#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:55:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181119 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/99/2219970.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219970_Fobs loop_ _publ_author_name 'Munro, Natasha H.' 'Hanton, Lyall R.' _publ_section_title ; A redetermination at low temperature of the structure of triethylammonium bromide ; _journal_coeditor_code PV2113 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2236 _journal_volume 64 _journal_year 2008 _space_group_IT_number 159 _symmetry_space_group_name_Hall 'P 3 -2c' _symmetry_space_group_name_H-M 'P 3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.3590 _cell_length_b 8.3590 _cell_length_c 7.3130 _exptl_crystal_F_000 188.00 _reflns_d_resolution_high 0.8267 _cod_data_source_file pv2113Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nmb in P31c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, z+1/2' '-x, -x+y, z+1/2' 'x-y, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -8 648.51 639.46 15.26 o 0 1 -8 151.34 154.83 2.12 o 1 1 -8 461.94 468.71 6.34 o -1 2 -8 469.62 466.08 6.33 o 0 2 -8 107.98 104.91 1.70 o 1 2 -8 67.62 77.73 1.58 o 2 2 -8 274.99 255.87 4.53 o -1 3 -8 74.37 80.01 1.62 o 0 3 -8 311.10 327.95 3.43 o 1 3 -8 89.43 97.61 1.93 o -2 4 -8 248.97 265.13 4.71 o -1 4 -8 102.70 95.95 1.83 o 0 1 -7 515.65 524.21 4.25 o 0 2 -7 498.98 478.52 4.40 o 1 2 -7 667.18 690.47 5.48 o -1 3 -7 687.03 674.54 6.11 o 0 3 -7 6.59 7.54 0.75 o 1 3 -7 613.08 608.43 5.59 o 2 3 -7 440.07 442.12 5.02 o -1 4 -7 612.90 609.85 5.89 o 0 4 -7 320.39 312.75 3.65 o 1 4 -7 3.62 3.66 0.82 o 2 4 -7 249.06 233.46 3.58 o -2 5 -7 451.59 453.55 4.88 o -1 5 -7 1.49 3.71 0.90 o 0 5 -7 303.32 312.99 3.87 o -2 6 -7 223.62 235.71 3.29 o 0 0 -6 1094.77 1080.84 17.30 o 0 1 -6 394.53 402.81 3.02 o 1 1 -6 1172.77 1175.12 11.64 o -1 2 -6 1170.02 1181.38 11.15 o 0 2 -6 158.45 155.55 1.67 o 1 2 -6 163.10 170.07 1.75 o 2 2 -6 384.25 382.85 4.86 o -1 3 -6 173.65 169.77 1.98 o 0 3 -6 760.63 757.53 6.37 o 1 3 -6 228.28 241.07 2.78 o 2 3 -6 166.63 174.23 2.33 o 3 3 -6 561.37 536.56 8.17 o -2 4 -6 385.73 378.06 5.40 o -1 4 -6 250.94 242.95 2.58 o 0 4 -6 71.82 74.40 1.52 o 1 4 -6 697.59 698.75 6.79 o 2 4 -6 77.62 76.48 1.79 o 3 4 -6 111.22 106.58 2.18 o -2 5 -6 174.89 173.85 2.30 o -1 5 -6 739.13 700.81 6.98 o 0 5 -6 168.66 164.82 2.60 o 1 5 -6 178.46 163.02 2.66 o 2 5 -6 442.44 432.46 5.27 o -3 6 -6 549.08 546.16 7.05 o -2 6 -6 80.42 81.25 