#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219612.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219612_Fobs loop_ _publ_author_name 'Zaidi, Syed Azeem Rashid Ali' 'Tahir, M. Nawaz' 'Iqbal, Javed' 'Chaudhary, Muhammad Ashraf' _publ_section_title ; 2-Carboxyanilinium chloride monohydrate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1957 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.605 _cell_angle_gamma 90.000 _cell_length_a 23.0942 _cell_length_b 4.7833 _cell_length_c 16.3810 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file hk2527Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NEWDATA in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 234.83 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6075.18 6548.56 76.28 o 6 0 0 3553.88 3640.99 44.43 o 8 0 0 55143.91 59796.85 661.11 o 10 0 0 8313.65 9357.58 126.88 o 12 0 0 4799.42 5858.11 110.62 o 14 0 0 157.68 114.68 9.24 o 16 0 0 8561.90 8794.31 124.85 o 18 0 0 63.71 45.87 13.22 o 20 0 0 742.65 772.15 24.06 o 22 0 0 34.93 22.43 12.34 o 24 0 0 939.63 862.21 49.28 o 26 0 0 633.75 687.18 45.97 o 28 0 0 135.86 168.98 30.63 o 30 0 0 46.61 22.13 27.76 o 1 1 0 1320.23 1275.17 14.34 o 3 1 0 2428.13 2424.57 17.65 o 5 1 0 621.76 663.95 6.01 o 7 1 0 120.08 119.70 3.31 o 9 1 0 193.49 147.95 4.21 o 11 1 0 961.76 976.94 11.41 o 13 1 0 359.25 447.94 8.66 o 15 1 0 107.64 125.40 6.20 o 17 1 0 902.26 911.61 17.10 o 19 1 0 13.55 0.95 6.09 o 21 1 0 33.76 16.90 8.67 o 23 1 0 50.54 39.81 11.62 o 25 1 0 8.26 2.26 14.73 o 27 1 0 112.55 83.51 18.22 o 29 1 0 11.40 3.39 10.51 o 0 2 0 15460.59 14405.57 364.44 o 2 2 0 744.13 781.79 15.29 o 4 2 0 2289.54 2356.46 23.68 o 6 2 0 5033.57 5320.62 45.60 o 8 2 0 2305.47 2250.99 26.27 o 10 2 0 2420.70 2405.61 25.95 o 12 2 0 978.88 933.26 11.21 o 14 2 0 716.84 682.40 10.45 o 16 2 0 5094.42 5057.72 56.71 o 18 2 0 240.65 230.83 9.91 o 20 2 0 392.31 389.15 16.07 o 22 2 0 59.12 61.52 8.92 o 24 2 0 166.86 173.94 9.82 o 26 2 0 8.97 5.84 12.08 o 28 2 0 136.82 116.71 11.62 o 1 3 0 1519.63 1423.75 25.89 o 3 3 0 51.79 45.23 4.70 o 5 3 0 475.83 479.60 8.62 o 7 3 0 397.58 372.70 12.62 o 9 3 0 26.34 10.70 3.78 o 11 3 0 659.16 632.08 13.26 o 13 3 0 3.11 -5.05 5.05 o 15 3 0 90.85 69.50 8.98 o 17 3 0 119.85 92.39 12.16 o 19 3 0 505.00 