#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219806_Fobs loop_ _publ_author_name 'Xie, Jian-Wu' 'Lv, Lu-Ping' 'Yu, Wen-Bo' 'Li, Wei-Wei' 'Hu, Xian-Chao' _publ_section_title ; (Methoxycarbonyl)hydrazinium chloride monohydrate ; _journal_coeditor_code CI2680 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2064 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.199 _cell_angle_gamma 90.000 _cell_length_a 12.6621 _cell_length_b 7.6444 _cell_length_c 6.6948 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7689 _[local]_cod_data_source_file ci2680Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CI2680 P 21/c R = 0.04' _shelx_refln_list_code 4 _shelx_F_calc_maximum 120.48 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 35.00 42.19 0.85 o 2 0 0 1963.11 1890.14 25.74 o 3 0 0 1.02 1.69 0.18 o 4 0 0 2250.77 2289.43 53.71 o 5 0 0 10.37 10.12 0.33 o 6 0 0 1064.24 1090.48 18.44 o 7 0 0 261.96 269.41 3.83 o 8 0 0 33.65 34.88 0.63 o 9 0 0 122.27 115.31 1.88 o 10 0 0 623.71 586.93 15.18 o 11 0 0 241.79 246.39 7.20 o 12 0 0 0.25 0.09 0.56 o 13 0 0 29.79 30.19 1.91 o 14 0 0 42.18 47.36 2.51 o 1 1 0 0.17 2.00 0.20 o 2 1 0 54.61 83.85 3.62 o 3 1 0 125.38 134.59 1.38 o 4 1 0 2385.66 2464.20 23.27 o 5 1 0 500.83 509.25 5.47 o 6 1 0 700.01 711.48 7.56 o 7 1 0 803.85 856.32 7.37 o 8 1 0 590.34 581.86 5.55 o 9 1 0 364.87 348.85 3.19 o 10 1 0 44.61 49.50 0.73 o 11 1 0 1.07 0.45 0.42 o 12 1 0 26.47 25.12 1.17 o 13 1 0 41.01 43.60 1.64 o 14 1 0 70.72 71.61 2.26 o 15 1 0 31.63 34.33 2.19 o 0 2 0 3358.94 3268.84 44.12 o 1 2 0 655.14 612.35 13.92 o 2 2 0 1024.21 968.42 11.15 o 3 2 0 835.09 857.05 8.95 o 4 2 0 49.41 43.07 0.64 o 5 2 0 59.96 58.80 0.75 o 6 2 0 8.77 7.02 0.47 o 7 2 0 486.09 472.62 4.21 o 8 2 0 22.44 20.09 0.40 o 9 2 0 12.06 13.19 0.39 o 10 2 0 3.09 3.03 0.23 o 11 2 0 13.51 10.87 0.43 o 12 2 0 0.24 0.03 0.43 o 13 2 0 0.51 0.38 0.46 o 14 2 0 8.75 8.91 0.90 o 15 2 0 6.21 6.87 1.20 o 1 3 0 2062.42 2176.86 25.02 o 2 3 0 7.02 2.84 0.23 o 3 3 0 1325.38 1306.53 10.36 o 4 3 0 51.94 55.28 0.68 o 5 3 0 395.02 411.69 3.69 o 6 3 0 526.87 541.89 4.81 o 7 3 0 134.35 154.58 1.46 o 8 3 0 875.35 885.03 7.72 o 9 3 0 625.94 608.01 5.85 o 10 3 0 17.02 19.01 0.58 o 11 3 0 147.89 156.82 1.98 