#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/99/2219954.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219954_Fobs loop_ _publ_author_name 'Nettleman, Joseph H.' 'LaDuca, Robert L.' _publ_section_title ; catena-Poly[[[tetraaquacobalt(II)]-\m-4,4'-bipyridine-\k^2^N:N'] bis(perchlorate) 4,4'-bipyridine disolvate dihydrate] ; _journal_coeditor_code NG2505 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1485 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 64.290 _cell_angle_beta 71.747 _cell_angle_gamma 66.848 _cell_length_a 8.9590 _cell_length_b 10.8458 _cell_length_c 11.4328 _exptl_crystal_F_000 431.00 _reflns_d_resolution_high 0.7509 _[local]_cod_data_source_file ng2505Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p1b in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 125.67 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6.65 1.11 0.18 o 2 0 0 4168.37 4272.20 58.90 o 3 0 0 723.99 752.59 9.13 o 4 0 0 49.49 57.55 1.01 o 5 0 0 1182.22 1159.99 16.54 o 6 0 0 24.88 28.89 1.50 o 7 0 0 485.05 446.05 7.07 o 8 0 0 172.30 157.28 3.98 o 9 0 0 59.48 64.41 2.54 o 10 0 0 171.04 183.05 4.91 o -10 1 0 84.87 72.65 4.24 o -9 1 0 42.15 38.84 2.02 o -8 1 0 31.95 32.65 1.73 o -7 1 0 57.45 50.14 2.04 o -6 1 0 9.89 10.56 0.78 o -5 1 0 42.56 45.69 2.23 o -4 1 0 2105.72 2313.83 32.20 o -3 1 0 4574.09 4666.74 54.96 o -2 1 0 9667.96 9994.92 156.04 o -1 1 0 3683.90 3858.13 45.73 o 0 1 0 911.09 843.70 13.64 o 1 1 0 2972.74 3089.77 36.95 o 2 1 0 8569.17 8817.13 114.73 o 3 1 0 48.00 61.21 0.96 o 4 1 0 1497.69 1451.61 17.38 o 5 1 0 4.83 12.18 0.92 o 6 1 0 595.35 552.12 8.32 o 7 1 0 14.56 19.45 1.04 o 8 1 0 330.60 336.20 6.98 o 9 1 0 282.32 260.12 6.94 o 10 1 0 57.19 51.69 2.42 o -9 2 0 46.11 36.19 2.13 o -8 2 0 2.74 3.27 1.04 o -7 2 0 92.84 98.27 2.36 o -6 2 0 119.47 123.50 2.54 o -5 2 0 3.85 4.35 0.59 o -4 2 0 1868.18 1999.96 23.88 o -3 2 0 98.85 80.65 1.46 o -2 2 0 1397.13 1338.10 15.98 o -1 2 0 13852.85 14019.80 165.28 o 0 2 0 942.10 939.90 15.53 o 1 2 0 11591.06 11540.12 136.54 o 2 2 0 2166.67 2162.71 27.02 o 3 2 0 2.37 1.18 0.21 o 4 2 0 977.19 1075.24 12.98 o 5 2 0 206.87 228.45 4.26 o 6 2 0 250.69 246.45 4.15 o 