#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2219986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219986_Fobs loop_ _publ_author_name 'Wen, Liyuan' 'Yin, Handong' 'Wang, Daqi' 'Cui, Liansheng' 'Yang, Minglei' _publ_section_title ; Bis(4-aminobenzoato-\kO)triphenylantimony(V) ; _journal_coeditor_code SG2267 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1426 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.543 _cell_angle_gamma 90.000 _cell_length_a 9.2831 _cell_length_b 18.9708 _cell_length_c 16.3868 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file sg2267Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080606f in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 270.40 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -22 0 621.73 646.64 101.16 o 1 -22 0 15.78 0.42 38.14 o 2 -22 0 252.82 243.62 53.49 o 1 -21 0 313.51 418.67 60.22 o 2 -21 0 127.98 126.77 45.37 o 3 -21 0 175.02 141.25 59.74 o 4 -21 0 211.49 204.58 52.65 o 0 -20 0 847.21 844.25 92.62 o 1 -20 0 8.70 48.04 39.46 o 2 -20 0 854.60 809.70 68.56 o 3 -20 0 48.73 -5.42 42.83 o 4 -20 0 303.08 252.17 52.57 o 5 -20 0 44.42 0.52 35.88 o 1 -19 0 1107.80 1034.10 52.77 o 2 -19 0 419.02 417.29 54.93 o 3 -19 0 487.56 593.09 82.05 o 4 -19 0 128.05 111.09 49.33 o 5 -19 0 260.07 186.63 72.15 o 0 -18 0 324.61 288.46 81.27 o 1 -18 0 87.81 90.62 22.03 o 2 -18 0 166.05 143.07 29.61 o 3 -18 0 567.99 651.54 63.99 o 4 -18 0 876.70 885.07 69.24 o 5 -18 0 288.20 346.14 70.70 o 1 -17 0 1783.79 1827.58 52.06 o 2 -17 0 91.41 98.03 26.16 o 3 -17 0 1447.53 1415.37 56.73 o 4 -17 0 70.43 64.96 28.08 o 5 -17 0 627.02 628.39 63.52 o 0 -16 0 1702.69 1592.13 65.88 o 1 -16 0 22.65 24.97 16.45 o 2 -16 0 2027.86 2013.91 63.76 o 3 -16 0 115.49 66.55 23.97 o 4 -16 0 558.59 614.61 45.47 o 5 -16 0 444.39 471.25 42.56 o 6 -16 0 442.45 380.04 70.86 o 1 -15 0 805.83 806.07 33.67 o 2 -15 0 517.06 504.71 37.85 o 3 -15 0 865.58 826.54 43.21 o 4 -15 0 626.25 747.79 47.68 o 5 -15 0 3162.44 3056.40 183.27 o 6 -15 0 668.01 688.55 125.39 o 7 -15 0 636.63 953.32 99.28 o 8 -15 0 68.68 -21.84 60.29 o 0 -14 0 2042.50 2059.80 69.55 o 1 -14 0 820.13 757.22 31.65 o 2 -14 0 1312.29 1328.11 78.08 o 3 -14 0 893.89 925.79 44.23 o 4 -14 0 1878.38 1774.65 60.15 o 5 -14 0 1879.75 1793.99 109.73 o 6 -14 0 1303.09 1123.62 75.44 o 7 -14 0 244.01 126.84 64.83 o 8 -14 0 270.36 282.33 71.09 o 1 -13 0 4205.24 3864.99 68.59 o 2 -13 0 917.59 777.06 40.16 o 3 -13 0 4559.19 4443.34 92.80 o 4 -13 0 557.19 626.87 39.73 o 5 -13 0 597.37 578.08 56.69 o 6 -13 0 44.41 61.95 31.94 o 7 -13 0 96.86 33.51 51.60 o 8 -13 0 298.01 214.53 69.13 o 0 -12 0 737.24 767.59 76.85 o 1 -12 0 188.65 158.20 17.54 o 2 -12 0 