#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/98/2219833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219833_Fobs loop_ _publ_author_name 'Jali, Samuel' 'Friedrich, Holger B.' 'Bala, Muhammad D.' _publ_section_title ; Dicarbonyl(\h^5^-cyclopentadienyl)bis(trimethylphosphine)molybdenum(II) trifluoromethanesulfonate ; _journal_coeditor_code DN2388 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1401 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.464 _cell_angle_gamma 90.000 _cell_length_a 10.8919 _cell_length_b 8.0864 _cell_length_c 23.4132 _exptl_crystal_F_000 1048.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file dn2388Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8m_kznd11_0a in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 355.17 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2291.78 2485.30 30.87 o 4 0 0 33179.42 34469.50 636.28 o 6 0 0 32010.98 30468.88 582.14 o 8 0 0 2183.61 2051.68 54.42 o 10 0 0 12142.58 12388.19 251.73 o 12 0 0 1669.93 1526.84 53.58 o 14 0 0 149.09 129.91 25.13 o 1 1 0 63048.07 63790.22 614.42 o 2 1 0 14037.68 14379.94 136.33 o 3 1 0 1880.74 1927.28 24.81 o 4 1 0 3115.86 3607.41 51.76 o 5 1 0 43266.95 41777.20 438.78 o 6 1 0 160.39 165.35 7.25 o 7 1 0 3647.91 3673.55 51.18 o 8 1 0 653.51 626.42 15.32 o 9 1 0 240.07 260.37 11.62 o 10 1 0 588.08 605.33 19.97 o 11 1 0 5380.19 5163.58 62.16 o 12 1 0 0.89 9.40 9.24 o 13 1 0 2017.65 1991.78 61.40 o 14 1 0 137.74 176.23 19.18 o 0 2 0 59834.11 56604.46 1497.73 o 1 2 0 24.01 43.88 3.43 o 2 2 0 197.20 245.90 5.90 o 3 2 0 2834.28 2481.48 54.49 o 4 2 0 5545.26 5722.32 136.54 o 5 2 0 753.69 862.66 26.84 o 6 2 0 10305.84 10336.56 102.29 o 7 2 0 1658.83 1713.85 20.13 o 8 2 0 24.72 44.90 6.06 o 9 2 0 1652.67 1577.33 31.26 o 10 2 0 4759.90 4605.42 83.01 o 11 2 0 494.00 494.85 19.38 o 12 2 0 131.83 127.37 13.22 o 13 2 0 804.87 856.87 31.58 o 14 2 0 211.14 235.12 21.11 o 1 3 0 811.02 827.58 40.28 o 2 3 0 8474.39 8049.07 126.94 o 3 3 0 949.46 986.36 15.43 o 4 3 0 583.05 477.60 17.36 o 5 3 0 327.78 296.18 11.00 o 6 3 0 20.79 28.15 4.34 o 7 3 0 291.75 243.45 32.61 o 8 3 0 5678.48 5259.49 49.11 o 9 3 0 25.27 24.44 7.54 o 10 3 0 1474.83 1433.02 48.47 o 11 3 0 0.94 9.34 9.01 o 12 3 0 1.26 25.95 10.12 o 13 3 0 13.63 9.24 10.61 o 0 4 0 3744.32 3644.02 100.78 o 1 4 0 1780.05 1764.18 23.82 o 2 4 0 5958.38 5998.36 149.54 o 3 4 0 25053.06 24470.83 443.34 o 4 4 0 682.47 696.31 14.81 o 5 4 0 221.95 234.91 10.21 o 6 4 