#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219716.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219716_Fobs loop_ _publ_author_name 'Wang, Guo-Ming' 'Li, Zeng-Xin' 'Zheng, Qing-Hua' 'Liu, Hui-Luan' _publ_section_title ; Poly[tetraaqua-\m~4~-bromido-di-\m~2~-bromido-\m~2~-hydroxido-di-\m~3~-isonicotinato-tetra-\m~2~-isonicotinato-tetracopper(I)dithulium(III)] ; _journal_coeditor_code SJ2536 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1260 _journal_page_last m1261 _journal_volume 64 _journal_year 2008 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.1815 _cell_length_b 6.6973 _cell_length_c 34.7044 _exptl_crystal_F_000 3144.00 _reflns_d_resolution_high 0.7967 _[local]_cod_data_source_file sj2536Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in Cmcm' _shelx_refln_list_code 4 _shelx_F_calc_maximum 948.33 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' 'x, -y, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 96261.13 101425.70 2786.58 o 4 0 0 187924.11 190995.63 5245.19 o 6 0 0 3817.67 4015.66 226.92 o 8 0 0 646682.56 573994.00 22300.27 o 10 0 0 365923.25 331356.63 12941.23 o 12 0 0 5.63 1036.96 681.73 o 14 0 0 12497.66 11903.14 434.93 o 16 0 0 29075.37 28246.56 832.09 o 18 0 0 234899.30 218491.86 6323.23 o 20 0 0 75368.91 74352.30 2406.57 o 22 0 0 6106.93 6816.86 779.16 o 24 0 0 20293.24 21536.20 1457.07 o 1 1 0 139196.67 155998.33 3043.91 o 3 1 0 537893.94 574890.44 9890.51 o 5 1 0 63486.63 62057.97 1136.02 o 7 1 0 36877.19 39927.87 705.28 o 9 1 0 44630.45 44072.89 788.83 o 11 1 0 1589.64 1569.10 108.88 o 13 1 0 12134.22 12280.35 309.39 o 15 1 0 27274.94 25498.56 543.17 o 17 1 0 1895.85 1942.43 197.65 o 19 1 0 17446.15 16308.37 708.35 o 21 1 0 5523.65 5166.37 474.31 o 23 1 0 6721.96 7585.38 893.07 o 2 2 0 8840.91 9127.15 235.98 o 4 2 0 583101.88 625752.81 12183.28 o 6 2 0 56328.89 52498.64 908.16 o 8 2 0 326838.34 323651.63 5204.79 o 10 2 0 167836.08 173218.56 2849.42 o 12 2 0 10669.58 10165.27 337.19 o 14 2 0 75793.78 75074.58 1335.89 o 16 2 0 393.31 273.29 118.64 o 18 2 0 93547.16 92093.12 2344.71 o 20 2 0 26731.88 27596.51 1158.05 o 22 2 0 14073.62 13177.60 795.82 o 1 3 0 245448.48 256480.47 4131.28 o 5 3 0 9199.66 9011.12 341.87 o 7 3 0 96848.50 98478.34 1832.61 o 9 3 0 194236.16 192630.33 3473.70 o 11 3 0 40756.27 39362.01 848.65 o 13 3 0 0.35 -80.96 95.63 o 15 3 0 5482.76 5597.31 315.87 o 17 3 0 5971.56 5888.82 408.81 o 19 3 0 30030.99 28100.77 1010.81 o 21 3 0 9176.18 8789.55 678.06 o 0 4 0 235759.83 250591.77 5754.36 o 2 4 0 24330.83 24925.79 495.61 o 4 4 0 340316.38 351754.72 6207.69 o 6 4 0 62034.69 58889.15 1712.98 o 8 4 0 32307.70 30276.71 686.49 o 10 4 0 61328.18 61455.96 1248.62 o 12 4 0 17328.61 16217.04 509.60 o 14 4 0 76370.60 74494.02 1955.11 o 16 4 0 113.86 67.33 145.47 o 18 4 0 38851.72 38653.45 1202.94 o 20 4 0 16184.22 16275.09 700.27 o 1 5 0 78720.15 73047.84 1667.58 o 3 5 0 2.96 33.88 100.36 o 5 5 0 27493.15 27601.82 651.24 o 7 5 0 9315.06 8762.40 417.09 o 9 5 0 53997.02 47396.80 1024.46 o 11 5 0 16909.38 16035.51 479.46 o 13 5 0 3574.03 3091.66 309.96 o 15 5 0 4493.32 4211.82 376.77 o 17 5 0 4947.63 4134.44 435.93 o 19 5 0 21485.83 23576.29 1867.24 o 0 6 0 57261.18 60283.98 1998.61 o 2 6 0 20435.11 19832.29 612.53 