#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/97/2219758.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219758_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Sinthiya, A' 'Jebas, Samuel Robinson' 'Ravindran Durai Nayagam, B.' 'Alfred Cecil Raj, S.' _publ_section_title ; Octaakis(4-aminopyridine)-1\k^4^N^1^,2\k^4^N^1^-aqua-2\kO-\m-carbonato-1:2\k^3^O,O':O''-dinickel(II) dichloride pentahydrate ; _journal_coeditor_code AT2653 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1436 _journal_page_last m1437 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.797 _cell_angle_beta 68.748 _cell_angle_gamma 75.191 _cell_length_a 12.8877 _cell_length_b 14.7920 _cell_length_c 15.0510 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.7330 _[local]_cod_data_source_file at2653Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s1am in P-1 (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 253.37 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 220.64 764.40 27.01 o 2 0 0 5562.22 4973.98 145.36 o 3 0 0 2408.72 3263.17 105.69 o 4 0 0 1648.57 1707.58 29.81 o 5 0 0 7335.75 8628.62 109.24 o 6 0 0 2999.84 3307.25 43.20 o 7 0 0 2320.09 2466.19 35.07 o 8 0 0 1985.72 1999.29 32.24 o 9 0 0 184.61 143.82 12.09 o 10 0 0 299.75 580.88 36.14 o 11 0 0 5891.87 6779.78 117.77 o 12 0 0 1798.48 1658.23 59.75 o 13 0 0 30.68 59.98 27.03 o 14 0 0 36.63 0.54 32.74 o 15 0 0 93.92 79.15 41.83 o -15 1 0 219.76 292.48 56.99 o -14 1 0 76.69 59.82 38.19 o -13 1 0 1325.64 1463.34 73.13 o -12 1 0 10.84 15.50 19.93 o -11 1 0 39.10 88.38 19.11 o -10 1 0 15.87 66.37 15.70 o -9 1 0 1051.39 915.58 50.86 o -8 1 0 1449.81 1358.27 36.52 o -7 1 0 2836.48 2944.89 41.47 o -6 1 0 5424.54 4574.73 75.35 o -5 1 0 3244.83 3692.74 61.17 o -4 1 0 14925.98 15558.52 236.38 o -3 1 0 2339.82 1871.24 47.49 o -2 1 0 40873.97 36766.12 684.61 o -1 1 0 947.19 655.30 11.09 o 2 1 0 24361.26 21633.47 542.99 o 3 1 0 12.49 40.87 14.11 o 4 1 0 3425.88 3115.81 70.52 o 5 1 0 10742.29 10640.60 118.52 o 6 1 0 338.65 605.47 15.34 o 7 1 0 3000.67 3305.35 42.70 o 8 1 0 13.33 25.96 7.46 o 9 1 0 3541.06 3114.56 44.74 o 10 1 0 2039.97 2011.43 44.93 o 11 1 0 638.06 733.68 43.09 o 12 1 0 4.52 101.78 26.37 o 13 1 0 1054.41 1131.35 73.05 o 14 1 0 172.92 134.74 33.64 o 15 1 0 76.95 41.48 29.66 o 16 1 0 26.96 17.04 40.75 o -15 2 0 427.46 344.28 57.39 o -14 2 0 6.42 22.83 32.13 o -13 2 0 290.49 329.22 42.20 o -12 2 0 85.21 86.72 23.06 o -11 2 0 4768.45 4565.45 105.95 o -10 2 0 667.75 714.65 38.49 o -9 2 0 9.93 30.70 13.13 o -8 2 0 1.06 22.55 11.68 o -7 2 0 5785.47 6249.02 