7 2 0 1.21 0.76 0.57 o 8 2 0 942.50 1001.25 42.25 o 9 2 0 144.02 148.32 4.33 o 10 2 0 217.92 211.62 5.31 o -9 3 0 12.66 14.53 1.73 o -8 3 0 1.21 0.37 1.09 o -7 3 0 65.53 61.23 5.80 o -6 3 0 14.28 17.85 2.51 o -5 3 0 387.81 408.60 6.44 o -4 3 0 85.03 90.27 1.62 o -3 3 0 8316.39 8841.99 103.76 o -2 3 0 1266.14 1243.30 14.92 o -1 3 0 699.06 768.69 11.08 o 0 3 0 1928.93 1915.74 22.70 o 1 3 0 1188.33 1252.00 14.92 o 2 3 0 28.40 24.44 0.74 o 3 3 0 941.90 1130.54 13.57 o 4 3 0 270.92 295.25 3.85 o 5 3 0 860.12 843.99 10.35 o 6 3 0 123.69 134.37 4.74 o 7 3 0 653.39 639.66 9.61 o 8 3 0 221.68 214.39 3.96 o 9 3 0 290.56 289.04 6.35 o 10 3 0 172.82 170.54 4.90 o -8 4 0 66.64 77.06 4.08 o -7 4 0 89.37 97.06 3.00 o -6 4 0 96.21 97.29 2.32 o -5 4 0 1314.91 1298.23 18.65 o -4 4 0 37.66 31.70 0.95 o -3 4 0 5096.29 5181.18 61.05 o -2 4 0 706.73 731.33 9.03 o -1 4 0 1182.20 1163.73 13.98 o 0 4 0 1535.72 1609.43 19.20 o 2 4 0 2246.49 2142.63 25.43 o 3 4 0 953.63 1009.31 12.20 o 4 4 0 269.17 230.11 3.14 o 5 4 0 649.55 654.00 11.76 o 6 4 0 322.75 326.42 5.80 o 7 4 0 655.56 677.19 10.17 o 8 4 0 394.90 398.30 13.22 o 9 4 0 974.93 979.01 38.12 o 10 4 0 34.04 33.66 1.96 o 11 4 0 50.23 43.75 3.59 o -8 5 0 7.86 5.39 2.29 o -7 5 0 162.69 154.93 5.88 o -6 5 0 269.98 288.79 6.28 o -5 5 0 146.44 152.03 4.65 o -4 5 0 1168.14 1155.45 26.49 o -3 5 0 422.10 415.97 5.48 o -2 5 0 556.89 585.56 9.24 o -1 5 0 2278.39 2307.66 40.25 o 0 5 0 4.58 8.59 0.65 o 1 5 0 2577.81 2590.24 30.69 o 3 5 0 100.68 81.36 1.40 o 4 5 0 601.58 623.33 7.76 o 5 5 0 1496.58 1565.67 18.85 o 6 5 0 1948.42 1932.83 23.23 o 7 5 0 269.92 273.53 4.68 o 8 5 0 789.54 800.77 11.99 o 9 5 0 296.17 287.21 6.28 o 10 5 0 248.03 224.95 5.48 o 11 5 0 38.70 35.10 3.27 o -7 6 0 84.59 84.24 4.41 o -6 6 0 155.27 131.31 3.69 o -5 6 0 129.33 120.42 3.34 o -4 6 0 591.85 584.52 11.00 o -3 6 0 182.45 189.75 4.72 o -2 6 0 1283.21 1298.68 23.75 o -1 6 0 151.26 141.48 3.37 o 0 6 0 56.98 70.56 1.14 o 1 6 0 708.40 712.49 8.80 o 2 6 0 1.97 2.35 0.36 o 3 6 0 1108.17 1049.44 12.78 o 4 6 0 41.94 37.54 1.27 o 5 6 0 1867.65 1852.29 22.25 o 6 6 0 480.67 495.73 7.80 o 7 6 0 625.73 628.42 9.51 o 8 6 0 876.52 875.08 13.02 o 9 6 