o 4 6 0 77054.20 71179.81 1627.79 o 6 6 0 13625.76 11925.52 457.99 o 8 6 0 48061.49 46006.97 1155.40 o 10 6 0 46360.61 42835.63 1143.02 o 12 6 0 902.43 1042.73 225.81 o 14 6 0 31986.69 31336.45 1055.54 o 16 6 0 466.98 396.64 228.57 o 1 7 0 13973.15 13258.88 514.44 o 3 7 0 113.45 477.83 175.66 o 5 7 0 20166.36 19480.44 654.78 o 7 7 0 1605.81 1078.55 206.91 o 9 7 0 14098.90 14182.26 1230.53 o 11 7 0 6201.60 6027.63 594.14 o 13 7 0 2234.63 2611.87 562.77 o 0 8 0 30769.32 29374.19 1269.32 o 2 8 0 4490.40 3859.46 557.10 o 4 8 0 15319.81 14663.85 641.24 o 6 8 0 3622.10 4228.56 428.21 o 1 1 1 2517.03 2843.70 56.56 o 3 1 1 9367.52 9737.55 137.27 o 9 1 1 3038.34 3396.34 100.60 o 11 1 1 1982.16 2226.96 88.59 o 13 1 1 86.57 128.13 69.22 o 15 1 1 1124.40 1386.27 88.88 o 17 1 1 922.56 917.23 93.88 o 19 1 1 3.29 -135.01 102.30 o 21 1 1 131.22 165.15 142.83 o 23 1 1 34.18 97.65 247.06 o 0 2 1 64605.02 72015.99 1306.14 o 2 2 1 61454.20 65067.43 803.96 o 6 2 1 229.70 360.59 36.59 o 8 2 1 31.96 144.60 96.24 o 10 2 1 230.19 218.03 49.47 o 12 2 1 1513.70 1603.88 90.43 o 14 2 1 727.46 804.61 78.95 o 16 2 1 1975.98 2017.54 143.72 o 18 2 1 173.26 243.95 113.37 o 20 2 1 4.63 -33.02 152.28 o 22 2 1 30.62 31.09 183.16 o 1 3 1 28114.64 29981.03 391.55 o 3 3 1 7478.09 7871.90 167.61 o 5 3 1 9538.96 9745.40 199.14 o 7 3 1 34.42 39.78 52.97 o 9 3 1 874.05 1214.60 95.44 o 11 3 1 1456.81 1475.19 102.62 o 13 3 1 1.36 84.04 75.88 o 15 3 1 489.35 547.69 124.85 o 17 3 1 175.25 192.25 109.51 o 19 3 1 1411.15 1548.20 175.88 o 21 3 1 446.87 417.69 199.01 o 0 4 1 28156.89 28280.58 554.94 o 2 4 1 5805.31 5819.52 165.03 o 4 4 1 128.19 460.98 77.30 o 6 4 1 12.52 36.25 59.48 o 8 4 1 2240.16 2327.68 122.74 o 10 4 1 2.78 213.19 77.61 o 12 4 1 46.01 199.84 84.39 o 14 4 1 114.45 103.17 101.28 o 16 4 1 189.25 249.37 116.09 o 18 4 1 171.20 103.62 123.37 o 20 4 1 169.94 266.17 148.62 o 1 5 1 1629.59 1607.11 129.73 o 3 5 1 2028.68 2109.33 119.31 o 5 5 1 154.20 198.08 90.81 o 7 5 1 331.50 361.36 81.15 o 9 5 1 0.15 -15.03 75.56 o 11 5 1 0.80 107.90 82.39 o 13 5 1 2.76 143.43 115.83 o 15 5 1 1583.59 1757.77 189.07 o 17 5 1 940.71 639.20 156.23 o 19 5 1 32.99 66.34 149.36 o 0 6 1 5.40 164.15 216.18 o 2 6 1 155.96 156.50 95.79 o 4 6 1 897.42 962.74 128.10 o 6 6 1 3.97 98.50 95.37 o 8 6 1 46.57 193.71 101.96 o 10 6 1 889.91 864.62 130.63 o 12 6 1 37.23 -91.46 113.41 o 14 6 1 150.21 525.98 155.99 o 16 6 1 50.64 -77.39 139.06 o 1 7 1 40.17 27.76 105.22 o 3 7 1 111.55 128.26 108.70 o 5 7 1 7.74 204.61 121.26 o 7 7 1 46.38 31.33 106.29 o 9 7 1 6.04 184.00 205.71 o 11 7 1 242.74 463.33 191.33 o 13 7 1 2.27 188.64 192.61 o 0 8 1 404.01 457.76 193.10 o 2 8 1 229.93 99.92 125.04 o 4 8 1 434.00 444.91 152.49 o 6 8 1 422.10 424.12 155.41 o 4 0 2 76641.80 77331.66 1267.64 o 6 0 2 261137.97 250365.84 4500.30 o 8 0 2 125277.03 128009.31 2090.16 o 10 0 2 22366.20 21846.22 436.49 o 12 0 2 13570.37 13719.84 320.96 o 14 0 2 137220.28 131892.30 2215.57 o 16 0 2 45895.78 43100.99 827.00 o 18 0 2 9603.03 8940.59 324.28 o 20 0 2 7481.01 7532.46 764.91 o 22 0 2 13312.82 12867.27 1581.74 o 24 0 2 29202.24 29964.82 1806.11 o 3 1 2 4593.85 4657.65 88.06 o 5 1 2 296349.41 298139.59 3367.38 o 7 1 2 14106.53 14356.11 211.25 o 9 1 2 217845.61 213951.33 2453.53 o 11 1 2 