1.70 o -1 6 -6 164.13 169.17 2.78 o 0 6 -6 373.65 363.29 4.80 o -3 7 -6 104.65 107.56 2.04 o -2 7 -6 434.98 429.63 4.96 o 0 1 -5 880.66 856.97 5.40 o 0 2 -5 663.44 674.39 4.41 o 1 2 -5 1147.54 1226.76 8.48 o -1 3 -5 1259.32 1217.79 8.41 o 0 3 -5 12.70 17.09 0.65 o 1 3 -5 1010.16 1032.24 8.78 o 2 3 -5 701.96 722.31 5.95 o -1 4 -5 1061.25 1038.32 7.76 o 0 4 -5 402.70 394.81 4.14 o 1 4 -5 1.93 3.23 0.66 o 2 4 -5 316.95 293.85 3.36 o 3 4 -5 505.67 505.48 5.24 o -2 5 -5 751.26 721.23 6.08 o -1 5 -5 4.26 2.65 0.52 o 0 5 -5 501.85 494.58 4.78 o 1 5 -5 434.40 425.24 4.59 o 2 5 -5 11.39 13.02 1.01 o 3 5 -5 339.97 344.67 4.21 o -2 6 -5 286.13 296.15 3.31 o -1 6 -5 432.45 428.60 4.54 o 0 6 -5 0.15 -0.74 0.74 o 1 6 -5 296.99 287.15 3.86 o 2 6 -5 209.46 211.23 3.32 o -3 7 -5 514.83 514.45 5.19 o -2 7 -5 8.57 11.59 0.89 o -1 7 -5 281.93 274.96 3.77 o 0 7 -5 243.27 239.85 3.42 o -3 8 -5 317.73 345.82 4.09 o -2 8 -5 207.32 211.58 3.13 o 0 0 -4 3225.71 3328.97 44.19 o 0 1 -4 774.25 799.03 4.82 o 1 1 -4 2169.51 2288.89 19.48 o -1 2 -4 2293.19 2288.95 18.15 o 0 2 -4 402.02 417.41 2.97 o 1 2 -4 332.20 343.47 2.90 o 2 2 -4 901.23 1032.33 9.95 o -1 3 -4 344.56 342.40 2.51 o 0 3 -4 1410.19 1409.08 10.30 o 1 3 -4 387.90 422.56 3.52 o 2 3 -4 288.32 288.28 2.62 o 3 3 -4 931.63 934.72 11.78 o -2 4 -4 1094.62 1037.53 10.01 o -1 4 -4 453.47 431.58 3.36 o 0 4 -4 189.16 204.26 1.93 o 1 4 -4 1252.13 1253.30 9.87 o 2 4 -4 171.51 184.01 2.25 o 3 4 -4 203.44 187.98 2.47 o 4 4 -4 407.40 375.84 5.85 o -2 5 -4 302.88 292.25 2.68 o -1 5 -4 1285.69 1244.95 10.07 o 0 5 -4 311.55 309.46 3.10 o 1 5 -4 301.07 281.14 3.32 o 2 5 -4 765.77 731.84 6.97 o 3 5 -4 84.93 91.87 1.81 o 4 5 -4 119.31 120.38 2.44 o -3 6 -4 961.49 933.57 10.95 o -2 6 -4 198.02 182.21 2.37 o -1 6 -4 284.13 283.36 3.15 o 0 6 -4 817.86 792.88 7.29 o 1 6 -4 185.62 188.35 2.71 o 2 6 -4 147.99 140.04 2.45 o -3 7 -4 173.84 185.16 2.46 o -2 7 -4 753.08 723.10 6.96 o -1 7 -4 188.01 186.62 2.66 o 0 7 -4 152.90 149.35 2.42 o 1 7 -4 431.99 442.61 5.27 o -4 8 -4 334.75 366.51 5.99 o -3 8 -4 86.48 91.25 1.90 o -2 8 -4 127.29 136.63 2.40 o -1 8 -4 435.16 445.98 5.19 o -4 9 -4 122.82 122.66 2.74 o 0 1 -3 1059.95 1031.37 6.16 o 0 2 -3 1503.36 1539.27 10.20 o 1 2 -3 1654.70 1704.83 11.51 o -1 3 -3 1731.63 1710.32 11.59 o 0 3 -3 20.60 27.25 0.51 o 1 3 -3 1319.99 1406.95 10.03 o 2 3 -3 956.86 939.70 6.82 o -1 4 -3 1505.16 1415.63 9.77 o 0 4 -3 775.54 756.12 6.16 o 1 4 -3 1.05 8.23 0.45 o 2 4 -3 560.59 552.13 5.08 o 3 4 -3 614.91 605.95 