#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:54:30 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181121 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/00/2220027.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220027_Fobs loop_ _publ_author_name 'Yang, Shu-Ping' 'Wang, Da-Qi' 'Han, Li-Jun' 'Liu, Yu-Fen' _publ_section_title ; 4-Methyl-2-oxo-2,3-dihydro-1-benzopyran-7-yl benzenesulfonate ; _journal_coeditor_code XU2456 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2088 _journal_volume 64 _journal_year 2008 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 23.3191 _cell_length_b 9.0865 _cell_length_c 13.7280 _exptl_crystal_F_000 1312.00 _reflns_d_resolution_high 0.8407 _cod_data_source_file xu2456Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080902f in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 371.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9.44 -3.78 4.21 o 4 0 0 11752.04 12281.85 210.11 o 6 0 0 5543.84 5483.75 105.06 o 8 0 0 409.98 327.99 18.83 o 10 0 0 71.08 73.24 16.07 o 12 0 0 605.47 602.65 31.15 o 14 0 0 844.71 861.02 39.67 o 16 0 0 3185.01 3179.28 90.18 o 18 0 0 4286.48 4385.38 117.49 o 20 0 0 117.11 157.58 50.87 o 22 0 0 2120.92 2131.32 123.45 o 24 0 0 255.28 267.21 67.94 o 26 0 0 121.40 143.65 63.40 o 1 1 0 3350.30 3239.30 42.92 o 3 1 0 98246.72 92555.11 1281.89 o 5 1 0 22653.61 22461.86 345.87 o 7 1 0 1450.50 1566.87 34.86 o 9 1 0 286.67 291.53 15.06 o 11 1 0 5015.12 5557.82 84.91 o 13 1 0 797.56 715.38 25.31 o 15 1 0 1852.11 1759.10 43.60 o 17 1 0 1356.51 1281.96 39.10 o 19 1 0 0.91 -32.79 23.17 o 21 1 0 421.87 523.63 57.41 o 23 1 0 313.97 390.51 53.72 o 25 1 0 100.96 104.24 39.35 o 27 1 0 13.19 2.51 36.19 o 2 2 0 3282.12 3466.13 57.51 o 4 2 0 195.62 199.38 10.62 o 6 2 0 2448.50 2749.88 51.48 o 8 2 0 24311.93 25932.26 314.15 o 10 2 0 1104.52 1400.78 37.01 o 12 2 0 744.91 751.14 25.46 o 14 2 0 197.24 195.80 19.53 o 16 2 0 788.39 806.24 34.25 o 18 2 0 543.90 532.24 35.68 o 20 2 0 1353.76 1229.13 65.88 o 22 2 0 104.91 27.05 30.52 o 24 2 0 21.21 13.66 32.29 o 26 2 0 250.75 382.47 109.57 o 1 3 0 602.61 698.18 21.53 o 3 3 0 20.94 32.25 8.78 o 5 3 0 278.16 217.77 24.73 o 7 3 0 2806.36 2734.77 49.49 o 9 3 0 4998.37 5766.40 99.25 o 11 3 0 2616.88 2806.64 55.52 o 13 3 0 1980.73 1978.50 46.99 o 15 3 0 1031.62 1005.42 38.36 o 17 3 0 471.87 470.53 34.28 o 19 3 0 210.87 176.13 38.38 o 21 3 0 131.24 115.39 