133383.92 131953.25 1615.45 o 13 1 2 156567.31 151038.31 1847.70 o 15 1 2 115536.05 110546.26 1339.00 o 17 1 2 21686.55 20520.08 356.67 o 19 1 2 99071.58 98675.68 1783.41 o 21 1 2 1134.50 1147.56 224.21 o 23 1 2 52375.95 55949.69 2041.37 o 2 2 2 785.14 1230.35 73.70 o 4 2 2 24328.53 24718.84 340.39 o 6 2 2 103904.67 106272.83 1243.55 o 8 2 2 548.85 830.50 55.57 o 10 2 2 59360.53 58678.32 736.98 o 12 2 2 58.90 115.99 52.27 o 14 2 2 84831.33 85723.69 1114.79 o 16 2 2 38144.98 38245.76 756.39 o 18 2 2 6994.37 6805.36 379.15 o 20 2 2 6819.54 7225.71 357.09 o 22 2 2 6320.82 6750.15 429.73 o 1 3 2 19701.87 19906.07 278.61 o 3 3 2 99837.64 101996.59 1257.32 o 5 3 2 448259.31 473157.59 5849.21 o 7 3 2 57938.45 56498.88 741.38 o 9 3 2 118018.32 119211.92 1562.09 o 11 3 2 10367.55 10619.49 402.51 o 13 3 2 171492.97 171379.38 2347.07 o 15 3 2 139000.73 138095.67 2198.26 o 17 3 2 6051.33 6166.10 448.34 o 19 3 2 30993.10 30754.90 708.33 o 21 3 2 3095.20 3274.13 272.97 o 0 4 2 16616.28 14209.03 440.61 o 2 4 2 14840.20 14387.84 255.23 o 4 4 2 3412.81 3507.88 141.78 o 6 4 2 34871.71 34458.01 586.38 o 8 4 2 342.14 596.57 95.31 o 10 4 2 44233.83 42312.92 648.17 o 12 4 2 185.66 335.83 88.02 o 14 4 2 30662.20 30039.28 621.57 o 16 4 2 2569.28 3003.61 215.61 o 18 4 2 8111.52 8024.91 351.83 o 20 4 2 11296.37 11138.28 418.14 o 1 5 2 30526.18 29730.53 546.11 o 3 5 2 33248.47 30409.32 489.33 o 5 5 2 170615.88 165106.16 2260.56 o 7 5 2 19961.67 17068.53 335.26 o 9 5 2 63624.86 60474.43 887.65 o 11 5 2 2474.20 2639.12 171.92 o 13 5 2 69517.11 66837.77 1183.95 o 15 5 2 48521.48 45703.65 961.40 o 17 5 2 4828.74 5014.99 292.99 o 19 5 2 16634.56 16835.88 520.32 o 0 6 2 2623.92 2243.60 229.71 o 2 6 2 0.94 -32.90 83.99 o 4 6 2 26300.10 25706.58 523.53 o 6 6 2 33620.53 33504.50 636.30 o 8 6 2 2831.67 2578.81 172.30 o 10 6 2 10119.86 9999.56 393.99 o 12 6 2 1891.31 1932.24 213.78 o 14 6 2 25766.78 26373.23 999.38 o 16 6 2 4999.31 4916.50 367.43 o 1 7 2 19682.13 19235.73 451.32 o 3 7 2 3825.56 3738.11 245.56 o 5 7 2 34653.94 31823.93 641.70 o 7 7 2 16.61 53.94 115.92 o 9 7 2 33706.94 31914.45 766.27 o 11 7 2 5534.82 5444.63 406.35 o 13 7 2 12316.86 13613.50 630.17 o 0 8 2 8302.55 8859.06 487.76 o 2 8 2 53.57 126.39 120.54 o 4 8 2 12035.62 12859.72 464.36 o 6 8 2 9015.63 8646.22 407.03 o 1 1 3 24212.17 26543.06 320.80 o 3 1 3 9297.51 9898.42 141.26 o 9 1 3 823.56 913.37 59.70 o 11 1 3 306.33 307.10 47.64 o 13 1 3 2154.81 2214.84 97.33 o 15 1 3 3121.96 3134.37 155.10 o 17 1 3 2526.00 2331.53 138.86 o 19 1 3 137.65 306.28 179.26 o 21 1 3 1305.20 1458.53 247.66 o 23 1 3 2.16 397.11 209.93 o 0 2 3 1621.77 1462.98 97.08 o 2 2 3 60177.90 63850.54 755.96 o 4 2 3 3968.30 4272.32 89.53 o 6 2 3 31004.76 33768.99 432.67 o 8 2 3 4486.92 4750.73 143.24 o 10 2 3 7590.99 8034.89 232.39 o 12 2 3 8238.48 8374.91 206.11 o 14 2 3 4698.28 4771.65 166.90 o 16 2 3 206.54 227.33 84.30 o 18 2 3 2330.34 2414.65 196.42 o 20 2 3 987.58 933.73 176.97 o 22 2 3 604.64 313.06 234.97 o 1 3 3 1432.12 1743.72 75.45 o 3 3 3 2481.58 2812.88 91.28 o 5 3 3 10703.48 10801.98 213.84 o 7 3 3 30.43 73.13 41.82 o 9 3 3 4677.89 5930.57 227.40 o 11 3 3 313.51 361.92 72.15 o 13 3 3 2970.59 2997.92 213.11 o 15 3 3 11.09 -75.38 82.16 o 17 3 3 143.10 121.17 102.25 o 19 