#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219619.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219619_Fobs loop_ _publ_author_name 'Arshad, Muhammad Nadeem' 'Tahir, M. Nawaz' 'Khan, Islam Ullah' 'Shafiq, Muhammad' 'Siddiqui, Waseeq Ahmad' _publ_section_title ; Methyl 3-hydroxy-4-oxo-3,4-dihydro-2H-1,2-benzothiazine-3-carboxylate 1,1-dioxide monohydrate ; _journal_coeditor_code HK2537 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2045 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7504 _cell_length_b 14.5638 _cell_length_c 21.0615 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.7461 _[local]_cod_data_source_file hk2537Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' matrix_0m in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 341.91 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25554.61 27087.99 642.40 o 4 0 0 39.66 36.98 19.56 o 6 0 0 27.32 29.47 25.51 o 8 0 0 415.54 321.39 50.07 o 10 0 0 7.11 14.15 65.83 o 2 1 0 45956.73 47442.03 704.67 o 4 1 0 1132.76 896.72 33.36 o 6 1 0 6221.13 5983.37 127.76 o 8 1 0 22.62 13.89 23.75 o 10 1 0 58.36 17.67 49.09 o 2 2 0 19146.38 20244.66 305.78 o 4 2 0 610.11 726.89 55.00 o 6 2 0 63.21 72.27 21.20 o 8 2 0 80.67 36.42 25.03 o 10 2 0 256.78 225.12 58.35 o 2 3 0 3549.35 3271.88 83.43 o 4 3 0 20934.39 21714.46 375.53 o 6 3 0 407.24 321.94 27.28 o 8 3 0 39.13 92.66 33.20 o 10 3 0 197.55 260.06 49.44 o 2 4 0 10382.33 10980.56 169.18 o 4 4 0 5297.77 5590.16 111.31 o 6 4 0 4442.03 4536.20 103.75 o 8 4 0 925.37 1005.84 61.40 o 10 4 0 913.05 1030.52 73.46 o 2 5 0 1268.69 1106.53 32.97 o 4 5 0 3139.44 3315.90 81.40 o 6 5 0 527.47 586.25 54.45 o 8 5 0 226.80 210.90 38.70 o 10 5 0 118.36 176.92 47.59 o 0 6 0 16859.21 17377.78 412.88 o 2 6 0 545.95 507.13 19.09 o 4 6 0 37.06 57.54 13.11 o 6 6 0 5.20 35.29 24.63 o 8 6 0 607.82 637.86 53.03 o 2 7 0 275.62 267.50 14.08 o 4 7 0 2983.73 3106.70 106.84 o 6 7 0 978.30 1050.55 52.65 o 8 7 0 143.29 155.46 37.87 o 0 8 0 546.02 684.38 26.20 o 2 8 0 5469.05 5506.98 129.84 o 4 8 0 3.19 -9.10 15.01 o 6 8 0 1355.46 1305.57 74.01 o 8 8 0 1465.65 1483.26 115.41 o 2 9 0 893.87 907.90 26.71 o 4 9 0 402.26 403.61 41.19 o 6 9 0 52.27 89.24 33.95 o 8 9 0 88.14 156.58 51.86 o 0 10 0 