#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/00/2220067.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220067_Fobs loop_ _publ_author_name 'Feng, Min' 'Zhao, Ming' 'Zhang, Jingze' 'Yang, Zaixin' 'Chen, Hong' _publ_section_title ; 4-Desoxy-4\b-[(5-methoxy-1H-indol-3-yl)oxalylamino]podophyllotoxin methanol solvate ; _journal_coeditor_code BH2197 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2339 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.580 _cell_angle_gamma 90.000 _cell_length_a 12.2280 _cell_length_b 9.8360 _cell_length_c 26.6670 _exptl_crystal_F_000 1360.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file bh2197Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R80713E1 in P2(1) P21' _shelx_refln_list_code 4 _shelx_F_calc_maximum 171.72 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1417.12 2410.08 48.01 o 2 0 0 15284.48 18166.04 132.30 o 3 0 0 52.23 40.57 2.28 o 4 0 0 909.49 829.53 21.79 o 5 0 0 209.26 237.66 5.55 o 6 0 0 15.57 20.88 6.25 o 7 0 0 1480.22 1429.90 28.99 o 8 0 0 576.03 516.66 21.54 o 9 0 0 291.22 246.55 11.87 o 10 0 0 186.69 223.71 15.08 o 11 0 0 333.20 341.09 22.86 o 12 0 0 18.74 24.79 7.58 o 13 0 0 258.44 245.65 23.58 o 14 0 0 117.89 131.55 33.91 o 15 0 0 28.59 19.34 14.96 o 1 1 0 14212.08 15655.97 83.53 o 2 1 0 5695.59 6477.35 30.61 o 3 1 0 7894.36 7949.00 33.41 o 4 1 0 843.12 749.69 12.63 o 5 1 0 990.62 931.96 14.84 o 6 1 0 3784.29 3903.06 75.53 o 7 1 0 1364.42 1247.97 22.67 o 8 1 0 340.11 275.24 12.40 o 9 1 0 288.13 289.82 8.44 o 10 1 0 554.52 609.31 24.16 o 11 1 0 11.34 11.37 3.83 o 12 1 0 345.69 355.33 17.22 o 13 1 0 160.35 154.32 26.92 o 14 1 0 163.41 172.27 29.59 o 15 1 0 58.67 65.40 21.15 o 0 2 0 6211.51 4865.23 43.11 o 1 2 0 3032.79 1998.08 48.75 o 2 2 0 722.96 607.87 9.07 o 3 2 0 489.68 522.23 8.47 o 4 2 0 4855.02 4562.06 74.05 o 5 2 0 698.01 639.95 18.69 o 6 2 0 388.19 436.29 8.85 o 7 2 0 1075.88 1083.97 22.26 o 8 2 0 52.89 73.74 10.58 o 9 2 0 73.17 74.76 14.17 o 10 2 0 43.19 55.48 8.85 o 11 2 0 505.36 549.23 20.61 o 12 2 0 243.77 232.69 36.07 o 13 2 0 4.38 3.90 6.39 o 14 2 0 100.29 85.47 14.01 o 15 2 0 126.83 127.64 24.79 o 1 3 0 9547.72 9108.69 53.63 o 2 3 0 10347.28 9528.30 220.80 o 3 3 0 1524.75 1709.78 50.09 o 4 3 0 591.81 628.83 10.76 o 5 3 0 424.12 393.26 14.15 o 6 3 0 147.67 159.71 10.19 o 7 3 0 5.13 11.41 3.82 o 8 3 0 944.05 1037.67 29.02 o 9 3 0 86.36 100.68 16.67 o 10 3 0 18.23 29.40 