o 12 3 0 161.07 162.85 2.25 o 13 3 0 72.15 79.84 3.46 o 0 4 0 1116.57 1152.48 13.08 o 1 4 0 240.33 260.27 3.64 o 2 4 0 2.29 0.57 0.15 o 3 4 0 554.80 531.10 5.68 o 4 4 0 927.78 926.02 7.36 o 5 4 0 159.51 170.07 1.99 o 6 4 0 154.02 145.84 1.50 o 7 4 0 64.41 58.87 0.78 o 8 4 0 185.97 182.75 2.59 o 9 4 0 96.28 98.77 1.65 o 10 4 0 55.71 58.78 1.00 o 11 4 0 64.98 61.70 1.05 o 12 4 0 38.34 38.44 0.82 o 13 4 0 62.63 65.75 1.40 o 1 5 0 92.04 102.25 0.98 o 2 5 0 39.68 43.06 0.74 o 3 5 0 13.98 16.69 0.34 o 4 5 0 34.17 36.95 0.64 o 5 5 0 103.44 100.52 1.28 o 6 5 0 64.04 60.30 1.30 o 7 5 0 0.48 -0.24 0.24 o 8 5 0 76.70 76.45 1.20 o 9 5 0 14.47 12.97 0.49 o 10 5 0 8.05 8.61 0.43 o 11 5 0 40.37 43.95 0.91 o 12 5 0 7.71 9.16 0.48 o 13 5 0 1.59 0.88 0.76 o 14 5 0 0.69 0.84 0.50 o 0 6 0 241.66 239.63 2.95 o 1 6 0 59.83 63.33 0.73 o 2 6 0 23.56 17.17 0.38 o 3 6 0 878.93 830.03 8.28 o 4 6 0 231.99 221.09 2.62 o 5 6 0 190.60 201.24 3.88 o 6 6 0 14.81 16.78 0.48 o 7 6 0 180.36 187.00 2.57 o 8 6 0 93.49 98.01 1.62 o 9 6 0 101.09 103.56 1.71 o 10 6 0 3.90 4.35 0.42 o 11 6 0 0.01 0.32 0.31 o 12 6 0 27.22 31.16 1.23 o 13 6 0 40.96 42.50 1.79 o 1 7 0 349.83 338.78 3.35 o 2 7 0 17.29 19.60 0.51 o 3 7 0 209.94 203.07 2.26 o 4 7 0 25.71 24.73 0.60 o 5 7 0 590.27 570.67 5.98 o 6 7 0 0.03 -0.02 0.26 o 7 7 0 42.71 39.54 0.96 o 8 7 0 9.29 7.59 0.50 o 9 7 0 74.00 71.96 1.68 o 10 7 0 47.32 44.98 1.48 o 11 7 0 25.56 31.49 1.26 o 0 8 0 58.24 51.26 1.71 o 1 8 0 2.55 2.42 0.28 o 2 8 0 4.69 4.28 0.32 o 3 8 0 11.22 9.72 0.43 o 4 8 0 25.36 21.30 0.63 o 5 8 0 0.06 -0.15 0.25 o 6 8 0 0.05 0.21 0.29 o 7 8 0 4.67 6.69 0.68 o 8 8 0 59.32 67.57 2.40 o 9 8 0 1.67 1.73 1.09 o 1 9 0 1.60 1.37 0.47 o 2 9 0 8.83 7.74 0.51 o 3 9 0 28.31 23.89 1.16 o 4 9 0 9.92 12.47 0.71 o 5 9 0 87.81 83.56 2.14 o 6 9 0 8.94 10.87 1.49 o -15 1 1 40.70 39.93 2.36 o -14 1 1 303.98 299.61 6.22 o -13 1 1 97.33 94.46 2.56 o -12 1 1 71.42 68.99 2.20 o -11 1 1 343.20 321.45 4.65 o -10 1 1 116.43 110.17 2.04 o -9 1 1 26.50 25.47 0.55 o -8 1 1 259.02 254.96 2.55 o -7 1 1 1311.27 1264.52 10.85 o -6 1 1 66.03 66.16 1.82 o -5 1 1 83.32 84.60 0.93 o -4 1 1 549.90 622.35 5.95 o -3 1 1 141.76 164.61 1.73 o -2 1 1 0.10 0.80 0.12 o -1 1 1 2360.93 2549.45 29.18 o 0 1 1 