#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219922.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219922_Fobs loop_ _publ_author_name 'Zhan, Dan' 'Xiao, Zuo-An' _publ_section_title ; [N,N,N',N'-Tetrakis(benzimidazol-2-ylmethyl)cyclohexane-1,2-diamine]nickel(II) dinitrate dihydrate ; _journal_coeditor_code LH2699 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1361 _journal_page_last m1362 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.501 _cell_angle_gamma 90.000 _cell_length_a 15.3395 _cell_length_b 13.1695 _cell_length_c 19.6064 _exptl_crystal_F_000 1768.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file lh2699Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 050901am in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 545.94 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 37825.04 20653.67 18355.31 o 4 0 0 721.33 171.00 92.94 o 6 0 0 51.41 7.51 14.82 o 8 0 0 9326.90 2847.24 4426.69 o 10 0 0 6527.65 1945.11 3044.08 o 12 0 0 5818.98 4355.76 1637.45 o 14 0 0 10.82 78.26 54.52 o 16 0 0 126.51 139.24 124.49 o 18 0 0 42.33 122.22 129.78 o 1 1 0 74648.50 69126.81 2468.18 o 3 1 0 8933.99 4979.30 2775.36 o 5 1 0 15166.01 9540.54 4380.18 o 7 1 0 9461.93 5479.31 2570.09 o 9 1 0 4691.66 2714.40 1092.51 o 11 1 0 4796.94 2444.80 1591.41 o 13 1 0 858.23 752.74 169.81 o 15 1 0 543.83 682.05 88.37 o 17 1 0 147.10 156.14 90.43 o 0 2 0 12506.99 15142.83 209.25 o 2 2 0 704.14 556.94 30.68 o 4 2 0 5202.45 6024.53 108.09 o 6 2 0 4269.58 3233.16 462.53 o 8 2 0 2427.96 1643.98 395.13 o 10 2 0 756.61 259.25 269.09 o 12 2 0 110.41 28.70 27.36 o 14 2 0 11.17 15.94 30.53 o 16 2 0 604.08 626.98 143.32 o 18 2 0 12.84 78.91 87.75 o 1 3 0 1960.14 2380.30 61.83 o 3 3 0 31836.46 35474.01 727.12 o 5 3 0 1842.76 1839.65 68.93 o 7 3 0 84.13 84.44 33.26 o 9 3 0 1284.75 1182.61 68.95 o 11 3 0 48.85 41.76 32.39 o 13 3 0 667.59 215.13 202.49 o 15 3 0 20.12 34.30 42.66 o 17 3 0 12.95 18.01 73.62 o 0 4 0 5537.58 5072.61 127.30 o 2 4 0 4134.28 4391.50 100.55 o 4 4 0 660.75 641.34 78.03 o 6 4 0 6905.26 7496.51 153.19 o 8 4 0 701.86 812.26 70.13 o 10 4 0 1897.42 1766.61 111.55 o 12 4 0 266.53 370.76 72.50 o 14 4 0 702.11 663.15 101.46 o 16 4 0 18.70 42.44 65.27 o 18 4 0 22.55 41.85 80.68 o 1 5 0 4426.00 4429.55 95.36 o 3 5 0 5359.03 4881.76 123.76 o 5 5 0 17077.95 18146.38 406.59 o 7 5 0 2499.81 2546.80 99.37 o 9 5 0 6.71 12.60 21.30 o 