79.37 o -6 2 0 11004.71 11524.30 162.73 o -5 2 0 7.03 50.13 8.55 o -4 2 0 8860.44 9112.71 126.69 o -3 2 0 858.49 404.33 18.99 o -2 2 0 835.79 766.93 18.37 o -1 2 0 4126.53 4456.72 137.28 o 1 2 0 2581.49 4399.33 113.70 o 2 2 0 64.30 116.46 12.06 o 3 2 0 4.71 99.63 14.95 o 4 2 0 12809.71 13067.63 155.39 o 5 2 0 10698.83 11650.45 142.33 o 6 2 0 3.66 155.95 10.62 o 7 2 0 2197.18 2546.84 35.87 o 8 2 0 47.56 30.12 7.76 o 9 2 0 97.75 59.90 9.72 o 10 2 0 88.40 70.02 10.88 o 11 2 0 2823.59 3059.11 123.47 o 12 2 0 743.91 587.13 44.85 o 13 2 0 75.43 86.81 28.27 o 14 2 0 25.45 59.94 57.02 o 15 2 0 94.77 107.89 34.38 o 16 2 0 314.06 314.48 66.96 o -15 3 0 100.47 77.40 41.02 o -14 3 0 0.73 11.66 27.67 o -13 3 0 1066.10 1249.08 62.72 o -12 3 0 1.04 -26.33 17.34 o -11 3 0 1.18 29.53 18.93 o -10 3 0 6.63 -8.39 15.11 o -9 3 0 1296.23 1153.49 44.07 o -8 3 0 741.29 782.01 34.62 o -7 3 0 0.79 -1.68 10.19 o -6 3 0 3658.10 3160.60 56.55 o -5 3 0 620.20 788.43 26.81 o -4 3 0 227.83 175.76 13.73 o -3 3 0 7432.25 8085.24 220.27 o -2 3 0 6811.47 6229.16 75.84 o -1 3 0 470.05 414.53 31.69 o 0 3 0 991.48 802.92 20.70 o 1 3 0 18325.48 17904.88 441.68 o 2 3 0 6734.98 5671.35 150.21 o 3 3 0 8879.22 9767.58 129.52 o 4 3 0 2105.31 2434.25 42.43 o 5 3 0 4810.42 3995.06 64.73 o 6 3 0 4678.99 4577.86 77.15 o 7 3 0 2799.80 2859.75 45.17 o 8 3 0 8.54 11.28 7.04 o 9 3 0 3037.29 2698.62 46.87 o 10 3 0 120.88 120.65 17.21 o 11 3 0 91.37 131.90 19.39 o 12 3 0 482.47 580.60 70.63 o 13 3 0 43.91 133.42 31.23 o 14 3 0 909.01 1016.09 63.59 o 15 3 0 83.59 31.93 33.07 o 16 3 0 1.00 1.60 31.15 o -14 4 0 4.65 5.53 26.84 o -13 4 0 3.19 -15.21 21.38 o -12 4 0 109.96 130.16 26.64 o -11 4 0 894.04 889.87 80.90 o -10 4 0 2681.54 2752.76 74.34 o -9 4 0 9.48 7.74 14.67 o -8 4 0 52.77 14.89 13.06 o -7 4 0 46.10 20.00 12.03 o -6 4 0 4235.09 4102.40 82.53 o -5 4 0 14.00 8.62 8.59 o -4 4 0 4689.23 4341.74 79.47 o -3 4 0 14.93 6.93 4.75 o -2 4 0 674.78 600.01 26.92 o -1 4 0 111.33 116.07 8.10 o 0 4 0 76.56 69.55 9.53 o 1 4 0 42494.96 46575.48 823.03 o 2 4 0 5144.53 5327.83 87.24 o 3 4 0 2043.94 1337.45 26.14 o 4 4 0 395.97 467.82 30.17 o 5 4 0 2185.81 2243.82 42.75 o 6 4 0 2795.90 2441.92 47.92 o 7 4 0 11864.02 12142.72 151.62 o 8 4 0 43.22 34.34 10.26 o 9 4 0 130.99 90.52 12.17 o 10 4 0 40.46 28.25 11.50 o 11 4 0 645.41 683.39 27.39 o 12 4 0 286.43 192.69 28.14 o 13 4 0 166.71 213.65 51.83 o 14 4 0 11.82 42.75 29.84 o 15 4 0 209.76 253.04 62.88 o 16 4 0 172.50 72.10 37.43 o -14 5 0 41.67 40.01 25.02 o -13 5 0 335.33 423.32 38.49 o -12 5 0 132.52 87.71 27.72 o -11 5 0 21.52 -2.17 