#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220044.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220044_Fobs loop_ _publ_author_name 'Jiang, Mei-Xiang' 'Feng, Yun-Long' _publ_section_title ; Tetraaquabis(5-hydroxynicotinato-\kN)cadmium(II) ; _journal_coeditor_code AT2660 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1517 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.377 _cell_angle_beta 68.154 _cell_angle_gamma 65.717 _cell_length_a 7.2190 _cell_length_b 7.2510 _cell_length_c 8.9260 _exptl_crystal_F_000 229.97 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file at2660Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in P1 P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 114.88 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3336.55 3175.45 102.19 o 2 0 0 126.44 137.15 1.69 o 3 0 0 414.51 416.83 4.52 o 4 0 0 1743.12 1783.60 18.13 o 5 0 0 344.34 331.68 5.60 o 6 0 0 65.70 65.18 1.34 o 7 0 0 58.77 62.46 1.58 o 8 0 0 137.33 140.10 4.99 o -7 1 0 63.22 63.16 1.49 o -6 1 0 378.54 370.15 4.48 o -5 1 0 190.45 191.50 3.20 o -4 1 0 290.70 286.02 3.52 o -3 1 0 1960.72 2080.88 20.26 o -2 1 0 2100.15 2150.04 24.39 o -1 1 0 3015.49 2858.37 29.27 o 0 1 0 1744.16 1647.63 25.79 o 1 1 0 2457.27 2241.17 26.74 o 2 1 0 1627.24 1670.01 16.14 o 3 1 0 1028.39 974.08 7.42 o 4 1 0 1697.89 1762.52 13.24 o 5 1 0 355.23 359.80 3.59 o 6 1 0 7.67 8.10 1.05 o 7 1 0 216.50 217.24 3.97 o 8 1 0 178.95 182.83 4.41 o -7 2 0 70.18 65.87 2.06 o -6 2 0 90.29 88.81 1.55 o -5 2 0 251.46 258.68 3.42 o -4 2 0 168.83 175.94 2.55 o -3 2 0 659.30 656.40 6.90 o -2 2 0 1553.13 1572.96 17.66 o -1 2 0 1021.27 958.69 9.63 o 0 2 0 1882.43 2042.71 15.35 o 1 2 0 2633.52 2598.72 25.45 o 2 2 0 2298.90 2278.02 22.31 o 3 2 0 1968.92 2008.42 15.93 o 4 2 0 138.45 138.08 1.46 o 5 2 0 891.55 878.45 8.31 o 6 2 0 1067.08 1028.72 13.17 o 7 2 0 393.55 391.96 6.02 o 8 2 0 90.21 89.53 3.61 o -6 3 0 32.99 32.10 2.43 o -5 3 0 141.91 138.10 2.90 o -4 3 0 140.61 134.97 2.65 o -3 3 0 35.35 31.64 1.06 o -2 3 0 380.99 367.81 4.54 o -1 3 0 533.32 554.11 5.91 o 0 3 0 1395.63 1425.15 10.90 o 1 3 0 160.93 146.17 2.18 o 2 3 0 838.96 832.73 9.57 o 3 3 0 1236.98 1290.09 13.07 o 4 3 0 693.76 677.38 6.60 o 5 3 0 1188.26 1164.32 10.97 o 6 3 0 1207.39 1183.41 14.48 o 7 3 0 247.44 247.72 6.50 o 8 3 0 150.14 148.52 3.69 o -6 4 0 114.17 119.27 3.76 o -5 4 0 53.71 49.64 2.28 o -4 4 0 134.45 123.00 3.45 o -3 4 0 206.75 204.80 6.03 o -2 4 0 186.85 186.61 3.99 o -1 4 0 123.54 130.68 1.75 o 0 4 0 