#------------------------------------------------------------------------------
#$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $
#$Revision: 691 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219662.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2219662_Fobs
loop_
_publ_author_name
'Yamane, Hisanori'
'Ono, Takeshi'
'Yamada, Takahiro'
_publ_section_title
;
 <i>R</i>-Ferrite-type barium cobalt stannate, BaCo~2~Sn~4~O~11~
;
_journal_coeditor_code           MG2057
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i71
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           194
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   6.0880
_cell_length_b                   6.0880
_cell_length_c                   14.1049
_exptl_crystal_F_000             796.00
_reflns_d_resolution_high        0.7732
_[local]_cod_data_source_file    mg2057Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     'BCSO in P63/mmc'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            430.80
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-y, x-y, z'
'-x+y, -x, z'
'x-y, x, z+1/2'
'y, -x+y, z+1/2'
'x-y, -y, -z'
'-x, -x+y, -z'
'y, x, -z'
'-y, -x, -z+1/2'
'x, x-y, -z+1/2'
'-x+y, y, -z+1/2'
'-x, -y, -z'
'x, y, -z-1/2'
'y, -x+y, -z'
'x-y, x, -z'
'-x+y, -x, -z-1/2'
'-y, x-y, -z-1/2'
'-x+y, y, z'
'x, x-y, z'
'-y, -x, z'
'y, x, z-1/2'
'-x, -x+y, z-1/2'
'x-y, -y, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 1 0 1561.32 1472.97 24.84 o
-1 2 0 47519.28 47258.92 924.00 o
0 2 0 52444.68 51204.55 1035.84 o
-1 3 0 668.56 675.50 15.53 o
0 3 0 30281.90 30135.82 757.45 o
-2 4 0 185588.08 187816.14 5390.46 o
-1 4 0 495.16 477.20 20.61 o
0 4 0 28165.66 28282.49 905.07 o
-2 5 0 650.86 569.97 31.76 o
-1 5 0 16373.30 16333.65 518.68 o
0 5 0 423.55 370.40 77.59 o
-3 6 0 12685.71 12608.79 1060.59 o
-2 6 0 17125.79 16489.18 745.78 o
-1 6 0 190.93 155.57 43.62 o
0 6 0 53994.88 46951.43 9790.70 o
-3 7 0 272.09 160.68 47.86 o
-2 7 0 8023.38 7481.27 665.79 o
-1 7 0 202.62 149.41 79.56 o
0 1 1 1339.42 1330.13 21.54 o
0 2 1 749.14 683.80 17.79 o
-1 3 1 423.41 403.27 9.06 o
0 3 1 220.55 232.91 9.46 o
-1 4 1 673.62 716.27 17.69 o
0 4 1 301.56 399.20 30.17 o
-2 5 1 610.42 596.79 18.07 o
-1 5 1 60.38 71.92 11.98 o
0 5 1 112.97 188.37 27.11 o
-2 6 1 155.06 176.93 17.42 o
-1 6 1 235.87 262.76 27.46 o
0 6 1 0.22 3.79 19.12 o
-3 7 1 91.82 77.33 22.21 o
-2 7 1 75.27 57.28 25.33 o
-1 7 1 226.66 218.56 41.27 o
0 1 2 4116.92 4077.37 65.12 o
-1 2 2 52694.51 53121.20 820.75 o
0 2 2 42782.95 41744.88 605.54 o
-1 3 2 1084.85 1009.09 19.16 o
0 3 2 32643.26 32183.31 548.35 o
-2 4 2 1021.95 1080.19 32.49 o
-1 4 2 1479.81 1454.48 28.66 o
0 4 2 19222.16 19647.66 408.61 o
-2 5 2 1444.65 1398.49 30.07 o
-1 5 2 17902.40 18123.06 308.01 o
0 5 2 203.86 220.51 30.94 o
-3 6 2 14618.39 13391.21 632.36 o