16.75 o -10 5 0 621.34 610.86 38.21 o -9 5 0 1049.18 873.49 38.91 o -8 5 0 58.41 64.85 16.09 o -7 5 0 2304.56 2236.68 65.06 o -6 5 0 309.31 209.01 17.69 o -5 5 0 23.80 27.66 9.54 o -4 5 0 2658.74 2392.95 60.78 o -3 5 0 3861.79 3883.22 60.93 o -2 5 0 1949.20 1877.07 40.49 o -1 5 0 3634.21 4492.07 76.32 o 0 5 0 0.55 -4.69 4.37 o 1 5 0 5403.64 6004.64 101.63 o 2 5 0 1692.42 2870.14 53.22 o 3 5 0 8650.02 8170.71 110.38 o 4 5 0 32.95 43.14 7.44 o 5 5 0 14.65 19.48 7.87 o 6 5 0 517.23 629.83 22.99 o 7 5 0 727.57 704.83 23.15 o 8 5 0 4211.32 4081.98 66.33 o 9 5 0 2024.86 1612.01 39.51 o 10 5 0 106.63 112.85 14.40 o 11 5 0 80.90 43.02 13.31 o 12 5 0 1060.28 1091.00 38.96 o 13 5 0 957.74 948.48 49.52 o 14 5 0 396.19 347.96 43.21 o 15 5 0 24.11 8.51 29.91 o 16 5 0 22.86 33.39 34.53 o -14 6 0 4.49 3.44 23.07 o -13 6 0 3.47 -19.79 22.59 o -12 6 0 228.04 186.75 27.65 o -11 6 0 195.80 167.63 24.38 o -10 6 0 3131.79 3512.70 93.98 o -9 6 0 27.27 10.73 15.05 o -8 6 0 10.38 27.64 17.55 o -7 6 0 771.05 640.26 28.47 o -6 6 0 1389.86 1187.63 45.41 o -5 6 0 3666.41 3963.46 67.72 o -4 6 0 1137.19 966.00 30.49 o -3 6 0 224.74 247.80 10.64 o -2 6 0 1197.33 1001.62 41.96 o -1 6 0 1431.10 1227.92 25.72 o 0 6 0 3820.45 4005.13 79.85 o 1 6 0 19549.61 22434.93 331.82 o 2 6 0 492.04 801.48 37.03 o 3 6 0 4043.30 5247.75 91.48 o 4 6 0 18660.26 18574.49 240.49 o 5 6 0 553.87 604.30 20.97 o 6 6 0 13517.23 12759.14 176.36 o 7 6 0 114.36 185.67 15.70 o 8 6 0 125.89 241.80 17.02 o 9 6 0 849.19 929.95 30.34 o 10 6 0 1737.46 1427.96 36.05 o 11 6 0 19.48 24.43 13.33 o 12 6 0 812.20 782.64 39.24 o 13 6 0 208.62 134.67 36.19 o 14 6 0 116.80 61.10 42.30 o 15 6 0 476.75 614.93 78.54 o 16 6 0 26.29 16.57 50.05 o -13 7 0 36.00 54.16 21.31 o -12 7 0 601.51 527.08 34.32 o -11 7 0 8.99 31.09 16.95 o -10 7 0 105.06 76.18 24.39 o -9 7 0 75.56 130.37 25.85 o -8 7 0 1076.51 1121.88 54.31 o -7 7 0 1543.74 1319.78 64.28 o -6 7 0 83.05 19.98 21.91 o -5 7 0 275.57 184.13 26.53 o -4 7 0 1018.58 946.77 51.53 o -3 7 0 7026.10 8213.73 135.93 o -2 7 0 867.51 693.99 28.72 o -1 7 0 447.51 415.10 15.59 o 0 7 0 32.94 3.53 5.07 o 1 7 0 23858.38 25601.97 378.71 o 2 7 0 15103.06 17446.61 233.82 o 3 7 0 2862.32 3296.37 56.06 o 4 7 0 1293.61 1472.83 32.93 o 5 7 0 74.73 19.47 7.89 o 6 7 0 3814.44 3638.10 63.71 o 7 7 0 437.33 331.34 19.86 o 8 7 0 6402.40 6288.74 103.35 o 9 7 0 877.78 1166.15 37.86 o 10 7 0 617.81 615.83 28.07 o 11 7 0 1452.34 1488.37 56.08 o 12 7 0 915.03 1053.83 38.92 o 13 7 0 1449.40 1403.21 61.09 o 14 7 0 84.88 68.49 55.87 o 15 7 0 0.85 -14.08 36.91 o 16 7 0 72.37 66.48 54.70 