#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/98/2219887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219887_Fobs loop_ _publ_author_name 'Ahmadi, Roya' 'Ebadi, Amin' 'Kalateh, Khadijeh' 'Norouzi, Ali' 'Amani, Vahid' _publ_section_title ; Dichlorido(6-methyl-2,2'-bipyridine-\k^2^N,N')mercury(II) ; _journal_coeditor_code HK2551 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1407 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.705 _cell_angle_gamma 90.000 _cell_length_a 9.4742 _cell_length_b 16.1637 _cell_length_c 8.2107 _exptl_crystal_F_000 732.00 _reflns_d_resolution_high 0.7285 _[local]_cod_data_source_file hk2551Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2222H IN P2(1)/C' _shelx_refln_list_code 4 _shelx_F_calc_maximum 336.25 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 25612.90 23525.58 2172.31 o 2 0 0 42381.70 37887.19 1097.93 o 3 0 0 85311.60 109467.99 14350.26 o 4 0 0 168.06 269.83 80.60 o 5 0 0 18128.96 13186.97 123.64 o 6 0 0 18962.84 19606.60 153.64 o 7 0 0 38.41 127.69 80.46 o 8 0 0 17506.81 19155.59 144.51 o 9 0 0 9831.51 11265.12 117.82 o 10 0 0 1876.94 1962.85 86.49 o 11 0 0 5622.15 6426.26 111.23 o 12 0 0 1061.28 1117.31 93.11 o 1 1 0 21086.02 24378.20 7651.61 o 2 1 0 476.22 318.24 48.59 o 3 1 0 611.91 407.70 40.35 o 4 1 0 4546.51 3254.93 285.40 o 5 1 0 32.34 48.59 41.85 o 6 1 0 1618.44 1630.68 111.96 o 7 1 0 4071.32 4039.08 126.69 o 8 1 0 79.51 144.33 69.11 o 9 1 0 2045.93 2179.00 157.37 o 10 1 0 202.09 235.66 57.76 o 11 1 0 72.27 101.16 111.08 o 12 1 0 500.81 589.36 63.20 o 0 2 0 23413.12 4772.62 806.66 o 1 2 0 6803.68 6992.56 3012.35 o 2 2 0 53899.63 68875.04 16594.53 o 3 2 0 40537.30 44049.95 5677.90 o 4 2 0 97.10 76.85 33.76 o 5 2 0 22225.54 20128.03 1255.47 o 6 2 0 15440.42 16444.19 246.97 o 7 2 0 12.77 40.09 46.95 o 8 2 0 8729.09 8639.07 1044.46 o 9 2 0 6720.82 7827.89 118.68 o 10 2 0 256.96 214.67 47.87 o 11 2 0 5667.02 6464.09 76.09 o 12 2 0 380.72 561.38 61.93 o 1 3 0 29821.81 10785.40 1241.10 o 2 3 0 36435.41 35738.64 11180.56 o 3 3 0 2124.15 1825.36 305.89 o 4 3 0 46394.58 54971.18 4586.87 o 5 3 0 14888.41 12121.00 645.43 o 6 3 0 10469.64 8774.40 626.06 o 7 3 0 17177.88 17695.80 1150.92 o 8 3 0 414.34 448.87 39.76 o 9 3 0 6207.92 7057.09 411.02 o 10 3 0 3160.78 2600.55 90.58 o 11 3 0 41.76 171.68 57.50 o 12 3 0 2003.01 1918.41 184.32 o 0 4 0 11699.91 2701.33 270.50 o 1 4 0 2252.02 