8.31 o 11 3 0 22.14 37.17 8.77 o 12 3 0 252.74 251.22 29.51 o 13 3 0 234.83 212.94 34.74 o 14 3 0 107.76 107.05 20.23 o 15 3 0 47.09 47.61 12.04 o 0 4 0 299.94 318.25 11.54 o 1 4 0 2279.19 2274.16 27.89 o 2 4 0 5334.85 5563.42 52.51 o 3 4 0 3498.97 3812.89 59.99 o 4 4 0 317.65 336.67 6.94 o 5 4 0 1459.08 1580.10 39.81 o 6 4 0 824.97 828.83 20.35 o 7 4 0 57.71 79.40 8.12 o 8 4 0 15.46 27.00 6.17 o 9 4 0 299.81 343.08 13.12 o 10 4 0 23.06 12.88 9.14 o 11 4 0 642.38 663.92 31.16 o 12 4 0 47.53 65.46 17.47 o 13 4 0 96.16 86.47 19.56 o 14 4 0 59.54 45.05 10.80 o 15 4 0 10.78 18.30 11.45 o 1 5 0 1142.63 1267.80 17.02 o 2 5 0 1572.80 1715.80 23.42 o 3 5 0 538.98 547.13 16.87 o 4 5 0 135.93 122.52 14.72 o 5 5 0 1163.57 1299.06 29.68 o 6 5 0 546.36 552.37 14.17 o 7 5 0 962.09 1035.87 27.92 o 8 5 0 722.87 691.34 18.95 o 9 5 0 106.10 100.40 17.09 o 10 5 0 116.89 128.72 30.00 o 11 5 0 51.67 39.52 13.06 o 12 5 0 48.22 16.47 10.35 o 13 5 0 16.46 11.03 9.59 o 14 5 0 6.56 6.17 9.86 o 0 6 0 1736.52 1947.72 39.58 o 1 6 0 1429.91 1488.56 22.63 o 2 6 0 1804.48 1834.31 31.26 o 3 6 0 1036.51 1078.09 20.49 o 4 6 0 1650.03 1848.57 32.08 o 5 6 0 212.84 209.59 8.55 o 6 6 0 711.68 712.57 24.39 o 7 6 0 395.87 463.68 27.91 o 8 6 0 379.47 394.29 17.25 o 9 6 0 357.70 367.48 13.49 o 10 6 0 153.25 147.81 35.19 o 11 6 0 248.43 248.52 19.45 o 12 6 0 9.88 9.24 18.41 o 13 6 0 85.48 78.47 26.39 o 1 7 0 188.37 179.39 5.24 o 2 7 0 288.50 270.26 9.06 o 3 7 0 167.43 172.81 6.94 o 4 7 0 427.52 397.96 12.29 o 5 7 0 62.79 55.34 10.79 o 6 7 0 2044.99 2118.46 52.12 o 7 7 0 490.99 475.84 21.12 o 8 7 0 649.42 637.74 18.70 o 9 7 0 249.83 290.08 15.34 o 10 7 0 53.00 56.49 15.22 o 11 7 0 90.26 90.34 23.84 o 12 7 0 179.02 195.87 57.04 o 13 7 0 36.15 33.85 16.00 o 0 8 0 1378.36 1347.79 34.06 o 1 8 0 153.37 174.60 5.95 o 2 8 0 213.22 213.19 7.31 o 3 8 0 39.18 41.83 6.77 o 4 8 0 273.74 282.86 16.94 o 5 8 0 26.44 31.45 10.36 o 6 8 0 604.38 565.48 24.33 o 7 8 0 36.46 39.82 9.48 o 8 8 0 71.99 72.56 20.50 o 9 8 0 8.66 4.95 7.72 o 10 8 0 60.18 64.97 16.79 o 11 8 0 166.62 187.16 37.94 o 12 8 0 4.17 14.21 7.77 o 1 9 0 918.07 960.37 23.18 o 2 9 0 113.66 91.32 20.75 o 3 9 0 333.40 302.75 9.83 o 4 9 0 142.02 138.55 12.30 o 5 9 0 529.59 577.62 19.05 o 6 9 0 123.92 88.81 19.77 o 7 9 0 259.82 292.78 34.47 o 8 9 0 511.77 495.10 19.78 o 9 9 0 56.54 42.47 13.50 o 10 9 0 437.66 503.91 27.04 o 11 9 0 191.36 261.43 56.94 o 0 10 0 592.79 