#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:54:19 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181116 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/96/2219664.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2219664_Fobs
loop_
_publ_author_name
'Lyczko, Krzysztof'
'Bak, Joanna'
_publ_section_title
;
Poly[bis(\m~3~-acetato-\k^4^O,O':O:O')bis(\m~2~-acetato-\k^3^O,O':O)(\m~2~-2,5-dimethylbenzene-1,4-diol-\k^2^O:O')dilead(II)]
;
_journal_coeditor_code NC2114
_journal_issue 10
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m1341
_journal_page_last m1342
_journal_volume 64
_journal_year 2008
_space_group_IT_number 2
_symmetry_space_group_name_Hall '-P 1'
_symmetry_space_group_name_H-M 'P -1'
_cell_angle_alpha 93.043
_cell_angle_beta 100.787
_cell_angle_gamma 116.377
_cell_length_a 7.4905
_cell_length_b 7.5526
_cell_length_c 10.2522
_exptl_crystal_F_000 362.00
_reflns_d_resolution_high 0.7394
_cod_data_source_file nc2114Isup2.hkl
_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' pA_a2 in P1'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 198.92
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 679.16 744.54 8.54 o
2 0 0 10062.55 10026.93 280.48 o
3 0 0 12669.19 12753.79 303.49 o
4 0 0 1335.60 1278.71 20.96 o
5 0 0 7621.29 7448.52 241.73 o
6 0 0 468.15 446.91 17.65 o
7 0 0 5368.79 5464.44 200.40 o
8 0 0 801.88 822.54 76.59 o
-9 1 0 3716.20 3902.81 79.18 o
-8 1 0 156.93 153.04 25.09 o
-7 1 0 5925.11 5874.92 113.00 o
-6 1 0 3528.36 3436.81 56.97 o
-5 1 0 2576.74 2654.70 37.29 o
-4 1 0 14282.94 14388.33 133.55 o
-3 1 0 4.80 46.31 4.95 o
-2 1 0 25136.36 26242.05 306.60 o
-1 1 0 11636.82 11453.36 227.64 o
0 1 0 13071.52 12804.17 1617.99 o
1 1 0 4043.97 4000.44 144.40 o
2 1 0 22.47 57.46 4.73 o
3 1 0 17217.27 17450.44 348.86 o
4 1 0 1766.52 1836.94 46.12 o
5 1 0 4593.93 4514.37 223.49 o
6 1 0 5426.44 5485.89 433.57 o
7 1 0 622.88 646.52 57.41 o
8 1 0 3353.72 3006.98 86.66 o
-9 2 0 2082.73 2097.77 61.16 o
-8 2 0 4781.20 4838.88 104.18 o
-7 2 0 301.96 311.13 17.75 o
-6 2 0 11017.51 11296.68 80.64 o
-5 2 0 1245.37 1298.11 23.83 o
-4 2 0 4639.01 4825.55 68.30 o
-3 2 0 14708.37 14971.80 217.12 o
-2 2 0 814.78 842.76 40.50 o
-1 2 0 10077.99 10141.38 86.38 o
0 2 0 269.76 363.22 13.93 o
1 2 0 12721.82 12798.31 214.76 o
2 2 0 6692.33 6829.86 69.14 o
3 2 0 2750.66 2733.51 42.79 o
4 2 0 9604.73 9078.03 476.84 o
5 2 0 0.43 22.27 16.08 o
6 2 0 5538.95 5470.67 488.41 o
7 2 0 987.51 1045.44 66.71 o
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-8 3 0 5277.64 5565.37 69.86 o
-7 3 0 2116.53 2200.83 41.94 o
-6 3 0 3152.57 3295.85 87.84 o
-5 3 0 9218.17 9228.58 113.90 o
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-3 3 0 26768.91 26249.35 536.84 o
-2 3 0 2764.70 2780.19 26.14 o
-1 3 0 4449.43 4541.06 52.02 o
0 3 0 18577.36 18638.86 104.22 o
1 3 0 346.07 343.02 13.98 o
2 3 0 8140.28 8257.52 76.18 o
3 3 0 930.93 887.04 24.77 o
4 3 0 5647.20 5492.36 282.78 o
5 3 0 1625.25 1678.58 128.92 o
6 3 0 883.44 886.71 96.07 o
-9 4 0 2936.72 3026.94 61.38 o
-8 4 0 333.73 339.79 28.20 o
-7 4 0 5459.59 5642.79 121.94 o
-6 4 0 534.78 537.54 23.58 o
-5 4 0 8045.27 8148.18 152.42 o
-4 4 0 5802.72 5692.66 124.13 o
-3 4 0 4246.24 4409.24 124.06 o
-2 4 0 9732.58 9984.79 182.08 o