649.97 71.15 o 2 4 0 9595.85 7712.08 2651.68 o 3 4 0 6125.42 6964.74 1489.93 o 4 4 0 130.22 159.77 33.04 o 5 4 0 172.95 198.30 29.36 o 6 4 0 909.24 736.47 57.16 o 7 4 0 511.68 461.94 43.46 o 8 4 0 13.00 81.73 33.55 o 9 4 0 379.98 361.47 35.97 o 10 4 0 15.95 13.47 56.25 o 11 4 0 458.42 591.42 59.48 o 12 4 0 292.28 338.62 50.20 o 1 5 0 28131.28 11486.95 762.75 o 2 5 0 44517.48 26745.82 2732.78 o 3 5 0 1719.78 1682.09 393.74 o 4 5 0 45302.02 48837.42 6237.27 o 5 5 0 10565.90 10803.34 979.15 o 6 5 0 12894.21 12016.39 746.67 o 7 5 0 15956.37 16702.95 1008.85 o 8 5 0 344.81 370.05 35.58 o 9 5 0 5639.39 6532.01 205.78 o 10 5 0 3630.54 4344.66 258.54 o 11 5 0 110.50 51.61 69.11 o 12 5 0 1627.03 1061.15 103.01 o 0 6 0 3667.30 1181.37 236.76 o 1 6 0 530.12 3152.62 993.30 o 2 6 0 5948.71 2568.16 156.73 o 3 6 0 21025.88 20881.16 5699.27 o 4 6 0 12.45 28.76 29.74 o 5 6 0 6915.11 5944.42 514.13 o 6 6 0 3813.34 3931.94 283.39 o 7 6 0 3042.81 3012.40 151.40 o 8 6 0 1171.21 1129.79 49.55 o 9 6 0 57.33 96.30 36.66 o 10 6 0 1348.67 1501.87 49.96 o 11 6 0 1095.70 1194.99 199.45 o 12 6 0 43.21 0.00 89.20 o 1 7 0 5121.50 1941.81 230.08 o 2 7 0 2387.86 1306.71 152.17 o 3 7 0 163.22 180.94 49.97 o 4 7 0 9024.39 8384.59 1348.45 o 5 7 0 2432.56 2343.90 187.39 o 6 7 0 2784.57 2522.18 194.10 o 7 7 0 9325.74 9093.13 522.18 o 8 7 0 265.94 342.28 35.64 o 9 7 0 2425.77 2330.26 87.35 o 10 7 0 305.50 453.45 45.50 o 11 7 0 50.61 97.77 53.05 o 0 8 0 43868.69 19791.21 1187.70 o 1 8 0 6002.07 2215.25 192.35 o 2 8 0 16833.81 9914.75 923.44 o 3 8 0 15432.82 15617.46 3807.46 o 4 8 0 57.95 118.03 30.23 o 5 8 0 16437.60 16585.63 2066.08 o 6 8 0 8353.04 8736.66 496.60 o 7 8 0 93.67 185.39 33.11 o 8 8 0 11879.51 12677.00 807.13 o 9 8 0 1046.84 1379.66 117.20 o 10 8 0 1868.48 1979.31 105.97 o 11 8 0 3320.83 3478.67 164.68 o 1 9 0 5268.38 2323.79 292.06 o 2 9 0 43.42 115.15 36.36 o 3 9 0 1377.94 1084.04 82.43 o 4 9 0 621.46 652.61 101.10 o 5 9 0 13.32 33.44 34.11 o 6 9 0 77.71 144.63 36.26 o 7 9 0 1822.06 1796.42 110.62 o 8 9 0 912.17 846.21 72.99 o 9 9 0 284.14 320.69 71.76 o 10 9 0 471.96 548.88 49.43 o 11 9 0 1.85 81.58 45.69 o 0 10 0 24913.45 13948.02 2423.95 o 1 10 0 3648.71 1833.42 197.04 o 2 10 0 12260.79 7693.49 749.86 o 3 10 0 11413.81 7964.01 882.89 o 4 10 0 143.73 165.64 30.43 o 5 10 0 7688.88 8599.70 1149.45 o 6 10 0 1976.23 2150.32 152.76 o 7 10 0 1093.28 1134.87 74.90 o 8 10 0 