821.95 873.51 6.97 o 1 4 0 350.04 341.23 3.33 o 2 4 0 1775.56 1748.70 19.18 o 3 4 0 594.21 624.97 7.34 o 4 4 0 756.55 773.50 8.36 o 5 4 0 116.55 111.27 1.97 o 6 4 0 176.45 185.19 2.92 o 7 4 0 278.68 270.95 4.62 o 8 4 0 141.14 145.80 3.30 o -5 5 0 67.62 68.87 2.83 o -4 5 0 88.24 83.77 2.98 o -3 5 0 195.60 199.64 4.71 o -2 5 0 168.01 174.17 3.32 o -1 5 0 165.45 165.81 3.06 o 0 5 0 94.43 90.56 1.61 o 1 5 0 813.58 813.55 10.21 o 2 5 0 257.08 254.43 3.84 o 3 5 0 138.31 140.80 2.20 o 4 5 0 197.65 214.09 3.10 o 5 5 0 173.56 168.74 2.63 o 6 5 0 98.87 99.32 2.01 o 7 5 0 123.64 128.13 2.85 o 8 5 0 39.39 38.60 1.64 o -4 6 0 43.92 51.27 3.25 o -3 6 0 43.61 45.69 1.76 o -2 6 0 104.29 106.98 2.64 o -1 6 0 271.49 269.40 4.55 o 0 6 0 222.56 226.71 3.18 o 1 6 0 125.84 118.46 2.38 o 2 6 0 2.18 3.67 0.57 o 3 6 0 200.53 197.03 3.86 o 4 6 0 256.82 246.19 4.61 o 5 6 0 329.66 331.57 5.12 o 6 6 0 40.71 38.89 1.21 o 7 6 0 38.41 45.83 1.62 o -2 7 0 39.24 35.61 2.50 o -1 7 0 121.06 119.51 4.88 o 0 7 0 253.39 255.53 4.30 o 1 7 0 91.05 97.34 3.80 o 2 7 0 179.71 179.10 3.83 o 3 7 0 141.41 136.49 3.84 o 4 7 0 132.65 129.08 3.19 o 5 7 0 62.04 61.00 2.14 o 6 7 0 68.27 67.58 1.81 o 7 7 0 118.50 123.07 3.38 o 1 8 0 104.74 107.68 3.05 o 2 8 0 165.87 153.95 3.76 o 3 8 0 70.89 73.00 2.46 o 4 8 0 52.31 55.24 2.14 o 5 8 0 43.62 44.72 2.35 o 6 8 0 126.93 135.14 6.37 o -5 -8 1 153.34 165.00 7.35 o -4 -8 1 59.58 67.58 4.38 o -3 -8 1 70.54 72.35 3.32 o -2 -8 1 79.69 82.98 5.39 o -1 -8 1 73.79 75.43 4.44 o -6 -7 1 80.27 85.14 2.31 o -5 -7 1 121.86 121.81 2.23 o -4 -7 1 225.25 224.77 4.72 o -3 -7 1 279.61 283.27 5.44 o -2 -7 1 53.42 54.13 1.98 o -1 -7 1 83.03 80.53 3.25 o 0 -7 1 57.72 58.28 1.83 o 1 -7 1 17.39 19.45 1.24 o 2 -7 1 36.46 35.35 2.55 o -7 -6 1 53.88 54.78 3.04 o -6 -6 1 239.17 241.08 4.43 o -5 -6 1 68.06 64.49 2.91 o -4 -6 1 300.56 295.62 4.20 o -3 -6 1 255.73 253.05 4.75 o -2 -6 1 401.96 397.16 6.56 o -1 -6 1 167.56 160.72 3.44 o 0 -6 1 231.33 230.00 3.27 o 1 -6 1 188.10 192.92 3.84 o 2 -6 1 119.77 119.57 3.09 o 3 -6 1 71.51 73.21 3.60 o 4 -6 1 93.38 100.17 4.65 o -7 -5 1 136.84 142.68 3.39 o -6 -5 1 140.83 135.67 2.50 o -5 -5 1 358.90 360.94 4.70 o -4 -5 1 209.54 209.41 2.98 o -3 -5 1 123.81 122.23 2.09 o -2 -5 1 687.02 661.29 9.54 o -1 -5 1 518.63 527.67 6.45 o 0 -5 1 564.74 564.26 6.20 o 1 -5 1 414.44 407.60 5.21 o 2 -5 1 209.28 203.52 3.73 o 3 -5 1 140.85 133.85 3.54 o 4 -5 1 62.02 64.51 2.09 o 5 -5 1 52.51 53.57 3.33 o -8 -4 1 228.67 228.58 5.34 o -7 -4 1 71.16 72.23 2.11 o -6 -4 