41.15 40.90 12.14 o 2 10 0 330.76 366.28 17.72 o 4 10 0 3582.25 3677.52 117.51 o 6 10 0 7.13 24.22 37.35 o 8 10 0 9.04 22.89 53.72 o 2 11 0 3218.32 3116.14 72.98 o 4 11 0 204.23 273.29 33.14 o 6 11 0 174.84 193.38 37.76 o 8 11 0 105.84 142.46 47.24 o 0 12 0 914.44 810.73 36.56 o 2 12 0 364.06 346.14 25.73 o 4 12 0 222.28 223.71 31.40 o 6 12 0 67.55 152.31 38.51 o 8 12 0 403.75 541.34 65.73 o 2 13 0 105.43 94.67 20.08 o 4 13 0 4.86 -22.25 22.25 o 6 13 0 232.62 210.01 91.91 o 0 14 0 4.53 21.10 22.78 o 2 14 0 461.09 498.98 32.59 o 4 14 0 45.60 42.81 26.44 o 6 14 0 131.69 107.88 38.90 o 2 15 0 1048.35 1023.31 75.30 o 4 15 0 806.74 887.83 54.32 o 6 15 0 226.02 255.43 109.54 o 0 16 0 22.80 28.78 26.86 o 2 16 0 234.71 233.66 27.49 o 4 16 0 7.53 -25.79 25.79 o 2 17 0 50.94 56.62 40.83 o 4 17 0 334.81 497.47 81.90 o 0 18 0 142.18 151.45 37.17 o 2 18 0 16.85 91.25 42.21 o 4 18 0 30.83 -36.21 42.21 o 2 19 0 155.46 197.97 49.52 o 1 1 1 38.59 18.34 2.83 o 2 1 1 12045.26 12719.45 145.87 o 3 1 1 0.24 -1.73 7.54 o 4 1 1 1481.10 1611.88 32.11 o 5 1 1 11.26 13.16 10.56 o 6 1 1 20.82 43.45 14.15 o 7 1 1 58.90 79.91 16.74 o 8 1 1 1.40 -2.97 15.54 o 9 1 1 217.77 231.65 27.41 o 10 1 1 3.85 -5.36 32.32 o 0 2 1 5631.70 5606.89 111.44 o 1 2 1 20416.00 21012.60 203.18 o 2 2 1 13872.58 14556.25 157.13 o 3 2 1 9602.87 10463.75 131.86 o 4 2 1 2513.37 2732.20 45.30 o 5 2 1 2202.33 2154.22 41.31 o 6 2 1 2143.69 2072.78 44.11 o 7 2 1 14.09 20.90 14.57 o 8 2 1 124.45 123.43 23.73 o 9 2 1 28.05 3.07 22.44 o 10 2 1 6.97 15.22 26.20 o 1 3 1 466.65 512.14 9.01 o 2 3 1 1342.11 1352.99 21.93 o 3 3 1 1331.40 1545.52 28.37 o 4 3 1 604.79 628.95 21.65 o 5 3 1 59.59 47.49 11.36 o 6 3 1 475.67 460.53 21.91 o 7 3 1 11.58 -9.57 14.10 o 8 3 1 60.41 55.57 21.86 o 9 3 1 201.95 202.03 29.83 o 10 3 1 10.81 9.43 26.48 o 0 4 1 15099.65 15847.35 468.19 o 1 4 1 236.25 218.91 9.71 o 2 4 1 1614.12 1588.95 27.26 o 3 4 1 2219.95 2199.74 33.54 o 4 4 1 7240.93 7573.52 101.50 o 5 4 1 77.01 106.99 13.38 o 6 4 1 110.38 103.29 15.79 o 7 4 1 5.18 -14.40 14.40 o 8 4 1 114.10 133.69 25.11 o 9 4 1 236.69 363.41 33.75 o 10 4 1 0.48 28.92 27.77 o 1 5 1 18.20 23.14 5.35 o 2 5 1 1926.35 1963.17 29.39 o 3 5 1 1324.54 1400.79 24.50 o 4 5 1 1514.59 1540.19 30.70 o 5 5 