3 3 516.80 530.94 163.39 o 21 3 3 164.69 497.09 168.04 o 0 4 3 383.41 152.21 74.36 o 2 4 3 4280.29 4361.60 128.66 o 4 4 3 3599.05 3838.66 163.28 o 6 4 3 71.60 144.51 61.28 o 8 4 3 493.65 558.54 79.80 o 10 4 3 23.30 183.25 76.79 o 12 4 3 161.02 154.06 82.30 o 14 4 3 16.55 16.07 90.21 o 16 4 3 63.67 28.61 107.15 o 18 4 3 379.91 498.33 151.50 o 20 4 3 210.38 317.76 174.72 o 1 5 3 131.89 185.76 80.95 o 3 5 3 1310.02 1264.29 100.82 o 5 5 3 702.68 697.53 95.59 o 7 5 3 1280.12 1521.34 120.07 o 9 5 3 1076.51 1188.76 112.79 o 11 5 3 730.80 547.33 108.26 o 13 5 3 177.20 320.10 118.01 o 15 5 3 511.10 560.17 146.76 o 17 5 3 98.42 77.06 130.49 o 19 5 3 49.75 95.60 168.11 o 0 6 3 46.54 -42.92 131.53 o 2 6 3 0.72 -69.95 83.45 o 4 6 3 1425.45 1335.46 138.33 o 6 6 3 2484.09 2104.98 161.94 o 8 6 3 337.61 374.67 96.74 o 10 6 3 9.66 91.83 104.94 o 12 6 3 51.23 127.00 112.85 o 14 6 3 883.26 973.00 167.94 o 16 6 3 105.95 115.13 142.08 o 1 7 3 113.70 105.78 109.02 o 3 7 3 32.97 -49.13 102.37 o 5 7 3 88.86 410.12 124.18 o 7 7 3 158.25 69.84 128.52 o 9 7 3 645.26 713.05 169.90 o 11 7 3 75.99 406.68 196.35 o 13 7 3 1.38 67.67 190.23 o 0 8 3 454.93 750.56 220.93 o 2 8 3 1.18 14.75 122.90 o 4 8 3 30.89 -67.84 133.82 o 6 8 3 864.10 736.34 179.18 o 2 0 4 202261.39 204519.20 3273.66 o 4 0 4 425930.19 408373.38 12561.52 o 6 0 4 3866.68 3832.02 155.08 o 8 0 4 513609.72 472477.50 10692.29 o 10 0 4 354573.59 333544.66 5350.58 o 12 0 4 89.64 84.55 58.56 o 14 0 4 60126.72 58458.01 1160.76 o 16 0 4 17.87 118.10 91.26 o 18 0 4 112081.27 107723.91 2333.02 o 20 0 4 55727.06 54636.89 1543.36 o 22 0 4 3733.17 3755.08 476.17 o 1 1 4 191995.47 215190.63 2541.36 o 5 1 4 65246.07 64309.21 762.65 o 7 1 4 7117.76 8005.36 137.96 o 9 1 4 13461.60 11464.64 189.47 o 11 1 4 7143.60 7266.43 148.14 o 13 1 4 467.86 524.02 68.13 o 15 1 4 6084.42 6041.27 174.02 o 17 1 4 771.39 921.67 119.74 o 19 1 4 39983.74 37679.91 740.26 o 21 1 4 10047.08 9881.61 477.60 o 23 1 4 6463.35 6054.83 569.89 o 0 2 4 299363.84 329209.44 5259.09 o 2 2 4 26352.92 27011.64 347.61 o 4 2 4 375818.59 396197.59 4472.43 o 6 2 4 28501.02 27875.35 367.94 o 8 2 4 323153.88 328503.28 3735.85 o 10 2 4 176832.39 181927.25 2111.84 o 12 2 4 2023.72 1610.96 87.97 o 14 2 4 92168.06 90686.77 1248.78 o 16 2 4 9710.69 9440.70 266.64 o 18 2 4 64090.75 63182.53 1214.48 o 20 2 4 30165.03 31281.67 1752.24 o 22 2 4 6776.42 6809.64 622.30 o 1 3 4 176981.73 181785.70 2185.13 o 3 3 4 1271.71 1455.70 70.70 o 5 3 4 16302.22 16462.49 263.51 o 7 3 4 19761.36 18317.59 307.35 o 9 3 4 69428.03 65360.69 991.52 o 11 3 4 29573.90 28488.99 465.96 o 13 3 4 741.51 723.28 103.55 o 15 3 4 3959.64 4048.29 197.97 o 17 3 4 5712.51 5349.57 307.35 o 19 3 4 36693.20 35171.38 881.92 o 21 3 4 9761.03 9860.74 447.80 o 0 4 4 244824.30 255517.14 4553.88 o 2 4 4 1018.45 1272.10 78.04 o 4 4 4 124784.77 123801.14 1615.16 o 6 4 4 49431.20 46839.70 991.74 o 8 4 4 56030.31 54662.40 789.33 o 10 4 4 85724.92 84368.77 1165.64 o 12 4 4 3084.84 3123.84 174.79 o 14 4 4 68182.98 67357.27 1109.11 o 16 4 4 2928.33 2998.10 204.65 o 18 4 4 34148.86 33374.95 767.43 o 20 4 4 23001.56 22699.82 911.32 o 1 5 4 45569.64 43381.48 737.24 o 3 5 4 1612.56 1927.03 141.76 o 5 5 4 11238.54 10833.00 354.54 o 7 5 4 87.11 69.13 68.74 o 9 5 4 31910.47 