1 25.03 27.96 2.00 o -5 -4 1 915.00 896.90 9.87 o -4 -4 1 451.94 453.65 6.50 o -3 -4 1 327.44 309.33 4.65 o -2 -4 1 22.32 31.54 0.68 o -1 -4 1 845.12 842.95 8.11 o 0 -4 1 877.17 874.75 8.81 o 1 -4 1 462.63 452.35 5.43 o 2 -4 1 286.51 303.67 4.03 o 3 -4 1 394.57 385.30 7.18 o 4 -4 1 145.55 133.50 3.63 o 5 -4 1 104.60 101.11 3.30 o 6 -4 1 8.68 11.13 1.83 o -8 -3 1 47.57 44.21 2.81 o -7 -3 1 192.05 193.51 3.79 o -6 -3 1 311.58 309.27 4.27 o -5 -3 1 41.14 42.76 1.04 o -4 -3 1 278.99 285.88 3.28 o -3 -3 1 409.27 395.18 3.66 o -2 -3 1 480.90 471.34 4.55 o -1 -3 1 1307.41 1293.46 10.80 o 0 -3 1 538.45 524.34 5.41 o 1 -3 1 500.07 514.22 4.99 o 2 -3 1 438.68 453.30 6.66 o 3 -3 1 323.73 324.26 5.98 o 4 -3 1 516.30 498.57 8.71 o 5 -3 1 182.27 168.94 4.22 o 6 -3 1 154.77 151.73 4.22 o -8 -2 1 67.02 65.94 2.53 o -7 -2 1 347.99 346.38 5.62 o -6 -2 1 458.92 460.57 15.57 o -5 -2 1 0.83 1.07 0.32 o -4 -2 1 319.13 332.28 2.98 o -3 -2 1 1338.42 1378.20 11.30 o -2 -2 1 8413.24 7416.49 83.72 o -1 -2 1 95.49 92.39 0.95 o 0 -2 1 105.48 98.23 1.24 o 1 -2 1 967.33 1000.89 8.10 o 2 -2 1 1563.44 1526.32 11.37 o 3 -2 1 276.54 254.66 3.07 o 4 -2 1 189.41 183.03 2.51 o 5 -2 1 181.24 192.05 2.76 o 6 -2 1 448.23 440.68 5.38 o 7 -2 1 91.96 84.06 2.91 o -8 -1 1 129.85 127.33 3.60 o -7 -1 1 144.73 137.18 3.03 o -6 -1 1 424.35 429.32 5.35 o -5 -1 1 1679.20 1659.73 14.94 o -4 -1 1 1044.27 1046.46 8.14 o -3 -1 1 1786.33 1871.51 13.94 o -2 -1 1 593.99 587.69 4.29 o -1 -1 1 363.09 334.53 3.15 o 0 -1 1 1702.35 1732.03 15.38 o 1 -1 1 1787.83 1633.94 76.77 o 2 -1 1 1042.41 1072.59 9.57 o 3 -1 1 251.16 227.77 2.67 o 4 -1 1 11.72 6.70 0.43 o 5 -1 1 407.16 412.92 4.92 o 6 -1 1 122.72 121.53 2.15 o 7 -1 1 210.56 200.80 2.88 o -7 0 1 178.25 182.71 3.58 o -6 0 1 394.71 388.82 4.45 o -5 0 1 1095.11 1103.02 10.32 o -4 0 1 898.65 903.05 8.42 o -3 0 1 1348.57 1369.58 12.14 o -2 0 1 2.37 5.47 0.27 o -1 0 1 4617.50 4378.32 57.55 o 0 0 1 333.62 343.95 8.93 o 1 0 1 294.79 286.88 4.21 o 2 0 1 48.13 47.43 0.95 o 3 0 1 1049.25 1069.51 10.65 o 4 0 1 1338.36 1334.83 12.16 o 5 0 1 611.96 605.77 6.68 o 6 0 1 41.41 44.19 1.18 o 7 0 1 166.54 173.92 2.57 o 8 0 1 73.59 77.64 2.58 o -7 1 1 142.18 139.18 2.49 o -6 1 1 104.79 100.78 1.91 o -5 1 1 60.64 62.18 1.25 o -4 1 1 749.98 733.48 7.03 o -3 1 1 513.52 492.96 4.82 o -2 1 1 2317.29 2363.87 22.78 o -1 1 1 1540.25 1574.00 13.78 o 0 1 1 1648.00 1623.30 54.46 o 1 1 1 1756.86 1817.60 17.54 o 2 1 1 2501.79 2351.04 23.00 o 3 1 1 2344.83 2470.87 23.40 o 4 1 1 1669.17 1744.25 14.16 