1 688.84 696.91 22.99 o 6 5 1 1096.92 1115.65 33.43 o 7 5 1 6.03 12.41 17.83 o 8 5 1 4.75 -4.92 20.43 o 9 5 1 313.05 410.08 35.76 o 10 5 1 256.06 353.91 41.84 o 0 6 1 2425.20 2566.49 68.38 o 1 6 1 14.48 37.40 9.17 o 2 6 1 312.08 335.58 11.70 o 3 6 1 184.98 204.78 11.73 o 4 6 1 159.76 193.20 13.14 o 5 6 1 1910.69 1963.26 42.32 o 6 6 1 575.98 579.53 30.69 o 7 6 1 1728.67 1601.65 49.82 o 8 6 1 596.38 627.75 37.04 o 9 6 1 516.26 568.61 39.50 o 1 7 1 82.94 80.23 8.21 o 2 7 1 30.54 28.27 7.98 o 3 7 1 98.27 82.99 10.09 o 4 7 1 6.09 1.16 9.39 o 5 7 1 1.48 11.45 15.36 o 6 7 1 14.37 10.53 16.41 o 7 7 1 262.01 311.22 34.60 o 8 7 1 33.71 10.01 21.51 o 9 7 1 94.96 142.59 36.43 o 0 8 1 261.35 273.43 17.17 o 1 8 1 935.68 983.11 31.03 o 2 8 1 110.47 107.86 8.14 o 3 8 1 1161.61 1154.92 30.97 o 4 8 1 59.41 63.41 14.76 o 5 8 1 115.88 124.44 21.73 o 6 8 1 441.90 461.21 41.61 o 7 8 1 109.34 72.05 43.34 o 8 8 1 205.38 172.24 33.73 o 9 8 1 0.22 71.83 32.67 o 1 9 1 624.92 554.87 18.78 o 2 9 1 22.55 27.71 6.64 o 3 9 1 1846.74 1866.13 34.36 o 4 9 1 2319.79 2254.86 52.04 o 5 9 1 819.06 823.29 45.76 o 6 9 1 713.84 748.83 58.00 o 7 9 1 47.72 81.22 26.16 o 8 9 1 5.26 -2.04 25.66 o 9 9 1 49.81 -1.32 30.60 o 0 10 1 2171.68 2243.81 45.51 o 1 10 1 1102.59 1129.23 34.32 o 2 10 1 866.10 858.16 20.94 o 3 10 1 964.75 961.85 25.75 o 4 10 1 1019.40 919.80 36.89 o 5 10 1 344.58 357.71 28.42 o 6 10 1 79.90 99.29 24.56 o 7 10 1 716.03 689.05 68.57 o 8 10 1 42.53 13.92 28.11 o 1 11 1 389.87 316.33 17.03 o 2 11 1 124.21 127.38 11.65 o 3 11 1 1101.54 1007.03 33.90 o 4 11 1 249.88 255.32 22.88 o 5 11 1 234.45 239.79 25.85 o 6 11 1 2.77 -8.73 20.23 o 7 11 1 8.40 9.46 23.16 o 8 11 1 1.76 3.35 28.02 o 0 12 1 1690.26 1627.37 69.66 o 1 12 1 145.37 121.69 9.81 o 2 12 1 41.78 30.39 11.56 o 3 12 1 312.67 353.43 26.34 o 4 12 1 69.01 60.89 17.96 o 5 12 1 77.48 67.62 21.13 o 6 12 1 136.59 130.11 26.05 o 7 12 1 84.75 99.38 28.92 o 8 12 1 15.54 7.07 28.60 o 1 13 1 1831.28 1725.29 41.34 o 2 13 1 401.17 385.89 19.84 o 3 13 1 1366.88 1345.94 41.10 o 4 13 1 74.84 52.03 18.26 o 5 13 1 9.32 -11.26 17.91 o 6 13 1 242.46 286.16 46.82 o 7 13 1 13.43 -4.94 25.16 o 0 14 1 197.26 208.71 22.31 o 1 14 1 1424.90 1427.97 37.74 o 2 14 1 180.54 198.40 16.94 o 3 14 1 