11 5 0 2092.94 1688.96 122.21 o 13 5 0 501.55 446.54 84.71 o 15 5 0 198.56 175.89 61.26 o 17 5 0 251.87 223.82 100.42 o 0 6 0 446.75 461.49 56.79 o 2 6 0 2633.04 2472.50 89.36 o 4 6 0 6154.68 5560.64 147.12 o 6 6 0 1889.19 1821.43 95.82 o 8 6 0 286.86 289.32 46.84 o 10 6 0 51.14 53.53 29.20 o 12 6 0 232.67 290.74 68.61 o 14 6 0 870.86 862.65 120.01 o 16 6 0 45.96 56.08 76.18 o 1 7 0 4951.43 4869.08 118.17 o 3 7 0 691.29 797.71 67.98 o 5 7 0 751.95 815.19 69.89 o 7 7 0 97.62 162.13 42.14 o 9 7 0 723.68 742.90 88.53 o 11 7 0 580.43 624.27 79.63 o 13 7 0 865.15 992.21 124.59 o 15 7 0 136.22 189.16 84.22 o 0 8 0 9929.53 9824.18 252.13 o 2 8 0 2598.91 2388.02 90.82 o 4 8 0 7.92 18.22 22.93 o 6 8 0 733.96 684.91 75.83 o 8 8 0 14.61 30.90 26.60 o 10 8 0 1553.05 1590.13 106.28 o 12 8 0 668.04 784.91 140.33 o 14 8 0 491.47 563.40 124.52 o 16 8 0 5.94 97.24 99.51 o 1 9 0 6841.16 6640.75 191.21 o 3 9 0 851.20 922.21 68.29 o 5 9 0 2464.74 2342.33 155.28 o 7 9 0 677.89 656.41 110.17 o 9 9 0 30.78 40.99 50.51 o 11 9 0 599.56 649.64 125.90 o 13 9 0 161.08 286.06 127.89 o 15 9 0 4.30 28.00 87.78 o 0 10 0 43.42 41.62 62.81 o 2 10 0 2.94 21.90 29.55 o 4 10 0 1849.77 1543.30 115.63 o 6 10 0 4734.04 4027.16 218.67 o 8 10 0 95.86 69.19 51.46 o 10 10 0 125.96 106.45 69.05 o 12 10 0 35.70 64.49 59.48 o 14 10 0 47.66 156.12 79.72 o 1 11 0 35.68 49.43 44.82 o 3 11 0 177.35 267.48 79.06 o 5 11 0 323.03 289.58 89.87 o 7 11 0 156.87 78.66 54.02 o 9 11 0 1.20 38.32 53.31 o 11 11 0 64.34 60.92 61.27 o 13 11 0 3.32 13.01 65.71 o 0 12 0 409.54 281.52 127.89 o 2 12 0 28.52 57.25 45.17 o 4 12 0 1009.10 1211.46 167.16 o 6 12 0 211.54 233.83 84.00 o 8 12 0 334.94 336.09 97.94 o 10 12 0 3.88 9.46 77.57 o 12 12 0 4.48 0.00 69.62 o 1 13 0 604.29 595.44 126.95 o 3 13 0 1212.41 1057.39 162.52 o 5 13 0 670.23 832.29 150.25 o 7 13 0 273.44 296.01 97.50 o 9 13 0 176.10 231.58 93.38 o 11 13 0 96.75 148.70 110.11 o 0 14 0 654.88 756.76 206.60 o 2 14 0 1138.86 1216.44 186.32 o 4 14 0 1129.21 1081.64 175.69 o 6 14 0 328.32 313.78 136.97 o 8 14 0 171.62 175.10 84.38 o 1 15 0 784.05 975.93 174.58 o 3 15 0 340.69 490.79 130.58 o 5 15 0 113.46 47.03 66.73 o 7 15 0 28.89 107.97 83.29 o 0 16 0 69.88 56.38 105.57 o 2 16 0 40.35 61.16 70.04 o -17 1 1 19.32 67.54 80.04 o -15 1 1 103.72 212.88 88.41 o -13 1 1 1047.06 1050.20 94.81 o -11 1 1 3195.96 2821.05 117.54 o -9 1 1 1297.32 1366.75 59.36 o -7 