37.85 o 23 3 0 23.90 68.60 35.76 o 25 3 0 24.86 21.76 32.90 o 0 4 0 3073.31 3632.36 83.27 o 2 4 0 11180.92 11294.29 169.94 o 4 4 0 10689.77 11280.54 171.65 o 6 4 0 2499.17 2830.62 113.68 o 8 4 0 527.10 594.15 23.05 o 10 4 0 631.15 605.36 24.29 o 12 4 0 408.21 450.48 34.13 o 14 4 0 590.00 557.64 26.98 o 16 4 0 531.53 542.09 35.96 o 18 4 0 779.23 777.11 55.01 o 20 4 0 508.75 604.55 71.34 o 22 4 0 3.77 55.21 34.02 o 24 4 0 51.28 24.19 36.27 o 1 5 0 4305.03 4354.77 102.16 o 3 5 0 3263.75 3426.19 74.99 o 5 5 0 371.06 309.02 23.01 o 7 5 0 204.12 279.44 26.00 o 9 5 0 230.47 232.78 23.73 o 11 5 0 69.65 97.97 19.03 o 13 5 0 2115.91 2016.01 52.40 o 15 5 0 466.83 527.68 34.64 o 17 5 0 11.98 -27.24 18.16 o 19 5 0 72.78 79.07 46.55 o 21 5 0 47.19 13.85 53.03 o 23 5 0 145.22 168.69 47.15 o 0 6 0 38.92 21.36 16.50 o 2 6 0 1289.85 1245.01 39.61 o 4 6 0 367.12 320.64 28.62 o 6 6 0 465.87 468.86 37.65 o 8 6 0 1602.87 1650.03 51.27 o 10 6 0 3330.02 3120.06 132.96 o 12 6 0 0.78 -29.02 19.35 o 14 6 0 579.28 633.27 80.37 o 16 6 0 233.21 233.38 35.54 o 18 6 0 351.82 428.53 53.38 o 20 6 0 15.81 5.51 41.58 o 22 6 0 0.32 -48.17 41.37 o 1 7 0 11.17 -21.71 18.41 o 3 7 0 540.83 611.98 107.63 o 5 7 0 138.92 110.35 31.36 o 7 7 0 5064.02 4763.44 195.17 o 9 7 0 3650.54 3537.59 111.21 o 11 7 0 22.25 -11.87 29.68 o 13 7 0 270.18 261.10 47.40 o 15 7 0 369.44 344.09 52.75 o 17 7 0 0.23 -18.52 31.53 o 0 8 0 0.85 -41.26 33.16 o 2 8 0 1484.74 1131.28 60.08 o 4 8 0 24.39 -8.75 25.77 o 6 8 0 155.38 199.40 42.61 o 8 8 0 123.09 67.53 35.25 o 10 8 0 351.56 339.12 52.05 o 12 8 0 140.97 120.53 51.74 o 14 8 0 84.25 113.37 42.44 o 16 8 0 180.75 157.51 45.19 o 18 8 0 33.89 -40.94 44.93 o 1 9 0 1555.90 1255.70 67.99 o 3 9 0 31.26 15.64 32.77 o 5 9 0 14.08 -24.67 31.33 o 7 9 0 16.46 -44.07 29.38 o 9 9 0 38.00 18.87 34.49 o 11 9 0 48.65 15.21 34.24 o 13 9 0 11.75 10.40 39.65 o 15 9 0 49.82 12.50 41.11 o 0 10 0 49.64 81.65 55.30 o 2 10 0 18.39 20.64 35.95 o 4 10 0 29.18 -4.28 36.39 o 6 10 0 0.03 6.84 64.86 o 8 10 0 4.97 -18.69 37.37 o 10 10 0 176.52 263.77 57.46 o 1 1 1 198.30 133.33 5.65 o 2 1 1 7899.88 7917.15 69.53 o 3 1 1 2157.31 2122.46 22.83 o 4 1 1 4557.96 4691.94 57.96 o 5 1 1 10848.96 11439.25 100.42 o 6 1 1 31.88 39.94 5.61 o 7 1 1 101.11 97.88 7.02 o 8 1 1 273.84 256.23 10.86 o 9 1 1 188.36 212.34 12.07 o 10 1 1 74.50 81.21 8.42 o 11 1 1 1289.02 1386.13 23.38 o 12 1 1 78.50 85.22 9.72 o 13 1 1 743.01 