o 5 1 1 189.20 181.29 2.28 o 6 1 1 602.95 606.16 6.11 o 7 1 1 62.16 66.03 1.87 o 8 1 1 91.97 89.64 2.42 o -7 2 1 26.79 26.75 2.18 o -6 2 1 60.59 57.87 1.62 o -5 2 1 189.04 185.25 2.41 o -4 2 1 362.88 366.57 3.92 o -3 2 1 123.98 122.88 2.25 o -2 2 1 1057.67 1057.64 16.85 o -1 2 1 2038.46 2053.90 20.11 o 0 2 1 13196.90 11371.13 345.86 o 1 2 1 2853.49 2951.34 25.56 o 2 2 1 2227.24 2214.02 21.66 o 3 2 1 1627.85 1636.24 20.60 o 4 2 1 653.14 685.52 5.41 o 5 2 1 296.53 303.12 2.77 o 6 2 1 301.52 301.36 4.02 o 7 2 1 138.80 139.72 2.92 o 8 2 1 142.15 143.24 3.17 o -6 3 1 73.37 75.44 2.20 o -5 3 1 154.62 156.64 2.80 o -4 3 1 132.28 128.86 2.31 o -3 3 1 752.76 767.70 9.61 o -2 3 1 516.29 536.95 9.32 o -1 3 1 1658.40 1673.78 16.63 o 0 3 1 1062.16 1123.25 9.40 o 1 3 1 1482.70 1466.21 11.16 o 2 3 1 1113.40 1190.79 10.59 o 3 3 1 1557.59 1552.17 15.52 o 4 3 1 890.74 893.30 8.39 o 5 3 1 480.54 485.04 5.03 o 6 3 1 1.18 1.77 0.37 o 7 3 1 372.57 360.05 4.83 o 8 3 1 161.92 174.51 3.83 o -5 4 1 27.03 27.15 1.73 o -4 4 1 93.50 87.97 2.84 o -3 4 1 476.41 480.64 11.00 o -2 4 1 494.94 500.49 6.60 o -1 4 1 88.93 84.41 1.45 o 0 4 1 83.28 97.95 1.19 o 1 4 1 1719.43 1714.74 13.11 o 2 4 1 1285.56 1283.71 12.82 o 3 4 1 244.40 237.79 2.56 o 4 4 1 230.87 230.02 2.99 o 5 4 1 857.65 883.26 9.53 o 6 4 1 1020.95 1006.91 10.94 o 7 4 1 299.56 302.50 4.89 o 8 4 1 115.18 109.84 4.56 o -5 5 1 30.80 29.47 1.95 o -4 5 1 44.11 40.54 1.68 o -3 5 1 10.94 13.37 1.24 o -2 5 1 155.93 156.14 3.79 o -1 5 1 121.65 120.68 2.12 o 0 5 1 397.06 405.90 3.67 o 1 5 1 221.84 225.07 2.25 o 2 5 1 406.88 395.00 4.86 o 3 5 1 193.32 199.51 3.18 o 4 5 1 404.35 414.86 4.83 o 5 5 1 962.09 956.93 10.29 o 6 5 1 1314.24 1332.33 14.13 o 7 5 1 124.33 126.24 2.73 o 8 5 1 128.45 127.91 8.51 o -4 6 1 40.05 40.22 2.16 o -3 6 1 15.93 18.28 1.28 o -2 6 1 24.40 27.48 1.31 o -1 6 1 181.26 177.95 3.90 o 0 6 1 346.26 349.18 4.30 o 1 6 1 26.68 27.18 1.02 o 2 6 1 228.21 222.21 4.07 o 3 6 1 729.34 747.16 8.73 o 4 6 1 561.66 562.44 7.60 o 5 6 1 69.71 66.43 1.37 o 6 6 1 19.10 18.88 0.86 o 7 6 1 249.50 242.86 4.21 o 8 6 1 170.75 181.76 4.34 o -2 7 1 34.33 34.38 1.92 o -1 7 1 44.00 45.39 1.69 o 0 7 1 40.50 46.78 1.55 o 1 7 1 158.43 160.02 3.04 o 2 7 1 74.17 69.06 2.11 o 3 7 1 145.69 149.78 4.09 o 4 7 1 144.77 136.56 3.54 o 5 7 1 32.86 31.28 2.67 o 6 7 1 3.33 3.41 0.48 o 7 7 1 138.43 142.10 6.73 o 0 8 1 31.60 34.68 2.04 o 1 8 1 67.64 65.06 2.24 o 2 8 1 25.78 28.03 1.48 o 3 8 1 10.17 11.00 1.05 o 4 8 1 44.81 46.02 2.48 o 5 8 1 134.56 131.69 6.79 