5.84 o -2 5 -3 966.14 944.68 6.42 o -1 5 -3 13.88 6.76 0.49 o 0 5 -3 592.82 558.03 5.00 o 1 5 -3 484.14 476.99 5.13 o 2 5 -3 30.94 22.97 1.04 o 3 5 -3 393.98 394.71 4.31 o 4 5 -3 360.91 351.32 4.69 o -2 6 -3 575.42 559.49 5.03 o -1 6 -3 512.93 485.68 4.86 o 0 6 -3 0.46 0.58 0.71 o 1 6 -3 352.26 331.04 3.91 o 2 6 -3 373.51 372.49 4.33 o 3 6 -3 10.34 14.04 1.23 o -3 7 -3 617.41 606.05 5.98 o -2 7 -3 8.02 22.26 1.19 o -1 7 -3 327.78 323.65 3.77 o 0 7 -3 301.65 297.51 3.74 o 1 7 -3 0.99 2.59 0.95 o 2 7 -3 257.64 265.47 3.94 o -3 8 -3 379.03 407.04 4.63 o -2 8 -3 374.45 376.65 4.51 o -1 8 -3 3.91 2.26 0.88 o 0 8 -3 347.73 350.76 4.57 o -4 9 -3 341.32 354.00 5.06 o -3 9 -3 9.96 15.29 1.40 o -2 9 -3 270.40 266.71 4.48 o 0 0 -2 13592.12 13178.63 178.70 o 0 1 -2 1388.97 1444.75 9.01 o 1 1 -2 3417.78 3717.51 33.77 o -1 2 -2 3816.42 3764.97 32.00 o 0 2 -2 1333.00 1341.09 8.86 o 1 2 -2 504.77 588.91 4.00 o 2 2 -2 2218.95 2725.70 24.24 o -1 3 -2 601.31 593.29 3.63 o 0 3 -2 2011.37 2031.75 13.08 o 1 3 -2 530.21 595.32 4.47 o 2 3 -2 343.74 329.07 2.86 o 3 3 -2 1260.55 1277.34 13.99 o -2 4 -2 3113.05 2778.38 23.65 o -1 4 -2 661.44 608.49 4.26 o 0 4 -2 458.01 482.34 3.75 o 1 4 -2 1746.89 1745.29 12.52 o 2 4 -2 381.04 420.51 3.64 o 3 4 -2 323.54 282.32 3.22 o 4 4 -2 845.88 785.16 10.34 o -2 5 -2 356.82 334.82 2.82 o -1 5 -2 1804.82 1759.10 12.61 o 0 5 -2 525.61 542.51 4.51 o 1 5 -2 459.99 428.38 4.28 o 2 5 -2 1052.17 992.16 9.19 o 3 5 -2 96.34 99.24 1.94 o 4 5 -2 124.80 128.04 2.66 o -3 6 -2 1281.11 1293.16 14.83 o -2 6 -2 464.13 427.79 3.89 o -1 6 -2 403.97 431.82 3.96 o 0 6 -2 1711.88 1694.48 14.99 o 1 6 -2 205.39 204.61 2.86 o 2 6 -2 291.14 269.66 3.51 o 3 6 -2 439.72 442.62 6.10 o -3 7 -2 269.15 287.27 3.22 o -2 7 -2 1013.30 999.99 9.06 o -1 7 -2 211.15 205.16 2.79 o 0 7 -2 163.46 156.70 2.56 o 1 7 -2 545.91 549.22 6.11 o 2 7 -2 107.59 115.91 2.47 o -4 8 -2 750.14 796.76 10.12 o -3 8 -2 100.70 102.55 1.90 o -2 8 -2 252.32 264.96 3.64 o -1 8 -2 540.97 545.02 6.27 o 0 8 -2 220.96 228.97 3.65 o -4 9 -2 134.22 128.90 2.69 o -3 9 -2 438.43 433.80 5.56 o -2 9 -2 102.25 109.97 2.54 o 0 1 -1 320.39 349.31 3.60 o 0 2 -1 4435.26 4479.95 25.04 o 1 2 -1 1475.87 1511.37 9.84 o -1 3 -1 1658.91 1526.02 9.63 o 0 3 -1 20.85 21.06 0.45 o 1 3 -1 1384.19 1475.33 10.33 o 2 3 -1 933.92 883.18 6.93 o -1 4 -1 1473.17 1494.19 10.45 o 0 4 -1 1515.95 1498.37 9.90 o 1 4 -1 14.53 25.55 0.69 o 2 4 -1 938.08 983.04 7.72 o 3 4 -1 532.60 511.74 5.27 o -2 5 -1 937.38 881.94 7.24 o -1 5 -1 