0 31.32 31.04 2.29 o 10 6 0 161.15 163.91 6.53 o -7 7 0 18.72 15.18 2.61 o -6 7 0 231.39 236.65 5.71 o -5 7 0 218.63 219.87 5.23 o -4 7 0 0.15 -0.64 0.86 o -3 7 0 214.91 221.29 3.94 o -2 7 0 0.68 0.77 0.59 o -1 7 0 78.99 81.00 1.87 o 0 7 0 82.99 87.22 2.49 o 1 7 0 35.26 51.66 1.34 o 2 7 0 865.64 810.00 14.46 o 3 7 0 97.89 87.39 4.33 o 4 7 0 440.03 438.02 7.20 o 5 7 0 604.10 575.69 8.66 o 6 7 0 446.64 456.67 9.11 o 7 7 0 564.27 602.71 11.60 o 8 7 0 0.26 1.06 1.22 o 9 7 0 310.07 310.68 9.80 o 10 7 0 33.30 32.16 2.94 o -6 8 0 114.49 109.45 7.84 o -5 8 0 26.53 26.85 2.02 o -4 8 0 179.40 194.29 4.82 o -3 8 0 58.34 60.85 1.85 o -2 8 0 33.74 40.60 1.47 o -1 8 0 145.35 147.58 4.85 o 0 8 0 2.08 1.67 0.74 o 1 8 0 473.25 467.12 8.98 o 2 8 0 5.81 9.95 1.71 o 3 8 0 466.01 439.62 9.55 o 4 8 0 609.61 612.32 11.35 o 5 8 0 336.40 318.20 6.45 o 6 8 0 1379.05 1371.44 23.96 o 7 8 0 158.89 146.25 3.87 o 8 8 0 84.24 87.67 2.89 o 9 8 0 46.49 42.61 3.10 o 10 8 0 7.82 9.80 2.12 o -5 9 0 57.20 53.22 3.92 o -4 9 0 63.71 60.57 3.92 o -3 9 0 0.13 -0.82 1.63 o -2 9 0 242.50 247.81 5.69 o -1 9 0 0.51 0.08 0.90 o 0 9 0 20.72 20.25 1.49 o 1 9 0 185.17 188.17 4.43 o 2 9 0 1140.40 1098.62 19.59 o 3 9 0 1080.67 1094.73 19.47 o 4 9 0 212.42 215.10 5.88 o 5 9 0 1027.71 1058.13 18.89 o 6 9 0 179.82 179.36 4.32 o 7 9 0 177.80 192.85 7.51 o 8 9 0 48.56 41.30 3.10 o -3 10 0 1.75 1.63 1.96 o -2 10 0 24.30 22.26 1.79 o -1 10 0 98.88 107.11 3.28 o 0 10 0 577.62 596.62 11.58 o 1 10 0 2.74 0.91 1.22 o 2 10 0 466.21 466.44 9.28 o 3 10 0 171.18 159.47 4.09 o 4 10 0 572.98 529.41 10.31 o 5 10 0 343.14 333.56 7.08 o 6 10 0 141.21 131.88 3.67 o 7 10 0 362.43 378.80 7.89 o 8 10 0 0.36 0.49 1.96 o -2 11 0 15.77 12.87 1.72 o -1 11 0 0.36 -0.02 1.21 o 0 11 0 20.01 17.74 1.62 o 1 11 0 130.26 133.70 3.92 o 2 11 0 390.17 392.81 14.04 o 3 11 0 211.09 188.17 4.78 o 4 11 0 335.76 319.55 6.97 o 5 11 0 8.58 7.82 1.32 o 6 11 0 156.82 148.38 7.51 o 7 11 0 2.43 5.01 1.32 o 8 11 0 6.13 6.86 2.45 o 1 12 0 140.05 134.76 4.09 o 2 12 0 30.61 26.51 2.02 o 3 12 0 249.87 243.88 5.99 o 4 12 0 29.35 26.61 2.61 o 5 12 0 0.78 2.72 1.37 o 6 12 0 63.83 72.09 2.93 o 7 12 0 1.38 1.96 1.80 o -4 -12 1 92.73 97.14 