o 6 8 1 81.18 77.09 4.64 o 2 9 1 58.47 59.73 4.11 o 3 9 1 44.38 40.62 3.37 o 4 9 1 21.45 22.77 2.88 o -3 -8 2 33.40 30.04 3.32 o -2 -8 2 37.52 39.40 3.33 o -1 -8 2 33.35 34.33 3.36 o -5 -7 2 29.90 31.72 1.94 o -4 -7 2 87.85 86.18 2.72 o -3 -7 2 193.23 192.84 5.75 o -2 -7 2 219.93 219.42 4.67 o -1 -7 2 104.04 99.80 2.86 o 0 -7 2 53.59 54.83 3.86 o 2 -7 2 36.76 40.88 2.81 o -6 -6 2 146.99 156.09 5.30 o -5 -6 2 270.12 270.76 4.88 o -4 -6 2 154.76 155.47 2.79 o -3 -6 2 316.83 309.86 4.28 o -2 -6 2 273.31 266.45 6.38 o -1 -6 2 157.02 157.40 4.53 o 0 -6 2 75.86 75.84 1.95 o 1 -6 2 162.25 168.88 2.99 o 2 -6 2 73.67 72.20 2.16 o 3 -6 2 10.69 13.10 1.78 o -7 -5 2 36.20 35.91 1.84 o -6 -5 2 144.03 142.05 6.38 o -5 -5 2 380.99 359.61 5.78 o -4 -5 2 515.49 518.13 6.73 o -3 -5 2 450.40 452.90 5.87 o -2 -5 2 251.14 241.05 3.43 o -1 -5 2 348.11 336.87 4.56 o 0 -5 2 257.84 251.31 3.70 o 1 -5 2 7.66 9.70 1.97 o 2 -5 2 175.54 173.20 3.37 o 3 -5 2 196.79 195.30 3.84 o 4 -5 2 90.38 88.45 4.06 o 5 -5 2 16.70 17.10 2.10 o -7 -4 2 9.13 7.92 1.06 o -6 -4 2 293.63 302.40 5.23 o -5 -4 2 271.70 284.13 3.99 o -4 -4 2 888.41 900.02 9.83 o -3 -4 2 242.62 245.65 3.02 o -2 -4 2 421.64 431.11 4.67 o -1 -4 2 856.87 842.83 8.34 o 0 -4 2 1153.50 1127.09 11.21 o 1 -4 2 335.30 326.33 4.24 o 2 -4 2 201.50 197.02 3.96 o 3 -4 2 281.96 287.45 4.71 o 4 -4 2 464.54 446.33 6.83 o 5 -4 2 54.10 50.06 2.30 o 6 -4 2 43.69 42.13 2.93 o -7 -3 2 316.86 318.49 6.21 o -6 -3 2 260.83 269.46 3.99 o -5 -3 2 393.94 401.53 4.58 o -4 -3 2 116.42 119.52 1.83 o -3 -3 2 339.14 329.11 3.24 o -2 -3 2 1649.84 1650.39 12.79 o -1 -3 2 1335.59 1377.29 10.66 o 0 -3 2 946.88 982.42 9.17 o 1 -3 2 1937.43 2002.68 16.44 o 2 -3 2 334.74 340.03 4.26 o 3 -3 2 476.81 462.91 7.95 o 4 -3 2 226.78 220.56 4.77 o 5 -3 2 279.04 263.64 5.70 o 6 -3 2 45.01 48.21 2.25 o -7 -2 2 179.97 189.59 3.83 o -6 -2 2 81.66 82.38 2.17 o -5 -2 2 616.84 608.73 7.08 o -4 -2 2 152.72 154.58 1.90 o -3 -2 2 1001.98 962.03 7.58 o -2 -2 2 429.41 395.48 3.35 o -1 -2 2 606.44 605.29 5.44 o 0 -2 2 267.70 254.51 2.81 o 1 -2 2 1299.76 1265.54 16.24 o 2 -2 2 2465.29 2502.88 20.13 o 3 -2 2 1091.35 1074.20 9.84 o 4 -2 2 96.96 99.90 1.67 o 5 -2 2 345.08 348.78 5.12 o 6 -2 2 97.49 102.73 2.23 o 7 -2 2 49.79 50.08 1.90 o -7 -1 2 73.78 72.87 2.70 o -6 -1 2 178.20 173.99 3.38 o -5 -1 2 37.26 37.57 0.97 o -4 -1 2 741.28 734.88 6.94 o -3 -1 2 409.71 402.64 3.26 o -2 -1 2 142.13 109.65 1.31 o -1 -1 2 1031.14 989.15 7.72 o 0 -1 2 2100.36 2090.95 24.59 o 1 -1 2 456.95 447.90 