674.48 32.56 o 1 10 0 128.50 126.21 39.04 o 2 10 0 83.67 69.93 20.33 o 3 10 0 453.98 480.61 17.03 o 4 10 0 491.31 542.05 30.31 o 5 10 0 139.40 152.71 18.61 o 6 10 0 223.53 232.51 14.34 o 7 10 0 149.26 127.66 23.34 o 8 10 0 299.90 318.02 16.85 o 9 10 0 179.86 153.35 47.05 o 1 11 0 146.51 121.99 37.51 o 2 11 0 103.28 81.76 22.73 o 3 11 0 47.68 31.47 12.45 o 4 11 0 28.92 20.23 9.13 o 5 11 0 36.41 43.58 12.59 o 6 11 0 31.88 27.18 10.12 o 7 11 0 103.36 93.99 22.90 o 8 11 0 17.66 20.20 14.68 o 0 12 0 231.03 257.71 52.99 o 1 12 0 14.57 15.86 7.69 o 2 12 0 115.11 92.21 29.92 o 3 12 0 52.83 40.77 14.97 o 4 12 0 24.22 38.97 16.46 o 5 12 0 54.51 66.81 39.28 o -15 0 1 183.22 225.07 56.23 o -14 0 1 52.82 42.60 10.91 o -13 0 1 64.25 50.76 14.69 o -12 0 1 312.82 376.65 18.14 o -11 0 1 715.06 698.86 46.84 o -10 0 1 5.50 4.29 6.95 o -9 0 1 118.21 115.60 24.08 o -8 0 1 65.53 52.80 16.52 o -7 0 1 7141.18 7357.22 130.87 o -6 0 1 2212.01 2588.70 54.63 o -5 0 1 25.93 14.02 5.07 o -4 0 1 2708.36 2427.08 40.95 o -2 0 1 12611.84 11819.75 52.42 o 1 0 1 14101.26 2106.62 60.82 o 2 0 1 2808.48 3922.54 52.78 o 4 0 1 205.27 143.60 13.90 o 5 0 1 221.86 300.02 16.41 o 6 0 1 7309.32 8383.04 88.49 o 7 0 1 3.37 5.54 2.93 o 8 0 1 1415.82 1387.52 23.56 o 9 0 1 673.63 685.53 33.96 o 10 0 1 1509.90 1680.39 45.09 o 11 0 1 569.18 529.09 23.08 o 12 0 1 936.93 957.14 34.47 o 13 0 1 153.24 157.71 24.25 o 14 0 1 111.35 117.89 23.90 o 15 0 1 17.65 26.47 13.49 o -15 1 1 124.95 106.61 21.43 o -14 1 1 268.63 277.94 15.50 o -13 1 1 252.94 257.01 15.91 o -12 1 1 372.42 375.13 28.66 o -11 1 1 218.01 251.08 21.57 o -10 1 1 20.72 31.28 6.25 o -9 1 1 1175.01 1337.94 36.42 o -8 1 1 1692.49 1860.40 32.39 o -7 1 1 4928.49 5337.47 123.91 o -6 1 1 3867.55 4157.60 95.40 o -5 1 1 23.19 35.15 4.11 o -4 1 1 3766.97 3461.90 44.74 o -3 1 1 607.57 513.33 12.07 o -2 1 1 770.96 788.73 12.80 o -1 1 1 15520.04 15755.64 118.32 o 0 1 1 4240.63 2503.98 22.41 o 1 1 1 645.32 224.91 3.45 o 2 1 1 3612.58 3806.22 44.66 o 4 1 1 1104.95 1068.31 26.44 o 5 1 1 1620.28 1581.47 23.20 o 6 1 1 1536.87 1613.90 16.72 o 7 1 1 281.36 243.77 5.10 o 8 1 1 255.32 307.73 7.94 o 9 1 1 93.42 122.34 7.44 o 10 1 1 80.20 101.78 13.87 o 11 1 1 92.34 117.02 15.01 o 12 1 1 377.82 411.89 13.37 o 13 1 1 198.43 191.04 31.36 o 14 1 1 260.01 215.16 41.16 o 15 1 1 15.58 21.28 7.04 o -15 2 1 112.71 88.66 34.48 o -14 2 1 4.45 3.44 5.78 o -13 2 1 137.79 131.63 23.94 o -12 2 1 36.70 