#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219817.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219817_Fobs loop_ _publ_author_name 'Xie, Hong-Zhen' 'Pan, Wei-Juan' 'Xu, Wei' 'Lin, Jian-Li' _publ_section_title ; \m-\a-Methylglutarato-bis{aqua[bis(2-pyridylcarbonyl)aminato]copper(II)} trihydrate ; _journal_coeditor_code CS2084 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1471 _journal_page_last m1472 _journal_volume 64 _journal_year 2008 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2712 _cell_length_b 26.9097 _cell_length_c 34.2072 _exptl_crystal_F_000 3344.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file cs2084Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Cu2(C10H8N3O2)2(C6H8O4)(H2O)2].3H2O in Pbcn' _shelx_refln_list_code 4 _shelx_F_calc_maximum 678.70 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 75993.16 84891.77 1434.77 o 4 0 0 5032.17 5374.57 100.24 o 6 0 0 2.54 41.35 59.80 o 8 0 0 2435.86 2646.81 144.73 o 3 1 0 367.85 428.12 29.21 o 5 1 0 761.32 765.40 55.44 o 7 1 0 103.42 73.48 30.80 o 9 1 0 128.17 68.10 53.27 o 2 2 0 53075.35 59588.52 636.70 o 4 2 0 1380.10 1569.15 60.57 o 6 2 0 45.10 37.02 24.41 o 8 2 0 303.98 358.38 48.70 o 1 3 0 208990.19 234575.53 4968.91 o 3 3 0 19297.53 19817.05 181.33 o 5 3 0 76.81 278.60 47.55 o 7 3 0 706.17 768.48 53.61 o 9 3 0 790.89 927.76 67.09 o 0 4 0 127.46 192.13 72.13 o 2 4 0 3429.49 3033.91 43.50 o 4 4 0 1479.83 1586.46 47.01 o 6 4 0 64.99 39.08 33.74 o 8 4 0 105.20 196.30 66.50 o 1 5 0 17567.55 16174.38 137.95 o 3 5 0 59235.49 59586.59 712.06 o 5 5 0 3101.53 2895.35 90.27 o 7 5 0 552.16 641.86 57.82 o 9 5 0 1126.63 1430.40 144.41 o 0 6 0 12214.80 11338.25 159.39 o 2 6 0 1960.03 1855.06 36.35 o 4 6 0 196.16 190.75 35.63 o 6 6 0 63.21 67.11 49.85 o 8 6 0 20.68 35.34 46.24 o 1 7 0 115.28 176.33 23.29 o 3 7 0 22357.72 22365.73 233.25 o 5 7 0 621.48 724.64 37.09 o 7 7 0 265.96 254.17 55.19 o 9 7 0 191.63 110.26 93.29 o 0 8 0 60302.00 60089.65 1142.18 o 2 8 0 75030.88 72656.33 1026.69 o 4 8 0 3131.66 3137.22 51.71 o 6 8 0 4.16 115.46 51.57 o 8 8 0 1210.61 1441.35 79.13 o 1 9 0 3405.21 3137.72 55.53 o 3 9 0 46.67 87.73 18.11 o 5 9 0 4400.22 4500.54 122.74 o 7 9 0 5.42 -31.09 47.33 o 9 9 0 1.82 50.70 73.77 o 0 10 0 1526.43 1730.18 93.29 o 2 10 0 2917.70 3483.66 67.82 o 4 10 0 148.46 163.55 30.67 o 6 10 0 871.83 989.81 81.72 o 8 10 0 84.46 22.89 67.36 o 1 11 0 1102.60 938.91 47.09 o 3 11 0 15826.90 16485.61 253.81 o 5 11 0 18.46 98.37 33.03 o 