-1 4 0 33.64 89.66 12.02 o
0 4 0 13772.54 13670.34 137.33 o
1 4 0 1803.00 1930.29 103.29 o
2 4 0 2792.67 2813.88 85.85 o
3 4 0 6425.42 6241.90 170.38 o
4 4 0 258.00 217.81 30.06 o
5 4 0 4638.68 4652.68 305.82 o
-9 5 0 3264.69 3418.21 124.32 o
-8 5 0 1079.16 1108.75 37.31 o
-7 5 0 1900.49 1881.28 54.41 o
-6 5 0 5829.92 5845.96 259.93 o
-5 5 0 431.91 430.95 15.03 o
-4 5 0 6210.17 6077.65 150.93 o
-3 5 0 545.45 517.22 17.89 o
-2 5 0 8051.15 8237.47 162.57 o
-1 5 0 4427.21 4280.92 121.44 o
0 5 0 1178.12 1136.93 23.64 o
1 5 0 8443.93 8865.94 365.01 o
2 5 0 314.67 336.52 29.53 o
3 5 0 7030.20 7537.27 721.67 o
4 5 0 2293.49 2197.38 75.71 o
5 5 0 912.91 595.48 96.36 o
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-6 6 0 6028.44 6111.74 224.99 o
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-2 6 0 3.44 11.23 15.04 o
-1 6 0 6617.30 6053.23 136.71 o
0 6 0 1350.71 1340.59 30.38 o
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2 6 0 4407.44 4590.83 141.37 o
3 6 0 465.93 430.37 41.47 o
4 6 0 4179.78 4155.31 118.15 o
-9 7 0 513.83 502.85 77.06 o
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-4 7 0 302.66 299.92 22.65 o
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-1 7 0 2083.17 2049.63 57.30 o
0 7 0 6552.56 6591.36 211.18 o
1 7 0 94.61 99.59 24.04 o
2 7 0 3959.74 4069.71 85.26 o
3 7 0 1188.13 1210.89 75.25 o
-8 8 0 16.59 41.49 36.32 o
-7 8 0 3316.60 3640.49 96.18 o
-6 8 0 1272.10 1295.02 38.37 o
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-3 8 0 209.31 194.07 30.40 o
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-1 8 0 1331.37 1277.09 78.83 o
0 8 0 2569.52 2593.84 54.86 o
1 8 0 2903.53 2895.47 71.32 o
-7 9 0 563.00 572.71 50.13 o
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3 -9 1 2846.86 2642.15 225.40 o
4 -9 1 1833.22 1822.82 72.94 o
5 -9 1 727.41 756.76 47.39 o
6 -9 1 3848.94 3993.27 133.32 o
7 -9 1 29.54 29.85 38.60 o
8 -9 1 1870.54 1939.48 99.63 o
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0 -8 1 2148.93 2116.16 77.87 o
1 -8 1 1390.86 1450.70 82.10 o
2 -8 1 5957.02 5498.42 132.56 o
3 -8 1 128.47 83.32 28.49 o
4 -8 1 5031.00 5127.58 127.10 o
5 -8 1 1409.96 1435.03 45.58 o
6 -8 1 1842.71 1975.88 52.93 o
7 -8 1 2975.28 3216.42 106.02 o
8 -8 1 220.46 191.90 37.80 o
-3 -7 1 3154.77 3127.70 100.89 o
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0 -7 1 7095.97 7033.86 350.88 o
1 -7 1 137.19 125.34 25.60 o
2 -7 1 5094.90 4627.71 353.76 o
3 -7 1 4484.02 4424.93 49.91 o
4 -7 1 1712.93 1737.04 56.51 o
5 -7 1 5389.34 5731.58 149.91 o
6 -7 1 2.99 15.36 18.56 o
7 -7 1 3883.54 4073.29 109.15 o
8 -7 1 831.19 938.44 140.54 o
-4 -6 1 3719.63 3218.45 79.27 o
-3 -6 1 12.96 15.27 42.19 o
-2 -6 1 3412.25 3561.04 123.12 o
-1 -6 1 2421.83 2389.12 123.63 o
0 -6 1 3388.17 3387.87 154.76 o
1 -6 1 4689.15 4464.78 128.63 o
2 -6 1 507.79 545.94 24.82 o
3 -6 1 9589.62 10028.54 357.90 o
4 -6 1 150.74 151.93 15.18 o
5 -6 1 3815.11 3767.94 143.52 o
6 -6 1 4336.91 4225.76 136.87 o
7 -6 1 823.86 764.82 26.75 o
8 -6 1 4779.94 4808.68 199.35 o
9 -6 1 121.60 117.87 61.75 o
-5 -5 1 135.07 101.58 46.55 o
-4 -5 1 2990.41 2772.42 122.15 o
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0 -5 1 12.06 19.69 13.43 o
1 -5 1 8481.54 8227.08 440.28 o