5.06 o -7 -11 1 85.37 88.95 3.17 o -6 -11 1 21.22 19.87 1.80 o -5 -11 1 3.54 6.04 1.32 o -4 -11 1 32.74 34.36 2.02 o -3 -11 1 2.47 2.96 1.22 o -2 -11 1 84.82 86.74 5.22 o -1 -11 1 0.34 -0.16 1.15 o 0 -11 1 4.63 4.22 1.44 o 1 -11 1 56.93 65.28 2.81 o -7 -10 1 37.19 29.97 2.00 o -6 -10 1 117.82 117.96 3.51 o -5 -10 1 239.04 242.06 5.59 o -4 -10 1 2.68 2.29 1.09 o -3 -10 1 89.64 89.26 2.93 o -2 -10 1 42.06 37.68 5.55 o -1 -10 1 6.74 3.14 1.06 o 0 -10 1 12.25 13.06 1.50 o 1 -10 1 0.53 2.12 1.71 o 2 -10 1 133.89 131.76 3.90 o 3 -10 1 7.95 11.26 2.45 o -7 -9 1 37.03 42.80 2.94 o -6 -9 1 282.17 264.74 5.82 o -5 -9 1 7.08 5.70 1.09 o -4 -9 1 37.96 37.74 2.61 o -3 -9 1 287.13 273.03 5.94 o -2 -9 1 35.67 29.82 1.62 o -1 -9 1 111.72 108.48 3.11 o 0 -9 1 142.70 142.85 3.74 o 1 -9 1 111.64 112.91 3.28 o 2 -9 1 64.49 64.49 2.46 o 3 -9 1 33.94 29.39 2.78 o 4 -9 1 15.47 17.14 2.61 o -7 -8 1 153.97 153.85 3.86 o -6 -8 1 186.67 187.80 5.88 o -5 -8 1 25.08 22.03 1.49 o -4 -8 1 342.73 348.19 9.96 o -3 -8 1 43.95 51.00 1.90 o -2 -8 1 692.55 680.16 19.84 o -1 -8 1 98.01 95.02 3.10 o 0 -8 1 0.38 0.14 0.51 o 1 -8 1 218.12 228.92 5.28 o 2 -8 1 4.82 5.85 1.23 o 3 -8 1 116.70 118.52 2.69 o 4 -8 1 21.03 22.45 1.73 o 5 -8 1 48.51 52.95 2.94 o 6 -8 1 29.22 31.29 2.42 o -10 -7 1 54.34 59.26 3.92 o -9 -7 1 68.69 67.92 3.92 o -8 -7 1 25.25 23.84 2.45 o -7 -7 1 163.37 170.52 4.21 o -6 -7 1 108.65 98.86 3.17 o -5 -7 1 466.21 436.10 8.35 o -4 -7 1 33.90 37.16 1.24 o -3 -7 1 39.23 43.69 1.31 o -2 -7 1 116.57 114.66 2.48 o -1 -7 1 3.95 4.33 1.02 o 0 -7 1 385.82 374.32 6.01 o 1 -7 1 14.27 14.99 0.79 o 2 -7 1 644.76 625.79 9.34 o 3 -7 1 15.16 16.66 1.09 o 4 -7 1 0.41 -0.24 0.92 o 5 -7 1 10.16 9.73 1.37 o 6 -7 1 0.26 2.04 1.63 o -10 -6 1 61.62 57.51 2.78 o -9 -6 1 32.66 34.91 1.95 o -8 -6 1 115.13 121.19 3.39 o -7 -6 1 76.52 78.40 2.01 o -6 -6 1 452.67 443.56 7.02 o -5 -6 1 61.65 61.38 1.35 o -4 -6 1 39.61 35.60 0.97 o -3 -6 1 427.29 392.55 6.39 o -2 -6 1 3.59 4.23 0.53 o -1 -6 1 915.44 915.05 12.98 o 0 -6 1 66.40 66.66 1.60 o 1 -6 1 5.51 4.59 0.51 o 2 -6 1 243.29 234.72 3.98 o 3 -6 1 24.43 29.00 1.18 o 4 -6 1 206.92 201.82 4.67 o 5 -6 1 12.50 15.08 1.44 o 6 -6 1 