0 449.83 511.75 19.81 o 7 4 0 4835.15 4572.44 66.69 o 8 4 0 640.69 624.42 19.22 o 9 4 0 2625.95 2543.48 43.73 o 10 4 0 148.43 113.83 32.31 o 11 4 0 793.17 812.35 29.37 o 12 4 0 1900.62 1794.63 63.91 o 13 4 0 1157.89 1234.75 36.11 o 1 5 0 15464.77 15780.18 316.03 o 2 5 0 8050.35 7908.92 146.07 o 3 5 0 3.95 6.77 5.91 o 4 5 0 2477.89 2500.75 46.93 o 5 5 0 4379.77 4414.08 100.13 o 6 5 0 0.74 24.44 6.87 o 7 5 0 2384.33 2295.98 34.80 o 8 5 0 7628.08 7310.05 82.67 o 9 5 0 75.13 88.02 11.02 o 10 5 0 78.94 85.93 11.72 o 11 5 0 1896.17 1834.46 37.80 o 12 5 0 106.96 117.50 21.32 o 0 6 0 1501.56 1405.02 34.91 o 1 6 0 0.10 -2.29 6.17 o 2 6 0 1511.93 1558.43 24.38 o 3 6 0 4774.38 4748.87 54.16 o 4 6 0 1274.93 1280.10 44.26 o 5 6 0 0.44 27.06 9.54 o 6 6 0 6575.69 6356.65 75.05 o 7 6 0 1565.44 1544.12 30.28 o 8 6 0 76.94 90.39 11.11 o 9 6 0 119.90 148.60 13.76 o 10 6 0 1260.11 1179.59 35.93 o 11 6 0 3.82 -7.15 15.27 o 1 7 0 3531.21 3562.03 48.16 o 2 7 0 714.72 758.61 19.69 o 3 7 0 55.03 72.35 9.35 o 4 7 0 918.41 972.45 23.54 o 5 7 0 3183.63 3196.53 84.44 o 6 7 0 97.58 111.23 16.47 o 7 7 0 988.77 966.81 28.81 o 8 7 0 29.22 42.57 15.00 o 9 7 0 50.55 76.46 20.51 o 10 7 0 533.38 509.56 27.40 o 0 8 0 2084.83 2337.49 77.45 o 1 8 0 977.77 1063.81 28.07 o 2 8 0 332.73 371.59 16.37 o 3 8 0 125.09 151.25 12.06 o 4 8 0 134.44 221.16 14.04 o 5 8 0 709.58 669.61 35.23 o 6 8 0 811.65 824.71 34.02 o 7 8 0 3.68 8.93 14.36 o 8 8 0 84.31 87.77 17.98 o 9 8 0 2259.37 2179.01 71.29 o 1 9 0 44.29 62.70 10.39 o 2 9 0 277.23 347.69 16.67 o 3 9 0 5.58 20.94 8.97 o 4 9 0 2621.10 2614.69 93.53 o 5 9 0 1229.50 1284.67 38.22 o 6 9 0 200.46 209.10 23.88 o 7 9 0 88.63 101.07 19.66 o 0 10 0 233.81 235.34 28.94 o 1 10 0 155.05 200.67 19.33 o 2 10 0 499.89 535.31 26.95 o 3 10 0 548.74 613.97 34.88 o 4 10 0 7.78 13.94 15.84 o 5 10 0 185.59 186.00 23.25 o -13 0 1 40.54 27.58 16.58 o -11 0 1 445.87 488.39 31.21 o -9 0 1 4880.82 4885.84 114.53 o -7 0 1 1966.76 2078.06 58.28 o -5 0 1 15351.82 14944.17 179.70 o -3 0 1 1460.14 1585.12 25.09 o -1 0 1 105.13 141.74 6.82 o 1 0 1 10533.01 10578.85 223.98 o 3 0 1 21660.76 22493.22 461.42 o 5 0 1 10.97 17.71 6.67 o 7 0 1 2615.48 2791.86 49.49 o 9 0 1 2944.75 2939.07 45.19 o 11 0 1 0.66 -5.73 8.24 o 13 0 1 1743.17 1761.72 61.10 o -14 1 1 286.40 322.02 23.40 o -13 1 1 798.95 817.37 30.88 o -12 1 1 5.10 7.13 8.71 o -11 1 1 214.02 278.35 15.67 o -10 1 1 6486.53 6404.85 103.31 o -9 1 1 345.18 392.91 13.47 o -8 1 1 74.28 83.93 7.00 o -7 1 1 4867.96 4875.69 67.03 o -6 1 1 4581.56 4635.82 55.84 o -5 1 1 1036.59 1125.95 15.65 o -4 1 1 20105.59 20472.82 250.17 o -3 1 1 7690.85 7856.47 87.28 o -2 1 1 2977.51 3008.56 29.36 o -1 1 1 4716.31 4917.75 36.93 o 0 1 1 1620.92 1616.03 19.43 o 1 1 1 331.68 379.47 6.06 o 2 1 1 913.30 1010.57 19.31 o 3 1 1 3130.31 3234.24 38.87 o 4 1 1 4191.02 4356.95 63.72 o 5 1 1 169.41 191.63 15.78 o 6 1 1 5166.66 5013.55 56.90 o 7 1 1 35.92 43.48 5.35 o 8 1 1 310.10 411.33 13.68 o 9 1 1 26.25 87.83 12.28 o 10 1 1 4.49 -7.13 7.61 o 11 1 1 284.38 308.48 16.33 o 12 1 1 13.70 29.58 9.54 o 13 1 1 20.55 43.37 12.37 o 14 1 1 2261.28 2259.44 56.96 o -14 2 1 707.01 726.77 31.57 o -13 2 1 1.10 17.01 11.57 o -12 2 1 2975.19 2909.69 45.16 o -11 2 1 14.54 25.58 8.30 o -10 2 1 500.82 519.06 19.09 o -9 2 1 1720.95 1738.68 33.08 o -8 2 1 3872.22 4004.14 73.55 o -7 2 1 27.33 55.04 5.32 o -6 2 1 9710.21 9643.26 122.45 o -5 2 1 653.99 548.79 13.11 o -4 2 1 3000.41 3016.32 39.62 o -3 2 1 4109.34 4679.79 96.37 o -2 2 1 1555.20 1598.92 13.18 o -1 2 1 919.05 1027.47 15.98 o 0 2 1 3091.28 3381.13 40.49 o 1 2 1 2215.67 2184.33 78.13 o 2 2 1 60.20 92.04 7.46 o 3 2 1 2965.30 3267.48 59.97 o 4 2 1 9370.66 9418.97 157.28 o 5 2 1 26.64 52.66 6.92 o 6 2 1 3873.73 4188.29 110.07 o 7 2 1 214.49 302.16 10.80 o 8 2 1 613.11 614.93 14.34 o 9 2 1 339.45 329.35 14.74 o 10 2 1 206.04 229.55 15.65 o 11 2 1 26.36 46.54 9.48 o 12 2 1 602.53 626.37 22.45 o 13 2 1 578.99 561.59 27.42 o 14 2 1 21.41 49.54 14.39 o -13 3 1 1976.94 1995.64 41.01 o -12 3 1 186.54 222.70 16.33 o -11 3 1 953.41 934.42 28.50 o -10 3 1 955.46 925.90 27.18 o -9 3 1 603.27 575.23 18.79 o -8 3 1 1214.14 1220.33 24.94 o -7 3 1 9669.25 9681.35 129.49 o -6 3 1 527.34 603.49 15.83 o -5 3 1 40.07 34.90 5.26 o -4 3 1 6.71 27.54 10.80 o -3 3 1 6024.25 5962.44 74.63 o -2 3 1 264.05 264.64 7.79 o -1 3 1 5596.66 5746.38 82.11 o 0 3 1 15205.96 17189.89 284.26 o 1 3 1 932.72 998.39 23.70 o 2 3 1 3711.13 3672.51 52.78 o 3 3 1 4749.05 4667.24 67.48 o 4 3 1 360.74 391.62 17.92 o 5 3 1 3588.54 3819.35 68.53 o 6 3 1 1011.83 1143.69 25.63 o 7 3 1 170.95 196.52 11.56 o 8 3 1 2111.63 2079.48 36.31 o 9 3 1 141.00 115.10 10.06 o 10 3 1 306.34 300.66 15.52 o 11 3 1 1173.62 1168.45 31.50 o 12 3 1 1177.82 1228.18 34.42 o 13 3 1 179.08 216.76 17.47 o -13 4 1 0.08 24.60 11.87 o -12 4 1 2156.14 2203.98 46.52 o -11 4 1 1295.21 1349.39 35.35 o -10 4 1 365.72 341.47 17.00 o -9 4 1 214.63 259.18 14.47 o -8 4 1 2841.58 2810.84 