#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/98/2219813.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219813_Fobs loop_ _publ_author_name 'Lv, Lu-Ping' 'Zhang, Yong-Zhao' 'Ding, Xiao-Min' 'Yu, Wen-Bo' 'Hu, Xian-Chao' _publ_section_title ; (E)-Methyl N'-(2-furylmethylene)hydrazinecarboxylate ; _journal_coeditor_code CI2688 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2146 _journal_volume 64 _journal_year 2008 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.251 _cell_angle_gamma 90.000 _cell_length_a 14.9185 _cell_length_b 7.8124 _cell_length_c 15.1299 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file ci2688Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n in C 1 2 1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 212.03 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1130.29 1121.15 12.28 o 4 0 0 1218.87 1190.98 18.57 o 6 0 0 2041.52 1948.88 24.44 o 8 0 0 268.12 331.12 5.35 o 10 0 0 80.27 87.38 3.06 o 12 0 0 83.48 80.52 3.97 o 14 0 0 108.25 110.36 5.04 o 16 0 0 1.42 0.66 1.78 o 1 1 0 104.15 95.51 2.95 o 3 1 0 4774.62 4547.31 35.98 o 5 1 0 394.96 349.60 4.11 o 7 1 0 191.03 207.27 2.71 o 9 1 0 231.49 222.54 3.17 o 11 1 0 45.90 46.61 2.85 o 13 1 0 81.03 85.08 3.03 o 15 1 0 37.72 37.90 2.55 o 17 1 0 4.49 2.10 2.29 o 0 2 0 20986.41 21117.79 250.63 o 2 2 0 4930.52 4992.04 66.40 o 4 2 0 1324.92 1289.06 12.34 o 6 2 0 271.45 306.73 3.71 o 8 2 0 300.51 279.15 3.88 o 10 2 0 73.65 66.60 2.23 o 12 2 0 250.27 257.51 4.49 o 14 2 0 53.55 55.19 2.75 o 16 2 0 2.29 0.78 1.69 o 1 3 0 106.52 103.30 2.62 o 3 3 0 915.03 975.78 11.09 o 5 3 0 121.60 108.64 2.35 o 7 3 0 622.87 641.36 6.47 o 9 3 0 18.91 19.07 2.01 o 11 3 0 71.07 63.50 2.44 o 13 3 0 114.64 114.41 4.19 o 15 3 0 19.43 19.02 1.91 o 0 4 0 4074.74 3841.20 72.33 o 2 4 0 1110.86 1140.70 9.17 o 4 4 0 790.08 783.56 6.69 o 6 4 0 503.50 504.01 8.24 o 8 4 0 18.67 20.41 1.84 o 10 4 0 14.77 14.05 1.44 o 12 4 0 16.83 20.84 2.13 o 14 4 0 23.45 22.73 2.04 o 1 5 0 155.27 158.53 2.85 o 3 5 0 456.34 475.15 5.63 o 5 5 0 778.84 778.74 8.42 o 7 5 0 390.46 367.34 5.54 o 9 5 0 49.04 50.62 2.87 o 11 5 0 84.57 82.26 3.02 o 13 5 0 6.74 6.02 1.52 o 0 6 0 138.82 146.71 4.70 o 2 6 0 16.22 19.40 1.56 o 4 6 0 57.68 54.49 4.19 o 6 6 0 