2 -5 1 3926.17 4219.96 120.55 o
3 -5 1 2711.16 2786.84 68.17 o
4 -5 1 6417.62 6283.25 145.39 o
5 -5 1 72.78 83.93 10.72 o
6 -5 1 9046.21 8752.80 160.22 o
7 -5 1 855.38 896.10 24.74 o
8 -5 1 3025.37 3242.37 88.16 o
9 -5 1 3127.32 3747.18 193.29 o
-6 -4 1 2122.13 1852.27 269.00 o
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0 -4 1 10514.21 10983.32 119.67 o
1 -4 1 1300.40 1315.24 26.95 o
2 -4 1 11825.85 12232.29 103.56 o
3 -4 1 98.20 98.97 8.99 o
4 -4 1 10610.04 10201.19 180.66 o
5 -4 1 4721.08 4816.55 79.38 o
6 -4 1 2647.14 2683.35 32.63 o
7 -4 1 5306.47 5766.69 195.14 o
8 -4 1 8.39 0.42 22.66 o
9 -4 1 4062.51 4554.08 228.28 o
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-6 -3 1 158.40 178.01 32.26 o
-5 -3 1 4338.61 4298.55 293.85 o
-4 -3 1 1670.36 1658.37 37.79 o
-3 -3 1 2707.04 2605.16 68.88 o
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-1 -3 1 252.16 309.24 10.20 o
0 -3 1 21487.78 22184.75 568.57 o
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2 -3 1 14393.77 14826.98 299.90 o
3 -3 1 17065.52 17090.24 207.11 o
4 -3 1 129.99 153.87 7.18 o
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7 -3 1 2881.78 3005.70 94.58 o
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-1 -2 1 10812.07 11446.40 70.30 o
0 -2 1 3944.19 3959.96 73.24 o
1 -2 1 28182.90 28378.55 570.09 o
2 -2 1 627.52 676.44 8.47 o
3 -2 1 9754.34 9929.75 91.94 o
4 -2 1 5224.41 5456.43 96.62 o
5 -2 1 3582.46 3657.62 53.77 o
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1 -1 1 7526.19 7680.20 170.05 o
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3 -1 1 1650.66 1641.32 22.32 o
4 -1 1 17886.56 17862.93 245.76 o
5 -1 1 530.27 536.85 10.87 o
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6 0 1 235.60 244.27 16.98 o
7 0 1 2848.24 2785.37 94.82 o
8 0 1 683.57 674.26 40.67 o
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-8 1 1 351.81 360.27 24.34 o
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-6 1 1 3279.16 3175.68 125.77 o
-5 1 1 5193.88 5225.87 165.65 o
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-3 1 1 401.97 436.41 18.09 o
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0 1 1 7115.86 6591.74 83.79 o
1 1 1 15827.13 16879.36 254.41 o
2 1 1 1600.21 1575.49 31.65 o
3 1 1 10822.31 10817.20 236.83 o
4 1 1 227.39 241.74 10.32 o
5 1 1 6171.36 6158.71 284.71 o
6 1 1 1671.97 1696.43 74.70 o
7 1 1 1122.29 1140.55 56.11 o
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-8 2 1 2817.91 2744.42 95.17 o
-7 2 1 169.37 160.93 21.23 o
-6 2 1 12916.09 12641.21 281.53 o
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0 2 1 11.22 76.78 12.23 o
1 2 1 22784.65 23877.39 355.00 o
2 2 1 1017.74 1010.29 23.20 o
3 2 1 8658.39 8821.63 257.74 o
4 2 1 5370.14 5351.29 463.48 o
5 2 1 718.45 727.96 67.38 o
6 2 1 6842.42 6844.38 509.05 o
7 2 1 421.41 376.05 38.64 o
-9 3 1 50.51 56.81 22.54 o
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6 3 1 2552.47 2508.60 166.89 o
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4 4 1 473.62 473.41 27.68 o
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1 -9 2 4885.81 4765.40 273.94 o
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6 -9 2 3071.36 3294.85 170.65 o
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