136.57 131.53 18.27 o 4 14 1 46.38 11.70 25.82 o 5 14 1 1.53 13.81 19.68 o 6 14 1 164.99 162.11 29.03 o 7 14 1 259.51 301.99 36.41 o 1 15 1 99.33 85.49 13.90 o 2 15 1 88.25 82.38 15.09 o 3 15 1 287.24 321.73 22.82 o 4 15 1 1.99 40.55 19.13 o 5 15 1 596.81 716.73 38.89 o 6 15 1 194.17 199.97 35.58 o 0 16 1 4.35 34.44 18.08 o 1 16 1 173.95 187.06 23.83 o 2 16 1 15.39 -11.52 16.79 o 3 16 1 39.64 18.12 16.12 o 4 16 1 427.45 510.45 49.66 o 5 16 1 163.74 177.16 26.61 o 1 17 1 26.42 24.35 16.08 o 2 17 1 116.28 153.30 26.81 o 3 17 1 361.64 437.77 27.11 o 4 17 1 105.66 181.16 24.61 o 5 17 1 9.91 -21.37 21.37 o 0 18 1 135.03 131.92 26.17 o 1 18 1 138.25 166.25 36.28 o 2 18 1 243.73 302.97 28.22 o 3 18 1 56.50 153.32 31.42 o 4 18 1 6.04 -14.68 23.55 o 1 19 1 10.15 19.02 39.15 o 2 19 1 38.28 37.39 29.76 o 1 0 2 15456.25 16233.39 192.76 o 2 0 2 941.03 911.45 35.19 o 3 0 2 158.30 108.02 14.19 o 4 0 2 1946.53 2072.92 53.34 o 5 0 2 1305.39 1369.73 45.24 o 6 0 2 22.74 47.65 23.38 o 7 0 2 8632.78 8563.24 176.95 o 8 0 2 477.97 519.66 40.25 o 9 0 2 64.65 61.99 29.55 o 10 0 2 49.61 37.21 49.35 o 1 1 2 27827.96 28901.12 248.34 o 2 1 2 2607.59 2978.56 39.74 o 3 1 2 430.45 398.06 14.19 o 4 1 2 414.99 375.43 15.88 o 5 1 2 1679.26 1640.27 35.56 o 6 1 2 1763.70 1839.53 41.37 o 7 1 2 458.79 473.93 25.21 o 8 1 2 24.35 14.81 16.79 o 9 1 2 153.54 101.27 23.63 o 10 1 2 35.38 44.87 35.32 o 0 2 2 77.66 48.26 4.36 o 1 2 2 5.77 1.60 3.23 o 2 2 2 10236.61 10896.62 125.89 o 3 2 2 5472.34 5984.45 80.07 o 4 2 2 3416.45 3753.66 57.38 o 5 2 2 21.16 31.68 11.02 o 6 2 2 15.26 31.51 14.57 o 7 2 2 1357.27 1242.44 36.84 o 8 2 2 23.11 19.70 16.51 o 9 2 2 18.29 -21.29 21.71 o 10 2 2 34.18 -4.62 26.47 o 1 3 2 33.43 5.88 3.61 o 2 3 2 657.19 608.20 15.04 o 3 3 2 7500.73 7916.20 102.35 o 4 3 2 345.89 329.41 15.35 o 5 3 2 8.76 20.49 10.69 o 6 3 2 23.79 35.44 13.59 o 7 3 2 60.93 57.40 16.09 o 8 3 2 17.13 6.00 20.36 o 9 3 2 9.04 -3.24 22.99 o 10 3 2 2.90 -20.50 26.17 o 0 4 2 17541.89 16911.81 327.64 o 1 4 2 2734.13 2833.95 40.59 o 2 4 2 10072.91 10450.07 131.38 o 3 4 2 8348.42 8963.34 114.65 o 4 4 2 376.28 382.60 16.30 o 5 4 2 3632.55 3891.68 62.01 o 6 4 2 6.26 17.09 13.40 o 7 4 2 2027.92 2034.19 50.84 o 8 4 2 186.06 205.30 27.27 o 9 4 2 185.65 