7 11 0 914.48 1176.11 90.04 o 0 12 0 6555.10 5699.45 118.42 o 2 12 0 13315.75 12938.83 137.07 o 4 12 0 3022.15 2793.11 69.57 o 6 12 0 651.75 571.18 57.09 o 8 12 0 922.19 998.56 76.82 o 1 13 0 16751.81 15515.48 192.58 o 3 13 0 6915.53 6195.70 93.03 o 5 13 0 2.95 12.51 28.19 o 7 13 0 5.86 -12.44 37.28 o 0 14 0 25638.72 27569.21 543.18 o 2 14 0 223.81 327.69 33.58 o 4 14 0 2.37 -31.37 31.44 o 6 14 0 5.71 -5.88 31.26 o 8 14 0 75.65 131.33 45.40 o 1 15 0 48376.61 45804.26 664.79 o 3 15 0 2979.04 2795.22 140.08 o 5 15 0 3402.74 3607.61 103.13 o 7 15 0 1168.95 1328.35 97.59 o 0 16 0 5711.89 5139.08 477.93 o 2 16 0 5334.91 5145.27 193.40 o 4 16 0 1402.53 1459.88 48.78 o 6 16 0 157.34 151.80 42.15 o 8 16 0 264.04 258.63 50.78 o 1 17 0 12504.56 12600.46 223.09 o 3 17 0 1686.47 1667.61 88.05 o 5 17 0 106.57 144.79 49.36 o 7 17 0 274.85 387.98 56.45 o 0 18 0 4262.11 3832.20 128.68 o 2 18 0 1332.93 1407.50 49.94 o 4 18 0 1155.59 1227.68 74.26 o 6 18 0 11.62 64.71 41.96 o 8 18 0 3.92 -5.32 43.75 o 1 19 0 4222.50 4371.86 379.52 o 3 19 0 1765.44 1854.88 76.62 o 5 19 0 395.86 456.11 63.72 o 7 19 0 20.03 -53.07 53.07 o 0 20 0 80484.86 79185.02 1982.49 o 2 20 0 28724.31 29117.64 410.15 o 4 20 0 8878.81 8584.41 185.91 o 6 20 0 942.94 1006.42 62.13 o 1 21 0 2062.81 2007.65 81.62 o 3 21 0 152.70 148.31 66.26 o 5 21 0 1484.35 1553.18 74.88 o 7 21 0 212.36 144.28 51.14 o 0 22 0 591.74 405.38 83.68 o 2 22 0 3737.78 3742.37 94.16 o 4 22 0 3741.05 3522.13 145.82 o 6 22 0 1340.24 1218.10 65.19 o 1 23 0 14640.67 14792.07 238.87 o 3 23 0 3509.23 3346.75 100.40 o 5 23 0 229.20 74.85 35.41 o 7 23 0 424.49 322.18 58.15 o 0 24 0 560.42 566.67 98.20 o 2 24 0 677.52 807.92 60.96 o 4 24 0 41.17 40.67 46.77 o 6 24 0 672.03 537.65 84.66 o 1 25 0 5388.39 5887.27 134.18 o 3 25 0 213.94 200.47 63.37 o 5 25 0 195.57 188.20 68.55 o 0 26 0 6000.49 5918.61 210.31 o 2 26 0 77.15 63.52 45.50 o 4 26 0 12.49 27.45 53.71 o 6 26 0 13.78 -55.29 55.29 o 1 27 0 2632.99 2623.00 96.61 o 3 27 0 37.09 26.89 63.52 o 5 27 0 180.48 77.85 46.14 o 0 28 0 5463.44 5819.76 226.40 o 2 28 0 7984.59 8534.85 187.38 o 4 28 0 517.90 540.76 123.31 o 1 29 0 9.65 4.30 68.25 o 3 29 0 0.08 -37.76 62.26 o 5 29 0 5.06 -70.95 70.95 o 0 30 0 3248.35 3094.29 180.87 o 2 30 0 27.00 34.62 55.38 o 4 30 0 106.39 100.60 60.42 o 1 31 0 4040.48 4523.46 172.14 o 3 31 0 971.41 1185.79 129.63 o 0 32 0 2345.48 2865.50 197.47 o 2 32 0 818.68 891.77 77.76 o 1 33 0 184.36 184.41 69.84 o 3 33 0 10.86 81.00 70.67 o 0 34 0 165.70 