815.76 19.75 o 14 1 1 1453.66 1493.87 34.67 o 15 1 1 36.98 50.73 10.14 o 16 1 1 0.28 -8.26 8.81 o 17 1 1 202.49 240.99 19.49 o 18 1 1 893.99 868.56 28.46 o 19 1 1 2.81 -2.37 14.91 o 20 1 1 0.38 -22.46 14.98 o 21 1 1 376.55 370.46 35.92 o 22 1 1 0.91 -21.13 18.75 o 23 1 1 188.69 243.23 33.02 o 24 1 1 137.03 143.47 28.85 o 25 1 1 2.82 -25.61 19.74 o 26 1 1 13.92 -8.13 21.28 o 27 1 1 7.08 16.69 25.32 o 0 2 1 874.58 968.37 60.48 o 1 2 1 12807.16 13254.82 130.97 o 2 2 1 144.20 145.10 6.17 o 3 2 1 2.57 -0.62 4.59 o 4 2 1 5533.90 5794.76 79.87 o 5 2 1 1023.75 1008.00 16.05 o 6 2 1 138.35 172.24 8.55 o 7 2 1 1116.56 1038.95 18.56 o 8 2 1 4073.99 4506.29 49.24 o 9 2 1 5584.69 5895.92 61.94 o 10 2 1 141.97 174.91 13.27 o 11 2 1 302.88 351.34 15.14 o 12 2 1 217.86 289.39 15.40 o 13 2 1 0.17 -10.19 6.80 o 14 2 1 20.99 7.69 8.14 o 15 2 1 163.32 174.49 14.76 o 16 2 1 282.61 378.50 20.31 o 17 2 1 696.30 627.21 21.49 o 18 2 1 88.58 100.95 17.98 o 19 2 1 280.48 378.37 27.38 o 20 2 1 576.80 568.05 30.27 o 21 2 1 1.10 -17.27 18.65 o 22 2 1 13.67 -19.09 18.65 o 23 2 1 33.84 20.27 27.50 o 24 2 1 5.30 -9.91 20.23 o 25 2 1 13.53 -8.25 22.15 o 26 2 1 15.27 24.36 26.92 o 27 2 1 3.13 -19.69 24.08 o 1 3 1 552.98 556.10 13.20 o 2 3 1 902.28 900.87 18.71 o 3 3 1 52.89 44.20 5.92 o 4 3 1 625.15 579.06 14.10 o 5 3 1 2054.62 2177.43 28.71 o 6 3 1 2919.93 3070.88 37.28 o 7 3 1 359.64 356.55 11.53 o 8 3 1 520.49 477.38 13.39 o 9 3 1 20.88 -2.68 6.76 o 10 3 1 304.28 355.22 17.11 o 11 3 1 154.96 150.60 12.32 o 12 3 1 2142.45 2061.06 33.17 o 13 3 1 8.13 -6.38 8.30 o 14 3 1 1134.56 985.48 23.27 o 15 3 1 97.13 94.88 13.71 o 16 3 1 1044.27 1029.33 25.40 o 17 3 1 47.02 40.03 13.81 o 18 3 1 25.02 2.18 14.63 o 19 3 1 21.93 6.29 15.85 o 20 3 1 16.79 6.95 17.12 o 21 3 1 0.01 -27.24 18.16 o 22 3 1 12.89 -6.80 20.39 o 23 3 1 0.58 -30.25 20.17 o 24 3 1 21.70 -0.54 22.69 o 25 3 1 6.55 -14.13 21.59 o 26 3 1 3.84 -19.41 23.34 o 0 4 1 454.37 437.41 21.30 o 1 4 1 18.08 25.48 6.99 o 2 4 1 779.24 829.59 19.07 o 3 4 1 219.16 192.64 11.87 o 4 4 1 47.30 15.06 7.53 o 5 4 1 830.76 826.12 18.49 o 6 4 1 315.07 327.99 16.74 o 7 4 1 592.19 534.99 15.88 o 8 4 1 0.45 -8.45 6.62 o 9 4 1 1635.78 1654.97 28.48 o 10 4 1 2.41 -4.08 7.62 o 11 4 1 1181.15 1109.33 25.20 o 12 4 1 61.14 67.90 11.34 o 13 4 1 997.91 1062.28 24.74 o 14 4 1 110.12 127.96 14.34 o 15 4 1 0.46 -15.72 10.53 o 16 4 1 25.92 7.54 11.70 o 17 4 1 286.57 359.79 24.28 o 