43.55 o -7 4 1 99.90 77.33 25.28 o -6 4 1 122.86 124.70 14.16 o -5 4 1 2046.85 2275.88 63.59 o -4 4 1 322.94 333.83 11.00 o -3 4 1 4702.92 4804.14 88.03 o -2 4 1 15971.44 16290.85 238.42 o -1 4 1 39.46 43.29 5.72 o 0 4 1 493.03 539.80 12.21 o 1 4 1 3872.32 3666.92 64.56 o 2 4 1 3771.25 3766.15 62.87 o 3 4 1 4735.31 4697.95 58.00 o 4 4 1 363.83 357.20 10.86 o 5 4 1 48.43 76.03 7.21 o 6 4 1 355.93 408.83 13.67 o 7 4 1 4867.88 4634.03 45.37 o 8 4 1 17.16 22.66 7.69 o 9 4 1 202.33 225.80 13.85 o 10 4 1 10.93 5.23 7.66 o 11 4 1 325.74 359.34 18.58 o 12 4 1 1230.25 1252.61 43.21 o 13 4 1 897.32 949.16 35.17 o -12 5 1 920.12 940.69 40.44 o -11 5 1 10.64 27.16 10.29 o -10 5 1 1564.06 1521.77 32.87 o -9 5 1 11.80 22.78 8.60 o -8 5 1 549.05 612.76 20.32 o -7 5 1 2374.82 2290.79 35.05 o -6 5 1 1888.48 1876.34 34.81 o -5 5 1 978.23 1015.22 19.94 o -4 5 1 5743.47 5725.73 93.02 o -3 5 1 252.07 240.19 11.52 o -2 5 1 2964.85 2982.38 43.57 o -1 5 1 637.08 701.35 20.69 o 0 5 1 2325.35 2287.78 40.35 o 1 5 1 1642.15 1680.59 28.57 o 2 5 1 12558.18 12889.06 119.11 o 3 5 1 643.06 602.44 16.32 o 4 5 1 315.81 293.53 12.88 o 5 5 1 2585.50 2597.63 81.96 o 6 5 1 1561.97 1679.88 42.42 o 7 5 1 170.34 186.54 12.36 o 8 5 1 4783.75 4740.71 50.64 o 9 5 1 630.13 610.83 21.01 o 10 5 1 155.32 149.00 13.41 o 11 5 1 87.94 89.34 12.98 o 12 5 1 2073.43 2105.56 54.70 o -11 6 1 2347.07 2380.97 51.59 o -10 6 1 22.16 30.62 10.72 o -9 6 1 3091.86 3073.48 45.57 o -8 6 1 177.42 208.90 14.48 o -7 6 1 21.08 41.07 9.45 o -6 6 1 1244.19 1222.20 30.73 o -5 6 1 8911.35 8998.87 296.41 o -4 6 1 446.35 443.77 16.41 o -3 6 1 6010.03 6266.12 106.44 o -2 6 1 85.82 113.34 9.63 o -1 6 1 47.08 47.04 7.46 o 0 6 1 2439.38 2417.74 29.07 o 1 6 1 4695.67 4608.62 40.90 o 2 6 1 1.71 3.60 6.60 o 3 6 1 1024.56 1124.80 23.47 o 4 6 1 4695.13 4679.74 95.74 o 5 6 1 679.07 692.25 34.59 o 6 6 1 296.53 286.07 20.33 o 7 6 1 2737.60 2708.62 43.85 o 8 6 1 192.01 224.39 14.57 o 9 6 1 998.74 973.55 26.79 o 10 6 1 1555.27 1556.08 40.86 o 11 6 1 422.83 410.30 25.68 o -10 7 1 2112.45 2106.45 50.05 o -9 7 1 375.42 396.36 23.97 o -8 7 1 196.67 213.82 17.30 o -7 7 1 1115.54 1098.14 37.02 o -6 7 1 793.81 834.36 31.96 o -5 7 1 2051.20 1986.86 71.64 o -4 7 1 4730.13 4855.01 67.58 o -3 7 1 1005.94 1008.24 22.08 o -2 7 1 1543.64 1604.61 26.83 o -1 7 1 3007.91 3087.42 56.22 o 0 7 1 4040.26 3912.40 39.46 o 1 7 1 137.05 161.59 11.53 o 2 7 1 5375.06 5628.28 103.83 o 3 7 1 2380.94 2337.12 46.85 o 4 7 1 8.48 21.58 