#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220047.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220047_Fobs loop_ _publ_author_name 'Harding, David J.' 'Harding, Phimphaka' 'Adams, Harry' _publ_section_title ; Tris(phenanthroline-\k^2^N,N')cobalt(II) tetrafluoridoborate acetonitrile solvate ; _journal_coeditor_code AT2665 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1538 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.361 _cell_angle_gamma 90.000 _cell_length_a 18.0443 _cell_length_b 9.3623 _cell_length_c 22.0702 _exptl_crystal_F_000 1652.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file at2665Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' WU5110' _shelx_refln_list_code 4 _shelx_F_calc_maximum 349.86 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1277.83 1116.95 21.68 o 4 0 0 8142.30 9342.19 114.97 o 6 0 0 200.87 295.57 11.52 o 8 0 0 6808.47 6161.18 75.06 o 10 0 0 2574.40 3139.16 46.05 o 12 0 0 24.27 48.89 12.71 o 14 0 0 904.07 1121.75 33.59 o 16 0 0 864.81 717.85 46.22 o 18 0 0 3331.23 3464.41 107.51 o 20 0 0 1901.96 2058.60 102.69 o 1 1 0 1512.70 1499.44 17.41 o 2 1 0 3446.95 3125.28 32.95 o 3 1 0 117.64 226.10 8.37 o 4 1 0 4633.07 4787.46 45.94 o 5 1 0 11094.94 11493.23 86.15 o 6 1 0 1436.46 1276.13 16.67 o 7 1 0 3119.91 3430.46 32.92 o 8 1 0 2623.83 2611.77 31.46 o 9 1 0 9892.35 8878.58 73.98 o 10 1 0 1838.51 1901.68 24.25 o 11 1 0 3116.42 3069.76 33.84 o 12 1 0 1348.68 1409.97 23.48 o 13 1 0 298.67 236.27 12.34 o 14 1 0 788.87 992.36 26.77 o 15 1 0 2012.89 2202.81 45.20 o 16 1 0 282.60 220.99 17.83 o 17 1 0 386.02 348.39 24.24 o 18 1 0 238.46 324.93 22.78 o 19 1 0 221.67 246.88 24.91 o 20 1 0 43.35 42.63 17.33 o 0 2 0 30220.74 33902.85 383.18 o 1 2 0 1076.40 984.35 14.40 o 2 2 0 4297.51 5167.00 51.19 o 3 2 0 533.15 538.14 11.58 o 4 2 0 1018.21 1491.64 18.61 o 5 2 0 1600.21 1863.38 20.90 o 6 2 0 57.12 39.86 5.13 o 7 2 0 216.72 373.27 11.11 o 8 2 0 1098.80 1036.41 16.98 o 9 2 0 259.65 285.20 12.02 o 10 2 0 14.12 25.89 6.18 o 11 2 0 8.52 7.44 6.32 o 12 2 0 396.60 585.42 19.40 o 13 2 0 43.73 137.50 13.15 o 14 2 0 2007.07 2299.54 48.21 o 15 2 0 1063.25 868.84 30.30 o 16 2 0 25.23 2.98 11.99 o 17 2 0 40.85 -0.17 13.34 o 18 2 0 714.44 970.55 43.13 o 19 2 0 415.92 300.23 30.94 o 20 2 0 471.39 517.28 31.47 o 1 3 0 675.09 760.78 12.62 o 2 3 0 9160.58 9237.34 69.62 o 3 3 0 15.59 12.81 3.93 o 4 3 0 944.29 857.67 13.46 o 5 3 0 164.31 158.05 7.11 o 6 3 0 3547.24 