503.80 19.31 o 21 3 0 735.75 649.45 22.66 o 23 3 0 3.99 7.39 8.05 o 25 3 0 79.03 66.01 11.58 o 27 3 0 472.78 382.35 33.26 o 0 4 0 65.98 69.92 12.23 o 2 4 0 19.20 18.76 6.76 o 4 4 0 1.78 -0.61 4.61 o 6 4 0 64.24 50.81 7.02 o 8 4 0 282.68 292.87 10.78 o 10 4 0 16.20 16.65 5.82 o 12 4 0 56.76 61.79 8.67 o 14 4 0 14.71 14.05 8.18 o 16 4 0 4.35 -7.95 7.95 o 18 4 0 62.95 44.08 9.52 o 20 4 0 225.45 202.31 17.81 o 22 4 0 0.29 6.38 8.71 o 1 5 0 267.65 274.23 15.76 o 3 5 0 0.22 -9.39 9.39 o 5 5 0 12.85 14.96 7.16 o 7 5 0 33.36 25.75 10.48 o 9 5 0 361.99 381.75 13.96 o 11 5 0 260.50 242.30 12.27 o 13 5 0 14.89 0.44 6.66 o 15 5 0 40.99 58.59 9.39 o 17 5 0 99.65 109.93 18.97 o 19 5 0 25.10 14.10 11.80 o 0 6 0 62.49 33.99 19.75 o 2 6 0 320.87 306.66 33.69 o 4 6 0 5.46 19.99 18.40 o 6 6 0 549.67 527.06 41.39 o 8 6 0 103.05 127.27 18.56 o 10 6 0 0.02 -8.04 8.89 o -29 1 1 77.96 55.15 12.45 o -27 1 1 9.96 15.63 9.66 o -25 1 1 145.89 112.88 12.40 o -23 1 1 3161.92 3182.32 59.06 o -21 1 1 18.70 17.11 7.72 o -19 1 1 58.21 52.68 8.48 o -17 1 1 2377.56 2504.98 32.29 o -15 1 1 1189.51 1148.74 16.82 o -13 1 1 2336.77 2363.75 33.71 o -11 1 1 0.40 -1.42 2.04 o -9 1 1 44.05 32.48 3.95 o -7 1 1 16591.77 16855.75 124.30 o -5 1 1 162.99 122.56 3.71 o -3 1 1 7076.34 7633.06 49.46 o -1 1 1 618.54 579.36 8.23 o 1 1 1 878.74 779.37 7.33 o 3 1 1 6749.21 7454.68 44.34 o 5 1 1 12073.75 13317.23 80.90 o 7 1 1 930.36 923.17 10.78 o 9 1 1 1042.15 1107.84 12.52 o 11 1 1 64.74 45.58 3.07 o 13 1 1 9176.84 9651.23 73.40 o 15 1 1 1254.36 1283.20 15.51 o 17 1 1 7.10 -3.41 4.55 o 19 1 1 1086.07 1117.33 29.74 o 21 1 1 2358.81 2468.64 79.90 o 23 1 1 156.90 165.81 15.04 o 25 1 1 240.02 229.34 21.62 o 27 1 1 76.60 94.34 18.63 o 29 1 1 796.28 846.60 38.42 o -28 2 1 20.42 9.32 18.06 o -26 2 1 613.34 639.41 24.37 o -24 2 1 44.43 36.75 6.94 o -22 2 1 43.47 33.95 6.83 o -20 2 1 564.95 504.16 16.03 o -18 2 1 2257.79 2222.76 33.75 o -16 2 1 289.71 286.35 8.28 o -14 2 1 111.57 101.09 4.67 o -12 2 1 2897.73 2863.78 24.70 o -10 2 1 840.49 873.56 12.91 o -8 2 1 423.06 411.41 7.97 o -6 2 1 48.24 21.73 3.66 o -4 2 1 5732.50 5546.17 61.04 o -2 2 1 170.95 134.09 7.26 o 0 2 1 725.80 622.34 30.72 o 2 2 1 54.54 48.23 3.37 o 4 2 1 25442.43 24942.81 212.73 o 6 2 1 107.62 124.12 6.96 o 8 2 1 921.28 981.53 