1 1 255.03 413.09 34.58 o -5 1 1 3644.41 4185.28 71.98 o -3 1 1 57053.65 69159.40 433.77 o -1 1 1 23685.03 25153.30 292.11 o 1 1 1 16964.32 17499.66 342.18 o 3 1 1 902.08 713.30 33.81 o 5 1 1 5709.18 6339.83 145.29 o 7 1 1 2430.40 2890.82 68.35 o 9 1 1 506.20 427.22 53.74 o 11 1 1 1915.54 1924.67 102.85 o 13 1 1 154.95 194.28 47.06 o 15 1 1 138.37 36.82 59.20 o 17 1 1 41.66 201.60 95.25 o -18 2 1 30.16 74.83 96.59 o -16 2 1 574.03 442.22 126.01 o -14 2 1 2.96 12.21 29.42 o -12 2 1 2130.12 2313.46 113.46 o -10 2 1 2316.55 2494.97 85.29 o -8 2 1 603.50 643.91 42.44 o -6 2 1 18563.80 18692.63 1277.05 o -4 2 1 2351.65 1623.06 1125.12 o -2 2 1 1810.51 545.57 374.06 o 0 2 1 14739.02 16062.23 350.75 o 2 2 1 70247.68 81722.70 511.52 o 4 2 1 33972.08 37010.49 405.35 o 6 2 1 2033.44 1829.33 73.40 o 8 2 1 1221.50 1058.05 50.11 o 10 2 1 7020.69 6443.88 203.06 o 12 2 1 3534.10 3239.77 163.11 o 14 2 1 327.41 323.36 61.16 o 16 2 1 250.13 454.26 121.12 o 18 2 1 55.68 80.34 90.92 o -17 3 1 196.50 281.96 102.59 o -15 3 1 76.53 100.83 66.73 o -13 3 1 20.60 25.43 36.26 o -11 3 1 3790.75 3757.07 164.08 o -9 3 1 1771.53 1067.66 284.62 o -7 3 1 9031.92 6205.82 1823.24 o -5 3 1 3419.78 2884.93 293.92 o -3 3 1 52.71 43.05 36.68 o -1 3 1 33937.21 36033.29 242.05 o 1 3 1 22631.44 23522.00 653.75 o 3 3 1 73156.84 80382.02 1271.82 o 5 3 1 14359.30 15803.24 200.40 o 7 3 1 5282.30 5065.56 159.68 o 9 3 1 4181.23 4177.01 117.31 o 11 3 1 3927.89 3877.49 171.10 o 13 3 1 82.11 182.56 55.34 o 15 3 1 428.66 476.96 94.71 o 17 3 1 303.52 436.61 127.89 o -18 4 1 168.41 165.65 104.40 o -16 4 1 432.76 537.79 125.64 o -14 4 1 4.79 47.84 40.93 o -12 4 1 562.85 203.09 201.67 o -10 4 1 989.04 897.29 271.60 o -8 4 1 2671.30 3096.54 95.89 o -6 4 1 3917.35 4119.79 131.63 o -4 4 1 4619.75 4481.26 581.56 o -2 4 1 7307.26 8453.49 255.98 o 0 4 1 618.12 731.07 34.52 o 2 4 1 19716.39 19958.56 372.19 o 4 4 1 44422.55 48704.54 537.25 o 6 4 1 2663.97 2669.26 92.05 o 8 4 1 225.68 147.72 38.38 o 10 4 1 1582.40 1668.78 109.39 o 12 4 1 118.03 138.05 48.73 o 14 4 1 520.92 413.79 81.40 o 16 4 1 773.77 783.64 120.42 o 18 4 1 304.59 261.17 115.46 o -17 5 1 64.88 176.57 92.14 o -15 5 1 426.93 729.11 141.23 o -13 5 1 33.45 0.00 34.98 o -11 5 1 1640.89 1841.36 124.79 o -9 5 1 101.76 102.50 31.14 o -7 5 1 5710.86 5430.85 166.25 o -5 5 1 214.06 170.27 36.83 o -3 5 1 2249.25 2221.80 104.88 o -1 5 1 2688.22 2875.18 