4977.55 5546.41 367.07 o 9 10 0 1964.35 2011.39 101.65 o 10 10 0 725.50 699.88 44.05 o 11 10 0 2110.10 1820.93 135.15 o 1 11 0 34615.33 22262.70 2940.32 o 2 11 0 14522.37 10522.03 949.41 o 3 11 0 2755.05 1909.08 181.34 o 4 11 0 14791.02 17745.89 3136.93 o 5 11 0 2088.53 2269.28 304.85 o 6 11 0 1934.03 2134.44 167.48 o 7 11 0 5332.42 5977.00 258.01 o 8 11 0 540.12 601.83 49.34 o 9 11 0 2512.80 2189.14 214.50 o 10 11 0 3025.33 3131.54 195.56 o 0 12 0 428.92 358.90 42.10 o 1 12 0 8.32 54.58 27.54 o 2 12 0 908.90 638.15 64.00 o 3 12 0 452.40 437.06 37.19 o 4 12 0 114.23 174.13 31.25 o 5 12 0 116.71 157.98 33.15 o 6 12 0 235.36 286.77 30.76 o 7 12 0 43.75 84.82 26.85 o 8 12 0 18.19 75.16 27.90 o 9 12 0 78.09 118.89 33.87 o 10 12 0 24.05 61.62 53.27 o 1 13 0 17285.47 12947.00 1613.21 o 2 13 0 12127.79 8613.51 664.63 o 3 13 0 3030.06 2750.14 130.33 o 4 13 0 20800.13 25015.84 4066.41 o 5 13 0 5299.32 5981.10 759.91 o 6 13 0 4032.38 5004.90 507.99 o 7 13 0 9471.29 11075.73 679.59 o 8 13 0 554.68 757.15 55.80 o 9 13 0 2862.32 2804.35 147.79 o 10 13 0 3676.73 3021.10 277.91 o 0 14 0 2088.54 1613.77 240.87 o 1 14 0 1803.71 1460.15 128.61 o 2 14 0 1012.88 873.60 51.55 o 3 14 0 7380.68 6722.52 482.42 o 4 14 0 1288.61 1720.65 322.81 o 5 14 0 4805.21 5932.08 866.09 o 6 14 0 3528.08 3701.82 369.29 o 7 14 0 320.57 367.77 45.53 o 8 14 0 2013.52 2466.56 163.63 o 9 14 0 370.57 361.20 43.08 o 1 15 0 10567.78 7821.87 574.05 o 2 15 0 6390.97 5664.98 694.80 o 3 15 0 271.75 332.36 73.81 o 4 15 0 5357.08 7145.32 1200.95 o 5 15 0 1631.44 2484.27 314.18 o 6 15 0 1015.40 1325.48 111.20 o 7 15 0 4021.22 4360.86 395.12 o 8 15 0 353.80 455.23 53.78 o 9 15 0 1070.21 993.76 91.84 o 0 16 0 14225.96 12234.34 2192.63 o 1 16 0 2758.94 2286.83 223.39 o 2 16 0 4860.64 4377.67 550.73 o 3 16 0 12991.24 12875.63 788.70 o 4 16 0 381.86 549.85 103.98 o 5 16 0 8347.79 11878.88 1356.27 o 6 16 0 6731.65 8857.73 724.73 o 7 16 0 335.02 480.02 70.21 o 8 16 0 4318.47 4815.18 313.21 o 1 17 0 72.60 149.98 65.78 o 2 17 0 45.73 82.13 36.86 o 3 17 0 130.69 167.09 32.33 o 4 17 0 54.09 117.26 30.81 o 5 17 0 278.49 300.89 32.36 o 6 17 0 3.41 -6.51 33.09 o 7 17 0 68.02 67.82 36.91 o 8 17 0 118.45 174.59 61.82 o 0 18 0 8262.32 8023.06 1969.30 o 1 18 0 1496.69 1436.71 119.00 o 2 18 0 2836.34 2840.69 316.53 o 3 18 0 9236.68 10821.27 602.68 o 4 18 0 408.96 534.73 116.09 o 5 18 0 4599.87 6391.01 621.79 o 6 18 0 4833.66 