31.90 27.16 0.67 o 0 5 -1 457.16 422.11 3.90 o 1 5 -1 388.37 368.30 3.68 o 2 5 -1 50.89 39.58 1.16 o 3 5 -1 353.96 335.68 4.39 o 4 5 -1 389.32 395.70 5.23 o -2 6 -1 1016.54 981.66 8.07 o -1 6 -1 386.47 368.48 3.53 o 0 6 -1 1.82 2.04 0.62 o 1 6 -1 307.72 298.06 3.45 o 2 6 -1 609.57 622.40 6.69 o 3 6 -1 4.67 7.26 1.06 o -3 7 -1 547.42 520.76 4.91 o -2 7 -1 29.69 39.69 1.03 o -1 7 -1 312.13 302.89 3.37 o 0 7 -1 315.50 315.41 3.97 o 1 7 -1 4.18 7.20 0.95 o 2 7 -1 230.69 231.84 4.22 o -3 8 -1 344.23 341.76 4.33 o -2 8 -1 615.38 629.89 6.40 o -1 8 -1 6.21 5.34 0.94 o 0 8 -1 543.00 532.18 7.06 o 1 8 -1 177.89 182.62 3.74 o -4 9 -1 376.11 391.05 4.94 o -3 9 -1 4.55 3.40 0.98 o -2 9 -1 237.09 228.99 3.86 o -1 9 -1 185.62 182.33 3.95 o 1 1 0 4175.50 4246.66 39.59 o -1 2 0 4238.07 4238.17 34.83 o 0 2 0 2976.85 3002.34 16.51 o 1 2 0 570.50 626.10 4.10 o 2 2 0 4513.50 4609.48 47.63 o -1 3 0 592.94 628.84 4.34 o 0 3 0 2096.17 2062.33 13.51 o 1 3 0 665.22 656.33 4.95 o 2 3 0 341.07 318.23 2.82 o 3 3 0 1390.14 1411.58 15.43 o -2 4 0 4627.45 4628.84 45.75 o -1 4 0 680.50 664.62 4.84 o 0 4 0 688.56 669.67 5.15 o 1 4 0 1959.53 1937.73 14.28 o 2 4 0 621.67 653.97 5.73 o 3 4 0 363.53 326.24 3.67 o 4 4 0 1096.34 1078.06 16.46 o -2 5 0 342.15 319.01 2.76 o -1 5 0 1967.76 1919.83 13.86 o 0 5 0 648.62 694.20 5.82 o 1 5 0 513.10 514.81 4.54 o 2 5 0 1154.91 1116.09 10.22 o 3 5 0 95.32 91.92 2.08 o 4 5 0 122.56 117.97 2.97 o 5 5 0 347.26 351.94 9.20 o -3 6 0 1385.46 1411.04 16.24 o -2 6 0 633.91 656.96 5.29 o -1 6 0 499.96 519.92 4.58 o 0 6 0 2398.85 2434.44 20.23 o 1 6 0 196.14 196.36 2.64 o 2 6 0 366.80 354.99 4.65 o 3 6 0 467.68 467.89 5.95 o 4 6 0 105.11 111.89 3.09 o -3 7 0 353.00 330.99 3.69 o -2 7 0 1135.15 1130.07 9.90 o -1 7 0 201.21 197.38 2.71 o 0 7 0 153.16 153.56 2.39 o 1 7 0 568.95 557.72 7.21 o 2 7 0 129.64 143.16 3.16 o -4 8 0 1081.06 1087.43 15.60 o -3 8 0 96.23 95.90 1.89 o -2 8 0 359.72 365.92 4.43 o -1 8 0 568.07 561.44 6.67 o 0 8 0 294.26 306.68 4.59 o 1 8 0 51.68 62.26 2.31 o -4 9 0 122.41 119.29 2.57 o -3 9 0 469.86 465.69 5.94 o -2 9 0 130.34 141.65 2.80 o -1 9 0 53.08 63.00 2.15 o -5 10 0 353.68 359.04 6.92 o -4 10 0 102.84 108.19 2.51 o 0 1 1 374.98 410.05 2.98 o 0 2 1 4370.91 4388.32 26.73 o 1 2 1 1772.15 1586.62 10.80 o -1 3 1 1458.79 1599.88 10.74 o 0 3 1 20.86 21.20 0.49 o 1 3 1 1546.05 1544.16 10.49 o 2 3 1 987.07 923.67 7.30 o -1 4 1 1378.45 1538.47 11.59 o 0 4 1 1488.53 1446.02 11.14 o 1 4 1 31.91 27.28 0.69 o 2 4 1 978.67 972.67 7.98 o 3 