5.62 o 2 -1 2 1917.43 1913.43 18.50 o 3 -1 2 405.56 424.42 4.64 o 4 -1 2 1224.13 1254.91 12.67 o 5 -1 2 250.76 247.86 3.30 o 6 -1 2 466.37 440.11 5.37 o 7 -1 2 187.35 177.26 2.92 o 8 -1 2 70.75 71.81 2.04 o -7 0 2 219.80 223.75 4.85 o -6 0 2 210.33 212.72 2.94 o -5 0 2 0.68 1.25 0.35 o -4 0 2 524.82 543.27 5.47 o -3 0 2 1164.86 1209.48 8.70 o -2 0 2 3114.49 3093.23 24.52 o -1 0 2 240.22 253.61 2.84 o 0 0 2 2061.09 2020.52 26.18 o 1 0 2 3752.98 3706.00 31.70 o 2 0 2 127.34 119.31 1.55 o 3 0 2 197.89 202.64 2.20 o 4 0 2 1221.27 1201.86 10.85 o 5 0 2 522.61 500.23 5.66 o 6 0 2 523.24 501.73 5.89 o 7 0 2 200.00 193.09 3.04 o 8 0 2 153.44 158.09 3.35 o -7 1 2 88.73 81.14 2.60 o -6 1 2 238.13 223.27 4.45 o -5 1 2 1007.91 999.85 9.61 o -4 1 2 364.44 367.92 4.43 o -3 1 2 1167.70 1160.99 10.54 o -2 1 2 984.37 1047.14 9.41 o -1 1 2 671.10 641.61 5.82 o 0 1 2 669.76 670.89 5.64 o 1 1 2 3311.04 3191.76 27.43 o 2 1 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380.97 5.94 o 7 1 8 97.10 91.24 6.74 o -3 2 8 234.29 239.51 3.55 o -2 2 8 69.64 70.10 1.76 o -1 2 8 204.43 207.67 3.50 o 0 2 8 1025.88 1031.14 12.52 o 1 2 8 783.52 781.06 8.42 o 2 2 8 199.08 206.71 2.94 o 3 2 8 38.06 41.91 1.10 o 4 2 8 477.01 471.99 6.44 o 5 2 8 538.28 550.95 7.36 o 6 2 8 109.01 123.41 3.21 o 7 2 8 176.75 173.92 6.09 o 8 2 8 138.20 138.74 8.17 o -3 3 8 114.29 121.57 3.70 o -2 3 8 157.14 154.51 4.02 o -1 3 8 117.08 109.26 3.13 o 0 3 8 0.64 1.48 0.55 o 1 3 8 286.05 294.15 3.78 o 2 3 8 230.46 234.67 3.19 o 3 3 8 382.10 391.44 4.71 o 4 3 8 393.15 394.66 4.77 o 5 3 8 412.84 411.58 5.77 o 6 3 8 157.32 168.13 8.35 o 7 3 8 256.59 280.33 5.66 o 8 3 8 198.80 206.78 5.28 o -2 4 8 76.72 77.05 2.84 o -1 4 8 46.99 45.83 3.02 o 0 4 8 29.83 28.63 1.65 o 1 4 8 79.50 80.08 2.06 o 2 4 8 248.81 241.34 3.97 o 3 4 8 381.86 383.56 4.56 o 4 4 8 215.10 223.66 3.08 o 5 4 8 472.25 470.45 7.81 o 6 4 8 746.50 722.70 11.36 o 7 4 8 207.49 206.10 4.53 o 8 4 8 146.73 150.26 4.96 o -2 5 8 25.22 23.28 1.76 o -1 5 8 118.43 117.13 2.92 o 0 5 8 273.93 270.49 4.68 o 1 5 8 38.40 37.07 1.44 o 2 5 8 171.64 176.25 3.30 o 3 5 8 274.28 266.48 4.29 o 4 5 8 338.47 344.77 6.33 o 5 5 8 150.39 157.18 3.21 o 6 5 8 203.64 193.56 6.49 o 7 5 8 156.37 138.45 3.42 o 8 5 8 101.25 100.66 2.99 o -1 6 8 76.69 77.12 3.90 o 0 6 8 67.10 64.41 3.12 o 1 6 8 120.41 126.91 2.90 o 2 6 8 176.95 175.09 3.42 o 3 6 8 204.74 205.48 4.59 o 4 6 8 76.59 74.34 2.47 o 5 6 8 0.74 1.42 0.79 o 6 6 8 7.97 9.08 1.49 o 7 6 8 184.32 179.34 3.77 o 8 6 8 66.91 58.99 2.09 