3554.74 34.23 o 7 3 0 2812.03 3157.88 35.14 o 8 3 0 2285.53 2480.81 30.65 o 9 3 0 551.61 324.16 13.24 o 10 3 0 3042.69 2460.39 37.79 o 11 3 0 1628.04 1904.88 33.49 o 12 3 0 2406.76 2473.26 40.31 o 13 3 0 639.76 515.81 20.88 o 14 3 0 4876.86 5068.94 73.63 o 15 3 0 309.33 394.42 23.11 o 16 3 0 144.56 127.62 20.53 o 17 3 0 430.33 387.37 27.02 o 18 3 0 163.54 157.23 21.34 o 19 3 0 426.29 420.24 32.51 o 0 4 0 8.51 53.07 8.91 o 1 4 0 14048.28 13824.16 91.65 o 2 4 0 677.57 1063.75 13.80 o 3 4 0 40.32 92.84 5.92 o 4 4 0 233.37 279.89 8.47 o 5 4 0 4916.86 4705.37 41.56 o 6 4 0 1360.35 1589.73 28.96 o 7 4 0 4041.47 3748.56 39.13 o 8 4 0 811.61 995.38 20.62 o 9 4 0 593.45 417.64 15.74 o 10 4 0 269.52 373.19 20.39 o 11 4 0 215.64 182.66 12.89 o 12 4 0 1589.97 1251.57 27.59 o 13 4 0 293.72 371.82 19.64 o 14 4 0 1072.92 1352.43 44.39 o 15 4 0 517.90 538.52 36.07 o 16 4 0 245.66 306.91 23.21 o 17 4 0 358.50 366.10 26.91 o 18 4 0 258.31 124.38 21.47 o 19 4 0 401.50 340.48 28.03 o 1 5 0 192.24 200.82 8.10 o 2 5 0 1274.20 1430.93 17.75 o 3 5 0 65.32 23.79 5.19 o 4 5 0 502.73 441.52 11.24 o 5 5 0 14.89 16.14 5.66 o 6 5 0 556.19 699.12 16.87 o 7 5 0 1102.96 1227.49 24.44 o 8 5 0 3559.96 3412.79 44.87 o 9 5 0 1746.76 2131.00 34.51 o 10 5 0 3275.91 2600.71 39.80 o 11 5 0 48.80 64.67 10.87 o 12 5 0 8.19 22.26 11.61 o 13 5 0 8.99 -5.25 11.20 o 14 5 0 2025.49 1637.68 38.42 o 15 5 0 117.81 107.12 15.95 o 16 5 0 186.04 204.59 19.17 o 17 5 0 56.42 34.26 15.41 o 18 5 0 101.09 122.31 19.41 o 0 6 0 370.98 202.83 14.24 o 1 6 0 7720.07 7568.65 71.54 o 2 6 0 670.56 882.64 15.44 o 3 6 0 1823.82 2193.22 27.60 o 4 6 0 49.92 62.58 7.89 o 5 6 0 2683.26 2151.72 32.48 o 6 6 0 1068.52 1369.08 32.93 o 7 6 0 3501.01 3588.12 47.73 o 8 6 0 0.14 -4.56 8.61 o 9 6 0 246.17 240.45 18.81 o 10 6 0 42.33 67.05 11.97 o 11 6 0 670.68 671.23 25.27 o 12 6 0 358.68 410.12 23.07 o 13 6 0 151.01 147.49 16.19 o 14 6 0 431.39 438.47 28.17 o 15 6 0 279.91 308.55 21.75 o 16 6 0 169.76 136.58 18.24 o 17 6 0 381.42 341.21 26.52 o 1 7 0 789.13 1033.98 20.79 o 2 7 0 200.84 305.16 13.26 o 3 7 0 1098.26 921.91 19.87 o 4 7 0 669.26 616.53 17.57 o 5 7 0 3078.99 3195.59 46.66 o 6 7 0 479.01 518.94 19.13 o 7 7 0 121.04 179.81 15.34 o 8 7 0 881.95 1014.30 27.02 o 9 7 0 928.48 969.31 27.97 o 10 7 0 861.65 786.57 27.52 o 11 7 0 1005.13 1024.70 31.55 o 12 7 0 111.43 174.30 17.80 o 13 7 0 1581.02 1587.38 40.17 o 14 7 0 1095.18 1137.64 42.77 o 15 7 0 151.28 134.14 22.67 o 0 8 0 