#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219752.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219752_Fobs loop_ _publ_author_name 'Xia, Hai-Tao' 'Liu, Yu-Fen' 'Chen, Liang' 'Wang, Da-Qi' _publ_section_title ; Tetrakis(\m-naphthalene-1-acetato-1:2\k^2^O:O')bis(naphthalene-1-acetato)-1\k^2^O,O';2\k^2^O,O'-bis(1,10-phenanthroline)-1\k^2^N,N';2\k^2^N,N'-europium(III)samarium(III) ; _journal_coeditor_code AT2644 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1419 _journal_page_last m1420 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.333 _cell_angle_beta 74.517 _cell_angle_gamma 66.768 _cell_length_a 11.9803 _cell_length_b 12.4116 _cell_length_c 15.0408 _exptl_crystal_F_000 895.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file at2644Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070803d in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 225.68 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20846.12 22912.08 539.34 o 2 0 0 6704.16 6608.16 126.93 o 3 0 0 1259.48 1143.44 45.87 o 4 0 0 1181.85 1104.94 47.85 o 5 0 0 4436.12 4390.41 118.00 o 6 0 0 6896.39 6726.95 167.43 o 7 0 0 1607.41 1586.70 105.91 o 8 0 0 2080.09 2373.04 139.53 o 9 0 0 6.67 -4.12 39.92 o 10 0 0 1.31 -59.05 44.25 o 11 0 0 164.59 173.25 72.66 o 12 0 0 534.56 595.68 111.95 o -12 1 0 120.29 52.43 70.57 o -11 1 0 913.99 1111.05 140.99 o -10 1 0 601.10 821.42 111.54 o -9 1 0 976.06 1088.12 107.99 o -8 1 0 244.91 196.86 61.19 o -7 1 0 525.13 560.56 76.04 o -6 1 0 2201.84 2087.94 115.76 o -5 1 0 2440.42 2187.86 108.36 o -4 1 0 8252.71 8283.34 247.99 o -3 1 0 1729.82 1527.23 74.84 o -2 1 0 783.28 976.01 51.08 o -1 1 0 7723.55 7545.04 127.81 o 1 1 0 20517.44 21448.38 360.16 o 2 1 0 1969.86 2031.81 40.29 o 3 1 0 360.84 287.44 19.80 o 4 1 0 1669.38 1580.69 44.15 o 5 1 0 463.93 408.07 30.18 o 6 1 0 792.38 562.41 47.21 o 7 1 0 2677.56 2607.08 98.17 o 8 1 0 1972.64 2174.95 111.46 o 9 1 0 1425.20 1352.82 79.20 o 10 1 0 342.86 311.32 74.74 o 11 1 0 144.73 70.94 65.83 o 12 1 0 12.69 -51.49 57.59 o 13 1 0 128.29 134.78 80.06 o -12 2 0 0.58 -62.75 58.53 o -11 2 0 66.82 -36.80 52.64 o -10 2 0 538.02 506.20 96.42 o -9 2 0 1185.89 1396.31 123.89 o -8 2 0 1886.78 2115.20 142.08 o -7 2 0 2187.31 1900.41 124.98 o -6 2 0 360.67 271.08 58.69 o -5 2 0 327.01 159.70 40.34 o -4 2 0 4649.22 4376.45 161.52 o -3 2 0 12639.87 13105.26 352.91 o -2 2 0 19855.81 22131.73 358.36 o -1 2 0 11266.41 12506.39 206.34 o 0 2 0 14.91 12.14 9.43 o 1 2 0 249.35 219.17 24.34 o 2 2 0 11.36 -3.32 7.92 o 3 2 0 44.31 59.03 12.34 o 4 2 0 2333.26 2060.10 74.68 o 5 2 0 4959.85 4889.48 97.59 o 6 2 0 3268.19 3436.09 83.17 o 7 2 0 292.00 312.30 34.88 o 8 2 0 256.49 288.16 65.91 o 9 2 0 798.19 857.13 64.45 o 10 2 0 752.77 873.76 73.36 o 11 2 0 556.22 769.51 80.56 o 12 2 0 217.55 258.31 80.00 o 13 2 0 24.46 -24.39 55.40 o -11 3 0 82.64 -0.52 64.32 o -10 3 0 3.31 -68.41 45.61 o -9 3 0 329.65 333.83 86.21 o -8 3 0 1001.67 1199.45 111.17 o -7 3 0 2453.29 2535.19 149.53 o -6 3 0 3249.51 3279.47 163.61 o -5 3 0 3443.86 3402.58 154.33 o -4 3 0 370.39 357.81 54.31 o -3 3 0 1768.18 2209.64 104.08 o -2 3 0 4229.57 4951.82 106.16 o -1 3 0 8378.99 8547.34 255.44 o 1 3 0 1140.73 1184.36 85.71 o 2 3 0 4940.27 4736.88 97.31 o 3 3 0 587.86 612.51 24.81 o 4 3 0 434.03 467.25 25.04 o 5 3 0 2023.48 1866.18 59.94 o 6 3 0 2645.08 2835.39 73.34 o 7 3 0 5528.36 5547.92 119.30 o 8 3 0 1365.57 1329.05 57.71 o 9 3 0 160.46 120.30 31.03 o 10 3 0 18.16 -14.21 31.09 o 11 3 0 337.24 272.81 58.59 o 12 3 0 355.41 527.04 72.43 o 13 3 0 295.92 457.00 96.58 o -10 4 0 471.56 545.96 107.89 o -9 4 0 397.72 336.02 91.26 o -8 4 0 268.25 303.03 80.27 o -7 4 0 56.97 -3.70 46.70 o -6 4 0 960.90 785.51 82.92 o -5 4 0 3512.13 3295.42 157.30 o -4 4 0 7801.23 8234.35 269.51 o -3 4 0 6638.57 6831.73 224.48 o -2 4 0 5314.28 5597.32 183.31 o -1 4 0 1866.94 1835.02 53.37 o 0 4 0 787.52 674.40 24.42 o 1 4 0 1300.15 1366.63 41.64 o 2 4 0 6269.75 5817.46 116.27 o 3 4 0 9427.26 9499.95 182.15 o 4 4 0 6369.83 6653.39 115.96 o 5 4 0 842.99 761.43 33.67 o 6 4 0 61.63 35.91 17.19 o 7 4 0 1695.53 1582.43 56.88 o 8 4 0 2684.80 2583.00 79.71 o 9 4 0 1158.71 1384.64 62.28 o 10 4 0 621.75 665.86 107.20 o 11 4 0 73.07 14.69 37.77 o 12 4 0 0.04 -32.55 36.03 o 13 4 0 127.05 174.48 57.30 o -10 5 0 235.86 231.68 82.92 o -9 5 0 527.17 578.64 106.79 o -8 5 0 1099.33 1069.56 117.06 o -7 5 0 1926.34 1860.80 140.00 o -6 5 0 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540.89 33.36 o 5 6 0 3227.90 3111.96 75.53 o 6 6 0 3685.63 3706.81 141.04 o 7 6 0 1854.45 1868.31 61.63 o 8 6 0 75.60 48.99 24.95 o 9 6 0 178.87 79.33 28.35 o 10 6 0 8.77 -27.75 37.73 o 11 6 0 238.23 306.73 82.35 o 12 6 0 330.90 425.72 96.01 o 13 6 0 226.19 318.56 93.56 o -8 7 0 110.99 2.66 61.61 o -7 7 0 64.09 106.79 67.97 o -6 7 0 1323.03 1489.18 126.34 o -5 7 0 2801.53 2842.23 165.17 o -4 7 0 3437.94 3849.87 185.08 o -3 7 0 47.00 42.69 37.89 o -2 7 0 1150.12 1077.69 80.94 o -1 7 0 344.87 360.37 59.39 o 0 7 0 879.83 701.61 44.13 o 1 7 0 4899.35 5199.56 95.05 o 2 7 0 6053.58 5634.06 94.11 o 3 7 0 3348.86 3144.84 153.23 o 4 7 0 3871.19 3792.70 169.70 o 5 7 0 47.50 46.89 16.53 o 6 7 0 387.12 434.19 74.77 o 7 7 0 2106.04 2023.71 95.80 o 8 7 0 2300.45 2439.43 136.27 o 9 7 0 716.26 825.23 67.63 o 10 7 0 847.03 1000.93 74.96 o 11 7 0 212.18 219.43 54.87 o 12 7 0 20.84 13.76 57.38 o 13 7 0 26.16 -18.40 60.25 o -7 8 0 685.66 892.87 136.35 o -6 8 0 268.85 265.50 82.35 o -5 8 0 4.56 16.21 48.26 o -4 8 0 23.72 71.04 50.40 o -3 8 0 3473.31 3500.30 171.22 o -2 8 0 1486.46 1508.52 101.06 o -1 8 0 2462.28 2421.55 105.28 o 0 8 0 861.71 933.67 54.21 o 1 8 0 25.46 1.56 33.10 o 2 8 0 1701.72 1595.82 110.08 o 3 8 0 2449.23 2259.89 132.07 o 4 8 0 1408.03 1360.76 102.31 o 5 8 0 1444.91 1539.24 