12.64 o 10 2 1 791.29 717.43 12.05 o 12 2 1 5035.33 4838.82 40.34 o 14 2 1 670.84 608.00 10.46 o 16 2 1 1748.99 1639.66 19.83 o 18 2 1 132.61 122.56 6.50 o 20 2 1 725.72 699.90 16.61 o 22 2 1 43.67 45.88 9.06 o 24 2 1 25.80 15.75 6.40 o 26 2 1 183.96 175.64 11.21 o 28 2 1 18.53 29.93 13.81 o -27 3 1 38.25 29.41 17.67 o -25 3 1 1.96 -1.42 8.82 o -23 3 1 94.62 102.33 12.07 o -21 3 1 17.67 12.47 10.61 o -19 3 1 63.44 78.22 12.78 o -17 3 1 953.45 953.88 31.03 o -15 3 1 3.19 -5.97 7.35 o -13 3 1 20.49 19.40 5.65 o -11 3 1 514.58 525.50 12.42 o -9 3 1 1.04 0.77 4.60 o -7 3 1 2439.63 2475.11 29.08 o -5 3 1 618.14 645.75 13.17 o -3 3 1 533.91 548.11 20.11 o -1 3 1 356.03 344.99 15.27 o 1 3 1 159.19 144.45 8.75 o 3 3 1 1639.36 1831.49 25.86 o 5 3 1 390.78 427.19 8.20 o 7 3 1 5.95 -0.76 3.49 o 9 3 1 263.13 263.22 8.31 o 11 3 1 109.03 116.56 7.08 o 13 3 1 701.54 695.65 15.97 o 15 3 1 0.44 -0.12 5.27 o 17 3 1 38.00 29.68 7.06 o 19 3 1 167.61 155.09 11.10 o 21 3 1 43.79 38.04 9.47 o 23 3 1 64.08 54.00 10.30 o 25 3 1 2.72 1.12 14.56 o -22 4 1 1.15 4.64 8.78 o -20 4 1 42.93 50.46 14.15 o -18 4 1 8.52 -8.88 8.88 o -16 4 1 402.85 402.91 28.73 o -14 4 1 354.15 342.98 19.08 o -12 4 1 79.82 73.04 8.19 o -10 4 1 14.67 8.16 5.54 o -8 4 1 193.73 206.97 9.57 o -6 4 1 1258.11 1279.80 21.64 o -4 4 1 510.57 493.64 13.42 o -2 4 1 12.46 7.10 6.68 o 0 4 1 241.40 215.00 12.45 o 2 4 1 700.32 688.38 23.93 o 4 4 1 1972.88 1942.18 29.67 o 6 4 1 36.01 24.21 4.01 o 8 4 1 38.05 52.86 6.39 o 10 4 1 1855.23 1798.64 31.22 o 12 4 1 868.39 902.59 18.69 o 14 4 1 136.97 129.55 9.81 o 16 4 1 5.00 -7.67 7.67 o 18 4 1 488.56 469.46 19.15 o 20 4 1 1199.82 1241.67 40.30 o 22 4 1 143.87 133.56 13.51 o -19 5 1 1.09 -1.26 10.77 o -17 5 1 89.36 94.90 11.50 o -15 5 1 140.16 180.80 16.50 o -13 5 1 7.76 1.94 8.37 o -11 5 1 11.54 -10.42 11.99 o -9 5 1 0.05 -6.12 6.12 o -7 5 1 55.89 52.64 9.39 o -5 5 1 17.92 5.77 10.64 o -3 5 1 0.29 -11.82 11.86 o -1 5 1 220.86 257.63 15.55 o 1 5 1 121.25 121.67 12.15 o 3 5 1 7.46 8.88 11.87 o 5 5 1 0.16 2.58 6.27 o 7 5 1 139.49 166.92 8.93 o 9 5 1 0.70 -4.82 6.02 o 11 5 1 50.49 50.61 7.87 o 13 5 1 0.01 -9.38 9.38 o 15 5 1 46.65 28.52 11.86 o 17 5 1 2.81 -7.54 7.54 o 19 5 1 67.15 64.01 20.79 o -10 6 1 5.25 -4.80 9.18 o -8 6 1 63.28 59.01 9.13 o -6 6 1 