2413.83 2464.22 62.81 o 3 -12 0 1833.87 1858.44 55.95 o 4 -12 0 578.50 557.28 38.04 o 5 -12 0 2361.55 2270.80 78.13 o 6 -12 0 1396.22 1442.91 65.63 o 7 -12 0 465.74 443.54 71.41 o 8 -12 0 1058.73 1252.41 98.50 o 9 -12 0 174.72 120.50 65.69 o 1 -11 0 4433.25 4266.11 68.49 o 2 -11 0 1673.88 1627.68 48.86 o 3 -11 0 2102.35 2047.68 87.15 o 4 -11 0 2517.03 2675.20 67.51 o 5 -11 0 1910.47 1984.66 140.54 o 6 -11 0 968.89 968.36 53.29 o 7 -11 0 1604.94 1840.25 104.21 o 8 -11 0 189.16 52.46 54.49 o 9 -11 0 667.37 600.13 89.96 o 0 -10 0 15513.97 16107.28 254.73 o 1 -10 0 1364.52 1241.31 32.28 o 2 -10 0 8362.25 8603.91 132.31 o 3 -10 0 1046.97 980.05 37.96 o 4 -10 0 2017.02 1923.44 55.06 o 5 -10 0 511.55 548.00 39.42 o 6 -10 0 47.56 54.48 28.08 o 7 -10 0 233.20 231.21 55.51 o 8 -10 0 12.25 -31.00 43.22 o 9 -10 0 892.64 914.96 99.04 o 1 -9 0 8805.34 9945.91 128.88 o 2 -9 0 1838.05 1586.35 44.05 o 3 -9 0 2514.03 2341.72 56.56 o 4 -9 0 2771.60 2678.05 61.88 o 5 -9 0 1047.98 1057.64 52.03 o 6 -9 0 1250.50 1341.99 89.30 o 7 -9 0 1360.72 1409.15 90.74 o 8 -9 0 1306.83 1262.82 93.48 o 9 -9 0 903.65 975.79 91.76 o 10 -9 0 299.60 146.88 61.70 o 0 -8 0 2295.33 2205.38 95.28 o 1 -8 0 2012.10 2092.27 39.13 o 2 -8 0 5384.71 6007.73 96.81 o 3 -8 0 2890.68 2647.00 57.51 o 4 -8 0 4545.44 4503.15 97.14 o 5 -8 0 2938.16 2909.11 77.07 o 6 -8 0 2894.60 3048.50 84.81 o 7 -8 0 1312.23 1295.19 59.31 o 8 -8 0 2205.74 2480.23 123.71 o 9 -8 0 336.79 488.72 81.51 o 10 -8 0 287.02 264.95 73.28 o 1 -7 0 13817.25 12698.43 141.13 o 2 -7 0 2593.21 2349.48 70.83 o 3 -7 0 9700.41 10264.02 143.47 o 4 -7 0 1119.12 1002.74 40.83 o 5 -7 0 2256.39 2435.33 80.29 o 6 -7 0 1778.10 1814.88 62.84 o 7 -7 0 976.76 996.59 52.12 o 8 -7 0 344.20 254.85 56.29 o 9 -7 0 153.97 211.16 59.58 o 10 -7 0 493.74 538.12 88.55 o 0 -6 0 13504.21 13462.27 204.65 o 1 -6 0 177.65 237.63 13.61 o 2 -6 0 10731.42 10947.30 145.75 o 3 -6 0 5930.34 6272.78 95.30 o 4 -6 0 6433.07 6906.93 125.59 o 5 -6 0 502.44 493.12 33.16 o 6 -6 0 2113.38 2103.19 67.08 o 7 -6 0 715.08 790.25 46.10 o 8 -6 0 187.92 182.11 51.91 o 9 -6 0 620.95 677.10 86.59 o 10 -6 0 301.95 350.45 77.04 o 1 -5 0 1439.12 1836.85 31.19 o 2 -5 0 3931.06 3735.34 60.92 o 3 -5 0 1580.34 1750.80 45.99 o 4 -5 0 13379.75 14116.36 221.24 o 5 -5 0 7116.96 7705.85 141.20 o 6 -5 0 2222.13 2393.65 70.50 o 7 -5 0 3448.49 3721.54 95.86 o 8 -5 0 362.87 290.55 61.07 o 9 -5 0 890.47 1005.23 86.20 o 10 -5 0 88.81 68.43 59.43 o 0 -4 0 8987.17 9104.11 140.38 o 1 -4 0 3340.17 3522.67 46.09 o 2 -4 0 9813.86 9314.66 120.90 o 3 -4 0 13943.52 15225.31 228.15 o 4 -4 0 13889.00 14713.89 227.49 o 5 -4 0 792.40 814.48 54.06 o 6 -4 0 3480.01 3806.55 91.06 o 7 -4 0 272.11 225.33 