190.75 29.14 o 10 4 2 4.48 65.35 29.11 o 1 5 2 1408.49 1573.84 30.50 o 2 5 2 632.42 867.09 16.52 o 3 5 2 2260.67 2552.90 38.75 o 4 5 2 501.84 525.01 19.66 o 5 5 2 4494.24 4492.80 68.98 o 6 5 2 1782.45 1777.52 40.40 o 7 5 2 8.83 15.21 18.49 o 8 5 2 87.88 52.74 23.64 o 9 5 2 3.44 13.80 24.09 o 10 5 2 143.26 179.75 37.30 o 0 6 2 2677.40 2882.52 78.00 o 1 6 2 3239.92 3342.40 51.26 o 2 6 2 191.08 200.23 11.57 o 3 6 2 509.44 592.95 18.73 o 4 6 2 131.16 105.88 10.82 o 5 6 2 344.03 380.06 19.99 o 6 6 2 167.33 165.21 20.67 o 7 6 2 50.06 9.83 18.74 o 8 6 2 551.49 433.06 33.32 o 9 6 2 1.64 8.21 30.08 o 1 7 2 183.80 195.63 10.49 o 2 7 2 958.94 968.91 17.29 o 3 7 2 798.81 826.25 23.54 o 4 7 2 1124.47 1141.06 27.64 o 5 7 2 261.35 292.73 22.84 o 6 7 2 45.76 16.90 18.85 o 7 7 2 24.43 12.78 20.67 o 8 7 2 0.89 8.54 22.81 o 9 7 2 499.59 534.79 48.96 o 0 8 2 737.26 663.24 29.62 o 1 8 2 4504.61 4753.76 78.42 o 2 8 2 285.59 301.88 11.52 o 3 8 2 1261.40 1253.06 37.80 o 4 8 2 28.42 23.30 12.59 o 5 8 2 99.74 77.12 18.14 o 6 8 2 915.94 977.16 39.91 o 7 8 2 391.77 420.06 36.64 o 8 8 2 25.21 20.32 26.80 o 9 8 2 129.00 118.93 36.04 o 1 9 2 139.89 150.54 10.31 o 2 9 2 850.31 777.59 18.22 o 3 9 2 1671.30 1744.15 30.90 o 4 9 2 611.46 615.56 26.76 o 5 9 2 801.14 825.20 38.56 o 6 9 2 42.64 70.67 23.53 o 7 9 2 9.63 49.68 25.03 o 8 9 2 45.61 57.11 29.10 o 9 9 2 5.71 32.35 31.01 o 0 10 2 289.67 301.78 50.72 o 1 10 2 737.04 728.00 21.15 o 2 10 2 138.15 135.79 10.05 o 3 10 2 2076.19 1970.99 39.12 o 4 10 2 655.23 642.17 31.06 o 5 10 2 2.87 -16.55 16.55 o 6 10 2 21.38 10.24 21.05 o 7 10 2 33.15 15.78 24.21 o 8 10 2 0.95 26.49 28.39 o 1 11 2 350.89 375.36 15.97 o 2 11 2 2328.23 2370.95 63.67 o 3 11 2 246.44 244.83 19.32 o 4 11 2 16.73 24.36 23.49 o 5 11 2 470.91 448.33 30.81 o 6 11 2 17.10 14.93 20.50 o 7 11 2 11.47 4.54 23.38 o 8 11 2 44.26 9.63 28.14 o 0 12 2 3923.45 3563.95 98.10 o 1 12 2 928.57 942.33 34.50 o 2 12 2 2.26 5.90 9.96 o 3 12 2 675.04 693.87 28.89 o 4 12 2 1.05 9.60 16.40 o 5 12 2 33.63 31.76 24.77 o 6 12 2 116.32 141.76 26.15 o 7 12 2 508.83 515.58 45.30 o 8 12 2 8.52 -7.27 28.74 o 1 13 2 620.04 584.36 28.08 o 2 13 2 924.65 924.36 37.93 o 3 13 2 82.15 96.79 20.20 o 4 13 2 44.33 41.23 18.39 o 5 13 2 14.43 8.54 18.69 o 