96.46 109.30 o 2 34 0 29.31 137.40 83.78 o 2 1 1 150813.05 175244.89 1945.79 o 3 1 1 24323.43 25395.76 170.62 o 4 1 1 1801.14 1381.88 26.41 o 5 1 1 1624.15 1650.74 43.87 o 6 1 1 1828.82 1927.76 39.18 o 7 1 1 170.74 157.95 32.86 o 8 1 1 1158.97 1098.71 83.94 o 9 1 1 103.08 115.25 72.63 o 1 2 1 16309.16 18810.50 95.13 o 2 2 1 35592.16 39789.91 279.82 o 3 2 1 9915.72 10374.77 67.53 o 4 2 1 1404.99 1506.65 24.18 o 5 2 1 164.39 176.39 20.86 o 6 2 1 259.14 297.24 31.55 o 7 2 1 203.93 200.23 33.01 o 8 2 1 3.88 14.99 36.12 o 9 2 1 35.75 -0.20 37.28 o 1 3 1 45192.45 47043.70 368.50 o 2 3 1 13095.43 13569.54 81.13 o 3 3 1 20854.99 20054.09 135.13 o 4 3 1 6337.60 6325.70 81.89 o 5 3 1 137.49 140.24 21.61 o 6 3 1 2164.23 2238.36 51.46 o 7 3 1 0.86 21.08 27.06 o 8 3 1 721.72 781.46 50.40 o 9 3 1 207.15 194.58 60.47 o 0 4 1 68841.59 73975.41 955.47 o 1 4 1 17922.88 17073.17 98.79 o 2 4 1 4455.99 3957.60 30.98 o 3 4 1 38394.20 37882.71 269.65 o 4 4 1 2992.95 2924.81 35.96 o 5 4 1 10566.29 9993.88 85.00 o 6 4 1 323.25 318.27 25.52 o 7 4 1 4941.51 5169.91 83.13 o 8 4 1 1570.48 1648.30 86.20 o 9 4 1 934.13 1140.55 331.39 o 1 5 1 3800.39 4080.02 28.37 o 2 5 1 242.82 175.94 13.90 o 3 5 1 4.16 34.23 14.52 o 4 5 1 286.52 276.61 19.75 o 5 5 1 963.92 1089.09 26.57 o 6 5 1 0.03 59.39 26.66 o 7 5 1 389.80 426.16 33.85 o 8 5 1 13.90 16.49 28.40 o 9 5 1 8.98 -68.07 68.07 o 0 6 1 59757.71 61141.49 799.74 o 1 6 1 21795.44 23412.84 148.92 o 2 6 1 2307.10 2601.90 35.52 o 3 6 1 126.27 113.43 14.14 o 4 6 1 931.00 924.14 23.64 o 5 6 1 30.76 30.62 19.05 o 6 6 1 569.17 779.82 39.29 o 7 6 1 10.36 28.93 32.11 o 8 6 1 65.58 96.52 55.48 o 9 6 1 4.03 42.41 75.90 o 1 7 1 6273.43 6023.68 48.00 o 2 7 1 2772.03 2731.49 30.14 o 3 7 1 126.24 189.15 16.29 o 4 7 1 7179.85 6823.01 70.14 o 5 7 1 520.81 545.63 32.07 o 6 7 1 3703.65 3833.27 73.67 o 7 7 1 592.59 615.35 54.15 o 8 7 1 388.89 401.03 47.10 o 9 7 1 180.85 136.98 42.38 o 0 8 1 6688.12 7017.80 86.41 o 1 8 1 26527.96 26852.18 219.56 o 2 8 1 688.86 662.86 22.56 o 3 8 1 8633.44 8822.62 87.01 o 4 8 1 1578.78 1564.55 39.25 o 5 8 1 6046.55 6342.11 92.62 o 6 8 1 208.80 275.99 38.02 o 7 8 1 1494.87 1558.80 59.04 o 8 8 1 398.73 529.40 67.61 o 9 8 1 73.75 146.69 62.28 o 1 9 1 6461.77 5390.39 49.96 o 2 9 1 7628.01 7515.35 63.95 o 3 9 1 8111.15 8031.44 59.76 o 4 9 1 16226.05 15885.94 137.72 o 5 9 1 1101.48 1106.51 29.96 o 6 9 1 7374.72 7642.62 99.69 o 7 9 1 106.97 149.08 36.22 o 8 9 1 1059.79 1160.07 76.69 o 9 9 1 84.00 93.36 49.97 o 0 10 1 