77.04 o 1 5 1 4642.00 4908.20 107.37 o 3 5 1 30775.65 33902.36 950.39 o 5 5 1 68.83 65.17 25.85 o 7 5 1 843.87 878.18 66.57 o 9 5 1 1099.95 1083.55 95.48 o 11 5 1 311.37 199.78 55.54 o 13 5 1 158.73 154.51 85.32 o 15 5 1 292.34 320.85 79.99 o 17 5 1 127.79 64.51 81.15 o -16 6 1 6.49 0.00 65.51 o -14 6 1 202.79 241.00 116.30 o -12 6 1 779.96 744.18 101.74 o -10 6 1 1104.74 1129.22 94.31 o -8 6 1 747.50 643.64 103.36 o -6 6 1 638.09 685.83 70.71 o -4 6 1 2248.91 2480.14 99.43 o -2 6 1 25.04 70.96 19.56 o 0 6 1 8281.02 8356.52 193.77 o 2 6 1 16.83 44.27 18.53 o 4 6 1 322.75 284.94 42.36 o 6 6 1 1157.49 1346.21 133.23 o 8 6 1 375.05 412.84 55.46 o 10 6 1 2502.02 2682.61 142.62 o 12 6 1 2114.16 2099.29 140.44 o 14 6 1 54.35 154.40 61.27 o 16 6 1 8.49 0.00 47.44 o -15 7 1 0.26 3.03 59.59 o -13 7 1 271.11 244.87 68.10 o -11 7 1 313.46 277.86 56.28 o -9 7 1 328.17 363.31 54.58 o -7 7 1 3.42 5.31 21.97 o -5 7 1 354.93 532.12 63.62 o -3 7 1 1174.61 1322.07 66.59 o -1 7 1 5000.32 4824.32 117.65 o 1 7 1 496.91 626.16 47.34 o 3 7 1 458.99 540.83 54.68 o 5 7 1 2526.59 2697.00 126.94 o 7 7 1 302.48 299.64 46.88 o 9 7 1 318.32 323.95 53.18 o 11 7 1 376.07 389.45 77.52 o 13 7 1 81.17 97.70 67.23 o 15 7 1 0.03 0.00 55.51 o -16 8 1 0.39 5.68 89.68 o -14 8 1 189.71 227.45 81.77 o -12 8 1 16.28 64.90 39.88 o -10 8 1 237.79 225.20 49.98 o -8 8 1 11.26 0.00 28.10 o -6 8 1 126.11 146.27 39.90 o -4 8 1 396.47 491.03 53.50 o -2 8 1 462.54 408.14 47.00 o 0 8 1 209.06 235.59 35.99 o 2 8 1 1321.02 1461.81 70.37 o 4 8 1 27.49 43.94 25.13 o 6 8 1 767.12 806.27 80.78 o 8 8 1 126.58 105.61 41.67 o 10 8 1 51.42 132.31 49.53 o 12 8 1 76.89 91.19 82.49 o 14 8 1 158.08 126.45 71.89 o 16 8 1 0.38 0.00 79.46 o -15 9 1 82.45 116.54 113.89 o -13 9 1 300.28 363.12 102.03 o -11 9 1 269.84 278.82 89.30 o -9 9 1 13.08 21.52 43.89 o -7 9 1 9.61 2.22 28.28 o -5 9 1 103.36 57.46 27.15 o -3 9 1 2095.80 1917.82 89.36 o -1 9 1 1534.85 1468.30 86.46 o 1 9 1 1106.27 1020.21 88.04 o 3 9 1 519.87 507.36 71.39 o 5 9 1 792.92 677.18 104.58 o 7 9 1 435.21 381.25 85.72 o 9 9 1 294.29 263.59 79.08 o 11 9 1 64.51 132.22 63.12 o 13 9 1 179.29 125.07 75.71 o 15 9 1 8.80 0.00 111.81 o -14 10 1 8.43 0.00 59.52 o -12 10 1 172.85 291.39 90.50 o -10 10 1 356.47 384.09 97.56 o -8 10 1 38.04 40.96 49.09 o -6 10 1 902.71 912.35 103.02 o -4 10 1 170.57 219.63 57.30 o -2 10 1 2504.40 2599.53 181.43 o 0 10 1 3650.86 