29515.99 503.00 o 11 5 4 14489.66 13669.20 443.04 o 13 5 4 2730.10 2450.99 189.96 o 15 5 4 8227.10 7755.85 373.81 o 17 5 4 1524.35 1359.65 201.55 o 19 5 4 18237.75 18912.62 556.51 o 0 6 4 116827.10 115949.43 2489.46 o 2 6 4 8397.68 8806.23 286.55 o 4 6 4 25083.28 23548.83 621.01 o 6 6 4 11682.39 10623.71 317.78 o 8 6 4 36963.15 36790.89 739.39 o 10 6 4 59468.64 57205.13 988.56 o 12 6 4 11.88 154.69 113.28 o 14 6 4 22883.08 21963.57 934.58 o 16 6 4 200.92 262.56 154.80 o 1 7 4 7312.29 7583.29 296.78 o 3 7 4 2479.92 2019.76 223.87 o 5 7 4 7488.65 8311.84 313.36 o 7 7 4 279.10 389.13 148.45 o 9 7 4 12446.52 11795.06 529.88 o 11 7 4 7159.66 7144.99 460.79 o 13 7 4 3462.57 3764.23 356.64 o 0 8 4 40183.46 36213.53 1163.73 o 2 8 4 3731.96 3903.65 243.74 o 4 8 4 10048.31 10856.07 420.06 o 6 8 4 3838.46 4071.15 300.25 o 1 1 5 33083.30 35502.62 426.94 o 3 1 5 40671.79 42965.65 515.60 o 5 1 5 4839.06 5123.53 110.29 o 9 1 5 26095.17 27513.83 371.82 o 11 1 5 3137.74 3036.65 103.73 o 13 1 5 13231.37 12982.48 238.86 o 15 1 5 408.35 550.60 80.35 o 17 1 5 3915.09 3938.06 175.26 o 19 1 5 1372.69 1381.68 138.73 o 21 1 5 390.89 592.69 148.42 o 23 1 5 759.93 1289.06 289.95 o 0 2 5 109330.73 120168.83 1960.41 o 2 2 5 13857.03 13465.86 195.87 o 4 2 5 16450.72 15538.99 222.41 o 6 2 5 12226.77 12718.81 196.75 o 8 2 5 8602.80 8410.94 272.23 o 10 2 5 16165.09 16639.97 262.61 o 12 2 5 1097.34 1092.80 81.51 o 14 2 5 5445.61 5699.74 189.67 o 16 2 5 6482.70 6267.31 231.41 o 18 2 5 1598.12 1664.35 171.32 o 20 2 5 1054.99 901.75 159.23 o 22 2 5 51.48 370.83 390.45 o 1 3 5 24484.53 25433.04 345.19 o 3 3 5 6792.96 6862.91 143.00 o 5 3 5 3970.70 4052.89 139.04 o 7 3 5 779.42 1159.38 63.70 o 9 3 5 4731.88 5265.13 199.42 o 11 3 5 975.39 1099.97 99.31 o 13 3 5 5374.82 6028.74 225.68 o 15 3 5 158.18 230.05 103.90 o 17 3 5 2954.14 3134.07 198.61 o 19 3 5 1024.08 731.31 210.80 o 21 3 5 476.38 569.26 196.49 o 0 4 5 519.71 558.93 87.55 o 2 4 5 4.23 -27.88 47.72 o 4 4 5 3.14 -31.74 56.31 o 6 4 5 4.72 24.19 57.11 o 8 4 5 1644.93 1763.84 118.93 o 10 4 5 25.98 144.32 81.47 o 12 4 5 639.89 662.22 130.58 o 14 4 5 225.26 328.20 105.88 o 16 4 5 1101.56 1124.68 150.68 o 18 4 5 34.50 246.17 145.59 o 20 4 5 7.07 275.35 169.80 o 1 5 5 2603.64 2410.92 150.80 o 3 5 5 328.73 279.27 110.64 o 5 5 5 4451.72 4266.04 168.84 o 7 5 5 2258.43 2269.76 132.22 o 9 5 5 2892.90 3019.75 175.13 o 11 5 5 1222.89 1138.38 128.24 o 13 5 5 238.42 381.20 109.99 o 15 5 5 1942.72 2141.62 188.05 o 17 5 5 479.93 586.69 150.71 o 19 5 5 3.98 37.74 150.72 o 0 6 5 1034.41 976.31 237.24 o 2 6 5 217.10 286.64 100.16 o 4 6 5 39.19 29.04 96.39 o 6 6 5 158.40 160.42 98.14 o 8 6 5 2483.22 2060.39 176.11 o 10 6 5 598.45 675.27 126.23 o 12 6 5 826.24 771.25 130.22 o 14 6 5 15.88 135.56 131.65 o 16 6 5 527.62 418.27 158.09 o 1 7 5 1.28 -51.93 104.29 o 3 7 5 412.00 316.60 113.59 o 5 7 5 322.76 392.18 137.27 o 7 7 5 989.70 714.73 156.11 o 9 7 5 1127.78 826.43 173.80 o 11 7 5 14.16 59.13 153.01 o 13 7 5 8.93 297.96 194.54 o 0 8 5 276.15 651.68 213.18 o 2 8 5 65.07 -36.38 119.24 o 4 8 5 4.74 187.32 137.08 o 6 8 5 26.38 49.08 153.93 o 0 0 6 217.40 315.80 100.74 o 2 0 6 4980.63 4675.26 136.85 o 4 0 6 119594.57 116853.77 1897.97 o 6 0 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181.19 