6674.96 469.81 o 7 18 0 160.31 224.60 35.22 o 1 19 0 3467.79 3862.57 448.15 o 2 19 0 1214.13 1401.25 160.68 o 3 19 0 660.80 876.00 90.09 o 4 19 0 1338.32 1788.96 250.54 o 5 19 0 69.23 111.02 30.98 o 6 19 0 636.73 841.91 80.68 o 0 20 0 1929.56 2387.20 351.93 o 1 20 0 624.98 624.11 69.35 o 2 20 0 429.51 363.64 44.26 o 3 20 0 1678.68 1591.55 103.49 o 4 20 0 189.90 336.25 62.02 o 5 20 0 816.83 919.51 104.06 o 1 21 0 5007.64 5579.24 687.59 o 2 21 0 1899.34 2017.24 193.16 o 3 21 0 1081.13 1190.08 115.38 o 0 22 0 449.46 378.61 88.48 o 1 22 0 64.90 159.06 40.87 o -12 1 1 5153.33 4673.28 763.60 o -11 1 1 623.39 667.04 88.57 o -10 1 1 3264.89 3892.21 68.50 o -9 1 1 9688.97 10600.91 423.58 o -8 1 1 869.12 878.01 58.43 o -7 1 1 11692.28 9832.84 1279.02 o -6 1 1 31791.56 31051.40 3756.34 o -5 1 1 41.61 65.34 40.79 o -4 1 1 55114.51 53930.54 8384.10 o -3 1 1 50275.88 61009.37 6987.65 o -2 1 1 23772.73 31857.78 2737.95 o -1 1 1 81538.44 211099.88 3802.84 o 0 1 1 5925.20 7497.08 396.62 o 1 1 1 33749.95 66106.13 5916.93 o 2 1 1 31683.02 45602.74 3688.87 o 3 1 1 1516.98 1406.92 109.18 o 4 1 1 15166.28 14801.02 930.74 o 5 1 1 20515.89 17580.62 2056.15 o 6 1 1 75.02 79.28 45.46 o 7 1 1 15551.24 17440.48 626.35 o 8 1 1 3524.57 3921.64 281.04 o 9 1 1 3616.34 3195.35 478.46 o 10 1 1 4870.91 5105.72 656.87 o 11 1 1 24.68 55.96 59.36 o 12 1 1 1249.21 1192.13 67.74 o -12 2 1 5.00 82.19 68.20 o -11 2 1 1765.73 2103.72 64.80 o -10 2 1 1389.95 1845.92 60.98 o -9 2 1 1073.52 1257.71 93.24 o -8 2 1 12497.46 11278.30 935.15 o -7 2 1 4344.58 3960.25 293.92 o -6 2 1 6755.46 5359.39 773.30 o -5 2 1 11985.40 8765.22 1225.44 o -4 2 1 13.40 107.85 41.70 o -3 2 1 18413.13 18439.17 2195.60 o -2 2 1 16324.38 16788.58 1400.09 o -1 2 1 305.29 277.29 55.97 o 0 2 1 44470.83 64004.32 3728.45 o 1 2 1 21204.68 29815.09 4355.47 o 2 2 1 2810.10 2986.50 371.07 o 3 2 1 35900.70 44786.19 5218.53 o 4 2 1 1786.86 1735.29 198.61 o 5 2 1 8128.51 7387.52 779.44 o 6 2 1 10715.34 9840.32 1073.44 o 7 2 1 241.13 219.73 34.73 o 8 2 1 6292.74 6577.06 72.98 o 9 2 1 2833.12 2417.20 65.66 o 10 2 1 39.97 47.73 40.18 o 11 2 1 976.68 982.89 130.85 o 12 2 1 480.72 416.46 53.16 o -12 3 1 1497.97 1306.44 173.38 o -11 3 1 176.35 73.95 58.12 o -10 3 1 1529.88 1842.58 62.27 o -9 3 1 2398.71 2139.92 281.16 o -8 3 1 171.38 214.19 48.01 o -7 3 1 1713.14 1636.68 109.01 o -6 3 1 8779.91 7789.01 813.78 o -5 3 1 1333.97 826.36 131.33 