38.11 8.54 o -11 2 1 174.17 172.07 22.52 o -10 2 1 30.17 14.69 6.37 o -9 2 1 78.15 92.13 18.13 o -8 2 1 70.73 60.92 9.40 o -7 2 1 461.69 476.05 17.33 o -6 2 1 126.75 106.88 6.16 o -5 2 1 3042.81 3403.24 101.64 o -4 2 1 772.29 773.84 20.04 o -3 2 1 1145.33 1096.81 17.63 o -2 2 1 3910.42 3993.72 59.02 o -1 2 1 3673.88 2985.69 37.12 o 0 2 1 14296.37 15679.47 82.60 o 1 2 1 4592.25 5767.00 94.17 o 2 2 1 8184.48 8978.77 54.79 o 3 2 1 1972.82 1756.81 13.99 o 4 2 1 3133.82 2906.08 41.85 o 5 2 1 1940.84 2105.48 31.56 o 6 2 1 1910.22 1945.14 35.31 o 7 2 1 1853.25 1962.24 34.86 o 8 2 1 1030.12 1145.24 19.03 o 9 2 1 195.79 219.15 7.89 o 10 2 1 971.16 1016.41 24.03 o 11 2 1 503.02 482.74 27.95 o 12 2 1 69.75 98.33 17.31 o 13 2 1 52.00 57.30 18.99 o 14 2 1 23.37 17.64 5.25 o 15 2 1 82.35 90.02 16.07 o -15 3 1 121.67 101.35 29.43 o -14 3 1 76.89 83.34 16.31 o -13 3 1 65.89 70.60 12.01 o -12 3 1 127.76 147.82 25.48 o -11 3 1 880.12 878.43 42.16 o -10 3 1 250.02 241.12 15.72 o -9 3 1 47.81 31.77 9.57 o -8 3 1 446.40 504.97 19.30 o -7 3 1 697.76 705.19 37.02 o -6 3 1 380.73 345.08 7.94 o -5 3 1 2171.07 2178.71 38.51 o -4 3 1 947.85 1009.32 26.87 o -3 3 1 220.55 233.09 4.83 o -2 3 1 914.99 1057.40 13.56 o -1 3 1 4274.21 4767.59 41.04 o 0 3 1 3813.63 3937.83 103.17 o 1 3 1 4720.65 3707.22 56.68 o 2 3 1 1027.34 861.70 16.80 o 3 3 1 309.86 357.01 10.86 o 4 3 1 867.52 931.79 15.04 o 5 3 1 62.57 86.55 10.04 o 6 3 1 245.30 249.03 10.21 o 7 3 1 0.99 2.71 3.39 o 8 3 1 1141.71 1106.16 41.66 o 9 3 1 563.32 593.52 16.77 o 10 3 1 128.71 107.27 13.29 o 11 3 1 1094.30 1108.10 31.87 o 12 3 1 40.43 42.36 12.58 o 13 3 1 47.25 48.96 12.01 o 14 3 1 37.59 53.70 12.10 o 15 3 1 5.45 7.21 5.76 o -15 4 1 49.76 52.64 17.80 o -14 4 1 21.52 23.69 7.89 o -13 4 1 17.48 19.80 6.96 o -12 4 1 140.28 129.97 28.01 o -11 4 1 69.80 59.03 14.33 o -10 4 1 84.42 81.41 22.03 o -9 4 1 172.52 155.56 16.62 o -8 4 1 679.74 707.57 21.04 o -7 4 1 187.21 214.51 6.79 o -6 4 1 556.68 464.38 12.71 o -5 4 1 348.15 359.68 6.92 o -4 4 1 1700.83 1627.49 24.53 o -3 4 1 5359.78 5417.26 91.13 o -2 4 1 76.18 83.52 2.60 o -1 4 1 631.85 622.83 10.09 o 0 4 1 177.45 182.80 3.41 o 1 4 1 322.16 409.34 9.90 o 2 4 1 1044.52 894.03 14.38 o 3 4 1 550.43 579.60 10.67 o 4 4 1 426.20 396.29 8.43 o 5 4 1 1989.30 2220.64 20.12 o 6 4 1 387.96 391.24 13.07 o 7 4 1 821.28 791.99 16.15 o 8 4 1 179.00 149.81 10.80 o 9 4 1 1.24 9.07 4.06 o 10 4 1 801.46 775.03 17.04 