o -13 8 0 4.17 57.61 48.18 o -12 8 0 71.03 63.54 44.03 o -11 8 0 2.97 -3.51 35.20 o -10 8 0 2434.04 2759.73 121.79 o -9 8 0 672.70 771.52 94.14 o -8 8 0 265.00 338.77 42.08 o -7 8 0 89.21 75.99 26.72 o -6 8 0 514.31 445.16 39.83 o -5 8 0 2963.46 2755.28 89.33 o -4 8 0 185.12 182.19 23.27 o -3 8 0 382.87 293.55 20.23 o -2 8 0 757.61 1129.18 25.00 o -1 8 0 1292.92 1374.82 38.34 o 0 8 0 58.66 51.46 7.44 o 1 8 0 416.09 593.55 21.75 o 2 8 0 2514.52 2574.98 40.82 o 3 8 0 3119.53 3401.88 94.51 o 4 8 0 4127.76 4095.30 104.79 o 5 8 0 929.75 1053.90 28.27 o 6 8 0 3158.76 2626.81 75.42 o 7 8 0 268.59 320.68 19.43 o 8 8 0 860.72 809.64 31.56 o 9 8 0 2589.78 2903.53 81.12 o 10 8 0 1176.60 976.96 34.16 o 11 8 0 302.97 261.34 22.49 o 12 8 0 316.34 342.83 26.55 o 13 8 0 0.31 15.33 17.64 o 14 8 0 118.29 114.34 32.97 o 15 8 0 263.61 283.97 48.00 o 16 8 0 1.83 43.04 47.83 o -12 9 0 348.12 232.66 52.46 o -11 9 0 28.32 74.91 39.41 o -10 9 0 347.61 333.32 120.44 o -9 9 0 936.37 1039.88 69.62 o -8 9 0 838.97 930.20 62.46 o -7 9 0 314.27 270.39 38.30 o -6 9 0 6.82 3.01 20.01 o -5 9 0 368.88 380.45 29.15 o -4 9 0 1270.88 1359.01 40.42 o -3 9 0 1646.77 1388.30 55.27 o -2 9 0 2.76 39.28 8.51 o -1 9 0 49.25 122.09 12.98 o 0 9 0 7.17 15.46 6.45 o 1 9 0 83.83 66.53 13.52 o 2 9 0 4029.12 4144.00 50.13 o 3 9 0 550.92 832.36 24.16 o 4 9 0 3841.17 4225.48 72.17 o 5 9 0 3305.77 3112.09 58.26 o 6 9 0 8291.93 8150.67 147.13 o 7 9 0 2343.75 2283.18 48.17 o 8 9 0 99.11 113.38 15.78 o 9 9 0 296.67 234.19 23.47 o 10 9 0 4.33 18.22 13.41 o 11 9 0 168.29 151.10 19.47 o 12 9 0 151.05 156.39 21.16 o 13 9 0 969.62 827.52 73.40 o 14 9 0 1.17 18.76 23.88 o 15 9 0 199.59 137.77 41.66 o -11 10 0 67.59 75.74 39.92 o -10 10 0 799.58 873.09 74.77 o -9 10 0 34.14 9.94 31.20 o -8 10 0 83.20 160.77 36.55 o -7 10 0 59.87 24.24 26.56 o -6 10 0 351.76 370.10 40.63 o -5 10 0 971.91 941.43 37.98 o -4 10 0 58.55 62.29 14.73 o -3 10 0 1069.30 923.57 47.06 o -2 10 0 407.68 318.83 34.75 o -1 10 0 350.88 402.95 16.48 o 0 10 0 823.01 769.97 19.36 o 1 10 0 79.50 32.87 7.67 o 2 10 0 106.22 102.91 11.98 o 3 10 0 4743.10 5007.24 71.65 o 4 10 0 3104.24 3049.70 64.72 o 5 10 0 1050.20 1002.33 30.35 o 6 10 0 154.21 124.58 19.19 o 7 10 0 20.41 7.11 16.02 o 8 10 0 14.29 13.89 15.42 o 9 10 0 10.85 59.90 14.55 o 10 10 0 305.17 375.96 24.06 o 11 10 0 604.10 606.51 30.15 o 12 10 0 274.56 300.31 30.42 o 13 10 0 0.87 17.86 18.21 o 14 10 0 340.37 253.22 31.94 o 15 10 0 654.15 715.04 54.76 o -11 11 0 137.85 187.96 52.71 o -10 11 0 165.21 28.93 40.48 o -9 11 0 1171.16 1510.07 98.11 o -8 11 0 69.64 116.55 