o -4 3 1 18651.08 17363.86 3356.64 o -3 3 1 18591.28 16294.90 2428.78 o -2 3 1 2417.65 1894.26 90.35 o -1 3 1 26627.48 23716.06 914.83 o 0 3 1 2706.68 1825.03 90.68 o 1 3 1 2876.40 2142.70 202.24 o 2 3 1 4630.64 5549.33 995.69 o 3 3 1 870.07 855.94 137.08 o 4 3 1 1481.13 1726.47 214.26 o 5 3 1 4637.70 4469.43 482.26 o 6 3 1 90.01 82.38 36.12 o 7 3 1 2833.83 2595.87 271.08 o 8 3 1 2636.40 2639.42 306.16 o 9 3 1 27.22 157.46 83.95 o 10 3 1 769.43 957.02 73.72 o 11 3 1 56.91 146.93 59.37 o 12 3 1 139.99 146.98 87.49 o -12 4 1 15.26 -85.16 187.99 o -11 4 1 4390.44 4894.90 314.03 o -10 4 1 7512.83 7144.25 1080.05 o -9 4 1 1043.84 1012.95 52.14 o -8 4 1 12995.94 12225.57 726.23 o -7 4 1 2111.02 2050.95 182.51 o -6 4 1 17087.60 14906.32 1770.09 o -5 4 1 32550.11 31465.91 6901.41 o -4 4 1 364.69 457.73 82.23 o -3 4 1 36022.49 30638.49 5130.08 o -2 4 1 34685.54 33874.76 7522.16 o -1 4 1 113.09 148.58 49.02 o 0 4 1 62709.93 54470.59 5462.87 o 1 4 1 35641.61 28481.40 3866.41 o 2 4 1 11319.05 11000.69 2132.44 o 3 4 1 70529.39 108378.45 18847.56 o 4 4 1 2632.21 2316.32 348.37 o 5 4 1 26392.57 27521.75 2951.42 o 6 4 1 20997.62 22364.61 1778.81 o 7 4 1 189.06 223.19 36.13 o 8 4 1 6436.55 6577.36 545.96 o 9 4 1 4443.32 4387.58 142.53 o 10 4 1 568.15 428.56 154.30 o 11 4 1 5069.00 5132.25 109.07 o -12 5 1 74.83 49.93 89.21 o -11 5 1 4.24 -7.80 87.44 o -10 5 1 191.40 172.59 43.57 o -9 5 1 400.40 446.34 45.45 o -8 5 1 923.86 999.53 90.35 o -7 5 1 1223.82 1246.61 121.26 o -6 5 1 782.38 791.22 116.58 o -5 5 1 3438.52 2777.61 510.89 o -4 5 1 2289.48 1704.58 224.63 o -3 5 1 749.90 675.00 138.23 o -2 5 1 4420.37 2419.47 317.09 o -1 5 1 717.40 315.44 43.13 o 0 5 1 30.31 16.56 32.10 o 1 5 1 7680.35 5199.99 1122.02 o 2 5 1 5662.06 5757.77 1615.34 o 3 5 1 1763.92 1852.50 297.52 o 4 5 1 12194.55 12137.10 2008.43 o 5 5 1 803.16 778.05 97.23 o 6 5 1 2699.53 2689.89 241.34 o 7 5 1 2822.22 2761.82 137.58 o 8 5 1 49.48 79.83 31.39 o 9 5 1 48.96 23.96 39.64 o 10 5 1 769.76 653.36 40.98 o 11 5 1 12.44 44.59 63.83 o -12 6 1 13.94 69.07 83.94 o -11 6 1 2293.32 2492.23 63.13 o -10 6 1 2105.74 2043.36 116.02 o -9 6 1 888.63 971.81 54.08 o -8 6 1 15909.12 18215.88 1242.36 o -7 6 1 879.13 950.33 79.19 o -6 6 1 11284.31 10495.29 1155.97 o -5 6 1 15547.13 13540.73 1659.26 o -4 6 1 110.44 78.02 28.24 o -3 6 1 15110.72 12403.34 3273.13 o -2 6 1 20898.89 11801.67 1936.64 o -1 6 1 430.80 331.77 