24410.41 24622.23 277.05 o 1 10 1 3436.29 3985.47 41.82 o 2 10 1 39.82 52.82 16.88 o 3 10 1 314.42 296.97 22.21 o 4 10 1 3310.16 3502.37 56.15 o 5 10 1 280.71 327.45 26.81 o 6 10 1 243.28 197.96 30.21 o 7 10 1 179.77 116.66 34.18 o 8 10 1 30.46 26.02 50.47 o 9 10 1 3.23 -36.81 51.26 o 1 11 1 3347.08 2898.38 45.03 o 2 11 1 1764.22 1614.35 36.21 o 3 11 1 4496.44 4303.39 48.39 o 4 11 1 26912.56 27222.48 209.54 o 5 11 1 5785.22 6022.29 67.86 o 6 11 1 8376.60 7889.27 116.74 o 7 11 1 558.38 607.18 50.24 o 8 11 1 860.59 868.73 52.49 o 0 12 1 9493.25 9377.51 111.76 o 1 12 1 5.68 13.39 20.51 o 2 12 1 7743.18 7140.08 70.98 o 3 12 1 6940.27 6816.19 90.85 o 4 12 1 11744.39 12178.55 109.42 o 5 12 1 7716.18 7980.34 87.23 o 6 12 1 38.14 83.08 23.03 o 7 12 1 2082.77 2006.60 48.30 o 8 12 1 600.96 606.30 49.02 o 1 13 1 36.36 24.44 16.92 o 2 13 1 1304.62 1475.35 27.95 o 3 13 1 3091.94 3250.79 67.23 o 4 13 1 2847.96 2702.14 44.53 o 5 13 1 147.83 109.46 28.47 o 6 13 1 128.70 105.25 25.11 o 7 13 1 414.11 422.45 36.94 o 8 13 1 5.71 4.82 25.82 o 0 14 1 183.68 218.14 36.21 o 1 14 1 273.67 354.64 22.84 o 2 14 1 4288.73 4528.25 50.61 o 3 14 1 399.35 492.24 28.50 o 4 14 1 1442.78 1502.49 35.77 o 5 14 1 134.83 114.37 27.03 o 6 14 1 814.88 762.80 43.15 o 7 14 1 387.17 333.42 41.28 o 8 14 1 6.86 24.43 34.75 o 1 15 1 1431.25 1717.93 77.08 o 2 15 1 108.73 98.27 21.43 o 3 15 1 593.79 584.77 34.46 o 4 15 1 1079.50 1105.05 46.73 o 5 15 1 0.24 15.18 25.41 o 6 15 1 920.15 892.96 60.91 o 7 15 1 98.26 101.34 32.49 o 8 15 1 23.69 18.79 32.75 o 0 16 1 25189.95 24906.23 341.53 o 1 16 1 4044.55 3776.58 54.20 o 2 16 1 16576.64 15757.55 132.35 o 3 16 1 4056.23 3884.94 67.53 o 4 16 1 2040.46 1886.91 47.02 o 5 16 1 1711.64 1749.80 54.70 o 6 16 1 407.33 392.13 41.51 o 7 16 1 2609.51 2450.30 73.67 o 8 16 1 545.50 537.01 57.75 o 1 17 1 3121.36 2879.29 64.26 o 2 17 1 35.07 29.05 20.47 o 3 17 1 3283.72 3088.22 62.68 o 4 17 1 506.46 445.38 48.58 o 5 17 1 119.69 139.08 32.47 o 6 17 1 2552.15 2649.84 58.66 o 7 17 1 16.13 29.47 30.91 o 8 17 1 232.75 223.82 49.35 o 0 18 1 3.02 -6.63 30.97 o 1 18 1 1881.67 1952.94 59.83 o 2 18 1 240.83 249.06 28.53 o 3 18 1 268.44 264.73 36.67 o 4 18 1 514.61 586.67 49.79 o 5 18 1 67.14 96.22 32.96 o 6 18 1 7.84 40.07 32.66 o 7 18 1 10.90 -23.60 28.66 o 8 18 1 54.55 39.52 36.25 o 1 19 1 25477.74 26377.79 276.65 o 2 19 1 1225.33 1239.45 38.11 o 3 19 1 4992.46 4701.40 88.45 o 4 19 1 6740.90 6766.58 117.38 o 5 19 1 722.89 655.49 40.46 o 6 19 1 1907.59 1895.89 