3.48 2.90 1.15 o 8 6 0 252.58 262.37 4.80 o 10 6 0 61.67 66.12 2.88 o 12 6 0 0.88 1.03 1.36 o 1 7 0 3.43 4.29 1.24 o 3 7 0 65.86 64.28 2.64 o 5 7 0 295.70 307.76 6.32 o 7 7 0 81.54 87.26 4.67 o 9 7 0 16.79 17.42 2.18 o 11 7 0 8.99 10.43 2.00 o 2 8 0 86.80 84.66 10.33 o 4 8 0 62.86 68.16 10.81 o 6 8 0 4.83 4.61 3.47 o 8 8 0 6.11 3.57 2.77 o -16 0 1 11.22 17.34 2.97 o -14 0 1 142.84 135.65 9.91 o -12 0 1 121.50 122.20 4.53 o -10 0 1 1.79 2.00 0.95 o -8 0 1 0.34 0.00 0.72 o -6 0 1 3234.08 3201.49 34.87 o -4 0 1 2519.34 2525.62 38.19 o -2 0 1 2155.32 2109.24 32.26 o 0 0 1 3.59 5.09 0.62 o 2 0 1 68.51 66.30 1.97 o 4 0 1 260.71 292.62 4.94 o 6 0 1 1911.70 1823.64 16.77 o 8 0 1 482.68 448.93 6.51 o 10 0 1 62.41 77.12 3.82 o 12 0 1 916.12 876.41 13.55 o 14 0 1 0.01 0.00 1.42 o 16 0 1 13.58 17.08 2.89 o -17 1 1 6.74 4.54 2.92 o -15 1 1 47.92 48.57 2.68 o -13 1 1 76.10 76.65 3.15 o -11 1 1 7.25 5.27 0.95 o -9 1 1 539.40 538.61 5.32 o -7 1 1 592.22 606.10 5.27 o -5 1 1 274.79 325.88 3.95 o -3 1 1 38299.79 39121.34 316.00 o -1 1 1 151.71 140.78 1.75 o 1 1 1 280.35 270.28 3.94 o 3 1 1 1377.30 1477.26 11.82 o 5 1 1 1459.42 1449.24 12.24 o 7 1 1 99.58 104.65 2.67 o 9 1 1 96.83 96.44 2.10 o 11 1 1 518.04 492.11 6.06 o 13 1 1 271.60 264.66 5.06 o 15 1 1 11.47 11.62 2.87 o -16 2 1 39.89 45.28 2.81 o -14 2 1 10.83 10.05 1.92 o -12 2 1 192.77 187.28 3.78 o -10 2 1 4.72 5.67 0.93 o -8 2 1 964.63 981.03 8.48 o -6 2 1 1073.40 1105.90 9.80 o -4 2 1 11815.57 11854.85 84.50 o -2 2 1 5497.38 5489.06 43.73 o 0 2 1 12690.52 12435.95 131.52 o 2 2 1 334.61 400.58 4.82 o 4 2 1 503.97 462.15 5.88 o 6 2 1 2604.48 2707.04 18.02 o 8 2 1 608.80 584.03 6.10 o 10 2 1 133.52 140.32 4.39 o 12 2 1 223.71 226.65 4.26 o 14 2 1 36.19 34.60 2.36 o 16 2 1 4.21 7.40 1.70 o -15 3 1 42.27 54.08 2.75 o -13 3 1 3.24 3.36 1.19 o -11 3 1 31.80 32.61 1.89 o -9 3 1 82.77 74.60 2.29 o -7 3 1 404.83 382.19 5.43 o -5 3 1 365.36 375.31 4.54 o -3 3 1 349.04 331.66 5.31 o -1 3 1 40.02 46.12 3.62 o 1 3 1 18.59 17.11 3.87 o 3 3 1 891.92 873.58 9.41 o 5 3 1 700.96 724.02 6.60 o 7 3 1 228.45 217.73 3.91 o 9 3 1 19.60 21.19 1.50 o 11 3 1 45.66 40.20 2.19 o 13 3 1 32.24 30.49 2.07 o 15 3 1 13.49 11.05 1.99 o -14 4 1 29.09 28.65 2.24 o -12 4 1 134.80 130.34 3.91 