18 4 1 62.78 46.32 17.62 o 19 4 1 57.52 60.43 18.87 o 20 4 1 29.83 17.44 20.26 o 21 4 1 62.85 31.34 24.29 o 22 4 1 3.24 -30.09 20.93 o 23 4 1 4.48 -15.22 22.57 o 24 4 1 0.49 -11.81 23.75 o 25 4 1 24.88 50.82 27.65 o 1 5 1 1888.66 1889.33 29.83 o 2 5 1 586.92 617.17 18.25 o 3 5 1 27.49 15.65 8.69 o 4 5 1 380.67 394.55 20.27 o 5 5 1 23.85 17.92 8.92 o 6 5 1 258.37 274.17 16.64 o 7 5 1 74.72 88.90 12.46 o 8 5 1 1083.79 1071.72 40.17 o 9 5 1 4.37 -11.35 8.16 o 10 5 1 7.03 9.64 9.21 o 11 5 1 139.11 138.17 14.66 o 12 5 1 225.56 243.03 17.84 o 13 5 1 1.32 -16.07 10.71 o 14 5 1 372.38 428.57 23.65 o 15 5 1 234.11 279.36 20.64 o 16 5 1 207.92 261.92 21.54 o 17 5 1 183.73 206.07 25.73 o 18 5 1 664.69 641.90 29.81 o 19 5 1 97.13 70.06 19.75 o 20 5 1 45.86 38.86 20.67 o 21 5 1 76.03 83.04 26.84 o 22 5 1 50.66 68.14 27.07 o 23 5 1 0.05 -20.67 24.17 o 24 5 1 3.87 8.91 25.53 o 0 6 1 188.68 244.25 40.06 o 1 6 1 855.85 739.77 25.20 o 2 6 1 345.99 355.59 27.75 o 3 6 1 249.68 245.69 19.47 o 4 6 1 168.04 170.21 20.21 o 5 6 1 57.83 32.88 10.95 o 6 6 1 12.20 -10.25 9.84 o 7 6 1 278.89 329.19 21.64 o 8 6 1 0.71 -7.21 11.09 o 9 6 1 287.40 371.94 24.11 o 10 6 1 173.29 200.01 20.35 o 11 6 1 549.85 620.40 35.39 o 12 6 1 504.84 587.22 33.61 o 13 6 1 317.01 433.65 27.67 o 14 6 1 0.34 -21.10 14.07 o 15 6 1 56.65 19.21 15.86 o 16 6 1 44.49 41.14 16.54 o 17 6 1 51.10 65.75 19.32 o 18 6 1 6.89 0.97 19.23 o 19 6 1 4.61 19.98 21.63 o 20 6 1 36.52 30.34 39.64 o 21 6 1 126.98 114.86 39.63 o 22 6 1 5.23 -35.09 33.17 o 23 6 1 55.38 55.13 45.85 o 1 7 1 72.70 31.52 17.10 o 2 7 1 334.81 385.42 31.39 o 3 7 1 70.38 45.98 17.57 o 4 7 1 869.37 764.51 32.87 o 5 7 1 343.02 370.56 32.24 o 6 7 1 534.66 532.33 37.88 o 7 7 1 52.92 50.23 18.25 o 8 7 1 141.06 129.36 22.11 o 9 7 1 88.76 118.75 22.27 o 10 7 1 264.69 316.09 29.94 o 11 7 1 75.82 81.89 21.46 o 12 7 1 675.17 662.83 54.37 o 13 7 1 144.04 109.67 23.99 o 14 7 1 200.62 248.74 28.70 o 15 7 1 6.85 -27.05 18.03 o 16 7 1 140.86 137.47 26.16 o 17 7 1 34.66 12.66 23.52 o 18 7 1 47.10 24.53 28.24 o 19 7 1 3.14 -20.93 30.28 o 20 7 1 21.41 -12.96 48.93 o 21 7 1 3.11 1.73 49.58 o 0 8 1 69.99 22.11 36.02 o 1 8 1 830.43 681.68 33.71 o 2 8 1 12.80 -24.90 16.60 o 3 8 1 258.51 199.90 28.85 o 4 8 1 149.72 111.87 27.58 o 5 8 1 40.57 47.87 27.54 o 6 8 1 249.18 318.94 35.27 o 7 8 1 1027.77 1022.67 42.44 o 8 8 1 82.24 60.20 25.12 o 9 8 1 587.36 715.02 48.52 o 10 8 1 35.96 5.36 