-2 6 2 10484.26 10263.39 334.70 o
-1 6 2 416.85 382.97 33.94 o
0 6 2 346.72 341.29 54.21 o
-3 7 2 167.96 146.30 23.08 o
-2 7 2 7694.22 7471.27 353.87 o
-1 7 2 518.11 468.18 55.93 o
0 1 3 1042.69 1057.27 27.32 o
0 2 3 17315.45 18404.84 319.25 o
-1 3 3 596.89 572.74 12.45 o
0 3 3 12.40 12.39 5.60 o
-1 4 3 620.17 685.01 19.17 o
0 4 3 4907.99 4940.76 111.18 o
-2 5 3 406.12 411.69 17.24 o
-1 5 3 2.04 -6.42 6.42 o
0 5 3 208.70 214.26 26.26 o
-2 6 3 2179.39 2219.26 72.15 o
-1 6 3 297.30 317.97 28.13 o
0 6 3 0.18 11.71 25.44 o
-3 7 3 155.84 144.22 22.91 o
-2 7 3 1.14 3.65 17.04 o
-1 7 3 172.09 104.73 37.01 o
0 0 4 40970.66 40359.94 1833.99 o
0 1 4 68776.13 68104.09 1293.05 o
-1 2 4 6183.17 6195.55 122.13 o
0 2 4 9.20 23.47 8.52 o
-1 3 4 50006.94 50432.75 657.24 o
0 3 4 4076.05 4078.13 80.88 o
-2 4 4 15729.04 15701.63 301.99 o
-1 4 4 32280.23 32313.52 401.91 o
0 4 4 0.39 24.60 11.08 o
-2 5 4 20798.41 20733.96 293.49 o
-1 5 4 2155.78 2189.81 55.84 o
0 5 4 20189.21 21698.27 545.84 o
-3 6 4 1720.49 1661.77 62.32 o
-2 6 4 0.25 22.73 7.95 o
-1 6 4 15878.01 16992.34 389.30 o
0 6 4 4556.01 5004.24 196.72 o
-3 7 4 12752.95 13123.64 361.13 o
-2 7 4 1080.30 1096.56 57.10 o
-1 7 4 8863.63 9267.00 431.71 o
0 1 5 1069.58 1046.43 37.23 o
0 2 5 498.52 468.67 22.72 o
-1 3 5 437.11 433.88 17.01 o
0 3 5 152.97 172.04 16.98 o
-1 4 5 637.71 668.44 19.75 o
0 4 5 243.31 301.48 18.77 o
-2 5 5 566.83 562.04 22.81 o
-1 5 5 48.78 41.29 8.80 o
0 5 5 130.37 127.87 17.72 o
-2 6 5 126.30 112.78 13.62 o
-1 6 5 240.84 205.92 21.13 o
0 6 5 0.17 -9.71 21.44 o
-3 7 5 100.62 102.23 24.07 o
-2 7 5 67.02 52.17 22.55 o
-1 7 5 219.03 172.16 38.73 o
0 0 6 4569.11 3932.67 248.97 o
0 1 6 9088.71 9033.51 200.50 o
-1 2 6 3321.28 3256.51 83.57 o
0 2 6 126586.77 127918.85 2600.05 o
-1 3 6 6858.29 7014.55 115.94 o
0 3 6 1960.14 1916.84 65.54 o
-2 4 6 5083.57 5171.01 124.66 o
-1 4 6 4694.91 4632.75 83.57 o
0 4 6 60664.99 60549.82 1548.61 o
-2 5 6 3570.87 3627.97 75.15 o
-1 5 6 1239.54 1167.85 30.86 o
0 5 6 3239.50 3455.45 123.76 o
-3 6 6 1197.85 1130.31 50.22 o
-2 6 6 34737.28 34562.40 787.60 o
-1 6 6 2305.53 2423.11 76.88 o
0 6 6 2845.65 2998.15 137.86 o
-3 7 6 2029.21 2137.78 78.56 o
-2 7 6 340.08 285.01 34.77 o
0 1 7 1362.38 1337.12 51.98 o
0 2 7 1117.09 1143.69 47.42 o
-1 3 7 612.98 643.22 25.72 o
0 3 7 114.20 118.81 21.05 o
-1 4 7 780.13 783.49 29.41 o
0 4 7 509.07 497.93 29.99 o
-2 5 7 703.83 723.84 31.17 o
-1 5 7 40.02 40.81 8.42 o
0 5 7 173.29 165.17 23.54 o
-2 6 7 260.84 217.42 21.77 o
-1 6 7 280.48 200.83 28.39 o
0 6 7 0.19 4.12 24.05 o
-3 7 7 123.13 135.02 27.59 o
-2 7 7 58.52 46.64 22.29 o
0 0 8 101264.98 100936.30 5636.55 o
0 1 8 1040.74 993.84 47.55 o
-1 2 8 8266.74 8433.05 215.68 o
0 2 8 28037.04 28831.57 632.08 o
-1 3 8 1346.57 1423.24 42.13 o
0 3 8 6177.61 6287.27 168.90 o
-2 4 8 51244.38 51341.92 1175.53 o