92.18 140.42 17.61 o 1 8 0 177.23 199.93 20.42 o 2 8 0 567.07 498.01 27.00 o 3 8 0 17.06 65.64 10.85 o 4 8 0 114.20 45.16 10.70 o 5 8 0 253.24 205.90 14.86 o 6 8 0 798.16 936.86 27.97 o 7 8 0 14.89 65.59 13.06 o 8 8 0 10.24 9.04 11.60 o 9 8 0 170.49 143.16 23.46 o 10 8 0 247.41 331.99 22.68 o 11 8 0 0.84 1.49 13.90 o 12 8 0 151.36 117.09 18.37 o 13 8 0 107.17 65.43 17.49 o 14 8 0 9.77 -8.23 15.38 o 1 9 0 729.58 987.74 33.69 o 2 9 0 18.35 23.96 13.03 o 3 9 0 915.70 890.02 34.66 o 4 9 0 1012.18 927.37 33.58 o 5 9 0 897.44 1072.48 32.26 o 6 9 0 804.37 801.92 29.42 o 7 9 0 226.82 232.28 19.38 o 8 9 0 17.30 35.22 13.87 o 9 9 0 897.55 844.85 32.75 o 10 9 0 20.71 11.99 14.28 o 11 9 0 559.38 483.48 27.47 o 12 9 0 232.56 260.91 23.30 o 0 10 0 1748.75 1633.68 62.40 o 1 10 0 6.94 -7.46 15.77 o 2 10 0 1849.50 2243.57 84.85 o 3 10 0 633.08 734.55 39.66 o 4 10 0 190.82 123.31 26.55 o 5 10 0 138.92 102.71 19.18 o 6 10 0 1397.93 1334.70 47.58 o 7 10 0 168.03 162.88 21.71 o 8 10 0 511.37 422.77 31.53 o 9 10 0 0.96 5.67 17.03 o 1 11 0 3.50 -16.97 18.92 o 2 11 0 10.13 23.33 20.09 o 3 11 0 83.20 60.24 21.55 o -19 0 1 1258.47 1368.98 73.77 o -17 0 1 918.15 967.19 40.21 o -15 0 1 1489.38 1514.87 44.07 o -13 0 1 2091.62 2047.65 43.11 o -11 0 1 152.12 55.11 9.73 o -9 0 1 457.08 722.28 22.88 o -7 0 1 12176.67 9602.70 115.89 o -5 0 1 5382.90 7139.83 93.30 o -3 0 1 142.63 456.85 14.11 o -1 0 1 126.66 -1.95 0.97 o 3 0 1 19219.39 18344.83 234.55 o 5 0 1 11668.48 10421.62 118.68 o 7 0 1 6920.01 7081.23 82.46 o 9 0 1 5075.07 5634.38 76.69 o 11 0 1 1866.66 1529.77 32.94 o 13 0 1 5876.52 6634.48 106.17 o 15 0 1 182.29 82.16 20.56 o 17 0 1 811.79 1080.90 59.03 o 19 0 1 56.32 66.86 28.39 o -20 1 1 782.76 816.87 34.58 o -19 1 1 354.14 395.78 24.18 o -18 1 1 1902.72 1992.45 41.83 o -17 1 1 24.34 31.53 12.54 o -16 1 1 124.00 104.15 13.81 o -15 1 1 167.71 241.81 16.05 o -14 1 1 237.84 238.05 16.79 o -13 1 1 286.89 266.54 13.70 o -12 1 1 37.57 4.57 6.94 o -11 1 1 38.39 28.06 6.54 o -10 1 1 305.34 423.65 11.29 o -9 1 1 55.64 14.06 5.04 o -8 1 1 894.21 652.58 14.27 o -7 1 1 1445.58 1437.46 18.78 o -6 1 1 8474.65 10076.33 78.21 o -5 1 1 4890.75 4189.20 41.13 o -4 1 1 55671.42 52646.34 423.46 o -3 1 1 2533.27 2599.12 30.07 o -2 1 1 16766.74 20433.17 194.17 o -1 1 1 9022.74 9488.73 123.79 o 0 1 1 26188.47 23325.39 198.61 o 1 1 1 5299.62 5078.06 46.84 o 2 1 1 5045.44 6772.06 64.52 o 3 1 1 751.03 779.93 11.81 o 4 1 1 2277.49 3137.60 31.10 o 5 1 1 10.87 