22.50 23.63 1.73 o 7 -6 1 1.66 0.17 1.32 o -10 -5 1 10.84 10.94 1.50 o -9 -5 1 181.10 176.85 4.43 o -8 -5 1 60.16 62.40 2.86 o -7 -5 1 47.53 52.63 1.94 o -6 -5 1 228.98 225.51 3.30 o -5 -5 1 116.61 125.63 2.59 o -4 -5 1 1255.45 1289.54 15.63 o -3 -5 1 13.71 10.87 0.56 o -2 -5 1 2076.89 2164.54 25.74 o -1 -5 1 17.01 15.46 0.75 o 0 -5 1 333.30 338.35 4.42 o 1 -5 1 676.22 641.50 7.13 o 2 -5 1 3.82 3.86 0.57 o 3 -5 1 526.07 513.90 7.68 o 4 -5 1 17.70 15.14 1.25 o 5 -5 1 0.32 -0.16 0.86 o 6 -5 1 244.57 244.25 8.82 o 7 -5 1 40.94 31.53 2.02 o 8 -5 1 26.03 27.10 3.10 o -10 -4 1 120.18 112.38 3.57 o -9 -4 1 40.56 38.91 2.02 o -8 -4 1 42.83 38.53 1.79 o -7 -4 1 202.00 199.14 4.61 o -6 -4 1 0.39 0.28 0.38 o -5 -4 1 844.59 843.65 10.43 o -4 -4 1 552.30 627.33 7.85 o -3 -4 1 181.48 184.37 2.59 o -2 -4 1 353.23 317.55 4.43 o -1 -4 1 2468.81 2751.63 45.62 o 0 -4 1 1820.08 1732.41 20.68 o 1 -4 1 17.82 14.87 0.46 o 2 -4 1 1222.05 1212.61 14.65 o 3 -4 1 313.70 294.64 3.99 o 4 -4 1 50.46 49.38 2.21 o 5 -4 1 23.79 14.49 1.71 o 6 -4 1 38.94 31.32 1.80 o 7 -4 1 181.61 169.94 4.38 o 8 -4 1 29.11 24.33 2.78 o -10 -3 1 16.94 18.77 1.73 o -9 -3 1 1.93 0.34 0.90 o -8 -3 1 203.85 193.54 4.55 o -7 -3 1 0.41 0.76 0.64 o -6 -3 1 17.86 29.39 1.96 o -5 -3 1 481.56 497.26 6.33 o -4 -3 1 0.54 0.80 0.30 o -3 -3 1 3264.28 3471.34 40.92 o -2 -3 1 83.81 89.50 1.35 o -1 -3 1 4937.56 4826.26 56.87 o 1 -3 1 5.86 11.42 0.47 o 2 -3 1 31.17 21.44 0.71 o 3 -3 1 110.88 114.31 2.33 o 4 -3 1 902.62 884.86 12.14 o 5 -3 1 309.88 275.24 4.58 o 6 -3 1 5.20 5.91 0.85 o 7 -3 1 44.20 55.10 1.76 o 8 -3 1 13.61 11.93 2.53 o 9 -3 1 19.63 18.28 2.61 o -10 -2 1 16.15 19.84 1.79 o -9 -2 1 71.21 61.88 2.42 o -8 -2 1 46.42 43.77 2.04 o -7 -2 1 12.92 11.15 1.18 o -6 -2 1 166.61 152.33 2.82 o -5 -2 1 392.01 471.25 6.00 o -4 -2 1 332.51 306.74 3.99 o -3 -2 1 54.07 43.82 0.81 o -2 -2 1 705.03 697.57 8.44 o -1 -2 1 600.83 606.46 7.45 o 0 -2 1 1256.83 1253.42 17.13 o 1 -2 1 3146.92 3165.15 33.30 o 2 -2 1 144.34 129.55 1.84 o 3 -2 1 1629.47 1557.34 31.15 o 4 -2 1 378.48 403.73 10.79 o 5 -2 1 61.25 58.61 1.54 o 6 -2 1 59.73 57.51 1.63 o 7 -2 1 114.54 105.02 2.76 o 8 -2 1 72.78 65.28 4.82 o 9 -2 1 1.14 