o 1 7 8 95.45 96.68 2.58 o 2 7 8 39.66 44.61 2.06 o 3 7 8 27.89 29.83 1.44 o 4 7 8 27.64 28.23 1.41 o 5 7 8 102.35 100.91 3.33 o 6 7 8 65.24 66.15 2.69 o 7 7 8 36.98 40.57 2.16 o 2 8 8 18.75 21.41 1.69 o 3 8 8 13.29 14.83 1.21 o 4 8 8 87.38 88.80 2.93 o 5 8 8 194.80 197.41 6.96 o 6 8 8 76.53 67.93 2.81 o 0 -3 9 169.34 174.32 3.92 o 1 -3 9 199.63 211.32 5.13 o 2 -3 9 107.59 100.71 3.17 o -1 -2 9 70.32 73.18 2.27 o 0 -2 9 171.12 169.71 3.79 o 1 -2 9 180.19 176.24 3.84 o 2 -2 9 145.31 146.12 3.42 o 3 -2 9 77.80 73.39 2.33 o 4 -2 9 132.62 131.61 4.43 o -2 -1 9 329.19 346.19 9.17 o -1 -1 9 198.08 195.59 4.05 o 0 -1 9 145.57 139.62 3.81 o 1 -1 9 71.42 68.55 2.11 o 2 -1 9 104.05 108.70 4.18 o 3 -1 9 147.85 153.60 5.35 o 4 -1 9 262.14 255.11 5.70 o 5 -1 9 111.00 111.12 3.45 o -2 0 9 440.78 456.36 8.53 o -1 0 9 205.53 208.90 6.92 o 0 0 9 122.56 119.03 3.83 o 1 0 9 143.12 146.17 3.80 o 2 0 9 251.53 240.94 7.04 o 3 0 9 287.82 317.13 10.24 o 4 0 9 48.23 61.45 2.73 o 5 0 9 114.81 114.78 3.44 o 6 0 9 123.55 117.75 4.69 o -2 1 9 41.45 39.39 1.48 o -1 1 9 231.96 240.98 5.26 o 0 1 9 190.18 186.08 3.39 o 1 1 9 326.37 320.10 6.26 o 2 1 9 320.00 306.19 6.06 o 3 1 9 193.42 194.66 6.94 o 4 1 9 96.23 101.53 2.98 o 5 1 9 181.29 174.28 4.77 o 6 1 9 38.19 29.96 1.41 o 7 1 9 138.03 138.53 6.58 o -2 2 9 124.25 121.18 3.30 o -1 2 9 212.34 215.97 6.73 o 0 2 9 146.12 148.95 2.52 o 1 2 9 209.03 208.85 4.16 o 2 2 9 345.24 347.92 4.51 o 3 2 9 397.85 383.62 4.78 o 4 2 9 577.29 544.27 9.29 o 5 2 9 178.66 178.59 4.15 o 6 2 9 174.03 179.19 4.25 o 7 2 9 26.28 23.34 2.26 o -2 3 9 141.80 151.16 4.99 o -1 3 9 94.92 90.85 2.95 o 0 3 9 429.75 414.19 5.06 o 1 3 9 441.13 436.64 5.60 o 2 3 9 397.82 397.44 4.91 o 3 3 9 332.55 333.84 4.29 o 4 3 9 277.77 272.26 3.71 o 5 3 9 224.40 217.39 3.73 o 6 3 9 312.67 326.80 18.97 o 7 3 9 81.54 83.04 3.86 o 8 3 9 98.34 96.15 4.49 o -1 4 9 144.42 148.59 4.06 o 0 4 9 467.01 453.34 6.79 o 1 4 9 359.17 359.53 5.61 o 2 4 9 90.93 89.00 2.20 o 3 4 9 104.00 107.44 1.89 o 4 4 9 231.33 242.04 3.38 o 5 4 9 360.56 358.80 6.45 o 6 4 9 49.55 46.57 3.94 o 7 4 9 184.75 184.00 4.29 o 8 4 9 124.45 133.42 3.68 o -1 5 9 63.40 68.27 2.44 o 0 5 9 5.93 7.58 0.89 o 1 5 9 45.83 46.55 1.69 o 2 5 9 100.54 99.60 2.45 o 3 5 9 197.92 193.72 3.60 o 4 5 9 254.37 252.07 5.24 o 5 5 9 145.36 147.93 2.66 o 6 5 9 76.24 74.43 2.61 o 7 5 9 193.18 182.24 4.13 o 8 5 9 194.45 189.67 6.35 o 0 6 9 0.24 0.27 0.53 o 1 6 9 18.33 18.68 1.29 o 2 6 9 166.55 171.00 4.78 o 3 6 9 135.42 144.12 3.84 o 4 6 9 52.83 