49.36 4.60 o 6 1 1 109.44 183.76 6.79 o 7 1 1 53.03 76.96 6.73 o 8 1 1 1.26 0.80 4.53 o 9 1 1 1063.74 1074.77 18.09 o 10 1 1 1874.29 1939.99 26.17 o 11 1 1 12.79 4.17 6.73 o 12 1 1 3844.70 4210.77 53.20 o 13 1 1 202.34 238.12 14.83 o 14 1 1 452.95 284.21 19.75 o 15 1 1 1419.22 1555.45 43.72 o 16 1 1 890.19 1264.83 39.54 o 17 1 1 36.32 4.46 13.92 o 18 1 1 634.06 455.64 29.53 o 19 1 1 27.34 56.65 17.72 o 20 1 1 2038.87 2523.47 64.84 o -20 2 1 91.35 134.50 22.21 o -19 2 1 345.82 334.66 27.16 o -18 2 1 346.51 276.78 43.55 o -17 2 1 261.31 318.66 21.11 o -16 2 1 330.01 454.33 23.28 o -15 2 1 839.80 716.56 31.63 o -14 2 1 626.68 488.90 19.83 o -13 2 1 1119.96 1201.33 25.35 o -12 2 1 267.54 214.40 12.36 o -11 2 1 1681.11 1232.15 21.94 o -10 2 1 900.41 870.45 16.90 o -9 2 1 41.34 95.71 7.32 o -8 2 1 4437.33 3124.52 32.40 o -7 2 1 492.61 206.95 8.16 o -6 2 1 24.88 16.92 4.30 o -5 2 1 6541.43 6385.88 53.23 o -4 2 1 2220.26 2025.80 22.70 o -3 2 1 4757.86 5354.88 54.03 o -2 2 1 960.71 834.55 14.51 o -1 2 1 12936.48 13222.01 121.83 o 0 2 1 3246.63 3090.61 30.27 o 1 2 1 598.92 272.78 7.14 o 2 2 1 36.55 61.59 5.20 o 3 2 1 7865.59 7283.40 63.90 o 4 2 1 3378.32 3458.21 34.24 o 5 2 1 617.61 688.43 11.87 o 6 2 1 7495.83 6604.74 54.17 o 7 2 1 2943.38 2913.19 31.31 o 8 2 1 1162.64 1323.52 20.05 o 9 2 1 254.85 198.62 10.01 o 10 2 1 2341.28 2374.41 31.38 o 11 2 1 414.18 316.12 14.25 o 12 2 1 1839.46 1733.91 34.73 o 13 2 1 2933.23 3147.54 44.94 o 14 2 1 3380.81 3265.70 51.97 o 15 2 1 149.85 238.85 18.77 o 16 2 1 186.51 188.93 20.82 o 17 2 1 1747.37 1927.65 52.73 o 18 2 1 218.11 201.31 23.38 o 19 2 1 106.84 102.45 21.64 o -19 3 1 53.05 64.56 19.23 o -18 3 1 390.97 379.14 27.62 o -17 3 1 1826.14 1843.86 48.15 o -16 3 1 0.51 -6.50 13.89 o -15 3 1 751.06 756.52 30.94 o -14 3 1 341.01 361.74 21.25 o -13 3 1 220.27 221.39 17.32 o -12 3 1 37.29 77.09 12.03 o -11 3 1 201.81 121.48 11.36 o -10 3 1 51.14 116.93 11.22 o -9 3 1 1871.11 1832.70 29.87 o -8 3 1 2151.55 1988.29 25.38 o -7 3 1 53.83 53.00 6.03 o -6 3 1 4796.32 5134.05 43.83 o -5 3 1 13224.37 12977.37 95.58 o -4 3 1 263.38 135.49 6.35 o -3 3 1 2827.18 2600.85 25.69 o -2 3 1 678.68 935.01 13.13 o -1 3 1 189.66 146.49 7.17 o 0 3 1 10.89 164.60 6.60 o 1 3 1 3219.31 3083.49 28.03 o 2 3 1 11667.44 14550.44 101.39 o 3 3 1 8345.73 7462.34 53.73 o 4 3 1 1890.69 1208.62 16.04 o 5 3 1 903.15 1006.80 15.04 o 6 3 1 14542.87 17964.69 132.79 o 7 3 1 12.82 10.63 5.27 o 8 3 1 538.33 737.00 16.98 