55.53 o 7 19 1 813.53 876.41 55.97 o 0 20 1 21.20 1339.02 110.84 o 1 20 1 4078.62 3900.47 82.89 o 2 20 1 748.77 791.16 40.18 o 3 20 1 3320.01 3249.94 85.68 o 4 20 1 12.01 -43.78 43.78 o 5 20 1 1165.50 1149.97 58.17 o 6 20 1 16.29 50.99 40.70 o 7 20 1 14.02 37.87 32.77 o 1 21 1 529.78 509.34 38.90 o 2 21 1 605.81 605.23 34.73 o 3 21 1 2427.00 2242.13 78.99 o 4 21 1 3157.34 3044.23 76.71 o 5 21 1 0.47 -19.30 36.07 o 6 21 1 183.50 155.21 38.71 o 7 21 1 417.90 398.74 46.01 o 0 22 1 3758.32 3360.22 102.39 o 1 22 1 3378.57 3369.42 78.71 o 2 22 1 56.53 61.31 23.84 o 3 22 1 5506.59 5521.64 103.91 o 4 22 1 711.50 675.16 46.43 o 5 22 1 576.31 639.05 66.98 o 6 22 1 340.97 283.14 45.09 o 7 22 1 10.96 50.62 36.60 o 1 23 1 6.91 -2.69 32.87 o 2 23 1 332.03 335.03 34.64 o 3 23 1 1199.49 1250.86 59.46 o 4 23 1 48.09 86.66 41.54 o 5 23 1 722.21 650.27 48.93 o 6 23 1 1112.67 1265.23 65.70 o 7 23 1 8.56 7.01 36.40 o 0 24 1 4519.67 4495.68 111.13 o 1 24 1 678.34 710.22 43.01 o 2 24 1 3896.75 3876.83 63.42 o 3 24 1 2238.29 2347.95 73.38 o 4 24 1 856.62 836.22 62.05 o 5 24 1 2789.55 2840.05 78.04 o 6 24 1 28.90 -2.53 36.21 o 1 25 1 673.50 662.97 53.84 o 2 25 1 525.33 484.75 45.32 o 3 25 1 69.54 73.25 31.97 o 4 25 1 215.10 164.70 49.62 o 5 25 1 1231.32 1235.65 55.48 o 6 25 1 7.01 -32.82 32.82 o 0 26 1 43.33 50.85 47.82 o 1 26 1 403.94 387.26 42.01 o 2 26 1 3.13 17.99 29.07 o 3 26 1 350.30 259.83 44.13 o 4 26 1 77.13 96.50 37.68 o 5 26 1 311.81 206.81 44.43 o 6 26 1 153.78 40.83 39.16 o 1 27 1 2297.32 2149.54 73.81 o 2 27 1 47.35 48.53 35.68 o 3 27 1 1307.44 1188.15 51.87 o 4 27 1 606.53 543.34 60.34 o 5 27 1 21.27 15.03 38.06 o 0 28 1 3.05 44.86 56.32 o 1 28 1 736.94 620.39 54.44 o 2 28 1 203.38 145.47 36.24 o 3 28 1 230.76 206.67 50.77 o 4 28 1 14.08 26.14 45.94 o 5 28 1 144.45 122.61 39.42 o 1 29 1 1344.51 1604.62 64.60 o 2 29 1 523.80 494.37 43.22 o 3 29 1 61.21 2.09 35.10 o 4 29 1 606.03 605.56 55.89 o 5 29 1 99.38 106.62 37.77 o 0 30 1 25.63 86.92 59.17 o 1 30 1 399.81 420.59 61.43 o 2 30 1 12.25 56.35 35.03 o 3 30 1 427.71 465.28 57.93 o 4 30 1 2.50 24.19 47.22 o 1 31 1 839.75 921.43 82.70 o 2 31 1 677.98 637.90 55.38 o 3 31 1 736.50 899.46 65.88 o 4 31 1 591.69 591.33 54.53 o 0 32 1 2374.72 2693.65 152.46 o 1 32 1 56.61 138.95 47.87 o 2 32 1 607.66 775.86 52.92 o 3 32 1 475.48 561.49 64.00 o 1 33 1 72.02 141.37 59.88 o 2 33 1 83.66 94.91 42.41 o 3 33 1 30.85 223.96 62.30 o 0 34 1 1601.86 1915.71 125.47 o 1 34 1 3.09 -39.12 46.23 o 2 34 1 154.96 175.65 