024.85 7.05 o 3 2 3 570.35 543.28 11.78 o 4 2 3 1364.87 1392.59 22.20 o 5 2 3 39.59 41.54 1.48 o 6 2 3 465.57 453.42 6.44 o 7 2 3 507.42 517.45 17.21 o 8 2 3 165.13 175.98 6.99 o 9 2 3 286.48 291.91 6.77 o -9 3 3 39.37 33.46 12.31 o -8 3 3 135.71 133.61 6.60 o -7 3 3 502.67 483.78 29.31 o -6 3 3 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