o 0 6 25 90.70 242.78 320.88 o 2 6 25 1457.16 1395.47 281.05 o 4 6 25 2691.86 2614.88 278.66 o 6 6 25 1542.15 1790.31 250.36 o 8 6 25 570.37 249.94 168.76 o 0 0 26 14978.97 13955.22 535.10 o 2 0 26 1847.19 2228.63 181.31 o 4 0 26 4647.98 4996.99 478.88 o 6 0 26 78706.33 75802.73 1739.70 o 8 0 26 20053.37 20450.26 647.72 o 10 0 26 33645.21 31195.11 884.58 o 12 0 26 555.92 544.21 163.29 o 14 0 26 53239.36 52254.43 1358.79 o 16 0 26 14110.39 13879.17 592.89 o 18 0 26 11578.61 12913.45 622.49 o 1 1 26 31080.92 30964.10 487.46 o 3 1 26 27928.61 27345.13 475.08 o 5 1 26 103104.38 99243.30 1548.33 o 7 1 26 31516.76 30589.54 603.41 o 9 1 26 95097.05 92408.38 1479.30 o 11 1 26 33231.12 31955.91 644.92 o 13 1 26 75104.84 73261.07 1245.35 o 15 1 26 84168.56 83528.55 1410.96 o 17 1 26 4441.66 4900.00 278.06 o 19 1 26 42692.10 44110.09 961.28 o 0 2 26 2603.24 2731.07 325.32 o 2 2 26 17.73 135.08 78.15 o 4 2 26 9475.37 9381.83 249.16 o 6 2 26 41035.59 39309.60 722.05 o 8 2 26 636.98 737.50 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372.71 o 2 4 27 8.46 127.00 102.23 o 4 4 27 4281.73 4107.74 229.28 o 6 4 27 113.01 -15.06 101.89 o 8 4 27 666.12 610.09 143.36 o 10 4 27 2312.45 2433.73 231.89 o 12 4 27 11.26 -23.65 144.47 o 14 4 27 783.54 771.51 206.00 o 1 5 27 612.13 501.10 228.63 o 3 5 27 1352.09 1797.77 249.37 o 5 5 27 1151.93 1329.60 181.94 o 7 5 27 864.40 1038.94 220.69 o 9 5 27 658.54 813.80 196.74 o 11 5 27 276.11 444.90 165.08 o 0 6 27 850.04 1256.65 418.90 o 2 6 27 1600.47 1954.53 321.67 o 4 6 27 88.28 204.77 295.36 o 6 6 27 469.44 81.58 185.16 o 0 0 28 399310.47 417593.59 9590.55 o 2 0 28 14675.09 15500.40 525.83 o 4 0 28 81881.27 83224.05 1884.23 o 6 0 28 68777.19 65118.46 1547.77 o 8 0 28 98080.37 96493.27 2181.97 o 10 0 28 83786.46 80297.04 1885.14 o 12 0 28 11674.80 11484.36 522.93 o 14 0 28 28072.32 28077.50 881.40 o 16 0 28 586.50 447.75 191.18 o 18 0 28 38594.95 36496.05 1113.39 o 1 1 28 44695.95 43777.49 686.15 o 3 1 28 1209.87 1386.74 123.45 o 5 1 28 24864.63 24848.75 519.21 o 7 1 28 9249.48 9000.57 308.96 o 9 1 28 86593.46 82969.60 1363.75 o 11 1 28 10874.49 10579.89 352.13 o 13 1 28 3518.63 3705.77 234.41 o 15 1 28 4114.20 4172.88 298.19 o 17 1 28 258.34 150.18 137.76 o 0 2 28 207631.45 211241.17 4402.89 o 2 2 28 19277.93 18338.37 443.67 o 4 2 28 92235.90 87494.44 1313.95 o 6 2 28 43861.52 42251.12 776.04 o 8 2 28 82965.21 83024.41 1359.17 o 10 2 28 68240.04 67333.56 1155.53 o 12 2 28 4473.51 4672.46 255.28 o 14 2 28 27347.63 27374.46 660.03 o 16 2 28 46.76 244.83 145.55 o 1 3 28 39675.07 38329.99 732.29 o 3 3 28 1255.46 1181.58 136.86 o 5 3 28 18197.94 18317.42 517.13 o 7 3 28 5131.71 5551.65 273.97 o 9 3 28 49528.86 47140.83 935.91 o 11 3 28 10205.55 10116.83 388.71 o 13 3 28 2077.54 2314.81 239.88 o 15 3 28 7558.96 8978.98 442.41 o 0 4 28 103426.58 97645.48 2902.10 o 2 4 28 15063.62 14967.11 441.30 o 4 4 28 63941.03 63752.84 1170.69 o 6 4 28 13161.02 12841.67 407.21 o 8 4 28 22496.85 22296.47 1048.14 o 10 4 28 44237.28 45762.80 1019.57 o 12 4 28 970.20 869.86 199.10 o 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552.71 o 12 4 30 152.64 151.49 160.85 o 1 5 30 27592.19 27961.12 825.43 o 3 5 30 24190.47 23118.09 741.37 o 5 5 30 39477.03 37208.32 1004.51 o 