60.83 o -7 11 0 186.97 227.46 39.50 o -6 11 0 230.23 213.98 49.21 o -5 11 0 89.33 74.36 18.32 o -4 11 0 51.57 46.99 15.28 o -3 11 0 4.30 6.24 14.47 o -2 11 0 5.68 4.73 16.07 o -1 11 0 188.63 172.65 20.79 o 0 11 0 409.52 410.06 15.54 o 1 11 0 619.74 536.44 31.40 o 2 11 0 4454.93 4572.44 61.58 o 3 11 0 1649.34 1862.02 37.69 o 4 11 0 2453.75 2325.95 49.96 o 5 11 0 708.88 658.84 31.91 o 6 11 0 7.32 48.16 16.19 o 7 11 0 481.24 496.66 32.85 o 8 11 0 0.71 18.01 17.56 o 9 11 0 574.61 665.31 27.35 o 10 11 0 0.59 -16.14 11.27 o 11 11 0 367.58 366.46 24.52 o 12 11 0 6.08 3.45 16.16 o 13 11 0 490.70 420.95 29.87 o 14 11 0 1036.72 917.15 42.58 o 15 11 0 85.09 131.34 30.54 o -10 12 0 6.94 0.09 36.40 o -9 12 0 67.05 103.09 114.07 o -8 12 0 12.14 18.19 32.30 o -7 12 0 3.33 24.76 29.71 o -6 12 0 1049.18 1042.41 62.50 o -5 12 0 1.61 5.47 18.15 o -4 12 0 275.27 324.79 25.32 o -3 12 0 21.66 40.87 14.14 o -2 12 0 1175.43 1053.05 51.24 o -1 12 0 4745.14 5423.95 170.91 o 0 12 0 863.58 861.96 35.29 o 1 12 0 74.31 83.28 14.26 o 2 12 0 189.10 171.50 18.76 o 3 12 0 1563.50 1494.08 47.88 o 4 12 0 965.93 910.58 31.71 o 5 12 0 4006.82 3859.86 85.03 o 6 12 0 2.08 31.08 16.35 o 7 12 0 544.46 506.69 33.72 o 8 12 0 37.79 50.43 20.78 o 9 12 0 1202.23 1251.57 53.58 o 10 12 0 1702.56 1826.90 55.31 o 11 12 0 422.06 443.03 26.86 o 12 12 0 542.27 661.41 31.77 o 13 12 0 130.21 118.51 21.56 o 14 12 0 543.63 592.85 47.49 o 15 12 0 9.91 30.88 24.32 o -9 13 0 447.15 528.48 61.05 o -8 13 0 197.31 146.78 87.60 o -7 13 0 44.62 52.31 32.88 o -6 13 0 209.26 219.75 92.92 o -5 13 0 81.79 69.82 22.24 o -4 13 0 1031.96 950.69 40.43 o -3 13 0 998.74 924.27 36.61 o -2 13 0 926.37 854.86 61.47 o -1 13 0 207.10 145.29 25.94 o 0 13 0 714.01 683.67 34.27 o 1 13 0 691.45 677.61 54.80 o 2 13 0 1010.82 1070.69 34.00 o 3 13 0 2968.79 3189.33 78.13 o 4 13 0 24.37 6.90 29.79 o 5 13 0 724.16 807.27 37.40 o 6 13 0 35.25 25.40 17.35 o 7 13 0 7123.53 6967.97 139.39 o 8 13 0 1913.41 1867.46 66.86 o 9 13 0 183.29 231.31 30.33 o 10 13 0 58.75 110.86 23.06 o 11 13 0 1.33 15.20 24.86 o 12 13 0 1027.79 1002.19 49.46 o 13 13 0 83.44 66.35 26.79 o 14 13 0 747.59 790.13 37.05 o -8 14 0 362.41 413.71 70.59 o -7 14 0 3.25 -25.86 31.42 o -6 14 0 116.86 196.49 40.59 o -5 14 0 256.73 284.47 29.64 o -4 14 0 25.49 28.64 19.24 o -3 14 0 145.50 131.83 21.20 o -2 14 0 956.70 871.55 54.53 o -1 14 0 1446.91 1384.98 123.54 o 0 14 0 184.94 186.15 22.96 o 1 14 0 254.63 219.24 20.30 o 2 14 0 218.63 212.97 27.22 o 3 14 0 1253.98 1271.07 43.82 o 4 14 0 423.72 351.68 27.54 o 5 14 0 4419.64 4279.99 94.83 o 6 14 0 