837.87 775.84 8.14 o 1 1 1 360.81 364.36 3.53 o 2 1 1 3613.38 3304.22 31.39 o 3 1 1 14516.41 13686.91 467.67 o 4 1 1 1173.99 1216.56 12.32 o 5 1 1 144.83 149.76 2.11 o 6 1 1 238.95 207.43 1.98 o 7 1 1 571.17 518.65 10.57 o 8 1 1 37.58 35.37 0.98 o 9 1 1 158.43 159.39 2.36 o 10 1 1 430.82 426.58 6.24 o 11 1 1 1.20 1.24 0.26 o 12 1 1 53.11 49.43 1.27 o 13 1 1 125.10 120.63 3.14 o 14 1 1 35.23 35.78 1.54 o -15 2 1 56.58 64.94 3.03 o -14 2 1 29.58 28.85 1.37 o -13 2 1 102.79 98.97 2.64 o -12 2 1 55.40 51.52 1.65 o -11 2 1 330.61 308.92 3.86 o -10 2 1 155.52 155.29 2.11 o -9 2 1 209.02 202.87 2.14 o -8 2 1 2.90 4.88 0.57 o -7 2 1 454.67 498.13 4.36 o -6 2 1 436.61 388.27 3.46 o -5 2 1 4294.60 4336.93 36.83 o -4 2 1 169.55 190.83 1.94 o -3 2 1 3384.45 3361.49 35.62 o -2 2 1 3924.86 3869.61 36.57 o -1 2 1 4268.97 4211.94 53.29 o 0 2 1 535.03 505.56 5.37 o 1 2 1 945.77 984.98 10.16 o 2 2 1 1760.45 1894.78 17.87 o 3 2 1 433.50 469.10 4.56 o 4 2 1 907.80 920.11 8.84 o 5 2 1 70.55 55.34 0.82 o 6 2 1 273.04 264.97 2.30 o 7 2 1 1078.56 1095.03 8.75 o 8 2 1 286.68 281.10 3.88 o 9 2 1 62.73 64.30 1.76 o 10 2 1 289.49 288.49 3.15 o 11 2 1 116.87 114.88 1.90 o 12 2 1 310.77 304.79 4.14 o 13 2 1 0.03 0.96 0.38 o 14 2 1 4.26 6.18 1.12 o -13 3 1 0.93 1.47 0.43 o -12 3 1 9.72 11.85 0.62 o -11 3 1 1.10 1.99 0.49 o -10 3 1 17.91 18.38 0.46 o -9 3 1 0.83 1.79 0.30 o -8 3 1 143.32 132.51 1.52 o -7 3 1 386.72 397.11 4.26 o -6 3 1 104.78 105.41 1.03 o -5 3 1 93.32 95.26 0.93 o -4 3 1 573.70 638.48 6.06 o -3 3 1 95.61 100.33 0.95 o -2 3 1 125.03 143.41 1.84 o -1 3 1 550.94 636.72 6.11 o 0 3 1 8.97 9.24 0.25 o 1 3 1 258.47 294.68 3.82 o 2 3 1 408.25 391.05 5.57 o 3 3 1 469.92 484.28 3.72 o 4 3 1 299.29 297.09 2.58 o 5 3 1 40.84 45.42 0.57 o 6 3 1 47.44 51.69 0.65 o 7 3 1 94.34 89.74 0.98 o 8 3 1 11.67 9.92 0.44 o 9 3 1 24.08 22.55 0.58 o 10 3 1 4.44 4.97 0.58 o 11 3 1 0.00 0.18 0.21 o 12 3 1 9.49 11.34 0.70 o 13 3 1 2.18 2.59 0.46 o -13 4 1 21.65 21.28 0.75 o -12 4 1 14.40 16.11 0.64 o -11 4 1 0.30 0.27 0.23 o -10 4 1 96.83 102.38 1.68 o -9 4 1 13.29 16.81 0.53 o -8 4 1 277.34 283.13 3.19 o -7 4 1 116.52 125.94 1.61 o -6 4 1 212.10 189.12 1.87 o -5 4 1 853.77 882.11 7.55 o -4 4 1 242.68 223.81 1.97 o -3 4 1 35.49 