33.56 o 8 -4 0 1202.72 1087.91 80.72 o 9 -4 0 530.79 536.01 75.16 o 10 -4 0 122.53 57.70 58.41 o 1 -3 0 31070.51 31484.29 362.56 o 2 -3 0 2591.39 2997.67 56.25 o 3 -3 0 16795.78 18886.84 275.62 o 4 -3 0 769.10 889.71 35.13 o 5 -3 0 227.60 208.56 60.87 o 6 -3 0 1642.55 1822.00 59.48 o 7 -3 0 32.27 -5.99 34.18 o 8 -3 0 1163.66 1153.36 83.78 o 9 -3 0 111.98 47.37 46.43 o 10 -3 0 1027.17 1086.58 98.89 o 0 -2 0 8039.33 8437.05 123.32 o 2 -2 0 18749.78 20933.98 295.65 o 3 -2 0 1177.45 971.10 30.00 o 4 -2 0 5024.61 5359.29 99.96 o 5 -2 0 3877.58 3851.68 84.52 o 6 -2 0 4219.85 4111.90 94.65 o 7 -2 0 2631.93 2520.89 75.73 o 8 -2 0 1984.60 1775.26 100.45 o 9 -2 0 213.62 262.91 63.03 o 10 -2 0 846.33 819.98 97.40 o 1 -1 0 15232.73 17410.44 244.86 o 2 -1 0 2149.20 2201.26 43.49 o 3 -1 0 813.00 856.32 28.36 o 4 -1 0 9602.64 9488.08 156.24 o 5 -1 0 2358.87 2680.81 67.47 o 6 -1 0 1456.39 1348.43 50.66 o 7 -1 0 3263.09 3332.67 89.21 o 8 -1 0 1326.96 1224.61 87.77 o 9 -1 0 1212.33 1174.74 92.15 o 10 -1 0 723.27 877.45 95.68 o 1 0 0 852.11 1131.36 32.34 o 2 0 0 9989.26 9936.73 218.21 o 3 0 0 3740.68 3538.78 97.48 o 4 0 0 2745.30 2665.32 62.09 o 5 0 0 1046.69 910.81 38.94 o 6 0 0 373.40 335.41 40.24 o 7 0 0 155.88 241.69 33.38 o 8 0 0 98.52 100.76 29.68 o 9 0 0 1457.47 1470.69 99.59 o 10 0 0 41.83 90.82 58.72 o 1 1 0 14895.89 16201.50 341.68 o 2 1 0 2146.11 2130.48 63.34 o 3 1 0 585.06 618.61 34.45 o 4 1 0 9533.75 9492.33 230.03 o 5 1 0 2432.30 2712.53 97.32 o 6 1 0 1393.88 1309.50 83.46 o 7 1 0 3187.21 3355.18 90.84 o 8 1 0 1336.09 1342.76 60.42 o 9 1 0 1162.91 1110.14 88.47 o 10 1 0 733.84 703.17 88.94 o 2 2 0 18402.33 19921.69 424.36 o 3 2 0 902.82 767.29 42.04 o 4 2 0 5006.93 5434.77 151.11 o 5 2 0 3697.78 3487.34 117.52 o 6 2 0 4377.10 4207.18 140.77 o 7 2 0 2515.23 2496.23 78.06 o 8 2 0 2068.06 1905.80 72.19 o 9 2 0 239.16 187.91 53.01 o 10 2 0 801.60 930.30 102.72 o 3 3 0 16440.41 17702.10 392.57 o 4 3 0 619.63 618.37 46.90 o 5 3 0 205.46 133.34 33.59 o 6 3 0 1648.43 1648.74 83.46 o 7 3 0 25.49 6.81 27.79 o 8 3 0 1153.54 1170.97 59.01 o 9 3 0 106.63 123.39 51.60 o 10 3 0 1033.62 1138.88 97.16 o 0 4 0 9694.58 9725.18 209.13 o 3 4 0 13957.73 14186.81 327.19 o 4 4 0 13540.07 13914.50 331.03 o 5 4 0 593.54 657.05 51.75 o 6 4 0 3511.67 3615.04 134.67 o 7 4 0 225.33 230.89 45.80 o 8 4 0 1198.14 1150.25 59.43 o 9 4 0 552.46 556.21 80.57 o 10 4 0 116.20 21.84 51.05 o 3 5 0 1567.73 1805.48 76.26 o 4 5 0 13915.68 13550.98 328.37 o 5 5 0 7139.85 6925.97 201.53 o 6 5 0 2141.14 2160.71 102.96 o 7 5 0 3495.95 3499.79 140.93 o 8 5 0 367.29 424.05 63.73 o 9 5 0 881.82 962.09 88.24 o 10 5 0 94.78 24.82 49.87 o 0 6 0 13633.83 13736.78 296.03 o 4 6 0 6762.65 