o -10 4 1 195.03 183.34 3.73 o -8 4 1 470.90 439.30 5.53 o -6 4 1 367.48 395.51 4.92 o -4 4 1 214.42 213.18 4.53 o -2 4 1 403.98 390.44 4.98 o 0 4 1 2175.70 2225.91 18.88 o 2 4 1 781.40 789.48 9.23 o 4 4 1 87.17 78.37 4.54 o 6 4 1 71.18 84.97 2.27 o 8 4 1 430.27 425.97 6.42 o 10 4 1 167.93 171.46 4.81 o 12 4 1 172.77 166.01 7.52 o 14 4 1 6.98 6.62 1.50 o -13 5 1 72.99 78.00 3.22 o -11 5 1 64.34 60.23 2.66 o -9 5 1 3.60 4.41 1.61 o -7 5 1 68.44 61.51 2.33 o -5 5 1 191.96 188.44 3.49 o -3 5 1 74.34 91.06 3.32 o -1 5 1 11.78 9.42 3.66 o 1 5 1 43.70 44.29 2.20 o 3 5 1 109.83 110.43 6.13 o 5 5 1 444.57 430.15 6.44 o 7 5 1 9.88 6.85 1.20 o 9 5 1 101.26 91.98 3.82 o 11 5 1 149.60 142.12 3.71 o 13 5 1 50.71 53.17 2.83 o -12 6 1 14.85 25.04 2.33 o -10 6 1 16.21 19.16 2.24 o -8 6 1 85.26 69.61 2.97 o -6 6 1 108.33 116.67 5.36 o -4 6 1 76.77 78.33 4.07 o -2 6 1 41.61 50.60 2.13 o 0 6 1 95.84 89.76 2.92 o 2 6 1 447.98 481.02 10.38 o 4 6 1 137.91 149.06 4.63 o 6 6 1 149.09 152.59 3.53 o 8 6 1 354.81 363.74 7.89 o 10 6 1 20.66 17.65 1.88 o 12 6 1 18.52 18.19 1.97 o -11 7 1 2.46 3.88 1.85 o -9 7 1 17.16 15.99 2.61 o -7 7 1 32.64 33.63 3.32 o -5 7 1 129.49 143.94 4.23 o -3 7 1 166.64 161.96 4.31 o -1 7 1 5.65 4.26 1.58 o 1 7 1 3.35 2.84 1.62 o 3 7 1 64.53 63.31 3.72 o 5 7 1 139.64 139.00 4.16 o 7 7 1 130.21 132.80 3.90 o 9 7 1 1.18 0.00 1.46 o -8 8 1 15.30 23.58 2.85 o -6 8 1 81.96 94.03 5.12 o -4 8 1 29.10 30.64 3.78 o -2 8 1 33.96 37.95 3.79 o 0 8 1 51.14 41.99 4.54 o 2 8 1 79.57 81.00 8.75 o 4 8 1 46.63 49.37 4.51 o 6 8 1 33.64 39.87 5.42 o 8 8 1 9.17 10.22 4.86 o -16 0 2 1.01 0.41 1.78 o -14 0 2 31.24 33.36 3.11 o -12 0 2 115.66 109.81 4.47 o -10 0 2 66.14 60.62 2.64 o -8 0 2 928.34 959.19 10.68 o -6 0 2 2123.84 2339.36 26.35 o -4 0 2 27525.30 27229.59 596.48 o -2 0 2 11242.01 10440.79 188.70 o 0 0 2 3985.42 4014.15 40.84 o 2 0 2 8846.07 9238.83 128.15 o 4 0 2 877.02 974.21 12.20 o 6 0 2 55.17 70.32 2.14 o 8 0 2 1236.27 1256.21 13.42 o 10 0 2 234.49 210.10 4.72 o 12 0 2 27.45 28.00 2.83 o 14 0 2 19.49 18.67 2.64 o 16 0 2 5.95 5.97 2.27 o -17 1 2 4.97 5.56 1.57 o -15 1 2 7.85 6.76 1.54 o -13 1 2 226.86 219.67 4.15 o -11 1 2 161.09 159.16 3.18 o -9 1 2 880.75 858.44 7.28 o -7 1 2 2414.85 2267.88 14.48 o -5 