-1 4 8 668.26 662.89 30.09 o
0 4 8 15179.79 14080.13 478.38 o
-2 5 8 188.20 217.52 17.63 o
-1 5 8 3736.18 3554.18 96.03 o
0 5 8 597.47 551.74 40.25 o
-3 6 8 2940.93 2919.14 104.37 o
-2 6 8 9471.03 9620.15 242.43 o
-1 6 8 487.88 401.63 34.08 o
0 6 8 18805.96 20410.47 671.22 o
-3 7 8 377.24 284.15 34.07 o
0 1 9 952.33 985.96 53.89 o
0 2 9 7778.44 7704.03 205.24 o
-1 3 9 686.10 716.52 30.90 o
0 3 9 6.80 -1.73 14.45 o
-1 4 9 633.44 663.05 32.50 o
0 4 9 3325.54 3112.39 130.15 o
-2 5 9 422.83 431.65 25.90 o
-1 5 9 1.85 -2.98 10.59 o
0 5 9 269.10 233.38 34.25 o
-2 6 9 1741.47 1891.24 63.59 o
-1 6 9 318.24 214.32 33.54 o
0 0 10 3152.53 3414.51 283.43 o
0 1 10 15184.09 15184.61 395.59 o
-1 2 10 52285.64 53359.31 1290.15 o
0 2 10 4356.77 4449.37 141.80 o
-1 3 10 9488.48 9573.63 182.61 o
0 3 10 38240.54 38508.50 929.44 o
-2 4 10 1705.88 1729.91 81.71 o
-1 4 10 8604.76 8672.85 176.79 o
0 4 10 2220.10 2250.84 106.14 o
-2 5 10 7446.80 7100.79 154.91 o
-1 5 10 23822.95 22754.13 611.51 o
0 5 10 4005.58 3919.62 191.30 o
-3 6 10 19953.46 19394.44 593.94 o
-2 6 10 1212.03 1182.66 53.46 o
-1 6 10 4089.48 4072.45 154.50 o
0 1 11 943.24 951.07 60.26 o
0 2 11 513.09 507.19 44.86 o
-1 3 11 522.81 561.51 34.72 o
0 3 11 48.79 66.83 26.49 o
-1 4 11 617.74 625.34 38.64 o
0 4 11 261.62 293.19 38.08 o
-2 5 11 548.21 553.70 36.56 o
-1 5 11 21.70 19.14 16.37 o
0 5 11 157.19 109.32 35.96 o
-2 6 11 131.18 98.87 27.54 o
0 0 12 65994.58 65227.45 4037.44 o
0 1 12 4609.62 4633.48 169.72 o
-1 2 12 696.84 680.57 59.52 o
0 2 12 4149.67 4296.85 163.92 o
-1 3 12 3714.58 3787.44 98.85 o
0 3 12 547.84 615.08 52.31 o
-2 4 12 35698.36 35408.82 941.75 o
-1 4 12 2917.67 2993.31 90.90 o
0 4 12 2741.46 2724.85 119.44 o
-2 5 12 1961.64 1897.32 71.56 o
-1 5 12 347.99 307.27 32.26 o
0 5 12 1655.28 1567.43 116.94 o
0 1 13 1122.17 1116.25 74.15 o
0 2 13 1091.83 1135.67 79.07 o
-1 3 13 683.21 655.20 40.76 o
0 3 13 51.43 59.96 32.72 o
-1 4 13 699.63 708.34 43.49 o
0 4 13 572.79 480.22 60.14 o
-2 5 13 603.50 564.39 45.53 o
-1 5 13 26.16 12.63 19.94 o
0 0 14 21599.95 22509.29 2042.98 o
0 1 14 5344.73 5700.65 212.34 o
-1 2 14 20.97 19.33 31.25 o
0 2 14 41236.70 42123.10 1164.10 o
-1 3 14 5012.58 4869.36 130.78 o
0 3 14 3.91 38.18 32.67 o
-2 4 14 14028.75 13691.64 426.24 o
-1 4 14 3454.75 3353.63 106.85 o
0 4 14 26237.71 24428.38 1046.19 o
-2 5 14 2560.94 2498.50 95.34 o
0 1 15 740.90 797.77 76.35 o
0 2 15 3420.04 3481.66 161.69 o
-1 3 15 531.16 519.09 44.20 o
0 3 15 0.90 10.65 27.93 o
-1 4 15 493.30 477.47 43.00 o
0 0 16 11004.38 11752.85 946.43 o
0 1 16 9293.40 9692.87 344.92 o
-1 2 16 648.45 644.54 74.98 o
0 2 16 528.58 516.47 62.91 o
-1 3 16 8403.35 8456.54 209.73 o
0 3 16 539.66 502.08 61.92 o
0 1 17 625.83 675.01 78.87 o
0 2 17 359.65 336.46 65.04 o
0 0 18 1164.63 980.94 248.81 o
0 1 18 3024.26 3112.59 172.32 o