34.18 0.46 o -2 4 1 560.13 619.85 4.97 o -1 4 1 1.41 2.66 0.20 o 0 4 1 1682.99 1668.16 13.03 o 1 4 1 38.79 29.54 0.40 o 2 4 1 1187.19 1179.74 9.29 o 3 4 1 2.33 3.24 0.16 o 4 4 1 1558.91 1547.48 13.87 o 5 4 1 46.49 42.59 0.66 o 6 4 1 16.39 17.77 0.40 o 7 4 1 2.10 2.68 0.21 o 8 4 1 20.12 20.50 0.66 o 9 4 1 20.21 22.05 0.76 o 10 4 1 1.05 2.35 0.48 o 11 4 1 53.90 55.42 1.02 o 12 4 1 59.39 57.86 1.32 o 13 4 1 3.24 3.74 0.46 o 14 4 1 24.05 28.12 1.79 o -14 5 1 109.83 123.53 3.40 o -12 5 1 11.30 13.32 0.63 o -11 5 1 139.97 138.00 1.89 o -10 5 1 495.76 480.00 5.25 o -9 5 1 98.48 102.80 1.49 o -8 5 1 128.25 128.82 1.72 o -7 5 1 24.44 24.05 0.59 o -6 5 1 215.52 208.78 2.70 o -5 5 1 648.33 662.20 5.77 o -4 5 1 680.97 673.28 6.78 o -3 5 1 9.04 8.39 0.23 o -2 5 1 124.69 147.28 1.35 o -1 5 1 268.19 251.86 2.25 o 0 5 1 936.83 909.71 10.03 o 1 5 1 263.14 233.41 2.00 o 2 5 1 58.85 67.91 0.81 o 3 5 1 197.12 197.23 2.15 o 4 5 1 15.94 18.05 0.40 o 5 5 1 69.20 78.95 1.06 o 6 5 1 560.95 535.68 5.71 o 7 5 1 813.21 771.53 6.78 o 8 5 1 82.76 88.59 1.14 o 9 5 1 66.79 69.58 1.18 o 10 5 1 157.42 172.55 2.49 o 11 5 1 172.55 186.71 2.86 o 12 5 1 71.18 71.27 1.27 o 13 5 1 36.29 38.31 1.32 o -13 6 1 33.40 35.03 1.57 o -12 6 1 0.90 0.13 0.40 o -11 6 1 2.58 3.87 0.51 o -10 6 1 1.75 1.28 0.33 o -9 6 1 186.20 203.26 2.81 o -8 6 1 60.01 66.86 1.24 o -7 6 1 23.60 19.95 0.68 o -6 6 1 214.16 206.29 2.75 o -5 6 1 14.89 17.08 0.55 o -4 6 1 2.19 1.96 0.23 o -3 6 1 146.03 134.18 1.42 o -2 6 1 493.13 477.93 3.90 o -1 6 1 1.48 2.45 0.17 o 0 6 1 152.63 137.73 1.99 o 1 6 1 31.93 28.88 0.49 o 2 6 1 145.14 132.09 1.55 o 3 6 1 16.62 13.67 0.50 o 4 6 1 126.16 121.27 1.48 o 5 6 1 29.98 31.76 0.65 o 6 6 1 62.61 60.19 0.96 o 7 6 1 55.04 54.66 0.92 o 8 6 1 212.36 206.57 2.87 o 9 6 1 9.48 9.87 0.53 o 10 6 1 16.42 18.05 0.63 o 11 6 1 4.90 5.70 0.51 o 12 6 1 0.09 -0.10 0.52 o -11 7 1 36.50 38.07 1.36 o -10 7 1 40.59 37.94 1.19 o -9 7 1 2.77 2.68 0.49 o -8 7 1 15.10 17.64 0.83 o -7 7 1 14.90 17.00 0.79 o -6 7 1 5.81 7.34 0.57 o -5 7 1 4.21 2.63 0.44 o -4 7 1 31.04 29.45 0.93 o -3 7 1 5.52 6.75 0.50 o -2 7 1 1.24 1.56 0.28 o -1 7 1 3.63 3.53 0.27 o 0 7 1 13.65 15.74 0.41 o 1 7 1 10.38 6.67 0.33 o 2 7 1 0.39 -0.18 0.18 o 3 7 1 87.80 86.05 1.20 