1 2 11206.49 10726.70 77.90 o -3 1 2 4723.38 4635.32 41.34 o -1 1 2 1258.35 1132.46 17.63 o 1 1 2 2984.04 3002.17 40.61 o 3 1 2 911.79 954.85 9.14 o 5 1 2 2355.78 2378.76 18.94 o 7 1 2 132.74 163.36 3.10 o 9 1 2 288.25 299.81 4.22 o 11 1 2 287.56 272.36 4.44 o 13 1 2 3.17 1.07 1.04 o 15 1 2 10.18 12.29 1.85 o -16 2 2 5.75 4.27 1.37 o -14 2 2 12.37 12.78 1.53 o -12 2 2 95.72 85.80 2.73 o -10 2 2 7.41 6.70 1.01 o -8 2 2 895.37 929.94 7.48 o -6 2 2 2602.57 2474.82 17.31 o -4 2 2 1709.62 1760.10 15.72 o -2 2 2 1488.57 1408.14 11.57 o 0 2 2 5386.36 5184.75 146.85 o 2 2 2 4980.20 4624.22 62.43 o 4 2 2 141.53 150.11 2.57 o 6 2 2 259.55 286.87 3.31 o 8 2 2 110.04 122.78 3.82 o 10 2 2 123.32 119.63 2.85 o 12 2 2 27.11 30.17 1.96 o 14 2 2 13.61 16.53 2.14 o 16 2 2 11.42 5.81 2.26 o -15 3 2 19.33 22.28 2.00 o -13 3 2 216.30 216.08 4.36 o -11 3 2 90.74 88.11 2.70 o -9 3 2 76.10 78.13 2.30 o -7 3 2 1397.37 1432.30 13.77 o -5 3 2 561.36 558.54 6.35 o -3 3 2 513.64 551.29 6.81 o -1 3 2 1520.09 1579.77 14.70 o 1 3 2 0.84 0.39 0.65 o 3 3 2 264.91 267.29 3.90 o 5 3 2 2050.28 2168.14 15.36 o 7 3 2 324.44 356.97 4.61 o 9 3 2 73.61 86.36 2.56 o 11 3 2 183.06 161.62 3.66 o 13 3 2 13.44 14.35 1.63 o 15 3 2 3.74 3.80 1.52 o -14 4 2 4.61 0.94 1.28 o -12 4 2 15.84 18.46 1.69 o -10 4 2 7.34 5.50 1.43 o -8 4 2 544.76 543.34 6.63 o -6 4 2 664.20 715.60 8.13 o -4 4 2 246.22 262.31 5.66 o -2 4 2 998.19 1006.08 8.89 o 0 4 2 694.48 722.94 7.51 o 2 4 2 264.51 278.36 4.09 o 4 4 2 488.44 490.66 6.19 o 6 4 2 96.32 91.77 2.37 o 8 4 2 288.50 294.83 4.55 o 10 4 2 84.11 79.03 2.76 o 12 4 2 27.58 31.21 2.15 o 14 4 2 13.79 12.71 1.78 o -13 5 2 23.58 19.12 2.74 o -11 5 2 22.17 22.26 1.83 o -9 5 2 311.49 325.15 5.51 o -7 5 2 124.78 125.88 3.52 o -5 5 2 341.30 338.66 6.29 o -3 5 2 402.68 439.55 6.27 o -1 5 2 803.92 850.04 13.49 o 1 5 2 95.57 105.42 4.32 o 3 5 2 213.05 205.54 3.44 o 5 5 2 59.61 54.20 2.43 o 7 5 2 46.95 56.56 2.29 o 9 5 2 303.21 300.90 5.01 o 11 5 2 29.39 23.54 3.59 o 13 5 2 0.22 0.00 1.24 o -12 6 2 5.61 2.06 1.57 o -10 6 2 2.97 2.78 1.44 o -8 6 2 213.37 224.02 6.20 o -6 6 2 138.42 155.54 4.62 o -4 6 2 32.79 32.75 2.28 o -2 6 2 165.24 131.74 6.55 o 0 6 2 27.27 28.98 1.98 o 2 6 2 285.13 249.71 5.51 o 4 6 2 93.11 81.64 3.11 