2.85 1.25 o 10 -2 1 19.14 18.45 2.61 o -10 -1 1 0.91 2.56 1.32 o -9 -1 1 33.25 31.11 1.85 o -8 -1 1 1.02 -0.16 0.81 o -7 -1 1 730.36 703.43 17.06 o -6 -1 1 82.20 73.22 2.83 o -5 -1 1 62.20 63.58 1.18 o -4 -1 1 1096.19 1129.63 13.63 o -3 -1 1 213.54 208.98 4.41 o -2 -1 1 3365.42 3332.39 39.35 o -1 -1 1 22.23 18.17 0.41 o 0 -1 1 3438.43 3412.16 46.27 o 1 -1 1 7.58 14.13 0.78 o 2 -1 1 15794.03 16036.71 189.06 o 3 -1 1 3582.21 3664.22 69.28 o 4 -1 1 0.37 2.61 0.31 o 5 -1 1 948.83 910.16 13.12 o 6 -1 1 4.08 4.67 0.81 o 7 -1 1 178.62 171.30 3.30 o 8 -1 1 80.89 86.55 2.26 o 9 -1 1 11.41 9.31 1.39 o 10 -1 1 2.60 3.97 1.37 o -10 0 1 25.84 24.33 2.02 o -9 0 1 0.17 0.14 0.98 o -8 0 1 128.68 128.37 3.52 o -7 0 1 31.30 30.17 1.56 o -6 0 1 573.35 565.32 8.57 o -5 0 1 694.35 706.71 10.36 o -4 0 1 1038.90 1102.70 18.15 o -3 0 1 2856.68 2750.33 32.52 o -2 0 1 1090.41 1071.11 12.86 o -1 0 1 623.35 639.27 7.75 o 0 0 1 17.09 18.78 0.33 o 1 0 1 70.94 74.19 0.98 o 2 0 1 10828.99 10627.08 127.06 o 3 0 1 2.89 36.57 1.63 o 4 0 1 523.53 467.81 6.91 o 5 0 1 932.14 968.80 19.32 o 6 0 1 11.98 10.28 0.92 o 7 0 1 321.95 329.41 5.47 o 8 0 1 0.98 2.45 0.75 o 9 0 1 148.58 133.80 6.04 o 10 0 1 0.67 1.34 1.25 o -9 1 1 9.84 8.90 1.39 o -8 1 1 268.70 248.28 5.65 o -7 1 1 12.25 14.80 1.27 o -6 1 1 426.93 416.18 6.56 o -5 1 1 176.03 185.67 3.90 o -4 1 1 2415.90 2446.33 29.08 o -3 1 1 19.82 16.11 0.66 o -2 1 1 715.39 671.23 10.39 o -1 1 1 2403.86 2449.45 29.01 o 0 1 1 357.42 328.61 8.52 o 1 1 1 1776.18 1950.82 23.41 o 2 1 1 104.00 101.54 1.66 o 3 1 1 44.71 38.50 0.91 o 4 1 1 3104.70 3197.47 44.19 o 5 1 1 38.41 41.03 1.13 o 6 1 1 449.07 436.56 12.73 o 7 1 1 233.31 232.95 6.62 o 8 1 1 403.06 400.56 6.56 o 9 1 1 13.12 17.33 2.20 o 10 1 1 3.41 3.98 1.21 o -9 2 1 1.18 1.10 1.21 o -8 2 1 0.34 0.27 0.98 o -7 2 1 201.69 185.14 4.44 o -6 2 1 84.76 85.92 2.48 o -5 2 1 171.86 167.67 3.05 o -4 2 1 41.27 37.20 1.62 o -3 2 1 8.24 14.11 0.55 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93.14 99.97 3.29 o 8 7 12 73.08 76.19 4.73 o 9 7 12 1.66 0.97 1.32 o -1 8 12 2.69 2.45 1.27 o 0 8 12 197.32 194.55 5.01 o 1 8 12 1.20 1.55 1.06 o 2 8 12 63.43 56.58 2.36 o 3 8 12 77.05 71.36 