o 4 7 1 19.25 19.43 0.53 o 5 7 1 4.37 5.43 0.35 o 6 7 1 69.84 65.99 1.07 o 7 7 1 41.05 39.84 0.88 o 8 7 1 5.78 5.69 0.47 o 9 7 1 7.31 6.53 0.76 o 10 7 1 27.67 26.72 1.74 o 11 7 1 0.08 0.55 0.55 o -9 8 1 93.42 100.74 2.46 o -8 8 1 61.86 66.82 1.86 o -7 8 1 2.64 2.23 0.54 o -6 8 1 153.91 145.20 2.24 o -5 8 1 34.99 33.72 0.89 o -4 8 1 15.94 13.69 0.60 o -3 8 1 6.74 4.63 0.35 o -2 8 1 532.50 517.75 5.11 o -1 8 1 52.48 57.83 0.95 o 0 8 1 141.08 130.86 1.65 o 1 8 1 68.31 64.56 1.03 o 2 8 1 129.53 122.46 1.60 o 3 8 1 1.55 1.67 0.30 o 4 8 1 159.58 151.83 2.05 o 5 8 1 10.58 10.50 0.47 o 6 8 1 19.33 17.55 0.72 o 7 8 1 0.56 0.93 0.74 o 8 8 1 123.94 133.38 4.87 o 9 8 1 12.76 15.75 0.99 o -6 9 1 24.65 25.84 1.20 o -5 9 1 48.15 47.38 1.56 o -4 9 1 15.73 15.77 0.74 o -3 9 1 19.82 23.70 0.75 o -2 9 1 7.01 6.68 0.51 o -1 9 1 57.06 56.91 1.59 o 0 9 1 71.68 68.31 1.77 o 1 9 1 7.34 7.06 0.52 o 2 9 1 34.99 37.33 0.93 o 3 9 1 9.62 12.87 0.59 o 4 9 1 1.89 2.43 0.49 o 5 9 1 2.37 1.85 0.44 o 6 9 1 10.27 7.60 0.65 o -14 0 2 39.51 38.27 2.26 o -13 0 2 15.24 17.01 1.49 o -12 0 2 178.34 158.45 5.08 o -11 0 2 237.85 219.23 6.44 o -10 0 2 358.91 362.27 4.91 o -9 0 2 4.47 3.38 0.29 o -8 0 2 1459.80 1405.14 17.85 o -7 0 2 501.26 505.21 5.79 o -6 0 2 35.43 53.64 0.93 o -5 0 2 222.41 190.79 2.75 o -4 0 2 10408.65 10241.38 136.91 o -3 0 2 2159.38 2279.71 30.38 o -2 0 2 438.92 425.54 5.82 o -1 0 2 1078.69 1106.63 14.82 o 0 0 2 866.28 970.60 13.02 o 1 0 2 5.69 17.41 0.43 o 2 0 2 10203.04 9116.88 454.00 o 3 0 2 448.05 487.20 8.42 o 4 0 2 909.73 911.51 10.40 o 5 0 2 717.34 724.36 8.36 o 6 0 2 3186.42 3084.36 41.61 o 7 0 2 1073.34 1064.91 12.21 o 8 0 2 4.39 4.97 0.41 o 9 0 2 90.25 80.75 1.55 o 10 0 2 98.46 89.45 1.72 o 11 0 2 105.28 95.73 1.83 o 12 0 2 1.31 2.54 0.54 o 13 0 2 231.90 233.08 7.46 o 14 0 2 9.28 9.50 1.40 o -14 1 2 9.87 11.85 1.01 o -13 1 2 34.77 34.83 1.44 o -12 1 2 216.56 207.75 4.45 o -11 1 2 58.07 53.50 1.04 o -10 1 2 283.62 258.61 3.25 o -9 1 2 44.17 42.05 0.60 o -8 1 2 603.17 589.55 5.07 o -7 1 2 65.47 81.63 0.96 o -6 1 2 335.02 340.31 3.29 o -5 1 2 535.07 582.70 5.48 o -4 1 2 13.84 20.77 0.39 o -3 1 2 94.84 103.57 1.11 o -2 1 2 1207.57 1295.48 12.24 o -1 1 2 1.36 1.08 0.14 o 0 1 2 1947.64 2024.94 19.10 o 