7 5 30 1259.60 1156.14 195.87 o 9 5 30 34935.46 35276.67 1075.11 o 0 6 30 14457.15 14150.51 1008.80 o 2 6 30 932.64 1099.04 299.54 o 1 1 31 2545.96 3070.43 196.27 o 3 1 31 6962.00 7044.85 320.16 o 5 1 31 20.20 601.21 116.26 o 7 1 31 3725.93 3230.78 207.83 o 9 1 31 594.88 658.07 130.73 o 11 1 31 1356.10 1078.45 156.48 o 13 1 31 498.93 613.10 146.41 o 15 1 31 905.21 822.22 159.91 o 0 2 31 5118.33 5258.45 440.73 o 2 2 31 126.76 148.43 95.03 o 4 2 31 1841.78 1984.22 191.42 o 6 2 31 2390.22 2270.46 177.74 o 8 2 31 1369.81 1590.44 176.74 o 10 2 31 1286.76 1575.08 171.40 o 12 2 31 852.48 900.90 165.51 o 14 2 31 113.18 392.60 153.35 o 1 3 31 1701.99 1882.28 172.09 o 3 3 31 2670.88 2877.33 201.50 o 5 3 31 13.86 297.80 122.85 o 7 3 31 3489.42 3534.26 294.16 o 9 3 31 727.44 964.04 205.47 o 11 3 31 3109.22 3243.29 244.18 o 13 3 31 2.92 0.54 155.35 o 0 4 31 232.29 225.86 171.37 o 2 4 31 355.16 175.95 140.78 o 4 4 31 6.45 207.24 136.07 o 6 4 31 145.26 161.58 155.78 o 8 4 31 143.33 65.04 162.92 o 10 4 31 258.45 302.57 160.84 o 12 4 31 34.21 266.72 163.55 o 1 5 31 2.13 140.04 183.34 o 3 5 31 12.55 217.69 191.86 o 5 5 31 1208.85 1233.84 242.21 o 7 5 31 22.20 39.89 163.30 o 9 5 31 30.64 351.36 189.02 o 0 0 32 299237.66 313018.09 9040.67 o 2 0 32 20911.09 21726.44 792.24 o 4 0 32 66633.89 67610.38 1609.40 o 6 0 32 734.75 579.52 174.48 o 8 0 32 158383.11 152389.70 3316.16 o 10 0 32 115835.45 109708.63 2503.79 o 12 0 32 260.17 503.75 197.52 o 14 0 32 17850.21 17847.64 691.65 o 16 0 32 57.90 0.81 203.17 o 1 1 32 46420.05 45874.49 888.94 o 3 1 32 13628.70 14631.07 482.63 o 5 1 32 45257.18 43359.77 806.08 o 7 1 32 1684.51 1679.49 166.00 o 9 1 32 19842.36 19481.95 481.64 o 11 1 32 1208.11 1346.25 166.57 o 13 1 32 4824.53 4750.87 296.53 o 15 1 32 3311.25 3488.94 255.52 o 0 2 32 159070.72 170330.20 3992.67 o 2 2 32 8000.67 7900.09 360.60 o 4 2 32 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o 7 1 35 38.08 -29.26 113.46 o 9 1 35 548.02 656.82 145.59 o 11 1 35 319.05 489.47 147.07 o 13 1 35 68.60 263.94 145.36 o 0 2 35 17.26 832.12 218.81 o 2 2 35 616.80 506.48 154.94 o 4 2 35 96.94 542.23 151.18 o 6 2 35 1031.09 965.61 165.33 o 8 2 35 11.86 284.53 137.32 o 10 2 35 174.53 362.70 137.03 o 12 2 35 1528.04 1802.79 210.48 o 1 3 35 1068.39 1273.70 179.04 o 3 3 35 153.72 110.95 143.77 o 5 3 35 823.51 1210.89 190.00 o 7 3 35 1264.92 1241.05 196.60 o 9 3 35 158.63 324.30 166.22 o 11 3 35 1742.17 1488.99 221.00 o 0 4 35 59.38 291.65 242.01 o 2 4 35 178.67 206.09 162.46 o 4 4 35 178.51 484.61 189.89 o 6 4 35 387.89 829.01 258.93 o 8 4 35 118.36 100.24 174.79 o 0 0 36 282665.31 270158.47 11441.83 o 2 0 36 33518.55 32318.21 2993.65 o 4 0 36 79431.30 78655.46 2172.14 o 6 0 36 529.61 385.35 184.88 o 8 0 36 88010.15 86498.42 2059.47 o 10 0 36 77788.90 74301.40 1846.10 o 12 0 36 682.53 700.35 236.65 o 1 1 36 35686.91 35213.41 991.21 o 3 1 36 32218.96 28285.25 780.24 o 5 1 36 33794.78 34993.59 764.86 o 7 1 36 4596.57 4842.67 267.49 o 9 1 36 21510.90 20491.81 649.74 o 11 1 36 2339.26 2553.06 218.69 o 13 1 36 4955.27 4658.95 333.36 o 0 2 36 159376.97 155702.02 3932.16 o 2 2 36 11329.42 11092.97 439.76 o 4 2 36 89140.54 87046.77 1689.89 o 6 2 36 13016.71 12037.23 576.68 o 8 2 36 39304.08 38110.38 840.89 o 10 2 36 28273.44 