5.84 23.66 18.77 o -4 6 1 13.47 1.70 26.56 o -2 6 1 25.88 7.52 21.61 o 0 6 1 5.16 -4.50 10.59 o 2 6 1 21.88 20.11 13.37 o 4 6 1 271.49 260.97 26.31 o 6 6 1 0.14 -9.83 16.54 o 8 6 1 12.77 1.78 14.87 o 10 6 1 21.13 4.23 9.83 o -30 0 2 493.65 548.40 50.07 o -28 0 2 5.78 -10.58 23.78 o -26 0 2 12.72 -17.24 21.40 o -24 0 2 129.99 132.06 27.27 o -22 0 2 265.97 327.45 22.81 o -20 0 2 1026.90 1083.87 35.56 o -18 0 2 120.37 71.61 12.42 o -16 0 2 1026.32 1134.72 33.99 o -14 0 2 13398.53 14641.79 241.52 o -12 0 2 1073.49 1112.39 23.72 o -10 0 2 1624.89 2262.71 74.77 o -8 0 2 6812.50 7516.33 88.41 o -6 0 2 1473.13 1967.99 26.42 o -4 0 2 11337.39 12817.62 144.61 o -2 0 2 7817.04 7574.04 70.46 o 0 0 2 4214.32 4123.50 53.37 o 2 0 2 16290.35 15436.04 142.26 o 4 0 2 120.03 173.50 4.12 o 6 0 2 3895.18 4207.86 41.66 o 8 0 2 23143.03 24700.03 247.48 o 10 0 2 19.96 13.74 4.04 o 12 0 2 525.41 461.08 14.27 o 14 0 2 4074.95 4432.51 67.89 o 16 0 2 3094.30 3217.89 54.01 o 18 0 2 479.92 495.48 18.14 o 20 0 2 316.50 320.77 17.27 o 22 0 2 180.49 183.23 25.98 o 24 0 2 1954.16 1884.97 73.91 o 26 0 2 29.57 62.54 24.39 o 28 0 2 32.97 38.94 24.82 o 30 0 2 97.43 72.63 28.86 o -29 1 2 61.54 81.81 15.32 o -27 1 2 187.89 169.58 14.64 o -25 1 2 78.35 61.88 11.27 o -23 1 2 277.83 267.62 13.83 o -21 1 2 553.39 562.64 17.34 o -19 1 2 251.91 246.25 10.72 o -17 1 2 4.11 -3.94 3.94 o -15 1 2 0.21 -3.27 3.27 o -13 1 2 1725.16 1587.72 18.02 o -11 1 2 723.65 789.45 12.01 o -9 1 2 1689.84 1760.90 22.50 o -7 1 2 399.19 368.06 6.09 o -5 1 2 6583.79 6748.40 50.71 o -3 1 2 5152.37 5019.37 40.30 o -1 1 2 845.74 1019.43 8.29 o 1 1 2 130.63 118.50 2.19 o 3 1 2 26968.13 26944.96 153.29 o 5 1 2 1104.45 1215.81 8.82 o 7 1 2 541.14 636.20 8.00 o 9 1 2 1787.79 1963.68 18.54 o 11 1 2 1103.69 1328.20 13.71 o 13 1 2 134.16 100.75 4.57 o 15 1 2 1055.54 1155.72 15.85 o 17 1 2 2789.17 2792.64 29.95 o 19 1 2 162.52 150.95 10.90 o 21 1 2 821.27 773.87 21.72 o 23 1 2 15.56 -3.33 9.21 o 25 1 2 234.75 288.40 22.62 o 27 1 2 24.42 38.22 16.74 o 29 1 2 115.42 121.64 21.38 o -28 2 2 178.63 208.44 16.42 o -26 2 2 0.74 -6.95 6.95 o -24 2 2 337.07 344.07 13.91 o -22 2 2 56.10 66.95 8.67 o -20 2 2 1062.70 1099.83 21.91 o -18 2 2 35.38 24.64 5.61 o -16 2 2 105.65 75.49 5.25 o -14 2 2 239.70 258.30 6.95 o -12 2 