3536.77 153.05 o 2 10 1 6678.76 6397.08 211.10 o 4 10 1 641.57 627.04 86.38 o 6 10 1 1422.37 1679.39 152.73 o 8 10 1 190.67 240.91 76.89 o 10 10 1 177.92 259.94 85.21 o 12 10 1 48.80 71.99 66.84 o 14 10 1 19.76 3.16 67.55 o -13 11 1 21.32 82.23 70.88 o -11 11 1 507.88 463.55 111.82 o -9 11 1 664.46 695.47 129.03 o -7 11 1 2334.46 2220.72 262.98 o -5 11 1 1500.06 1427.83 166.94 o -3 11 1 211.92 154.00 63.09 o -1 11 1 76.60 53.81 49.91 o 1 11 1 1378.56 1513.88 166.13 o 3 11 1 364.39 387.45 93.30 o 5 11 1 3885.81 3392.69 195.17 o 7 11 1 1758.73 1844.65 172.86 o 9 11 1 642.34 738.51 136.30 o 11 11 1 115.48 147.74 91.00 o 13 11 1 180.46 258.92 93.53 o -12 12 1 28.90 129.03 98.38 o -10 12 1 280.13 299.30 138.11 o -8 12 1 280.73 486.70 112.91 o -6 12 1 1110.16 1170.48 165.82 o -4 12 1 89.98 70.32 51.30 o -2 12 1 1779.96 1466.18 174.20 o 0 12 1 2621.86 2495.64 231.76 o 2 12 1 502.44 590.22 156.84 o 4 12 1 785.73 626.48 129.73 o 6 12 1 1401.12 1267.22 175.77 o 8 12 1 691.52 735.95 205.46 o 10 12 1 113.47 109.82 69.60 o 12 12 1 126.04 74.86 76.00 o -11 13 1 17.75 14.54 60.68 o -9 13 1 82.19 135.24 79.45 o -7 13 1 64.42 105.98 69.44 o -5 13 1 273.70 383.63 102.30 o -3 13 1 71.01 101.09 65.03 o -1 13 1 970.24 925.84 152.30 o 1 13 1 328.09 417.49 110.44 o 3 13 1 157.56 79.25 63.37 o 5 13 1 96.58 157.70 72.35 o 7 13 1 283.72 312.76 98.80 o 9 13 1 190.59 179.73 106.33 o 11 13 1 98.12 188.06 117.68 o -8 14 1 8.62 23.95 61.42 o -6 14 1 0.31 0.00 43.10 o -4 14 1 102.06 148.47 81.64 o -2 14 1 54.85 43.98 61.42 o 0 14 1 62.49 75.47 66.24 o 2 14 1 43.24 14.14 56.90 o 4 14 1 14.27 26.38 64.54 o 6 14 1 16.84 0.00 55.62 o 8 14 1 0.07 0.00 56.57 o -7 15 1 0.62 0.00 60.37 o -5 15 1 38.66 37.36 59.98 o -3 15 1 72.89 142.55 75.63 o -1 15 1 120.79 75.75 73.81 o 1 15 1 191.07 165.39 90.81 o 3 15 1 415.60 551.83 141.59 o 5 15 1 108.69 40.93 64.38 o 7 15 1 44.20 0.00 77.57 o -2 16 1 88.90 56.70 65.42 o 0 16 1 92.25 60.54 77.60 o 2 16 1 209.86 216.15 97.69 o -18 0 2 1618.35 1454.88 306.49 o -16 0 2 570.47 535.79 189.95 o -14 0 2 8.27 7.95 77.57 o -12 0 2 1763.49 1791.37 144.40 o -10 0 2 15.32 33.58 22.70 o -8 0 2 515.74 480.16 49.87 o -6 0 2 7189.05 6451.73 116.79 o -4 0 2 1137.78 1275.61 43.00 o -2 0 2 1305.58 846.73 42.77 o 0 0 2 45845.02 40310.13 386.33 o 2 0 2 10617.85 12058.90 153.78 o 4 0 2 40.33 65.26 25.15 o 6 0 2 4355.49 4820.72 168.42 o 8 0 2 1051.33 1029.51 