30136.10 674.99 o 12 2 36 1000.48 972.12 200.35 o 1 3 36 51576.15 50289.08 1343.29 o 3 3 36 1095.73 1325.79 196.73 o 5 3 36 10568.46 10678.68 454.67 o 7 3 36 9185.26 8261.74 452.52 o 9 3 36 32614.73 29442.93 781.37 o 0 4 36 63932.68 63966.58 1918.83 o 2 4 36 205.30 573.14 169.94 o 4 4 36 42452.00 43364.50 1121.87 o 6 4 36 14975.10 14795.68 687.42 o 1 1 37 691.50 1640.73 245.28 o 3 1 37 213.37 455.23 201.61 o 5 1 37 164.16 603.06 145.79 o 7 1 37 71.35 144.38 134.86 o 9 1 37 91.78 325.20 142.32 o 11 1 37 114.52 363.49 145.48 o 0 2 37 417.27 1126.96 300.29 o 2 2 37 5.57 283.51 157.29 o 4 2 37 3876.10 4200.45 291.33 o 6 2 37 116.91 75.46 132.91 o 8 2 37 2236.57 2042.55 235.74 o 10 2 37 787.41 734.53 167.21 o 1 3 37 2.40 363.17 163.87 o 3 3 37 592.41 567.07 202.90 o 5 3 37 1803.50 2196.78 235.72 o 7 3 37 416.42 421.89 191.15 o 9 3 37 1292.09 1322.27 215.54 o 0 4 37 371.57 688.52 283.23 o 2 4 37 13.91 -216.73 165.03 o 4 4 37 684.84 921.10 212.47 o 0 0 38 171.80 353.28 401.83 o 2 0 38 1921.46 1459.69 497.12 o 4 0 38 30358.41 29384.65 1049.41 o 6 0 38 36893.94 36686.82 1561.97 o 8 0 38 1294.23 1251.50 253.88 o 10 0 38 17700.42 17145.05 696.91 o 1 1 38 33017.95 31223.14 1054.68 o 3 1 38 4083.57 3973.86 306.79 o 5 1 38 45203.91 44531.57 999.68 o 7 1 38 5651.90 6069.65 326.23 o 9 1 38 61364.19 60933.24 1250.95 o 11 1 38 10790.63 10625.41 450.37 o 0 2 38 2430.00 2498.22 637.77 o 2 2 38 691.32 564.21 177.03 o 4 2 38 14159.15 14550.78 506.13 o 6 2 38 32366.73 32741.21 826.96 o 8 2 38 416.61 483.59 161.88 o 10 2 38 13097.66 14586.88 534.67 o 1 3 38 8640.79 8539.90 581.16 o 3 3 38 10558.70 11031.35 464.97 o 5 3 38 74027.41 74543.83 2759.36 o 7 3 38 6947.01 6213.85 421.98 o 0 4 38 11802.42 13010.74 918.14 o 2 4 38 1314.06 1301.98 236.85 o 1 1 39 143.39 877.50 224.39 o 3 1 39 926.27 1022.98 203.42 o 5 1 39 1032.10 1181.99 310.80 o 7 1 39 717.67 797.57 167.89 o 9 1 39 173.34 444.48 166.84 o 0 2 39 2482.58 3301.10 456.79 o 2 2 39 1267.09 1389.37 216.36 o 4 2 39 572.10 988.15 196.66 o 6 2 39 1723.93 1898.34 261.57 o 8 2 39 802.88 617.41 170.82 o 1 3 39 349.78 423.12 179.65 o 3 3 39 1214.14 1230.72 203.51 o 5 3 39 141.92 562.59 331.75 o 0 0 40 182738.19 181927.50 8022.51 o 2 0 40 5249.16 6550.19 2039.46 o 4 0 40 58678.84 58803.49 2199.29 o 6 0 40 1755.59 2287.55 338.99 o 8 0 40 54382.37 55352.58 1724.68 o 1 1 40 41607.89 40958.75 1512.83 o 3 1 40 14992.29 14081.52 634.37 o 5 1 40 20048.62 20735.14 669.38 o 7 1 40 3213.27 3510.68 268.63 o 9 1 40 20208.02 20196.27 716.77 o 0 2 40 105169.45 105823.63 3812.23 o 2 2 40 5267.39 5778.75 427.82 o 4 2 40 58728.29 59131.45 1385.92 o 6 2 40 7756.70 8510.62 663.28 o 1 3 40 31607.36 31571.47 1132.66 o 3 3 40 2297.47 2830.87 287.13 o 1 1 41 1382.32 1815.66 266.42 o 3 1 41 1115.38 1048.65 238.97 o 5 1 41 650.62 920.66 208.08 o 7 1 41 538.97 640.74 186.86 o 0 2 41 453.98 1402.89 464.88 o 2 2 41 4947.78 5025.93 409.81 o 4 2 41 1157.58 1276.42 224.82 o 0 0 42 10554.48 11399.33 1165.42 o 2 0 42 791.26 1164.50 361.28 o 4 0 42 7439.39 7143.26 1099.71 o 6 0 42 25999.92 26922.02 1573.70 o 1 1 42 16671.97 16886.77 1121.62 o 3 1 42 7230.99 6790.17 476.16 o 5 1 42 42643.93 43901.79 1127.20 o 0 2 42 5547.12 6036.87 1129.12 o 2 2 42 194.72 364.82 284.63 o 1 1 43 884.13 1687.51 266.20 o