2 394.77 399.53 7.30 o -10 2 2 851.89 862.17 13.87 o -8 2 2 255.23 292.47 7.43 o -6 2 2 7.32 4.81 3.07 o -4 2 2 1945.74 2060.16 23.19 o -2 2 2 4519.93 4644.24 50.13 o 0 2 2 231.53 217.77 9.92 o 2 2 2 2053.15 2214.52 21.65 o 4 2 2 122.20 123.35 5.52 o 6 2 2 106.41 57.67 4.20 o 8 2 2 4194.43 4491.96 39.47 o 10 2 2 336.14 342.13 6.79 o 12 2 2 25.41 6.03 3.54 o 14 2 2 94.47 83.43 4.73 o 16 2 2 1116.57 1115.25 13.07 o 18 2 2 1371.31 1352.18 18.36 o 20 2 2 41.82 23.11 5.91 o 22 2 2 473.40 469.73 13.92 o 24 2 2 938.86 968.37 21.91 o 26 2 2 0.42 -7.27 10.70 o 28 2 2 4.62 -10.92 13.90 o -27 3 2 345.26 346.28 34.24 o -25 3 2 34.28 22.62 11.49 o -23 3 2 0.19 -8.62 8.62 o -21 3 2 667.35 701.86 81.59 o -19 3 2 3177.38 3102.65 81.74 o -17 3 2 157.81 138.51 14.09 o -15 3 2 107.99 104.73 10.69 o -13 3 2 5041.07 5101.60 63.37 o -11 3 2 3690.49 3700.88 45.89 o -9 3 2 50.17 57.12 5.34 o -7 3 2 913.31 957.96 14.96 o -5 3 2 2565.78 2576.88 33.46 o -3 3 2 6712.43 6637.72 74.38 o -1 3 2 476.78 558.67 11.88 o 1 3 2 333.34 320.90 12.19 o 3 3 2 937.49 854.81 10.70 o 5 3 2 2003.44 1934.56 21.05 o 7 3 2 1475.65 1471.52 17.23 o 9 3 2 260.81 261.73 7.00 o 11 3 2 110.37 87.72 5.22 o 13 3 2 1279.35 1253.16 27.55 o 15 3 2 308.93 331.61 15.59 o 17 3 2 620.89 609.19 17.38 o 19 3 2 41.09 15.87 8.36 o 21 3 2 60.12 38.78 9.20 o 23 3 2 128.66 144.55 13.91 o 25 3 2 470.45 487.35 68.17 o -22 4 2 59.18 58.48 13.94 o -20 4 2 168.43 159.48 36.65 o -18 4 2 132.38 116.84 14.73 o -16 4 2 14.75 8.75 9.21 o -14 4 2 58.01 53.37 10.68 o -12 4 2 268.69 263.44 15.50 o -10 4 2 0.02 -5.24 5.24 o -8 4 2 78.08 80.25 7.47 o -6 4 2 2.97 -0.37 4.71 o -4 4 2 169.36 197.30 10.47 o -2 4 2 13.68 13.70 4.65 o 0 4 2 84.33 86.95 9.22 o 2 4 2 19.64 22.88 7.87 o 4 4 2 0.02 -4.06 4.06 o 6 4 2 17.28 13.53 3.95 o 8 4 2 61.28 61.70 5.01 o 10 4 2 12.95 8.98 6.74 o 12 4 2 264.63 230.14 10.41 o 14 4 2 10.43 7.45 7.09 o 16 4 2 54.20 51.50 8.36 o 18 4 2 0.66 -5.11 7.10 o 20 4 2 2.23 -2.48 8.63 o 22 4 2 9.39 2.35 9.27 o -17 5 2 6.44 10.59 10.58 o -15 5 2 8.24 9.11 9.56 o -13 5 2 323.73 342.85 19.67 o -11 5 2 322.39 309.82 18.09 o -9 5 2 84.83 98.25 12.43 o -7 5 2 4.64 -4.32 5.52 o -5 5 2 412.66 435.87 18.45 o -3 5 2 1625.45 1646.43 112.19 o -1 5 2 13.74 19.33 9.28 o 1 5 2 5.89 6.11 8.18 o 3 5 2 218.09 236.79 