8.43 o 5 7 1 9373.98 9217.47 109.13 o 6 7 1 393.89 456.13 25.51 o 7 7 1 15.57 19.97 12.86 o 8 7 1 2322.99 2292.61 53.43 o 9 7 1 2343.66 2296.74 56.18 o 10 7 1 289.78 285.89 26.84 o -9 8 1 596.75 662.64 35.47 o -8 8 1 1241.83 1234.95 43.09 o -7 8 1 64.77 78.00 16.12 o -6 8 1 2287.51 2347.80 52.84 o -5 8 1 1298.32 1268.71 58.42 o -4 8 1 224.37 262.10 16.69 o -3 8 1 609.17 601.52 19.28 o -2 8 1 3291.55 3128.96 46.03 o -1 8 1 842.82 898.80 22.34 o 0 8 1 9170.98 9263.01 108.39 o 1 8 1 3001.55 3037.63 38.09 o 2 8 1 889.16 906.57 22.36 o 3 8 1 13.81 11.52 8.28 o 4 8 1 7247.43 7402.47 181.51 o 5 8 1 83.88 92.16 18.75 o 6 8 1 1130.63 1173.81 41.22 o 7 8 1 134.72 141.66 22.79 o 8 8 1 8.61 11.39 15.55 o 9 8 1 461.50 465.98 37.57 o -7 9 1 1007.79 951.96 40.79 o -6 9 1 27.17 24.76 15.20 o -5 9 1 1472.31 1397.79 50.33 o -4 9 1 71.81 82.96 12.77 o -3 9 1 1030.26 1027.97 25.40 o -2 9 1 445.30 457.75 18.65 o -1 9 1 5910.36 6062.76 89.92 o 0 9 1 47.05 79.72 12.57 o 1 9 1 223.35 250.75 15.03 o 2 9 1 1302.42 1273.76 36.96 o 3 9 1 1132.37 1100.08 29.33 o 4 9 1 0.13 19.82 11.50 o 5 9 1 5694.60 5471.12 104.42 o 6 9 1 0.36 0.51 14.06 o 7 9 1 88.29 102.44 20.09 o -5 10 1 91.37 128.84 28.80 o -4 10 1 146.09 170.51 23.87 o -3 10 1 1559.97 1553.18 50.58 o -2 10 1 619.51 696.20 29.92 o -1 10 1 10.69 -5.18 11.24 o 0 10 1 641.03 679.46 30.07 o 1 10 1 337.90 394.88 24.54 o 2 10 1 112.91 140.71 15.19 o 3 10 1 1270.91 1332.77 39.76 o 4 10 1 2014.39 2009.57 48.21 o -14 0 2 5561.39 5469.72 111.48 o -12 0 2 6.62 -5.01 11.13 o -10 0 2 17748.10 17526.94 454.16 o -8 0 2 1469.23 1552.20 68.51 o -6 0 2 3337.50 3472.59 66.19 o -4 0 2 24687.49 23497.53 496.23 o -2 0 2 30511.37 29588.63 354.35 o 0 0 2 368.69 490.01 10.02 o 2 0 2 13245.83 12376.30 1307.61 o 4 0 2 34966.50 35196.13 856.73 o 6 0 2 592.26 651.52 17.78 o 8 0 2 5115.32 5115.30 191.70 o 10 0 2 26328.82 26614.79 843.22 o 12 0 2 5.78 -2.41 12.17 o 14 0 2 7391.28 7632.91 208.57 o -14 1 2 15.76 31.39 13.92 o -13 1 2 1320.46 1307.91 37.95 o -12 1 2 1545.48 1472.86 37.44 o -11 1 2 601.82 613.73 20.86 o -10 1 2 2.21 16.62 8.69 o -9 1 2 11098.83 11020.84 204.45 o -8 1 2 625.17 586.47 15.38 o -7 1 2 6309.21 6487.81 78.31 o -6 1 2 76.58 120.08 6.81 o -5 1 2 2420.23 2314.48 30.42 o -4 1 2 2085.20 1998.89 21.75 o -3 1 2 25741.36 25496.32 282.86 o -2 1 2 3158.83 3239.29 20.29 o -1 1 2 22925.51 23354.79 220.18 o 0 1 2 8372.09 8725.94 91.40 o 1 1 2 20839.59 21636.38 117.16 o 2 1 2 8510.89 8774.70 106.52 o 3 1 2 