o 9 3 1 684.46 699.60 16.16 o 10 3 1 168.99 183.57 10.95 o 11 3 1 888.07 831.57 26.01 o 12 3 1 283.86 443.49 20.08 o 13 3 1 384.27 319.85 19.42 o 14 3 1 1237.90 1217.46 34.29 o 15 3 1 2110.80 2177.87 46.04 o 16 3 1 32.73 56.93 15.27 o 17 3 1 361.17 299.28 24.70 o 18 3 1 441.11 384.94 27.26 o 19 3 1 729.06 713.68 37.09 o -19 4 1 383.82 361.53 25.89 o -18 4 1 4.84 -18.13 13.72 o -17 4 1 1.96 -3.93 15.26 o -16 4 1 427.39 404.87 38.39 o -15 4 1 973.74 822.42 28.70 o -14 4 1 6171.25 5817.57 75.89 o -13 4 1 519.96 645.49 28.58 o -12 4 1 894.94 982.86 24.95 o -11 4 1 902.03 756.64 23.68 o -10 4 1 119.15 268.20 14.15 o -9 4 1 25.56 75.16 9.49 o -8 4 1 5304.17 4985.44 52.01 o -7 4 1 329.88 294.72 11.43 o -6 4 1 2676.15 3347.74 33.89 o -5 4 1 1842.07 1991.79 22.63 o -4 4 1 1152.53 1247.75 16.77 o -3 4 1 11565.31 12370.39 82.37 o -2 4 1 5008.47 5236.63 38.18 o -1 4 1 224.03 153.34 7.47 o 0 4 1 234.54 274.66 8.78 o 1 4 1 505.96 356.22 8.62 o 2 4 1 2279.42 2647.92 24.77 o 3 4 1 1364.50 1009.35 14.35 o 4 4 1 1486.48 1305.69 17.55 o 5 4 1 3618.15 4716.24 43.12 o 6 4 1 7963.29 6939.13 58.73 o 7 4 1 8472.21 8549.04 70.25 o 8 4 1 14.13 32.07 7.36 o 9 4 1 88.32 133.71 13.21 o 10 4 1 1693.05 1709.01 29.56 o 11 4 1 29.70 44.46 10.39 o 12 4 1 1198.95 968.53 32.78 o 13 4 1 623.79 615.22 26.07 o 14 4 1 2663.65 2886.30 64.49 o 15 4 1 2075.45 1918.02 44.51 o 16 4 1 124.86 110.47 20.01 o 17 4 1 1306.96 1279.26 43.68 o 18 4 1 74.87 78.19 20.07 o -18 5 1 101.46 107.63 19.15 o -17 5 1 1230.72 1275.77 43.69 o -16 5 1 5.91 10.46 13.48 o -15 5 1 247.20 264.02 19.85 o -14 5 1 37.99 24.51 11.90 o -13 5 1 920.94 1081.67 34.79 o -12 5 1 1490.23 1613.42 35.21 o -11 5 1 246.80 199.03 14.64 o -10 5 1 292.28 283.04 15.15 o -9 5 1 258.06 304.81 16.99 o -8 5 1 35.51 26.91 8.30 o -7 5 1 381.78 351.95 14.70 o -6 5 1 0.03 0.41 5.46 o -5 5 1 7939.82 8428.95 65.49 o -4 5 1 1490.39 1325.58 17.92 o -3 5 1 7867.09 7309.76 53.31 o -2 5 1 517.15 558.64 11.65 o -1 5 1 115.40 180.93 7.26 o 0 5 1 13.03 8.98 4.34 o 1 5 1 13404.70 13211.12 84.59 o 2 5 1 908.39 656.48 12.36 o 3 5 1 9969.69 9198.46 66.03 o 4 5 1 9.29 5.47 4.90 o 5 5 1 1096.45 1369.50 20.54 o 6 5 1 3177.76 3974.12 54.36 o 7 5 1 372.63 366.29 14.94 o 8 5 1 20.62 66.76 11.24 o 9 5 1 224.33 281.26 16.70 o 10 5 1 836.78 1070.79 25.62 o 11 5 1 573.66 720.14 28.83 o 12 5 1 1985.22 2145.21 40.68 o 13 5 1 850.49 910.47 28.93 o 14 5 1 56.40 82.57 14.59 o 15 5 1 200.63 138.37 19.45 o 16 5 1 0.06 10.46 