21.27 o 11 8 1 105.42 163.90 30.16 o 12 8 1 5.02 -6.90 22.42 o 13 8 1 8.12 -6.96 23.28 o 14 8 1 2.03 -24.82 21.65 o 15 8 1 53.61 28.48 26.60 o 16 8 1 36.94 16.26 27.09 o 17 8 1 24.69 7.33 33.20 o 18 8 1 24.60 -2.35 39.82 o 1 9 1 0.01 -6.18 21.50 o 2 9 1 574.92 602.60 46.34 o 3 9 1 131.55 77.16 27.66 o 4 9 1 765.69 812.29 53.39 o 5 9 1 3.47 -23.52 20.83 o 6 9 1 335.49 352.01 38.80 o 7 9 1 2.78 -12.32 21.76 o 8 9 1 9.26 -4.57 23.49 o 9 9 1 13.01 -7.67 23.91 o 10 9 1 210.33 197.26 34.01 o 11 9 1 2.36 -20.26 23.57 o 12 9 1 91.85 83.22 30.34 o 13 9 1 6.65 -24.28 25.22 o 14 9 1 338.56 384.05 44.05 o 15 9 1 0.70 -4.16 28.39 o 0 10 1 24.83 1.57 34.83 o 1 10 1 530.42 530.74 89.00 o 2 10 1 23.18 20.65 26.67 o 3 10 1 97.10 121.91 30.66 o 4 10 1 16.58 5.49 25.66 o 5 10 1 70.45 74.80 29.82 o 6 10 1 7.99 -3.09 26.98 o 7 10 1 148.07 136.29 34.22 o 8 10 1 30.86 71.74 29.80 o 9 10 1 335.52 425.60 46.43 o 10 10 1 0.08 -27.73 26.37 o 0 0 2 26377.77 24436.82 555.70 o 1 0 2 6587.69 6905.71 168.92 o 2 0 2 7280.12 7124.59 100.21 o 3 0 2 19468.13 18470.78 261.40 o 4 0 2 1028.37 1013.69 26.37 o 5 0 2 1355.76 1441.80 41.60 o 6 0 2 511.26 465.95 24.47 o 7 0 2 10286.15 10543.65 160.90 o 8 0 2 3376.34 3175.72 94.05 o 9 0 2 433.78 406.94 14.58 o 10 0 2 1212.92 1213.61 28.17 o 11 0 2 256.18 252.86 17.79 o 12 0 2 12.92 6.29 9.57 o 13 0 2 724.56 701.39 24.34 o 14 0 2 242.60 301.08 21.99 o 15 0 2 45.68 52.29 14.55 o 16 0 2 1024.41 999.96 87.43 o 17 0 2 7320.83 7301.07 241.05 o 18 0 2 763.15 966.52 43.10 o 19 0 2 9302.37 9350.42 236.80 o 20 0 2 511.24 724.08 45.87 o 21 0 2 1167.76 1073.19 50.15 o 22 0 2 485.13 494.48 66.21 o 23 0 2 76.10 37.03 31.80 o 24 0 2 3.57 25.14 31.10 o 25 0 2 4.68 -30.01 29.23 o 26 0 2 84.01 84.85 38.29 o 27 0 2 4.68 -10.93 35.64 o 1 1 2 2361.41 2339.34 43.10 o 2 1 2 234.10 183.35 6.04 o 3 1 2 15355.45 15299.83 142.15 o 4 1 2 250.83 207.48 6.72 o 5 1 2 14035.62 13770.16 218.32 o 6 1 2 2816.82 2873.90 60.29 o 7 1 2 2067.41 2006.16 30.20 o 8 1 2 645.58 725.81 15.29 o 9 1 2 369.84 361.72 16.76 o 10 1 2 1.82 -7.46 4.97 o 11 1 2 2210.90 2331.88 32.05 o 12 1 2 3904.28 4144.83 49.15 o 13 1 2 2141.53 2259.56 45.27 o 14 1 2 13.85 31.78 8.62 o 15 1 2 1251.41 1228.95 29.10 o 16 1 2 552.94 550.01 21.83 o 17 1 2 626.43 571.27 23.11 o 18 1 2 1155.21 1114.89 32.62 o 19 1 2 19.46 27.37 16.42 o 20 1 2 889.26 872.95 33.25 o 21 1 2 129.40 163.87 25.69 o 22 1 2 558.99 600.82 40.17 o 23 1 2 246.44 