o 11 4 1 574.99 646.80 43.77 o 12 4 1 36.38 33.83 13.40 o 13 4 1 35.63 35.24 14.45 o 14 4 1 21.44 25.54 9.34 o -14 5 1 116.81 114.01 24.66 o -13 5 1 30.20 28.11 9.80 o -12 5 1 42.24 23.56 13.83 o -11 5 1 59.87 58.40 16.52 o -10 5 1 32.88 50.28 16.60 o -9 5 1 252.14 216.57 15.43 o -8 5 1 408.98 381.53 8.68 o -7 5 1 1194.42 1168.34 27.50 o -6 5 1 162.94 159.83 9.70 o -5 5 1 15.47 12.53 1.56 o -4 5 1 441.50 434.88 8.65 o -3 5 1 2547.26 2431.62 25.66 o -2 5 1 790.74 740.75 14.84 o -1 5 1 1086.15 1079.13 12.63 o 0 5 1 438.36 507.71 6.75 o 1 5 1 740.95 804.58 15.25 o 2 5 1 564.52 568.53 10.45 o 3 5 1 3561.54 3827.38 96.91 o 4 5 1 577.43 558.71 19.31 o 5 5 1 830.24 892.84 20.37 o 6 5 1 470.35 480.15 14.19 o 7 5 1 41.67 51.92 8.07 o 8 5 1 1140.12 1120.86 42.20 o 9 5 1 142.64 124.08 20.99 o 10 5 1 307.93 313.60 16.66 o 11 5 1 319.71 292.23 20.63 o 12 5 1 33.66 16.47 10.18 o 13 5 1 7.22 12.74 11.54 o 14 5 1 45.17 38.97 16.96 o -13 6 1 68.35 52.11 18.48 o -12 6 1 68.81 64.06 31.77 o -11 6 1 143.13 150.58 32.86 o -10 6 1 247.75 282.42 15.74 o -9 6 1 808.40 753.91 28.78 o -8 6 1 214.80 245.30 44.15 o -7 6 1 650.13 647.04 19.93 o -6 6 1 1213.35 1176.69 28.91 o -5 6 1 823.02 945.53 22.15 o -4 6 1 478.13 474.66 17.18 o -3 6 1 1434.87 1413.15 16.60 o -2 6 1 248.88 212.43 12.64 o -1 6 1 1280.20 1338.26 20.95 o 0 6 1 734.53 863.47 31.88 o 1 6 1 322.95 306.86 8.72 o 2 6 1 42.29 46.86 3.17 o 3 6 1 1051.14 1036.17 18.60 o 4 6 1 28.54 25.94 7.83 o 5 6 1 171.04 154.91 11.91 o 6 6 1 12.22 12.47 5.53 o 7 6 1 2380.64 2477.11 73.59 o 8 6 1 145.89 176.44 16.52 o 9 6 1 3.10 6.84 6.69 o 10 6 1 190.58 163.94 21.49 o 11 6 1 42.19 49.09 23.64 o 12 6 1 6.99 6.44 8.87 o 13 6 1 25.69 19.07 10.52 o -13 7 1 67.69 58.47 20.62 o -12 7 1 47.18 62.20 27.06 o -11 7 1 48.76 45.73 14.20 o -10 7 1 28.77 23.29 6.24 o -9 7 1 1359.69 1430.05 42.64 o -8 7 1 33.29 33.12 11.07 o -7 7 1 95.04 102.53 29.07 o -6 7 1 252.79 297.81 21.96 o -5 7 1 702.39 749.81 35.96 o -4 7 1 1609.16 1720.85 45.99 o -3 7 1 187.19 193.38 4.84 o -2 7 1 240.98 238.74 4.82 o -1 7 1 644.51 686.79 12.98 o 0 7 1 310.71 318.71 7.09 o 1 7 1 310.57 321.19 7.90 o 2 7 1 221.70 234.92 9.76 o 3 7 1 558.31 611.67 21.11 o 4 7 1 926.15 929.39 21.56 o 5 7 1 74.69 72.97 11.54 o 6 7 1 621.03 636.18 27.84 o 7 7 1 41.69 32.48 7.14 o 8 7 1 3.55 -4.92 8.18 o 9 7 1 411.43 391.09 15.88 o 10 7 1 8.77 8.84 8.82 o 11 7 1 97.24 100.95 30.38 o 12 7 1 136.76 135.13 33.82 o 