47.37 o 1 0 2 6890.64 6734.59 40.28 o 2 0 2 36885.29 39471.32 435.89 o 3 0 2 68093.52 70288.23 831.76 o 4 0 2 10918.73 11648.04 118.67 o 5 0 2 6513.52 6283.65 90.91 o 6 0 2 139.07 239.58 37.63 o 7 0 2 3666.31 4037.46 98.83 o 8 0 2 11.30 -24.92 46.18 o 9 0 2 358.97 309.58 82.75 o 1 1 2 31691.72 35110.91 209.75 o 2 1 2 18984.68 19631.33 123.62 o 3 1 2 4204.49 4638.22 46.33 o 4 1 2 225.13 159.33 19.27 o 5 1 2 27.31 35.94 17.14 o 6 1 2 354.60 419.88 29.31 o 7 1 2 110.15 91.86 32.86 o 8 1 2 717.30 920.87 59.67 o 9 1 2 103.78 96.66 44.55 o 1 2 2 12461.78 13486.45 66.00 o 2 2 2 15448.11 16200.34 100.31 o 3 2 2 4514.00 4388.48 38.19 o 4 2 2 8.16 45.24 14.31 o 5 2 2 1440.61 1393.32 39.80 o 6 2 2 170.71 219.37 27.10 o 7 2 2 436.15 379.47 33.34 o 8 2 2 143.42 192.24 38.77 o 9 2 2 168.71 146.75 56.08 o 1 3 2 11716.29 13113.05 79.82 o 2 3 2 4941.44 5212.63 32.99 o 3 3 2 306.73 245.02 16.62 o 4 3 2 30129.84 30295.32 218.91 o 5 3 2 112.33 132.81 20.47 o 6 3 2 6685.58 6742.11 78.44 o 7 3 2 136.06 115.90 29.22 o 8 3 2 53.24 67.97 51.11 o 9 3 2 18.73 37.50 49.02 o 0 4 2 9577.28 10747.47 87.68 o 1 4 2 9951.82 9583.96 55.79 o 2 4 2 8391.68 7793.70 53.82 o 3 4 2 2633.70 2630.41 39.80 o 4 4 2 35.84 70.51 18.40 o 5 4 2 2370.41 2122.33 39.33 o 6 4 2 423.67 456.32 32.46 o 7 4 2 3390.54 3389.09 70.28 o 8 4 2 283.37 178.33 34.57 o 9 4 2 111.31 103.52 89.37 o 1 5 2 11302.47 11543.30 71.96 o 2 5 2 4291.44 4344.96 35.97 o 3 5 2 2594.90 2600.48 35.02 o 4 5 2 9203.14 8457.09 67.25 o 5 5 2 47.56 45.07 17.86 o 6 5 2 3937.51 3964.80 53.79 o 7 5 2 235.63 210.81 36.93 o 8 5 2 2019.03 1829.88 222.68 o 9 5 2 0.22 12.62 63.44 o 0 6 2 6496.22 6589.94 66.10 o 1 6 2 1497.08 1489.44 33.15 o 2 6 2 5147.42 4496.06 38.15 o 3 6 2 362.19 403.50 18.00 o 4 6 2 26.67 50.31 15.16 o 5 6 2 84.79 76.91 24.49 o 6 6 2 102.18 69.82 27.72 o 7 6 2 20.22 13.07 35.22 o 8 6 2 7.08 21.83 36.91 o 9 6 2 207.06 182.32 55.53 o 1 7 2 912.23 1102.41 26.52 o 2 7 2 3315.82 3163.29 29.96 o 3 7 2 7781.65 7517.19 62.26 o 4 7 2 25935.38 24792.17 198.47 o 5 7 2 57.93 53.60 22.26 o 6 7 2 8065.72 8274.86 105.92 o 7 7 2 13.15 -14.54 27.70 o 8 7 2 1399.06 1635.79 72.61 o 9 7 2 0.23 -71.29 71.29 o 0 8 2 24161.33 25096.16 272.78 o 1 8 2 27425.60 26811.67 211.25 o 2 8 2 305.56 405.49 25.27 o 3 8 2 41237.99 40673.02 316.66 o 4 8 2 699.37 712.51 26.51 o 5 8 2 30461.31 31030.89 306.53 o 6 8 2 42.65 61.62 27.30 o 7 8 2 7855.83 7661.25 131.29 o 8 8 2 12.79 1.64 37.79 o 9 8 2 603.09 735.38 64.71 o 1 9 2 11678.27 11262.35 