77.81 o 6 8 0 632.15 691.56 56.60 o 7 8 0 27.02 45.00 32.08 o 8 8 0 8.49 -6.64 30.26 o 9 8 0 339.66 313.41 52.60 o 10 8 0 685.81 907.08 76.50 o 11 8 0 484.94 601.03 73.42 o 12 8 0 180.09 340.50 91.99 o -6 9 0 927.17 1095.00 124.57 o -5 9 0 801.93 966.36 124.72 o -4 9 0 555.29 507.50 92.98 o -3 9 0 949.42 745.58 87.67 o -2 9 0 647.78 569.99 105.02 o -1 9 0 1936.93 2139.96 154.69 o 0 9 0 3398.80 3416.70 188.42 o 1 9 0 3465.99 3750.85 193.89 o 2 9 0 1708.68 1703.71 125.09 o 3 9 0 218.09 237.56 66.25 o 4 9 0 219.54 309.70 75.05 o 5 9 0 587.79 679.49 99.91 o 6 9 0 1899.68 1914.79 107.11 o 7 9 0 755.51 867.98 68.76 o 8 9 0 749.26 812.90 76.14 o 9 9 0 305.18 423.47 82.77 o 10 9 0 16.60 -27.39 48.06 o 11 9 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620.23 127.85 o 0 12 0 1320.07 1226.18 135.67 o 1 12 0 1047.17 1370.14 170.59 o 2 12 0 409.89 324.87 93.45 o 3 12 0 35.97 8.29 59.10 o 4 12 0 25.10 -36.54 50.82 o 5 12 0 716.12 646.81 115.45 o 6 12 0 1141.28 1176.78 85.97 o 7 12 0 963.74 1184.53 88.47 o 8 12 0 401.94 483.97 184.92 o 9 12 0 31.92 -31.06 47.69 o 10 12 0 83.60 -4.64 65.31 o 11 12 0 84.37 -2.66 62.28 o -1 13 0 6.12 11.15 70.00 o 0 13 0 122.66 151.62 84.85 o 1 13 0 521.12 641.76 132.23 o 2 13 0 930.34 1309.00 168.77 o 3 13 0 670.37 789.10 134.00 o 4 13 0 753.72 845.45 135.62 o 5 13 0 304.38 325.49 97.10 o 6 13 0 27.68 -3.47 41.05 o 7 13 0 307.07 369.17 90.22 o 8 13 0 507.63 504.06 104.24 o 9 13 0 242.92 260.08 90.17 o 2 14 0 143.65 148.13 80.21 o 3 14 0 387.51 461.27 117.27 o 4 14 0 596.17 817.30 140.31 o 5 14 0 473.10 650.51 127.33 o 6 14 0 566.68 635.14 110.13 o 7 14 0 140.14 102.57 70.36 o -6 -14 1 433.89 602.56 113.41 o -5 -14 1 481.36 348.95 90.48 o -9 -13 1 190.89 156.05 76.36 o -8 -13 1 215.94 190.19 77.35 o -7 -13 1 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2870.77 2807.78 167.36 o 1 -9 1 2064.20 2165.13 152.71 o 2 -9 1 5.01 11.99 46.02 o 3 -9 1 1115.82 980.59 97.99 o 4 -9 1 874.29 1204.24 113.57 o 5 -9 1 983.62 938.48 108.57 o 6 -9 1 670.27 643.17 116.54 o -11 -8 1 343.78 406.49 97.47 o -10 -8 1 206.48 250.62 72.03 o -9 -8 1 63.05 -1.33 32.17 o -8 -8 1 88.73 41.45 36.61 o -7 -8 1 504.69 620.33 110.02 o -6 -8 1 1145.91 1337.02 75.30 o -5 -8 1 2595.90 2443.66 99.56 o -4 -8 1 540.75 571.92 84.17 o -3 -8 1 1166.58 1014.63 86.10 o -2 -8 1 122.44 117.90 47.53 o -1 -8 1 171.34 232.55 44.43 o 0 -8 1 3644.98 3507.71 92.82 o 1 -8 1 1287.88 1427.75 54.14 o 2 -8 1 1645.66 1657.64 108.10 o 3 -8 1 1755.59 1564.19 114.20 o 4 -8 1 9.48 136.87 52.22 o 5 -8 1 26.84 20.27 47.64 o 6 -8 1 676.57 625.55 110.86 o 7 -8 1 788.08 766.12 122.69 o -11 -7 1 525.40 682.39 117.74 o -10 -7 1 464.25 645.75 72.66 o -9 -7 1 905.98 846.94 64.59 o -8 -7 1 1550.10 1639.08 83.89 o -7 -7 1 1000.61 802.62 59.24 o -6 -7 1 251.21 268.23 44.30 o -5 -7 1 767.39 684.41 38.06 o -4 -7 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