4 1 551.75 542.78 5.49 o -2 5 1 917.55 929.34 7.54 o -1 5 1 14.52 26.91 0.72 o 0 5 1 473.91 450.38 3.99 o 1 5 1 406.96 392.89 3.81 o 2 5 1 29.69 38.18 1.13 o 3 5 1 338.40 353.65 4.45 o 4 5 1 377.75 396.20 6.10 o -2 6 1 943.44 965.42 8.33 o -1 6 1 398.45 389.89 3.69 o 0 6 1 1.82 2.93 0.56 o 1 6 1 306.07 313.79 3.85 o 2 6 1 607.63 615.31 7.80 o 3 6 1 4.55 3.93 1.18 o -3 7 1 553.16 541.97 5.55 o -2 7 1 50.89 41.04 1.18 o -1 7 1 330.22 319.05 3.75 o 0 7 1 320.50 329.56 4.20 o 1 7 1 6.21 3.32 0.93 o 2 7 1 247.82 252.53 4.56 o -3 8 1 376.50 357.41 4.24 o -2 8 1 602.58 610.47 6.66 o -1 8 1 4.18 3.48 0.85 o 0 8 1 538.10 530.95 6.60 o 1 8 1 194.47 199.58 4.10 o -4 9 1 395.70 394.88 5.11 o -3 9 1 4.67 6.47 1.08 o -2 9 1 232.37 254.05 4.06 o -1 9 1 180.93 192.06 3.90 o 0 0 2 13345.74 12831.49 164.43 o 0 1 2 1400.77 1445.75 9.48 o 1 1 2 3789.07 3778.29 41.18 o -1 2 2 3471.13 3683.92 45.18 o 0 2 2 1291.47 1269.22 9.81 o 1 2 2 574.59 563.29 4.92 o 2 2 2 2921.69 2544.73 29.66 o -1 3 2 510.32 562.65 4.58 o 0 3 2 2000.39 1984.87 15.17 o 1 3 2 654.55 610.51 4.78 o 2 3 2 357.73 342.30 3.22 o 3 3 2 1288.32 1299.47 14.98 o -2 4 2 2190.28 2530.42 29.06 o -1 4 2 544.49 595.77 4.59 o 0 4 2 434.94 440.19 4.07 o 1 4 2 1794.72 1754.41 13.54 o 2 4 2 440.36 406.40 3.94 o 3 4 2 275.26 278.12 3.83 o 4 4 2 731.90 752.59 11.96 o -2 5 2 349.39 342.42 3.13 o -1 5 2 1756.26 1745.32 13.29 o 0 5 2 520.05 542.69 4.82 o 1 5 2 413.96 437.14 4.43 o 2 5 2 1026.69 992.57 10.15 o 3 5 2 100.62 101.01 2.59 o 4 5 2 136.29 125.69 3.42 o -3 6 2 1257.43 1270.03 15.58 o -2 6 2 375.76 400.26 3.77 o -1 6 2 448.40 427.51 4.58 o 0 6 2 1666.60 1631.27 14.98 o 1 6 2 208.57 212.72 3.19 o 2 6 2 251.16 254.88 4.00 o 3 6 2 435.10 436.81 7.27 o -3 7 2 311.45 277.30 3.66 o -2 7 2 1033.42 1006.90 9.63 o -1 7 2 212.51 212.17 2.97 o 0 7 2 165.94 165.61 2.62 o 1 7 2 541.68 548.63 8.30 o 2 7 2 98.30 108.51 3.47 o -4 8 2 798.56 759.20 11.23 o -3 8 2 97.22 101.72 2.03 o -2 8 2 277.87 261.76 3.55 o -1 8 2 545.49 549.47 6.46 o 0 8 2 214.70 215.16 4.05 o -4 9 2 126.81 133.44 2.76 o -3 9 2 440.37 439.26 5.79 o -2 9 2 105.01 107.88 2.61 o 0 1 3 1114.63 1085.52 8.41 o 0 2 3 1460.81 1437.93 12.01 o 1 2 3 1816.96 1783.35 13.45 o -1 3 3 1667.10 1769.63 16.24 o 0 3 3 20.61 29.46 0.68 o 1 3 3 1564.70 1474.59 11.87 o 2 3 3 1010.08 978.65 9.00 o -1 4 3 1332.63 1461.26 11.78 o 0 4 3 755.09 728.90 5.79 o 1 4 3 13.88 6.45 0.50 o 2 4 3 548.00 547.55 5.69 o 3 4 3 628.59 654.76 8.32 o -2 5 3 956.38 982.04 8.28 o -1 5 3 1.05 7.19 