13 7 1 121.65 93.08 38.28 o -12 8 1 70.07 54.61 30.59 o -11 8 1 115.86 113.72 37.36 o -10 8 1 58.72 73.47 39.51 o -9 8 1 39.42 26.65 7.94 o -8 8 1 39.83 59.23 15.32 o -7 8 1 80.68 78.96 20.11 o -6 8 1 1338.96 1334.71 42.87 o -5 8 1 605.50 659.89 20.83 o -4 8 1 50.57 34.94 9.30 o -3 8 1 348.95 364.60 13.65 o -2 8 1 622.11 658.22 16.68 o -1 8 1 367.92 359.19 7.73 o 0 8 1 183.00 206.92 6.18 o 1 8 1 875.12 867.90 16.53 o 2 8 1 342.15 332.24 10.31 o 3 8 1 1423.23 1408.32 30.81 o 4 8 1 2130.24 2177.80 62.60 o 5 8 1 323.59 295.99 16.09 o 6 8 1 929.42 903.43 41.27 o 7 8 1 290.14 312.35 13.73 o 8 8 1 26.55 35.95 10.56 o 9 8 1 122.42 127.58 28.98 o 10 8 1 10.58 16.10 10.12 o 11 8 1 15.40 9.78 17.99 o 12 8 1 51.55 62.65 21.55 o -11 9 1 3.62 2.23 15.20 o -10 9 1 57.83 55.17 25.42 o -9 9 1 15.13 15.22 15.52 o -8 9 1 73.09 80.47 21.95 o -7 9 1 616.70 645.34 19.73 o -6 9 1 24.34 25.48 10.38 o -5 9 1 0.21 6.20 6.89 o -4 9 1 60.73 44.30 15.01 o -3 9 1 1425.60 1547.02 41.05 o -2 9 1 3.86 5.10 5.79 o -1 9 1 438.94 426.25 14.83 o 0 9 1 149.43 151.23 8.68 o 1 9 1 2142.02 2259.93 47.44 o 2 9 1 324.20 333.84 10.02 o 3 9 1 403.24 362.21 11.84 o 4 9 1 1498.47 1564.01 40.32 o 5 9 1 19.08 15.17 6.26 o 6 9 1 49.24 40.76 8.53 o 7 9 1 185.62 178.59 40.79 o 8 9 1 101.58 62.60 21.48 o 9 9 1 18.07 20.97 11.31 o 10 9 1 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79.94 21.17 o 7 11 1 177.15 171.30 40.83 o -5 12 1 15.33 9.53 13.13 o -4 12 1 41.07 29.71 22.47 o -3 12 1 114.98 118.75 41.86 o -2 12 1 9.71 10.20 5.46 o -1 12 1 4.31 13.14 5.49 o 0 12 1 3.21 8.64 7.64 o 1 12 1 18.70 12.42 6.85 o 2 12 1 37.05 32.02 13.20 o 3 12 1 104.86 100.98 48.75 o 4 12 1 93.80 108.10 40.74 o 5 12 1 14.88 14.24 15.43 o -15 0 2 48.03 21.54 19.18 o -14 0 2 93.12 93.91 30.96 o -13 0 2 0.06 12.19 11.52 o -12 0 2 183.90 191.56 42.74 o -11 0 2 117.53 114.80 24.70 o -10 0 2 580.13 599.56 22.90 o -9 0 2 157.27 171.30 8.66 o -8 0 2 624.44 602.91 22.37 o -7 0 2 1551.40 1678.26 47.87 o -6 0 2 133.92 105.93 17.54 o -5 0 2 74.63 60.71 15.06 o -4 0 2 4376.24 4297.34 105.03 o -3 0 2 9227.42 9325.90 204.13 o -2 0 2 718.06 490.35 14.91 o -1 0 2 3407.88 1992.21 25.96 o 0 0 2 216.56 14.02 0.82 o 1 0 2 2849.17 3300.22 101.21 o 2 0 2 7169.80 6371.25 112.37 o 3 0 2 12.57 7.65 2.99 o 4 0 2 2518.26 2290.27 47.50 o 5 0 2 848.73 805.86 20.77 o 6 0 2 412.10 473.36 10.42 o 7 0 2 30.34 25.83 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