o 6 6 2 329.65 311.02 5.30 o 8 6 2 31.30 32.77 2.17 o 10 6 2 82.55 77.16 5.15 o 12 6 2 20.49 24.26 2.20 o -11 7 2 1.02 0.00 2.53 o -9 7 2 6.77 5.25 3.22 o -7 7 2 74.98 72.94 4.58 o -5 7 2 72.44 72.59 4.57 o -3 7 2 107.88 109.93 4.49 o -1 7 2 144.10 143.48 4.92 o 1 7 2 2.18 0.00 1.69 o 3 7 2 49.58 50.05 4.05 o 5 7 2 163.79 183.46 6.06 o 7 7 2 72.70 82.18 4.68 o 9 7 2 11.16 8.77 3.13 o -8 8 2 17.75 16.88 4.94 o -6 8 2 91.79 97.97 7.90 o -4 8 2 37.41 43.53 4.66 o -2 8 2 69.32 54.79 12.72 o 0 8 2 55.24 53.41 4.24 o 2 8 2 74.98 74.85 4.36 o 4 8 2 123.67 139.00 5.83 o 6 8 2 0.86 0.00 3.16 o -3 9 2 29.48 29.95 7.40 o -1 9 2 31.09 37.62 8.90 o 1 9 2 0.02 2.70 5.82 o 3 9 2 0.33 7.75 6.21 o -16 0 3 0.75 0.00 2.45 o -14 0 3 314.98 306.81 14.38 o -12 0 3 53.14 56.01 4.63 o -10 0 3 33.38 35.95 2.49 o -8 0 3 3044.17 3029.92 32.13 o -6 0 3 5172.91 5173.35 54.15 o -2 0 3 260.83 277.08 4.14 o 0 0 3 1134.71 1121.24 13.72 o 2 0 3 544.72 512.03 7.11 o 4 0 3 554.27 537.99 9.94 o 6 0 3 14.55 14.82 1.37 o 8 0 3 502.94 491.88 8.23 o 10 0 3 13.76 15.06 2.03 o 12 0 3 268.57 269.86 7.12 o 14 0 3 0.85 0.89 1.64 o 16 0 3 8.63 7.42 4.05 o -17 1 3 0.08 0.00 1.32 o -15 1 3 31.31 30.49 2.21 o -13 1 3 150.56 158.32 3.63 o -11 1 3 126.48 121.71 2.79 o -9 1 3 73.49 74.01 2.48 o -7 1 3 2099.46 2024.01 15.20 o -5 1 3 781.83 702.93 7.59 o -3 1 3 194.18 189.93 2.48 o -1 1 3 44956.57 46429.22 404.84 o 1 1 3 1617.53 1645.52 14.05 o 3 1 3 210.40 222.77 4.27 o 5 1 3 13.28 13.71 1.21 o 7 1 3 718.63 708.49 6.34 o 9 1 3 343.25 355.45 4.75 o 11 1 3 277.77 274.58 4.54 o 13 1 3 140.16 141.42 3.87 o 15 1 3 4.11 4.77 1.64 o -16 2 3 0.28 1.78 1.29 o -14 2 3 9.91 8.44 1.39 o -12 2 3 247.41 237.85 5.22 o -10 2 3 114.33 118.50 3.27 o -8 2 3 3048.13 3037.98 19.13 o -6 2 3 1346.17 1304.84 11.06 o -4 2 3 271.38 303.67 3.86 o -2 2 3 495.76 542.65 5.40 o 0 2 3 2170.16 2099.94 28.94 o 2 2 3 94.80 111.77 2.09 o 4 2 3 181.17 216.30 3.39 o 6 2 3 1647.77 1697.22 11.76 o 8 2 3 132.59 128.83 2.73 o 10 2 3 254.64 251.47 6.04 o 12 2 3 29.91 31.10 2.02 o 14 2 3 2.96 2.85 1.37 o -15 3 3 8.19 7.04 1.41 o -13 3 3 17.47 19.61 1.69 o -11 3 3 207.47 192.32 3.69 o -9 3 3 380.42 384.80 6.53 o -7 3 3 606.03 637.27 6.53 o -5 3 3 1364.73 1371.36 10.89 o -3 3 3 21.19 25.09 