0.51 o 0 5 3 616.77 592.99 5.24 o 1 5 3 538.87 522.19 5.34 o 2 5 3 8.02 20.32 1.33 o 3 5 3 380.89 434.47 6.71 o 4 5 3 346.52 371.88 7.01 o -2 6 3 559.09 539.72 5.50 o -1 6 3 502.74 513.59 5.10 o 0 6 3 0.46 0.93 0.63 o 1 6 3 331.21 347.28 5.11 o 2 6 3 366.16 373.70 6.33 o 3 6 3 9.96 15.73 1.90 o -3 7 3 641.79 656.98 6.45 o -2 7 3 30.94 21.92 1.05 o -1 7 3 375.72 348.62 4.52 o 0 7 3 310.26 310.24 4.68 o 1 7 3 3.91 2.50 1.05 o 2 7 3 284.85 287.36 5.41 o -3 8 3 419.53 428.49 5.37 o -2 8 3 364.87 369.10 4.98 o -1 8 3 0.99 6.26 1.16 o 0 8 3 341.76 338.79 5.51 o -4 9 3 369.91 371.25 5.47 o -3 9 3 10.34 14.68 1.49 o -2 9 3 264.38 287.94 4.94 o 0 0 4 3101.41 3112.07 55.39 o 0 1 4 773.86 786.66 6.97 o 1 1 4 2258.86 2224.27 26.42 o -1 2 4 2186.39 2217.55 25.79 o 0 2 4 381.77 374.93 3.91 o 1 2 4 330.32 324.23 3.49 o 2 2 4 993.32 937.79 12.22 o -1 3 4 333.50 323.76 3.47 o 0 3 4 1397.04 1386.82 12.58 o 1 3 4 443.54 425.77 4.06 o 2 3 4 300.22 293.37 3.04 o 3 3 4 955.14 939.93 12.02 o -2 4 4 886.27 937.94 11.94 o -1 4 4 394.69 418.74 4.42 o 0 4 4 177.28 185.55 2.44 o 1 4 4 1270.55 1248.46 11.59 o 2 4 4 182.49 171.35 2.65 o 3 4 4 177.86 185.51 3.59 o 4 4 4 322.26 326.20 10.62 o -2 5 4 290.09 287.54 3.52 o -1 5 4 1248.87 1246.36 12.95 o 0 5 4 306.48 302.54 4.11 o 1 5 4 288.71 282.49 4.42 o 2 5 4 757.19 734.51 9.68 o 3 5 4 85.28 83.65 3.48 o 4 5 4 122.86 126.00 4.33 o -3 6 4 923.93 938.61 13.90 o -2 6 4 167.52 169.45 2.75 o -1 6 4 291.44 286.67 3.85 o 0 6 4 785.18 770.90 8.93 o 1 6 4 184.64 191.28 3.83 o 2 6 4 125.93 126.31 3.20 o -3 7 4 192.78 185.20 3.34 o -2 7 4 746.54 747.99 8.57 o -1 7 4 189.49 189.55 3.52 o 0 7 4 153.18 156.62 3.38 o 1 7 4 430.88 438.63 6.91 o -4 8 4 371.12 326.03 7.30 o -3 8 4 84.77 86.49 2.39 o -2 8 4 137.81 138.62 3.25 o -1 8 4 428.96 431.10 6.86 o -4 9 4 119.59 127.22 3.16 o 0 1 5 910.55 887.21 7.67 o 0 2 5 664.22 662.27 7.11 o 1 2 5 1301.53 1264.80 11.23 o -1 3 5 1145.69 1251.63 12.00 o 0 3 5 12.70 17.15 0.71 o 1 3 5 1090.12 1061.36 10.54 o 2 3 5 781.17 758.56 8.13 o -1 4 5 1013.75 1061.65 10.48 o 0 4 5 408.67 402.81 4.96 o 1 4 5 4.26 3.17 0.85 o 2 4 5 283.04 302.11 4.58 o 3 4 5 518.60 535.47 7.56 o -2 5 5 701.07 751.10 8.49 o -1 5 5 1.93 3.42 0.75 o 0 5 5 514.67 505.64 6.37 o 1 5 5 446.47 443.37 6.12 o 2 5 5 8.57 10.83 1.33 o 3 5 5 317.25 356.93 6.05 o -2 6 5 330.05 307.32 4.71 o -1 6 5 444.38 440.33 6.46 o 0 6 5 0.15 0.48 0.91 o 1 6 5 284.45 293.05 5.24 o 2 6 5 210.17 223.15 4.61 o 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