320.06 35.62 o 24 1 2 0.07 -23.56 19.74 o 25 1 2 165.28 251.00 34.84 o 26 1 2 15.32 13.07 22.65 o 27 1 2 8.95 -3.92 23.94 o 0 2 2 45290.92 45460.48 987.20 o 1 2 2 8781.78 8934.48 107.16 o 2 2 2 23563.64 24127.47 302.98 o 3 2 2 10573.59 11059.72 134.65 o 4 2 2 1632.80 1687.20 26.43 o 5 2 2 2913.92 3089.28 49.96 o 6 2 2 568.36 528.73 18.69 o 7 2 2 9941.32 10924.18 182.41 o 8 2 2 1894.25 1910.28 34.41 o 9 2 2 7183.22 7981.76 169.15 o 10 2 2 329.63 379.67 19.71 o 11 2 2 13456.94 15281.36 265.84 o 12 2 2 8.59 2.56 9.19 o 13 2 2 543.68 548.70 16.02 o 14 2 2 10.89 -1.84 7.92 o 15 2 2 412.70 402.80 22.10 o 16 2 2 633.31 582.65 22.67 o 17 2 2 190.06 212.53 20.84 o 18 2 2 1265.54 1240.83 35.05 o 19 2 2 537.83 531.88 27.33 o 20 2 2 962.12 908.18 31.78 o 21 2 2 292.11 393.26 50.38 o 22 2 2 161.62 175.66 29.44 o 23 2 2 0.01 -19.15 19.39 o 24 2 2 7.24 3.78 21.25 o 25 2 2 20.05 23.57 24.29 o 26 2 2 60.45 51.43 26.57 o 27 2 2 31.29 32.82 26.65 o 1 3 2 540.69 514.40 20.25 o 2 3 2 552.18 561.63 13.46 o 3 3 2 2181.05 2066.76 29.62 o 4 3 2 2613.12 2627.69 43.08 o 5 3 2 598.98 513.05 12.90 o 6 3 2 167.10 170.67 10.01 o 7 3 2 9.34 1.26 5.69 o 8 3 2 222.10 274.48 14.69 o 9 3 2 7.40 5.11 6.72 o 10 3 2 1528.41 1704.32 30.52 o 11 3 2 142.63 173.91 12.96 o 12 3 2 40.36 64.94 10.17 o 13 3 2 912.94 843.66 22.98 o 14 3 2 739.55 630.95 18.87 o 15 3 2 1208.75 1130.51 25.81 o 16 3 2 566.62 540.88 21.87 o 17 3 2 592.36 601.46 27.05 o 18 3 2 61.22 56.27 16.71 o 19 3 2 32.62 33.35 16.68 o 20 3 2 1.15 -22.22 14.82 o 21 3 2 80.27 58.86 21.37 o 22 3 2 326.59 328.54 49.36 o 23 3 2 91.21 59.51 25.08 o 24 3 2 83.39 108.72 28.19 o 25 3 2 20.90 13.73 24.79 o 26 3 2 75.88 117.95 30.60 o 0 4 2 30.43 5.94 15.23 o 1 4 2 32.93 29.73 6.02 o 2 4 2 665.69 631.14 17.13 o 3 4 2 966.22 1051.11 21.81 o 4 4 2 1029.34 953.82 21.32 o 5 4 2 47.78 33.71 7.76 o 6 4 2 441.06 462.40 14.22 o 7 4 2 5.77 3.26 6.92 o 8 4 2 1.23 -0.32 7.35 o 9 4 2 49.65 59.79 9.79 o 10 4 2 364.55 371.03 17.28 o 11 4 2 1246.49 1270.99 26.14 o 12 4 2 316.99 349.96 19.07 o 13 4 2 49.21 70.00 12.60 o 14 4 2 16.68 -2.11 10.13 o 15 4 2 0.07 -14.64 9.76 o 16 4 2 287.25 346.84 23.10 o 17 4 2 6.62 1.39 15.06 o 18 4 2 463.87 564.55 33.56 o 19 4 2 2159.67 1800.21 45.48 o 20 4 2 205.22 287.41 27.84 o 21 4 2 17.78 25.07 20.50 o 22 4 2 8.92 -14.96 21.22 o 23 4 2 7.04 -14.99 21.88 o 24 4 2 0.02 -25.66 23.18 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