7146.61 203.57 o 5 6 0 651.56 596.69 56.53 o 6 6 0 2123.35 2148.73 106.72 o 7 6 0 725.23 774.18 70.31 o 8 6 0 199.48 172.17 48.86 o 9 6 0 598.92 742.86 89.88 o 10 6 0 294.30 310.36 72.66 o 1 7 0 14100.55 12818.22 279.83 o 4 7 0 1215.26 1028.40 68.59 o 5 7 0 2255.37 2122.97 101.31 o 6 7 0 1767.16 1944.93 102.64 o 7 7 0 964.33 939.85 76.96 o 8 7 0 325.01 247.41 59.03 o 10 7 0 474.63 593.40 98.65 o 0 8 0 2425.09 2408.04 63.11 o 1 8 0 1867.54 2000.28 59.27 o 5 8 0 2920.25 2816.19 124.80 o 6 8 0 2867.80 2925.10 133.10 o 7 8 0 1334.71 1120.95 88.71 o 8 8 0 2193.94 2267.74 127.46 o 9 8 0 343.11 363.45 73.36 o 10 8 0 298.63 500.30 92.31 o 1 9 0 8413.77 9421.24 221.34 o 5 9 0 1068.76 1042.89 79.16 o 6 9 0 1216.93 1179.51 87.53 o 7 9 0 1338.53 1213.18 92.31 o 8 9 0 1329.66 1272.29 100.14 o 9 9 0 887.08 860.54 88.08 o 1 10 0 1343.29 1187.81 42.98 o 2 10 0 8185.26 8391.89 201.22 o 5 10 0 538.29 509.23 70.15 o 6 10 0 59.16 23.96 41.65 o 7 10 0 221.21 265.03 63.34 o 8 10 0 10.70 26.62 45.10 o 9 10 0 902.23 885.44 94.89 o 1 11 0 4588.58 4433.61 109.30 o 2 11 0 1659.26 1631.59 57.94 o 5 11 0 1973.63 1976.40 121.83 o 6 11 0 941.36 1064.03 93.17 o 7 11 0 1646.67 1745.66 120.97 o 8 11 0 189.87 202.16 66.55 o 9 11 0 675.72 947.29 111.49 o 5 12 0 2311.04 2407.26 139.13 o 6 12 0 1365.79 1440.08 111.57 o 7 12 0 467.60 573.59 88.79 o 8 12 0 1086.85 1416.83 116.27 o 9 12 0 163.48 216.64 73.75 o 6 13 0 48.86 77.98 55.59 o 7 13 0 109.47 83.31 54.42 o 8 13 0 291.84 271.37 81.11 o 6 14 0 1317.81 1546.64 128.80 o 7 14 0 230.15 217.97 72.19 o 8 14 0 275.75 386.23 89.02 o 6 15 0 660.49 858.27 119.40 o 7 15 0 631.01 605.69 106.56 o 8 15 0 69.88 116.11 75.16 o 6 16 0 449.34 686.02 119.09 o 7 16 0 216.90 103.43 74.77 o 6 17 0 213.54 405.57 104.52 o 7 17 0 113.13 132.87 93.33 o 6 18 0 671.75 1043.28 154.79 o -2 -22 1 164.31 162.72 76.38 o -1 -22 1 389.45 499.96 66.26 o 0 -22 1 235.79 303.18 54.50 o 1 -22 1 359.95 574.00 151.62 o 2 -22 1 71.18 109.93 43.46 o -4 -21 1 298.08 244.32 54.86 o -3 -21 1 204.36 178.78 49.03 o -2 -21 1 500.82 557.87 65.09 o -1 -21 1 280.29 250.74 51.40 o 0 -21 1 651.58 601.17 67.32 o 1 -21 1 376.38 433.12 59.51 o 2 -21 1 165.84 204.63 50.57 o 3 -21 1 6.83 -29.46 32.60 o -5 -20 1 38.01 4.31 53.79 o -4 -20 1 195.28 249.77 60.48 o -3 -20 1 68.52 18.84 37.41 o -2 -20 1 135.46 156.82 41.96 o -1 -20 1 306.89 299.42 39.42 o 0 -20 1 38.60 22.58 27.48 o 1 -20 1 720.27 759.21 59.16 o 2 -20 1 82.32 51.46 37.34 o 3 -20 1 741.24 915.99 77.48 o 4 -20 1 14.12 -0.18 35.83 o 5 -20 1 531.55 709.04 107.89 o -5 -19 1 332.96 341.91 75.08 o -4 -19 1 300.65 380.62 113.57 o -3 -19 1 212.72 133.45 43.92 o -2 -19 1 585.75 831.04 121.16 o -1 -19 1 482.20 638.51 58.82 