2.60 o 4 8 12 200.73 196.91 4.78 o 5 8 12 86.32 91.96 2.94 o 6 8 12 2.71 0.98 1.47 o 7 8 12 69.97 78.00 2.89 o 8 8 12 6.01 3.95 1.32 o 9 8 12 42.95 42.14 2.36 o 0 9 12 15.87 16.88 3.02 o 1 9 12 142.23 139.31 4.04 o 2 9 12 175.80 174.25 4.61 o 3 9 12 1.84 2.53 1.04 o 4 9 12 277.29 268.90 15.67 o 5 9 12 19.32 16.39 1.55 o 6 9 12 111.04 110.69 4.90 o 7 9 12 24.79 23.83 1.95 o 8 9 12 139.20 144.20 4.27 o 9 9 12 57.91 67.26 4.24 o 1 10 12 164.73 164.07 4.61 o 2 10 12 1.64 2.36 1.21 o 3 10 12 167.25 167.24 4.50 o 4 10 12 55.15 50.74 2.36 o 5 10 12 103.36 101.65 3.35 o 6 10 12 93.79 93.69 3.16 o 7 10 12 11.96 11.43 1.56 o 8 10 12 156.98 157.79 6.04 o 2 11 12 44.35 43.10 2.42 o 3 11 12 12.92 10.94 2.12 o 4 11 12 73.52 83.01 2.99 o 5 11 12 66.17 67.44 2.76 o 6 11 12 2.80 1.95 1.21 o 7 11 12 80.55 84.25 3.17 o 8 11 12 2.98 2.94 2.12 o 4 12 12 20.89 14.69 2.45 o 5 12 12 4.37 3.92 1.96 o 6 12 12 62.90 60.08 3.75 o 1 0 13 10.31 6.71 1.44 o 2 0 13 3.33 0.98 1.27 o 3 0 13 54.31 45.97 2.53 o -1 1 13 0.59 1.14 1.96 o 0 1 13 75.98 75.01 4.24 o 1 1 13 2.46 2.45 1.32 o 2 1 13 79.77 72.45 3.18 o 3 1 13 3.60 3.10 1.27 o 4 1 13 6.60 5.06 2.12 o 5 1 13 25.06 29.56 2.39 o -1 2 13 48.00 41.20 2.37 o 0 2 13 17.41 24.11 1.88 o 1 2 13 0.79 0.49 1.15 o 2 2 13 25.92 22.59 1.79 o 3 2 13 16.54 19.88 3.59 o 4 2 13 110.79 103.83 4.73 o 5 2 13 8.00 6.37 1.96 o 6 2 13 52.37 62.48 4.24 o 7 2 13 3.47 4.15 3.10 o -2 3 13 29.12 29.71 3.10 o -1 3 13 9.22 10.23 3.92 o 0 3 13 2.52 6.62 1.32 o 1 3 13 14.64 7.90 1.32 o 2 3 13 0.51 1.85 1.09 o 3 3 13 42.14 46.71 3.51 o 4 3 13 2.21 2.78 1.15 o 5 3 13 23.48 25.31 2.78 o 7 3 13 2.65 3.59 1.96 o -2 4 13 0.66 1.96 1.96 o -1 4 13 0.56 -1.15 1.15 o 0 4 13 94.28 82.13 3.18 o 1 4 13 16.95 17.45 3.02 o 2 4 13 108.84 118.15 3.40 o 3 4 13 53.91 51.89 3.51 o 4 4 13 44.47 52.57 3.10 o 7 4 13 90.58 101.55 5.06 o 8 4 13 0.45 1.31 2.29 o -2 5 13 6.91 8.33 2.29 o -1 5 13 98.68 90.01 3.75 o 0 5 13 11.10 14.07 1.56 o 1 5 13 101.46 86.90 2.94 o 2 5 13 52.58 57.96 3.43 o 3 5 13 85.99 94.53 4.24 o 4 5 13 126.20 132.89 5.06 o 8 5 13 26.28 17.31 2.78 o -1 6 13 27.46 23.41 1.90 o 0 6 13 31.39 35.07 2.02 o 1 6 13 64.86 70.27 2.71 o 2 6 13 11.10 8.72 