13.93 o 17 5 1 57.42 64.12 16.75 o 18 5 1 69.23 98.03 19.57 o -17 6 1 128.16 121.50 19.45 o -16 6 1 770.01 799.13 33.29 o -15 6 1 303.83 273.27 21.44 o -14 6 1 2321.45 2098.03 44.42 o -13 6 1 319.65 232.94 18.15 o -12 6 1 1287.81 1281.92 33.63 o -11 6 1 210.91 190.88 15.57 o -10 6 1 1473.84 1638.16 32.56 o -9 6 1 948.87 780.99 23.15 o -8 6 1 3693.91 3814.04 50.34 o -7 6 1 404.88 382.39 16.51 o -6 6 1 1778.66 1754.94 29.55 o -5 6 1 12.13 2.94 6.54 o -4 6 1 271.89 245.36 10.90 o -3 6 1 21.90 31.22 5.89 o -2 6 1 260.05 372.90 10.70 o -1 6 1 3.67 5.39 4.88 o 0 6 1 19.71 12.03 5.07 o 1 6 1 164.02 170.31 8.32 o 2 6 1 22.63 15.55 5.82 o 3 6 1 30.59 72.06 7.27 o 4 6 1 3016.60 3187.29 37.53 o 5 6 1 64.35 75.81 9.30 o 6 6 1 4454.04 4203.78 52.21 o 7 6 1 6302.67 6991.49 76.92 o 8 6 1 3092.77 3185.04 45.14 o 9 6 1 1253.39 1155.21 27.33 o 10 6 1 291.57 387.62 19.10 o 11 6 1 186.89 219.90 16.69 o 12 6 1 1759.37 1283.47 33.73 o 13 6 1 844.37 738.94 27.91 o 14 6 1 1707.50 1801.51 50.77 o 15 6 1 5.35 -13.62 12.74 o 16 6 1 424.15 413.03 25.17 o -16 7 1 55.28 66.06 18.22 o -15 7 1 3.69 11.92 14.84 o -14 7 1 42.90 79.29 16.12 o -13 7 1 418.65 413.32 25.65 o -12 7 1 125.80 139.24 16.35 o -11 7 1 236.33 266.85 22.74 o -10 7 1 49.75 56.97 12.04 o -9 7 1 67.84 56.43 11.72 o -8 7 1 516.49 627.82 21.53 o -7 7 1 1526.06 1661.26 31.19 o -6 7 1 12.56 -2.94 8.44 o -5 7 1 548.48 679.30 19.23 o -4 7 1 681.88 794.20 19.35 o -3 7 1 869.34 694.59 18.59 o -2 7 1 39.03 24.46 7.57 o -1 7 1 1519.11 1852.84 27.40 o 0 7 1 2530.16 2926.65 35.78 o 1 7 1 1371.93 1287.04 23.97 o 2 7 1 11.78 8.74 7.28 o 3 7 1 3189.44 3146.76 37.53 o 4 7 1 2453.60 2703.53 37.84 o 5 7 1 701.03 825.13 25.58 o 6 7 1 24.51 8.61 8.96 o 7 7 1 33.53 14.70 9.11 o 8 7 1 137.22 182.21 17.30 o 9 7 1 3.54 0.43 10.89 o 10 7 1 68.15 105.24 15.08 o 11 7 1 87.23 94.79 15.30 o 12 7 1 417.82 485.43 32.06 o 13 7 1 93.11 21.72 15.05 o 14 7 1 1.39 22.93 15.42 o 15 7 1 184.68 156.08 20.57 o -14 8 1 355.65 266.22 23.96 o -13 8 1 766.49 704.62 32.25 o -12 8 1 5.42 22.80 14.59 o -11 8 1 887.32 959.57 38.31 o -10 8 1 337.55 384.18 22.59 o -9 8 1 840.47 768.56 28.43 o -8 8 1 1311.68 1103.56 30.61 o -7 8 1 994.59 1230.64 31.35 o -6 8 1 136.32 154.85 14.40 o -5 8 1 81.04 57.93 11.49 o -4 8 1 31.63 48.96 12.53 o -3 8 1 1269.59 1540.51 30.74 o -2 8 1 2424.27 2785.07 42.94 o -1 8 1 33.74 54.19 10.36 o 0 8 1 450.98 366.79 17.61 o 1 8 1 480.04 411.82 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