o 0 -19 1 569.76 634.65 48.45 o 1 -19 1 211.51 293.32 39.20 o 2 -19 1 971.61 1006.90 54.13 o 3 -19 1 50.78 51.36 27.64 o 4 -19 1 521.44 521.37 61.19 o 5 -19 1 5.02 -31.63 51.44 o -6 -18 1 93.23 136.00 57.94 o -5 -18 1 722.21 944.32 106.25 o -4 -18 1 445.74 431.07 58.09 o -3 -18 1 1489.34 1619.03 84.70 o -2 -18 1 511.35 616.05 48.32 o -1 -18 1 997.75 947.02 61.19 o 0 -18 1 907.99 923.66 48.53 o 1 -18 1 489.63 469.97 34.71 o 2 -18 1 285.29 321.74 37.36 o 3 -18 1 172.48 129.45 30.71 o 4 -18 1 24.07 0.62 26.52 o 5 -18 1 158.21 136.29 33.57 o -6 -17 1 53.39 28.11 48.54 o -5 -17 1 517.36 793.36 95.21 o -4 -17 1 318.43 253.54 46.66 o -3 -17 1 174.11 149.24 39.26 o -2 -17 1 268.06 289.65 28.53 o -1 -17 1 173.59 137.60 21.93 o 0 -17 1 541.53 633.03 35.41 o 1 -17 1 304.61 297.23 27.85 o 2 -17 1 477.98 515.39 47.48 o 3 -17 1 58.61 34.73 25.28 o 4 -17 1 2158.98 2141.55 96.90 o 5 -17 1 167.03 130.76 37.02 o 6 -17 1 1045.34 1178.57 94.89 o -6 -16 1 1161.96 1259.84 103.19 o -5 -16 1 314.31 429.92 73.36 o -4 -16 1 547.84 540.81 42.57 o -3 -16 1 353.50 374.85 36.23 o -2 -16 1 433.20 462.80 31.16 o -1 -16 1 738.47 749.25 34.25 o 0 -16 1 150.01 145.74 21.37 o 1 -16 1 1277.93 1294.10 45.34 o 2 -16 1 72.46 88.79 24.95 o 3 -16 1 916.40 846.01 49.87 o 4 -16 1 88.85 90.34 28.41 o 5 -16 1 2255.89 2197.88 73.18 o 6 -16 1 20.67 80.17 50.89 o 7 -16 1 355.85 420.84 79.31 o -6 -15 1 332.63 371.61 69.80 o -5 -15 1 1207.74 1137.74 61.61 o -4 -15 1 2308.72 2393.24 75.00 o -3 -15 1 675.66 643.13 41.75 o -2 -15 1 1695.65 1577.59 46.05 o -1 -15 1 1250.88 1235.86 40.37 o 0 -15 1 652.78 672.07 30.80 o 1 -15 1 1026.26 957.92 36.25 o 2 -15 1 976.20 900.84 44.04 o 3 -15 1 76.12 58.55 23.22 o 4 -15 1 418.74 349.40 36.13 o 5 -15 1 45.38 64.02 27.80 o 6 -15 1 515.36 512.83 79.55 o 7 -15 1 211.69 193.39 68.12 o 8 -15 1 284.17 153.30 67.10 o -7 -14 1 243.22 239.11 64.83 o -6 -14 1 888.19 812.41 58.04 o -5 -14 1 767.55 771.32 52.95 o -4 -14 1 241.69 328.36 55.12 o -3 -14 1 1905.64 1861.42 58.69 o -2 -14 1 958.25 992.65 36.09 o -1 -14 1 1541.57 1601.17 43.55 o 0 -14 1 1834.33 1719.44 44.98 o 1 -14 1 1373.59 1399.96 41.07 o 2 -14 1 445.42 416.21 34.50 o 3 -14 1 1660.27 1575.31 55.12 o 4 -14 1 6.77 -21.32 20.08 o 5 -14 1 1431.25 1457.74 57.94 o 6 -14 1 126.04 104.92 54.10 o 8 -14 1 79.45 7.12 60.29 o -9 -13 1 618.64 533.42 87.61 o -8 -13 1 35.84 9.00 52.22 o -7 -13 1 1776.96 1653.20 101.08 o -6 -13 1 129.98 112.16 35.67 o -5 -13 1 2202.07 2367.20 82.53 o -4 -13 1 52.93 27.38 26.08 o -3 -13 1 505.78 579.12 37.75 o -2 -13 1 458.54 465.43 28.14 o -1 -13 1 310.05 341.26 36.97 o 0 -13 1 1378.95 1528.32 40.63 o 1 -13 1 602.45 592.03 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