49.95 2.10 o 5 6 9 138.81 135.35 3.62 o 6 6 9 556.00 556.34 13.61 o 7 6 9 184.72 191.41 3.95 o 2 7 9 53.33 50.39 2.32 o 3 7 9 78.10 75.38 4.94 o 4 7 9 72.06 75.48 2.73 o 5 7 9 113.51 106.20 3.26 o 6 7 9 159.16 144.92 5.63 o 7 7 9 88.26 94.42 4.48 o 4 8 9 62.15 68.61 2.69 o 5 8 9 6.68 8.25 1.01 o 0 -1 10 183.77 186.48 4.10 o 1 -1 10 246.81 255.41 5.86 o 2 -1 10 163.22 171.58 4.59 o 3 -1 10 141.19 133.63 8.51 o 4 -1 10 59.91 55.90 2.49 o -1 0 10 94.55 95.05 3.18 o 0 0 10 116.16 119.08 3.55 o 1 0 10 61.43 52.02 2.39 o 2 0 10 310.15 307.18 6.48 o 3 0 10 161.75 165.08 4.34 o 4 0 10 152.50 157.22 3.52 o 5 0 10 65.87 69.12 5.55 o -1 1 10 157.07 166.60 4.24 o 0 1 10 109.73 107.80 3.22 o 1 1 10 90.90 90.01 7.88 o 2 1 10 96.85 98.63 3.04 o 3 1 10 149.18 151.57 3.98 o 4 1 10 261.97 249.41 7.01 o 5 1 10 113.93 116.06 3.44 o 6 1 10 280.80 315.26 6.66 o -1 2 10 91.64 90.56 1.99 o 0 2 10 62.80 63.88 1.61 o 1 2 10 251.84 246.13 4.17 o 2 2 10 158.06 156.24 3.85 o 3 2 10 174.86 178.12 7.10 o 4 2 10 33.06 37.33 1.76 o 5 2 10 196.75 187.95 4.46 o 6 2 10 131.25 135.63 3.72 o -1 3 10 88.18 88.86 2.54 o 0 3 10 129.05 135.17 3.47 o 1 3 10 180.22 178.45 2.84 o 2 3 10 238.69 240.57 4.43 o 3 3 10 94.11 92.60 1.90 o 4 3 10 67.75 74.59 1.70 o 5 3 10 179.91 164.38 6.52 o 6 3 10 62.21 59.20 3.20 o 7 3 10 80.24 72.76 3.75 o 0 4 10 153.07 158.46 3.49 o 1 4 10 38.88 38.40 1.56 o 2 4 10 91.61 85.28 2.28 o 3 4 10 236.76 223.02 3.23 o 4 4 10 557.00 558.57 6.56 o 5 4 10 124.04 126.26 3.22 o 6 4 10 97.91 89.22 3.41 o 7 4 10 23.51 15.58 1.30 o 1 5 10 175.89 175.63 3.70 o 2 5 10 132.27 133.62 3.05 o 3 5 10 258.54 258.46 4.52 o 4 5 10 215.83 211.04 4.82 o 5 5 10 105.81 110.38 2.24 o 6 5 10 119.46 125.28 5.54 o 7 5 10 105.03 100.11 2.92 o 2 6 10 111.06 117.82 2.95 o 3 6 10 52.19 55.59 2.38 o 4 6 10 31.51 30.46 1.85 o 5 6 10 142.63 134.36 3.76 o 6 6 10 62.11 62.10 3.52 o 4 7 10 57.26 61.61 5.54 o 5 7 10 62.01 61.01 3.09 o 1 1 11 206.40 211.23 5.08 o 2 1 11 190.14 201.86 4.92 o 3 1 11 161.08 144.40 4.03 o 4 1 11 78.97 72.93 2.78 o 1 2 11 81.87 75.90 3.37 o 2 2 11 316.21 300.91 6.22 o 3 2 11 101.72 109.53 3.29 o 4 2 11 98.89 86.86 3.24 o 5 2 11 83.70 79.46 4.53 o 1 3 11 85.73 88.18 1.91 o 2 3 11 62.76 60.16 1.77 o 3 3 11 75.93 83.16 2.63 o 4 3 11 148.16 145.68 3.75 o 5 3 11 144.57 132.32 3.61 o 2 4 11 31.92 33.70 2.57 o 3 4 11 103.53 104.49 2.01 o 4 4 11 71.03 74.86 1.73 o 5 4 11 128.94 147.36 4.69 o 6 4 11 72.36 74.27 3.43 o 3 5 11 65.27 65.83 2.22 o 4 5 11 63.73 62.39 2.47 o 5 5 11 63.59 62.00 2.47 o