31795.53 32376.43 354.31 o 4 1 2 614.95 686.91 11.24 o 5 1 2 5960.79 5797.46 100.30 o 6 1 2 74.47 69.22 6.34 o 7 1 2 1506.47 1518.57 20.31 o 8 1 2 1105.35 1029.59 18.41 o 9 1 2 25228.02 24613.10 560.23 o 10 1 2 24.84 38.71 7.90 o 11 1 2 428.56 437.41 18.04 o 12 1 2 1713.56 1731.37 34.65 o 13 1 2 1742.97 1680.02 42.36 o 14 1 2 3.03 9.13 12.86 o -14 2 2 1944.57 2030.14 49.68 o -13 2 2 1244.95 1265.69 37.55 o -12 2 2 51.74 75.93 11.93 o -11 2 2 2544.41 2471.82 39.54 o -10 2 2 3189.80 3102.68 41.78 o -9 2 2 228.83 230.49 13.15 o -8 2 2 1133.34 1242.50 26.63 o -7 2 2 3212.92 3156.48 34.66 o -6 2 2 1972.76 1970.66 31.00 o -5 2 2 2645.99 2369.40 47.84 o -4 2 2 8451.82 8561.26 50.69 o -3 2 2 1907.85 1915.86 21.99 o -2 2 2 1710.88 1618.13 14.07 o -1 2 2 1277.82 1261.13 17.75 o 0 2 2 0.68 3.70 2.52 o 1 2 2 2669.90 2650.61 34.97 o 2 2 2 0.91 11.57 2.70 o 3 2 2 470.78 488.07 9.36 o 4 2 2 16313.89 16501.55 264.99 o 5 2 2 5.63 38.49 4.22 o 6 2 2 61.29 76.06 5.65 o 7 2 2 7886.21 8139.89 144.90 o 8 2 2 1036.58 1130.21 19.07 o 9 2 2 11.94 12.33 5.74 o 10 2 2 5311.38 5129.23 71.16 o 11 2 2 1928.27 1928.11 38.69 o 12 2 2 15.49 23.87 9.60 o 13 2 2 1180.38 1172.96 31.49 o -13 3 2 0.01 7.26 10.30 o -12 3 2 4908.21 4984.59 110.43 o -11 3 2 15.32 30.16 9.08 o -10 3 2 1272.17 1214.61 30.81 o -9 3 2 317.61 324.42 16.72 o -8 3 2 1941.83 1804.29 29.78 o -7 3 2 56.30 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492.65 10.40 o 1 4 2 17707.58 17873.70 230.98 o 2 4 2 12188.58 12552.45 172.13 o 3 4 2 284.16 271.23 11.19 o 4 4 2 64.65 63.60 6.11 o 5 4 2 396.45 414.55 11.48 o 6 4 2 2.77 8.79 5.11 o 7 4 2 11053.25 11035.97 302.17 o 8 4 2 2668.29 2591.66 44.39 o 9 4 2 0.25 3.26 6.64 o 10 4 2 88.82 100.23 11.42 o 11 4 2 2617.37 2696.26 43.62 o 12 4 2 0.74 22.54 11.71 o 13 4 2 1394.83 1397.99 47.61 o -12 5 2 3158.64 3261.08 76.94 o -11 5 2 460.74 405.27 22.69 o -10 5 2 80.38 77.35 11.02 o -9 5 2 2658.80 2608.05 46.55 o -8 5 2 658.06 466.19 101.18 o -7 5 2 1687.38 1639.65 34.23 o -6 5 2 3251.22 3200.26 75.54 o -5 5 2 391.37 404.84 13.82 o -4 5 2 1116.86 1073.91 18.64 o -3 5 2 3696.92 3760.02 73.28 o -2 5 2 5094.82 5116.30 83.40 o -1 5 2 1901.50 1937.98 37.95 o 0 5 2 2331.12 2368.66 45.68 o 1 5 2 743.21 795.22 16.45 o 2 5 2 5114.15 5075.03 59.85 o 3 5 2 3303.99 3327.81 38.25 o 4 5 2 647.98 664.37 17.50 o 5 5 2 1279.96 1345.95 46.60 o 6 5 2 7161.25 7113.37 143.45 o 7 5 2 1022.70 1000.36 23.08 o 8 5 2 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