51.78 o 0 6 1 30649.95 16668.25 1834.76 o 1 6 1 24240.63 14096.06 2740.47 o 2 6 1 15900.76 10311.43 2349.32 o 3 6 1 40178.32 46527.50 11589.95 o 4 6 1 5362.32 5413.71 941.01 o 5 6 1 16084.95 17668.06 2122.60 o 6 6 1 8799.12 9231.09 796.28 o 7 6 1 45.96 28.87 31.45 o 8 6 1 5594.24 5656.52 339.64 o 9 6 1 1869.22 1995.74 104.96 o 10 6 1 31.93 55.59 39.24 o 11 6 1 1871.09 2025.27 163.08 o -12 7 1 1584.60 1565.08 70.42 o -11 7 1 310.95 308.48 67.32 o -10 7 1 1940.13 2192.91 189.11 o -9 7 1 5518.69 5259.22 351.62 o -8 7 1 28.83 27.78 48.28 o -7 7 1 9413.65 9485.12 1138.57 o -6 7 1 4042.65 3575.12 393.45 o -5 7 1 2337.61 2196.75 289.00 o -4 7 1 23848.66 19305.28 3757.26 o -3 7 1 1838.38 1724.74 412.44 o -2 7 1 15597.57 8371.53 1096.62 o -1 7 1 44777.29 28566.52 1417.60 o 0 7 1 697.49 257.62 35.12 o 1 7 1 35978.42 21294.53 4666.54 o 2 7 1 21854.84 14029.80 3300.77 o 3 7 1 2053.13 2219.87 571.00 o 4 7 1 25594.53 30066.27 5475.83 o 5 7 1 7512.71 8169.53 1098.00 o 6 7 1 5184.42 4756.69 300.28 o 7 7 1 12735.97 12712.19 462.28 o 8 7 1 1894.30 1947.68 142.27 o 9 7 1 5823.56 5905.24 341.52 o 10 7 1 4990.27 5712.48 266.62 o 11 7 1 53.23 69.76 52.21 o -11 8 1 9.38 -10.63 51.84 o -10 8 1 157.67 168.03 40.13 o -9 8 1 231.89 275.18 44.13 o -8 8 1 616.89 582.85 44.83 o -7 8 1 186.19 206.93 34.93 o -6 8 1 1287.13 1136.96 98.88 o -5 8 1 17.00 12.42 35.78 o -4 8 1 996.62 751.41 148.64 o -3 8 1 33.86 20.31 28.08 o -2 8 1 111.18 657.22 222.60 o -1 8 1 268.07 185.27 35.68 o 0 8 1 762.17 349.68 31.89 o 1 8 1 3751.61 2190.10 539.39 o 2 8 1 9.24 -2.33 28.43 o 3 8 1 3633.89 3834.18 1037.88 o 4 8 1 150.71 208.90 32.86 o 5 8 1 2318.87 2316.10 297.60 o 6 8 1 276.53 268.56 29.33 o 7 8 1 981.34 1107.10 89.43 o 8 8 1 430.51 415.20 32.20 o 9 8 1 68.82 117.45 34.34 o 10 8 1 213.31 198.76 59.18 o 11 8 1 92.74 238.32 65.24 o -11 9 1 63.12 68.07 43.56 o -10 9 1 2827.07 3059.84 340.38 o -9 9 1 2928.89 3050.82 212.70 o -8 9 1 32.34 98.59 44.24 o -7 9 1 11901.85 12520.18 1210.52 o -6 9 1 10309.53 9890.38 1170.12 o -5 9 1 2460.28 2077.49 233.40 o -4 9 1 31031.27 29971.81 5456.80 o -3 9 1 8139.88 5107.97 674.80 o -2 9 1 19581.37 10386.78 1417.73 o -1 9 1 41673.21 22063.71 2346.24 o 0 9 1 159.05 -30.22 33.89 o 1 9 1 32760.55 19098.52 3594.08 o 2 9 1 27588.05 18927.45 4054.21 o 3 9 1 747.34 1068.29 286.01 o 4 9 1 25931.56 30954.10 7001.00 o 5 9 1 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