93.91 o 2 9 2 2998.17 3275.41 49.42 o 3 9 2 1061.90 968.66 22.49 o 4 9 2 8064.56 8347.02 78.78 o 5 9 2 223.73 300.74 32.82 o 6 9 2 1535.12 1578.97 55.11 o 7 9 2 227.58 229.14 40.74 o 8 9 2 11.60 9.81 38.30 o 9 9 2 90.37 -26.92 63.34 o 0 10 2 6380.34 6545.11 80.25 o 1 10 2 372.27 640.60 35.17 o 2 10 2 3384.97 3733.34 42.67 o 3 10 2 757.50 701.93 22.23 o 4 10 2 1941.68 1865.23 32.23 o 5 10 2 950.91 938.94 35.27 o 6 10 2 548.03 549.79 36.21 o 7 10 2 1116.76 1179.20 57.08 o 8 10 2 89.03 73.05 35.30 o 9 10 2 52.97 83.59 56.01 o 1 11 2 132.63 64.70 19.04 o 2 11 2 4139.95 4549.10 48.04 o 3 11 2 4120.76 4136.35 54.49 o 4 11 2 748.39 832.14 41.93 o 5 11 2 56.12 41.47 25.56 o 6 11 2 7163.83 7427.13 99.24 o 7 11 2 204.08 139.47 30.68 o 8 11 2 176.34 146.85 46.50 o 0 12 2 8014.60 9630.30 123.85 o 1 12 2 30359.86 30671.45 281.32 o 2 12 2 1371.12 1273.50 75.82 o 3 12 2 20252.09 19895.64 186.38 o 4 12 2 1024.40 1112.84 47.85 o 5 12 2 20488.53 20091.78 169.28 o 6 12 2 26.21 45.99 24.27 o 7 12 2 4278.90 4264.45 85.05 o 8 12 2 97.41 113.12 35.28 o 1 13 2 5730.16 6083.55 66.22 o 2 13 2 11144.36 10708.08 101.68 o 3 13 2 242.99 291.56 29.42 o 4 13 2 3775.05 3322.47 57.65 o 5 13 2 7.96 11.80 20.42 o 6 13 2 3480.27 3501.41 67.08 o 7 13 2 1.07 17.96 28.32 o 8 13 2 283.70 285.21 46.33 o 0 14 2 2391.71 1997.82 54.45 o 1 14 2 85.70 149.99 23.02 o 2 14 2 1900.43 1529.15 30.34 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5 28 292.63 346.69 166.34 o 0 6 28 4388.63 4318.46 90.64 o 1 6 28 1531.94 1575.46 41.21 o 2 6 28 4.26 12.34 14.62 o 3 6 28 423.82 355.52 27.29 o 4 6 28 903.59 715.66 61.94 o 5 6 28 95.63 94.52 28.99 o 6 6 28 96.79 46.27 57.88 o 7 6 28 147.43 281.31 134.52 o 1 7 28 274.28 262.33 22.57 o 2 7 28 667.50 684.08 33.82 o 3 7 28 312.89 198.64 25.29 o 4 7 28 1004.27 966.61 62.40 o 5 7 28 1019.10 1056.28 85.03 o 6 7 28 614.50 534.24 52.97 o 7 7 28 94.44 89.97 98.07 o 0 8 28 30497.49 33452.97 1633.50 o 1 8 28 7.06 9.66 20.49 o 2 8 28 4571.40 4566.03 64.07 o 3 8 28 1125.80 1264.91 62.17 o 4 8 28 408.59 463.55 51.85 o 5 8 28 3605.29 3481.55 98.50 o 6 8 28 124.98 203.94 69.12 o 7 8 28 829.75 684.15 164.77 o 1 9 28 567.52 509.26 36.21 o 2 9 28 559.20 581.25 29.47 o 3 9 28 305.78 261.52 39.36 o 4 9 28 729.57 701.10 48.20 o 5 9 28 243.37 204.96 47.99 o 6 9 28 872.54 1023.17 78.04 o 0 10 28 50.47 86.76 39.74 o 1 10 28 22.42 34.34 20.33 o 2 10 28 2236.74 1988.20 59.83 o 3 10 28 15.40 14.84 31.55 o 4 10 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