6 13 2 0.03 8.32 27.45 o 7 13 2 15.82 4.66 25.98 o 0 14 2 437.81 338.42 27.05 o 1 14 2 423.60 370.86 59.69 o 2 14 2 233.05 220.11 22.59 o 3 14 2 30.67 35.36 15.43 o 4 14 2 19.86 9.59 17.53 o 5 14 2 159.41 182.65 25.79 o 6 14 2 5.21 21.40 23.15 o 7 14 2 302.46 275.27 36.05 o 1 15 2 11.06 16.02 11.80 o 2 15 2 322.38 303.26 19.55 o 3 15 2 676.51 630.37 51.59 o 4 15 2 148.16 177.11 23.01 o 5 15 2 110.27 136.35 25.42 o 6 15 2 6.16 15.21 25.94 o 0 16 2 114.64 88.94 38.61 o 1 16 2 47.43 45.64 13.65 o 2 16 2 137.19 141.86 27.75 o 3 16 2 2.05 -5.02 15.61 o 4 16 2 5.34 18.56 18.72 o 5 16 2 377.04 458.85 44.29 o 1 17 2 2.71 -16.02 16.02 o 2 17 2 9.84 0.73 18.91 o 3 17 2 131.71 160.55 26.42 o 4 17 2 33.15 -16.19 23.44 o 5 17 2 2.08 -12.32 22.08 o 0 18 2 0.02 8.15 35.37 o 1 18 2 142.70 153.56 24.04 o 2 18 2 98.71 120.62 24.10 o 3 18 2 4.34 -21.33 21.33 o 1 19 2 53.37 82.02 23.00 o 2 19 2 18.41 53.07 30.65 o 1 1 3 642.62 683.65 11.95 o 2 1 3 4047.04 3827.66 49.31 o 3 1 3 680.15 694.81 19.32 o 4 1 3 0.27 1.73 8.62 o 5 1 3 193.60 212.62 16.10 o 6 1 3 3.06 -4.31 12.64 o 7 1 3 23.15 19.65 15.78 o 8 1 3 3.67 -6.35 15.98 o 9 1 3 0.01 -13.27 19.82 o 10 1 3 60.06 36.84 30.42 o 0 2 3 827.82 777.16 15.05 o 1 2 3 2786.95 2858.46 34.31 o 2 2 3 15.88 -4.99 6.74 o 3 2 3 1770.23 1835.79 32.27 o 4 2 3 408.14 396.37 16.47 o 5 2 3 113.91 126.95 20.28 o 6 2 3 7087.03 6983.63 102.66 o 7 2 3 199.08 174.54 19.28 o 8 2 3 1003.14 973.33 35.60 o 9 2 3 6.07 26.68 23.32 o 10 2 3 61.18 42.93 30.77 o 1 3 3 223.37 182.15 8.75 o 2 3 3 6712.02 7600.15 102.35 o 3 3 3 3691.35 3978.12 57.02 o 4 3 3 248.81 256.85 13.99 o 5 3 3 117.07 108.12 13.12 o 6 3 3 950.53 932.99 29.36 o 7 3 3 41.52 23.86 15.19 o 8 3 3 111.24 101.92 21.38 o 9 3 3 9.87 -21.37 21.37 o 10 3 3 66.08 89.98 30.23 o 0 4 3 1909.87 1709.10 53.07 o 1 4 3 66.21 40.94 6.99 o 2 4 3 6346.93 6290.22 80.49 o 3 4 3 117.20 141.96 12.99 o 4 4 3 189.71 145.18 12.02 o 5 4 3 278.38 265.75 16.34 o 6 4 3 817.03 738.11 26.32 o 7 4 3 450.49 387.32 25.67 o 8 4 3 81.79 35.35 21.51 o 9 4 3 6.46 9.41 23.67 o 10 4 3 9.09 5.99 27.58 o 1 5 3 3114.72 3290.13 44.47 o 2 5 3 8215.92 8168.43 112.37 o 3 5 3 25.77 31.38 6.98 o 4 5 3 2380.52 2488.72 49.48 o 5 5 3 517.61 518.45 20.68 o 6 5 3 37.10 45.75 14.24 