#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:55:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181119 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/99/2219989.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2219989_Fobs loop_ _publ_author_name 'Wang, Jian-Ge' 'Qin, Jian-Hua' _publ_section_title ; catena-Poly[[[diaqualanthanum(III)]-tetrakis[\m-N-(4-acetamidophenylsulfonyl)glycinato]-[diaqualanthanum(III)]-bis[\m-N-(4-acetamidophenylsulfonyl)glycinato]] 4,4'-bipyridine disolvate tetradecahydrate] ; _journal_coeditor_code SI2111 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1364 _journal_page_last m1365 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.971 _cell_angle_beta 105.758 _cell_angle_gamma 93.692 _cell_length_a 9.6379 _cell_length_b 16.9589 _cell_length_c 17.6005 _exptl_crystal_F_000 1304.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file si2111Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 378.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19850.18 20388.32 195.67 o 3 0 0 3922.48 4116.62 63.34 o 4 0 0 300.78 323.62 18.48 o 5 0 0 64.89 57.26 15.41 o 6 0 0 8787.40 9032.33 118.59 o 7 0 0 452.31 393.61 42.63 o 8 0 0 3639.89 3838.39 114.01 o 9 0 0 371.88 361.10 56.69 o 10 0 0 400.47 404.10 72.86 o 11 0 0 73.96 49.89 32.06 o -11 1 0 168.54 119.00 38.68 o -10 1 0 471.09 535.41 60.43 o -9 1 0 1279.22 1213.29 60.20 o -8 1 0 1836.46 1821.74 89.59 o -7 1 0 2010.92 2158.56 79.41 o -6 1 0 6465.33 6266.37 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