1 1 2 1621.71 1631.01 17.01 o 2 1 2 1674.19 1647.27 15.55 o 3 1 2 367.78 406.74 4.00 o 4 1 2 52.63 51.40 0.59 o 5 1 2 715.03 709.20 5.80 o 6 1 2 83.46 90.61 1.02 o 7 1 2 66.95 72.97 1.85 o 8 1 2 9.47 11.25 0.31 o 9 1 2 95.22 101.07 1.30 o 10 1 2 232.06 226.23 3.67 o 11 1 2 162.59 152.44 2.44 o 12 1 2 1.64 2.18 0.33 o 13 1 2 18.23 20.91 1.50 o 14 1 2 2.75 4.29 1.08 o -15 2 2 34.21 35.18 2.17 o -14 2 2 6.69 7.49 0.85 o -13 2 2 8.00 7.91 0.54 o -12 2 2 31.03 26.32 0.83 o -11 2 2 129.02 126.44 1.85 o -10 2 2 61.96 62.38 1.08 o -9 2 2 52.78 49.62 0.91 o -8 2 2 113.80 116.62 1.32 o -7 2 2 221.72 231.84 2.35 o -6 2 2 0.00 -0.10 0.10 o -5 2 2 2.30 2.21 0.13 o -4 2 2 10.59 7.40 0.33 o -3 2 2 39.64 42.54 0.57 o -2 2 2 0.28 0.17 0.08 o -1 2 2 2416.88 2585.99 24.30 o 0 2 2 295.55 321.30 3.19 o 1 2 2 224.51 244.70 2.49 o 2 2 2 575.33 562.42 5.46 o 3 2 2 45.58 61.18 0.62 o 4 2 2 37.25 34.03 0.42 o 5 2 2 350.99 340.01 2.90 o 6 2 2 71.40 82.71 0.91 o 7 2 2 7.02 5.29 0.22 o 8 2 2 6.45 5.94 0.25 o 9 2 2 54.47 53.72 0.82 o 10 2 2 15.90 17.17 0.63 o 11 2 2 0.11 0.53 0.23 o 12 2 2 0.55 2.10 0.66 o 13 2 2 43.66 44.02 1.09 o 14 2 2 9.54 10.64 1.12 o -14 3 2 51.83 49.62 1.77 o -13 3 2 49.83 47.51 1.11 o -12 3 2 223.77 213.42 2.88 o -11 3 2 2.43 4.31 0.43 o -10 3 2 303.65 277.97 3.54 o -9 3 2 193.74 186.91 2.26 o -8 3 2 149.71 140.15 1.59 o -7 3 2 874.49 905.57 7.79 o -6 3 2 347.04 357.97 3.22 o -5 3 2 0.72 0.66 0.13 o -4 3 2 202.17 226.74 1.97 o -3 3 2 156.11 132.86 1.30 o -2 3 2 1514.53 1502.36 11.91 o -1 3 2 250.52 235.09 2.17 o 0 3 2 1.12 1.65 0.12 o 1 3 2 1178.94 1261.62 9.90 o 2 3 2 762.83 814.52 6.16 o 3 3 2 443.37 418.61 3.28 o 4 3 2 156.00 138.34 1.34 o 5 3 2 1610.83 1595.05 12.70 o 6 3 2 31.23 31.27 0.66 o 7 3 2 700.86 679.71 5.64 o 8 3 2 333.37 323.17 2.89 o 9 3 2 123.72 125.44 1.44 o 10 3 2 205.24 208.16 2.19 o 11 3 2 67.14 66.26 1.54 o 12 3 2 3.52 4.81 0.74 o 13 3 2 1.81 1.79 0.55 o 14 3 2 25.17 27.60 1.65 o -14 4 2 32.40 27.29 1.36 o -13 4 2 24.00 19.60 0.74 o -12 4 2 47.79 50.87 1.37 o -11 4 2 150.84 146.77 2.40 o -10 4 2 4.48 6.88 0.45 o -9 4 2 3.78 4.32 0.31 o -8 4 2 46.98 50.11 0.95 o -7 4 2 631.38 638.50 6.11 o -6 4 2 12.73 12.57 0.37 o 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