1.32 o 3 6 13 241.66 254.58 6.61 o 4 6 13 17.65 20.87 1.67 o 5 6 13 64.59 62.57 2.42 o 6 6 13 46.77 40.16 2.94 o 8 6 13 14.64 16.98 2.94 o -1 7 13 5.47 4.24 1.96 o 0 7 13 52.21 51.36 6.29 o 1 7 13 7.93 12.33 1.56 o 2 7 13 61.45 66.12 2.60 o 3 7 13 13.15 12.17 1.63 o 4 7 13 13.66 18.35 1.67 o 5 7 13 9.16 6.62 1.39 o 6 7 13 25.01 32.16 2.78 o 7 7 13 29.07 21.22 2.61 o 8 7 13 6.92 5.11 1.44 o 9 7 13 3.39 1.14 1.96 o 0 8 13 27.70 32.81 3.10 o 1 8 13 8.38 7.78 1.39 o 2 8 13 39.22 40.05 2.45 o 3 8 13 8.21 10.06 1.50 o 4 8 13 144.28 141.68 3.97 o 5 8 13 1.27 3.75 1.15 o 6 8 13 2.78 0.98 1.47 o 7 8 13 3.16 1.31 1.80 o 8 8 13 0.32 0.49 1.27 o 1 9 13 230.16 238.97 5.88 o 2 9 13 0.32 -1.09 1.09 o 3 9 13 32.08 32.30 2.02 o 4 9 13 10.65 8.02 1.44 o 5 9 13 15.32 9.62 1.44 o 6 9 13 20.34 21.22 2.61 o 7 9 13 3.10 3.43 1.80 o 8 9 13 19.59 19.10 2.94 o 3 10 13 128.66 114.80 3.69 o 4 10 13 0.46 -0.73 1.15 o 5 10 13 119.07 114.67 5.06 o 6 10 13 43.65 54.38 2.65 o 4 11 13 31.80 26.94 2.94 o 5 11 13 10.68 11.92 2.45 o 6 12 13 27.72 26.61 2.94 o 1 2 14 78.70 82.28 4.57 o 2 2 14 65.54 79.65 3.06 o 3 2 14 115.29 127.40 3.93 o 4 2 14 8.61 11.59 2.61 o 0 3 14 192.18 196.24 7.02 o 1 3 14 14.74 20.03 2.69 o 2 3 14 26.99 29.01 2.07 o 3 3 14 52.02 54.38 3.10 o 4 3 14 18.96 14.37 2.45 o 5 3 14 14.32 18.61 2.78 o 1 4 14 25.44 28.41 2.78 o 2 4 14 96.11 93.87 4.57 o 3 4 14 0.50 -0.49 1.63 o 4 4 14 75.21 69.71 3.92 o 1 5 14 104.88 108.57 4.90 o 2 5 14 4.09 0.82 1.80 o 3 5 14 220.93 220.24 7.51 o 4 5 14 60.67 59.10 3.59 o 0 6 14 157.80 156.08 6.53 o 1 6 14 41.07 36.24 3.10 o 2 6 14 37.88 36.05 2.13 o 3 6 14 38.59 31.51 2.78 o 4 6 14 1.98 0.49 1.63 o 1 7 14 2.74 1.31 1.80 o 2 7 14 31.37 25.47 2.78 o 3 7 14 32.95 31.36 2.08 o 4 7 14 137.82 145.54 4.15 o 5 7 14 4.22 4.69 1.32 o 7 7 14 126.05 144.48 6.04 o 2 8 14 11.88 13.88 2.45 o 3 8 14 0.52 -1.15 1.15 o 4 8 14 87.70 88.18 3.11 o 5 8 14 19.80 24.16 1.90 o 6 8 14 144.95 154.77 6.37 o 7 8 14 4.04 4.08 2.12 o 3 9 14 116.42 125.38 5.71 o 4 9 14 11.73 8.95 1.56 o 5 9 14 115.69 126.35 3.86 o 6 9 14 33.84 34.94 3.27 o 5 10 14 219.87 231.99 8.00 o 4 6 15 83.41 77.06 4.41 o 4 8 15 12.79 30.86 3.43 o 5 8 15 66.09 70.36 4.08 o