98.56 o 10 0 2 1656.07 1470.25 170.65 o 12 0 2 3713.23 3671.66 256.35 o 14 0 2 52.38 48.02 46.55 o 16 0 2 263.49 493.84 117.00 o 18 0 2 60.95 227.03 151.73 o -17 1 2 1275.02 1169.20 192.29 o -15 1 2 63.38 49.66 60.83 o -13 1 2 1110.28 1117.12 94.27 o -11 1 2 1436.40 1375.31 86.76 o -9 1 2 3555.82 3669.70 102.15 o -7 1 2 1817.44 1599.42 53.26 o -5 1 2 5405.14 4838.11 70.58 o -3 1 2 172.00 129.96 14.08 o -1 1 2 23223.20 30614.37 330.31 o 1 1 2 683.49 354.73 21.41 o 3 1 2 14991.24 14646.12 156.28 o 5 1 2 6462.65 6245.03 125.25 o 7 1 2 30126.78 31901.08 329.01 o 9 1 2 538.38 391.67 51.87 o 11 1 2 3114.66 2996.18 129.23 o 13 1 2 290.75 336.39 62.78 o 15 1 2 524.62 613.90 87.53 o 17 1 2 168.46 267.44 112.45 o -18 2 2 472.72 352.99 122.39 o -16 2 2 67.03 69.39 73.37 o -14 2 2 540.77 521.86 114.17 o -12 2 2 944.11 1052.04 87.31 o -10 2 2 1344.71 1318.32 64.71 o -8 2 2 10874.34 11508.58 171.46 o -6 2 2 3105.10 3214.60 88.44 o -4 2 2 8009.11 8367.60 122.73 o -2 2 2 874.84 1005.67 51.29 o 0 2 2 2334.16 2085.20 72.23 o 2 2 2 24837.09 24996.76 509.72 o 4 2 2 14728.83 15793.70 304.09 o 6 2 2 5932.22 6206.58 137.52 o 8 2 2 3577.63 3489.01 106.62 o 10 2 2 303.94 323.73 52.87 o 12 2 2 225.67 283.56 54.55 o 14 2 2 477.12 548.16 79.08 o 16 2 2 597.83 536.29 86.45 o 18 2 2 51.84 69.39 93.34 o -17 3 2 449.29 440.69 122.89 o -15 3 2 208.28 213.69 89.33 o -13 3 2 145.57 173.84 55.40 o -11 3 2 70.64 0.00 29.73 o -9 3 2 7110.79 7025.31 146.46 o -7 3 2 4862.94 4627.16 118.08 o -5 3 2 1530.83 1558.95 134.04 o -3 3 2 29.90 46.76 26.08 o -1 3 2 16936.59 19463.66 191.72 o 1 3 2 10105.77 11234.93 223.32 o 3 3 2 58965.61 64418.67 985.96 o 5 3 2 58.07 95.60 26.07 o 7 3 2 2222.66 2331.56 106.83 o 9 3 2 25.75 13.30 21.69 o 11 3 2 324.52 298.53 55.46 o 13 3 2 67.98 86.20 36.35 o 15 3 2 1071.11 1136.44 141.91 o 17 3 2 7.63 21.29 79.46 o -18 4 2 1.98 56.69 78.12 o -16 4 2 83.45 146.90 80.98 o -14 4 2 290.22 317.30 92.53 o -12 4 2 16.69 84.79 45.09 o -10 4 2 324.26 315.90 43.46 o -8 4 2 2.64 0.00 15.05 o -6 4 2 1797.68 1188.16 732.11 o -4 4 2 326.59 266.43 105.94 o -2 4 2 4461.60 5389.56 100.00 o 0 4 2 744.29 853.63 37.33 o 2 4 2 2189.00 2232.11 120.68 o 4 4 2 316.60 467.49 40.20 o 6 4 2 846.02 838.32 68.75 o 8 4 2 527.18 563.44 70.93 o 10 4 2 67.84 100.67 40.18 o 12 4 2 108.71 55.42 42.13 o 14 4 2 49.70 111.47 52.58 o 16 4 2 3.24 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