228.11 362.50 30.35 o 7 14 0 145.08 103.56 24.08 o 8 14 0 3.09 2.99 20.64 o 9 14 0 893.82 882.19 40.63 o 10 14 0 1742.36 2009.56 71.06 o 11 14 0 168.95 160.32 27.18 o 12 14 0 294.18 323.93 34.50 o 13 14 0 30.77 62.74 27.21 o 14 14 0 786.46 849.64 62.69 o -7 15 0 132.80 109.22 39.77 o -6 15 0 81.82 95.17 38.79 o -5 15 0 3.32 7.69 27.34 o -4 15 0 1881.32 2006.27 62.31 o -3 15 0 710.60 695.92 36.49 o -2 15 0 515.43 472.52 33.64 o -1 15 0 29.10 95.52 24.84 o 0 15 0 2.52 9.77 16.76 o 1 15 0 1493.05 1652.16 82.21 o 2 15 0 635.26 718.13 40.14 o 3 15 0 1731.03 1656.88 51.76 o 4 15 0 20.81 30.34 19.55 o 5 15 0 298.55 267.62 28.11 o 6 15 0 306.60 239.97 28.02 o 7 15 0 1056.08 1180.75 51.07 o 8 15 0 1581.13 1747.37 63.73 o 9 15 0 88.55 78.14 22.25 o 10 15 0 21.00 33.36 21.52 o 11 15 0 7.68 6.69 21.50 o 12 15 0 583.39 630.87 44.51 o 13 15 0 25.52 96.23 36.30 o -6 16 0 1163.70 1395.36 82.42 o -5 16 0 275.08 254.98 34.40 o -4 16 0 354.01 320.82 31.65 o -3 16 0 41.73 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30.47 o 6 9 19 177.24 121.57 40.12 o 7 9 19 17.37 49.27 28.93 o 8 9 19 30.29 56.72 29.10 o 9 9 19 160.72 179.58 39.77 o 10 9 19 129.91 82.59 36.95 o 5 -2 20 283.67 386.31 62.91 o 6 -2 20 178.80 157.62 51.80 o 4 -1 20 298.63 269.30 52.27 o 5 -1 20 26.37 39.61 38.46 o 6 -1 20 26.92 -29.98 36.37 o 7 -1 20 193.49 154.99 49.51 o 3 0 20 56.57 65.50 33.56 o 4 0 20 431.85 533.97 51.17 o 5 0 20 96.56 36.71 31.68 o 6 0 20 123.45 98.61 40.69 o 7 0 20 16.04 13.40 36.24 o 8 0 20 8.22 11.25 37.92 o 3 1 20 384.75 393.69 136.03 o 4 1 20 2.15 -8.65 28.09 o 5 1 20 1.98 41.90 31.10 o 6 1 20 1.70 -9.66 28.22 o 7 1 20 253.46 182.11 33.80 o 8 1 20 6.00 28.02 30.42 o 9 1 20 151.78 206.53 41.18 o 3 2 20 64.09 76.31 24.96 o 4 2 20 274.48 349.14 32.05 o 5 2 20 358.35 336.88 39.85 o 6 2 20 70.06 66.60 24.64 o 7 2 20 37.97 70.14 27.90 o 8 2 20 3.77 12.63 29.62 o 9 2 20 141.78 153.83 36.62 o 3 3 20 244.04 186.57 40.79 o 4 3 20 186.29 215.22 25.73 o 5 3 20 22.57 34.51 21.25 o 6 3 20 29.59 21.98 21.67 o 7 3 20 987.88 959.89 44.24 o 8 3 20 55.71 37.29 24.47 o 9 3 20 176.57 161.37 35.21 o 4 4 20 81.28 91.43 35.31 o 5 4 20 595.83 622.45 52.71 o 6 4 20 150.71 118.36 46.82 o 7 4 20 435.29 431.91 47.47 o 8 4 20 2.26 23.61 32.18 o 9 4 20 380.60 374.89 39.02 o 4 5 20 6.27 56.37 40.32 o 5 5 20 12.67 -27.68 28.09 o 6 5 20 4.09 48.21 33.22 o 7 5 20 563.47 524.22 50.21 o 8 5 20 347.49 412.15 94.97 o 9 5 20 81.14 80.05 39.21 o 5 6 20 299.02 332.06 44.05 o 6 6 20 503.37 688.55 83.64 o 7 6 20 12.01 -17.14 31.06 o 8 6 20 36.38 66.32 32.28 o 9 6 20 269.91 261.98 78.41 o