o 7 5 3 257.09 254.75 25.59 o 8 5 3 21.28 -10.56 19.95 o 9 5 3 47.80 61.52 25.82 o 0 6 3 7835.43 8148.16 163.54 o 1 6 3 893.32 962.18 18.57 o 2 6 3 14095.61 14847.10 169.48 o 3 6 3 1228.86 1269.19 29.12 o 4 6 3 622.17 740.95 21.12 o 5 6 3 8.70 2.90 10.14 o 6 6 3 374.61 453.69 27.27 o 7 6 3 281.44 196.21 24.42 o 8 6 3 306.63 387.19 31.66 o 9 6 3 101.56 71.60 28.94 o 1 7 3 1238.01 1540.91 26.72 o 2 7 3 851.29 865.09 17.70 o 3 7 3 12.26 9.77 6.68 o 4 7 3 1200.10 1084.88 27.18 o 5 7 3 1.57 25.49 12.99 o 6 7 3 291.41 271.99 25.33 o 7 7 3 78.42 92.18 23.48 o 8 7 3 57.21 82.91 29.34 o 9 7 3 76.11 40.55 35.56 o 0 8 3 198.14 242.60 20.07 o 1 8 3 352.73 309.41 11.73 o 2 8 3 356.54 354.16 13.46 o 3 8 3 391.53 434.65 15.95 o 4 8 3 57.88 58.14 19.27 o 5 8 3 547.63 555.40 32.79 o 6 8 3 145.74 94.48 21.27 o 7 8 3 8.32 4.20 22.11 o 8 8 3 5.47 22.23 25.98 o 9 8 3 11.15 64.19 49.12 o 1 9 3 42.14 31.71 8.32 o 2 9 3 2089.68 2004.54 43.09 o 3 9 3 660.04 696.53 26.39 o 4 9 3 3827.54 3914.25 77.55 o 5 9 3 465.40 491.26 39.15 o 6 9 3 467.27 470.61 36.24 o 7 9 3 4.48 -11.79 23.28 o 8 9 3 102.63 54.12 29.07 o 9 9 3 83.76 84.78 33.71 o 0 10 3 7288.11 7593.00 404.46 o 1 10 3 606.08 596.50 21.18 o 2 10 3 1803.80 1721.21 39.27 o 3 10 3 1212.95 1221.92 35.03 o 4 10 3 1073.36 1032.97 39.13 o 5 10 3 36.69 13.00 18.38 o 6 10 3 355.31 362.85 32.76 o 7 10 3 0.02 23.29 23.70 o 8 10 3 424.84 403.56 41.21 o 1 11 3 383.40 329.87 15.52 o 2 11 3 2319.00 2230.33 62.05 o 3 11 3 56.48 60.01 14.77 o 4 11 3 737.16 779.19 34.04 o 5 11 3 143.31 124.24 22.59 o 6 11 3 26.05 56.32 22.62 o 7 11 3 4.61 19.35 24.30 o 8 11 3 1.45 4.28 27.24 o 0 12 3 67.17 39.10 13.74 o 1 12 3 1682.12 1350.04 136.49 o 2 12 3 656.69 652.55 32.17 o 3 12 3 32.41 28.34 20.94 o 4 12 3 225.83 230.06 22.67 o 5 12 3 52.81 46.53 20.70 o 6 12 3 2.09 44.69 22.65 o 7 12 3 26.58 16.50 33.42 o 8 12 3 36.61 -12.38 28.21 o 1 13 3 168.00 141.47 18.58 o 2 13 3 907.04 963.57 39.96 o 3 13 3 133.99 133.60 17.32 o 4 13 3 1692.38 1697.39 66.75 o 5 13 3 122.79 154.35 23.78 o 6 13 3 225.19 255.71 30.44 o 7 13 3 51.33 70.52 27.99 o 0 14 3 3065.04 3031.23 89.65 o 1 14 3 130.21 95.96 17.78 o 2 14 3 742.55 711.63 35.30 o 3 14 3 1.79 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77.16 o