1.23 o -1 3 3 1430.70 1373.55 33.64 o 1 3 3 498.45 480.68 9.49 o 3 3 3 128.73 121.05 2.31 o 5 3 3 5.31 6.72 1.30 o 7 3 3 687.45 678.29 9.75 o 9 3 3 32.15 31.55 2.10 o 11 3 3 56.49 48.46 2.34 o 13 3 3 20.67 25.48 2.03 o 15 3 3 1.17 0.94 1.93 o -14 4 3 32.19 27.89 2.16 o -12 4 3 14.72 11.73 1.51 o -10 4 3 38.15 38.46 2.10 o -8 4 3 549.66 536.21 8.44 o -6 4 3 61.15 64.27 2.06 o -4 4 3 1655.42 1644.43 13.09 o -2 4 3 214.87 198.30 4.63 o 0 4 3 92.89 96.98 2.44 o 2 4 3 835.30 809.60 12.02 o 4 4 3 327.93 323.11 5.68 o 6 4 3 1074.65 1016.28 9.17 o 8 4 3 393.98 403.38 5.51 o 10 4 3 50.29 57.35 3.80 o 12 4 3 4.08 2.55 1.18 o 14 4 3 1.51 0.18 1.40 o -13 5 3 18.27 14.81 2.08 o -11 5 3 81.79 79.78 3.48 o -9 5 3 34.87 39.06 3.00 o -7 5 3 112.93 99.97 3.65 o -5 5 3 104.84 102.26 2.88 o -3 5 3 80.32 73.46 2.41 o -1 5 3 115.50 118.83 3.87 o 1 5 3 81.81 77.56 2.67 o 3 5 3 126.64 124.91 2.88 o 5 5 3 192.79 197.70 6.05 o 7 5 3 311.58 313.56 4.86 o 9 5 3 31.96 30.87 2.15 o 11 5 3 0.80 1.12 1.19 o 13 5 3 9.75 13.51 2.80 o -12 6 3 32.11 37.41 3.47 o -10 6 3 9.47 5.55 1.73 o -8 6 3 231.62 241.26 6.35 o -6 6 3 248.51 246.39 11.22 o -4 6 3 75.36 66.70 3.48 o -2 6 3 19.54 21.11 2.45 o 0 6 3 152.91 148.99 6.86 o 2 6 3 131.91 134.56 3.95 o 4 6 3 1421.86 1382.23 13.88 o 6 6 3 350.70 340.45 6.84 o 8 6 3 25.15 30.37 2.86 o 10 6 3 30.75 32.69 4.80 o -11 7 3 6.50 4.40 1.96 o -9 7 3 50.36 50.18 3.69 o -7 7 3 11.86 10.23 2.60 o -5 7 3 116.65 120.76 4.92 o -3 7 3 53.88 43.95 3.68 o -1 7 3 173.70 171.08 9.31 o 1 7 3 20.31 20.39 2.63 o 3 7 3 97.71 100.49 6.46 o 5 7 3 51.37 53.98 3.98 o 7 7 3 105.31 115.50 7.85 o 9 7 3 26.72 30.24 3.63 o -8 8 3 19.70 16.63 2.72 o -6 8 3 33.20 29.57 4.50 o -4 8 3 58.09 63.92 4.19 o -2 8 3 13.81 15.78 5.49 o 0 8 3 12.71 10.59 4.05 o 2 8 3 123.43 141.01 5.70 o 4 8 3 73.85 81.51 4.85 o 6 8 3 73.16 71.32 4.89 o -3 9 3 16.91 22.94 3.51 o -1 9 3 14.00 10.61 3.04 o 1 9 3 12.91 4.20 3.46 o -16 0 4 4.42 4.48 1.95 o -14 0 4 63.19 57.02 5.67 o -12 0 4 155.33 148.37 6.27 o -10 0 4 164.93 163.49 4.38 o -8 0 4 24.03 28.34 1.87 o -6 0 4 255.78 240.09 5.04 o -4 0 4 6801.99 6753.27 125.38 o -2 0 4 18865.63 19280.96 190.73 o 0 0 4 39.23 27.02 2.12 o 2 0 4 82.39 75.76 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