16.25 o 5 5 2 470.59 467.43 12.85 o 7 5 2 77.52 88.33 6.51 o 9 5 2 7.95 0.62 4.75 o 11 5 2 17.99 -1.22 5.94 o 13 5 2 62.95 54.00 8.48 o 15 5 2 129.21 108.36 15.05 o 17 5 2 193.66 217.76 20.30 o -10 6 2 51.88 48.48 21.76 o -8 6 2 77.78 52.76 57.07 o -6 6 2 17.14 17.86 13.17 o -4 6 2 148.53 113.88 20.99 o -2 6 2 39.36 20.68 14.98 o 0 6 2 54.03 32.76 19.32 o 2 6 2 0.39 -4.44 16.94 o 4 6 2 40.05 24.41 16.13 o 6 6 2 24.71 9.38 29.87 o 8 6 2 189.94 218.62 15.21 o 10 6 2 9.48 20.30 18.46 o -29 1 3 149.11 153.47 15.56 o -27 1 3 395.28 372.72 19.61 o -25 1 3 205.64 217.86 15.04 o -23 1 3 218.27 211.58 12.72 o -21 1 3 344.33 342.34 16.51 o -19 1 3 557.55 543.59 16.67 o -17 1 3 1768.17 1805.46 25.60 o -15 1 3 3480.66 3656.71 38.16 o -13 1 3 646.39 605.59 10.07 o -11 1 3 266.31 264.24 5.85 o -9 1 3 24470.46 25601.83 194.97 o -7 1 3 4123.80 4152.26 36.45 o -5 1 3 1489.51 1508.47 22.47 o -3 1 3 338.39 300.47 4.24 o -1 1 3 40304.09 38506.48 300.14 o 1 1 3 49097.59 45998.70 264.44 o 3 1 3 33525.77 32214.81 167.90 o 5 1 3 1.81 2.56 1.34 o 7 1 3 18853.35 19017.57 135.36 o 9 1 3 1836.79 1689.46 16.63 o 11 1 3 55.07 75.79 3.44 o 13 1 3 55.57 61.28 3.89 o 15 1 3 1311.19 1263.25 21.81 o 17 1 3 1234.63 1264.60 20.74 o 19 1 3 848.07 876.05 21.75 o 21 1 3 1573.33 1633.53 32.36 o 23 1 3 162.60 164.59 14.75 o 25 1 3 143.17 170.67 18.89 o 27 1 3 41.68 30.46 36.44 o 29 1 3 128.95 145.50 21.75 o -28 2 3 15.75 1.34 15.84 o -26 2 3 429.59 434.82 22.80 o -24 2 3 6.52 0.87 7.14 o -22 2 3 33.72 27.97 6.59 o -20 2 3 117.98 103.09 8.30 o -18 2 3 30.35 26.31 5.56 o -16 2 3 677.58 637.18 14.02 o -14 2 3 81.83 90.54 4.66 o -12 2 3 27.55 28.45 2.94 o -10 2 3 1754.33 1652.27 17.32 o -8 2 3 35.53 15.37 3.51 o -6 2 3 3832.62 4057.15 41.54 o -4 2 3 365.94 410.79 8.32 o -2 2 3 1412.07 1406.17 20.79 o 0 2 3 1919.07 1698.68 17.50 o 2 2 3 1207.02 1106.26 12.67 o 4 2 3 3365.87 3528.58 28.88 o 6 2 3 154.21 100.26 3.45 o 8 2 3 1167.21 1146.19 13.39 o 10 2 3 1751.51 1611.22 15.41 o 12 2 3 1606.75 1691.67 15.73 o 14 2 3 12.44 12.16 2.63 o 16 2 3 436.17 435.70 10.08 o 18 2 3 1477.19 1429.26 17.44 o 20 2 3 507.12 489.28 12.15 o 22 2 3 48.01 46.16 5.92 o 24 2 3 122.27 102.17 10.42 o 26 2 3 262.15 260.50 15.08 o 28 2 3 478.42 466.54 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