#------------------------------------------------------------------------------
#$Date: 2016-04-03 03:54:30 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181121 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/00/2220098.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2220098_Fobs
loop_
_publ_author_name
'Panagiotidis, Kosta'
'Glaum, Robert'
_publ_section_title
;
 Ag~2~PdP~2~O~7~
;
_journal_coeditor_code           BR2086
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i84
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_audit_update_record
;
2008-10-29 # Formatted by publCIF
;
_cell_angle_alpha                90.000
_cell_angle_beta                 116.750
_cell_angle_gamma                90.000
_cell_length_a                   15.7390
_cell_length_b                   5.7177
_cell_length_c                   8.1870
_exptl_crystal_F_000             904.00
_reflns_d_resolution_high        0.7130
_cod_data_source_file            br2086Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
' Ag2 O7 P2 Pd1 Mit den Parametern von Na2PdP2O7 (COL= 72751)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            458.75
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 13572.70 15721.85 228.45 o
4 0 0 88369.72 90278.95 1239.48 o
6 0 0 22884.93 23987.10 433.27 o
8 0 0 102448.40 106321.98 1873.56 o
10 0 0 14246.29 14770.43 525.55 o
12 0 0 30512.90 32078.83 795.94 o
14 0 0 442.13 812.50 389.75 o
16 0 0 1423.19 1933.44 476.77 o
18 0 0 10939.05 11269.18 798.40 o
1 1 0 14267.17 14445.96 224.07 o
3 1 0 15585.78 16766.08 768.01 o
5 1 0 35048.10 34685.46 496.12 o
7 1 0 275.68 322.84 316.86 o
9 1 0 39805.68 42175.33 1031.26 o
11 1 0 2318.53 2428.32 604.78 o
13 1 0 27466.85 29116.33 818.54 o
15 1 0 80.36 839.23 604.32 o
17 1 0 11511.77 13098.12 689.95 o
19 1 0 2.86 -650.34 650.34 o
0 2 0 2706.03 2751.36 282.19 o
2 2 0 27341.84 26841.38 422.47 o
4 2 0 27996.02 28573.95 1168.72 o
6 2 0 64984.64 67880.47 2092.83 o
8 2 0 1019.41 747.54 498.90 o
10 2 0 6701.00 6914.73 440.53 o
12 2 0 5496.88 6139.29 476.68 o
14 2 0 11274.13 12017.35 602.28 o
16 2 0 6862.52 7595.17 740.47 o
18 2 0 1955.20 2608.77 647.47 o
1 3 0 6497.62 6307.82 295.43 o
3 3 0 32489.72 33813.91 1697.54 o
5 3 0 757.39 832.40 469.51 o
7 3 0 31318.04 31602.91 2142.69 o
9 3 0 8.60 574.68 332.29 o
11 3 0 30965.44 33741.35 848.31 o
13 3 0 912.08 -754.62 1152.79 o
15 3 0 14452.10 14146.44 722.09 o
17 3 0 1257.65 660.84 1901.45 o
0 4 0 5724.69 6632.62 588.00 o
2 4 0 58457.03 60056.05 915.62 o
4 4 0 506.84 396.68 739.38 o
6 4 0 60253.70 61280.92 1262.60 o
8 4 0 667.60 817.76 398.09 o
10 4 0 12602.98 12183.37 600.55 o
12 4 0 1009.96 411.04 610.33 o
14 4 0 6139.83 7115.78 628.69 o
16 4 0 5999.85 7801.80 701.72 o
1 5 0 5424.69 5307.58 605.33 o
3 5 0 7592.50 7672.14 723.32 o
5 5 0 223.03 -94.82 598.48 o
7 5 0 7589.93 8560.16 529.03 o
9 5 0 1969.79 2048.10 1772.75 o
11 5 0 6066.44 5829.74 598.29 o
13 5 0 537.72 421.34 741.69 o
15 5 0 2925.45 2828.64 696.08 o
0 6 0 30720.22 30250.73 1088.41 o
2 6 0 112.18 569.12 398.28 o
4 6 0 6435.22 6175.67 564.18 o
6 6 0 164.36 838.85 443.86 o
8 6 0 10595.28 9913.45 651.06 o
10 6 0 3127.10 3305.61 647.49 o
12 6 0 5451.83 5481.45 1286.42 o
1 7 0 535.08 -392.20 1607.77 o
3 7 0 1404.26 1330.07 580.29 o
5 7 0 10787.28 12269.27 768.55 o
7 7 0 52.48 -405.55 1320.13 o
9 7 0 4214.97 4861.70 1438.74 o
0 8 0 5506.93 6954.79 1057.32 o
-19 1 1 4520.81 5007.80 692.59 o
-17 1 1 9497.39 9543.03 631.90 o
-15 1 1 2537.90 1150.03 1086.15 o
-13 1 1 11159.77 11429.11 1153.91 o
-11 1 1 39328.20 39501.31 790.81 o
-9 1 1 12156.40 11934.53 445.72 o
-7 1 1 7273.75 7171.70 524.24 o
-5 1 1 62363.39 65792.70 3137.05 o
-3 1 1 30736.39 30835.63 671.04 o
-1 1 1 1952.85 1844.92 170.55 o
1 1 1 9037.02 9124.86 313.88 o
3 1 1 8236.97 7784.48 258.41 o
5 1 1 15161.75 14901.14 376.29 o
7 1 1 11328.50 10818.32 399.24 o
9 1 1 49.60 302.27 310.41 o
11 1 1 8801.76 9466.78 747.18 o
13 1 1 15584.81 15038.14 718.87 o
15 1 1 2175.49 2376.47 501.79 o
17 1 1 2091.19 1932.92 2160.09 o
-18 2 1 1076.52 2587.62 2857.95 o
-16 2 1 2576.73 2583.84 518.46 o
-14 2 1 50.93 -840.69 962.20 o
-12 2 1 1763.98 1413.34 409.37 o
-10 2 1 101.24 44.42 891.82 o
-8 2 1 7863.89 7323.06 382.68 o
-6 2 1 36417.05 34710.04 573.89 o
-4 2 1 45278.44 46898.28 717.28 o
-2 2 1 41170.63 40267.45 579.42 o
0 2 1 92196.97 87973.12 1243.45 o
2 2 1 67657.69 65345.37 924.53 o
4 2 1 40149.57 39953.34 604.51 o
6 2 1 43822.43 42382.06 688.09 o
8 2 1 37790.86 35281.97 1035.06 o
10 2 1 7820.23 7466.45 888.14 o
12 2 1 4963.69 5039.60 910.66 o
14 2 1 4602.58 4313.24 698.99 o
16 2 1 135.64 -915.28 915.28 o
18 2 1 167.37 -856.32 856.32 o
-19 3 1 454.38 -1701.60 2047.79 o
-17 3 1 1331.41 1859.54 585.09 o
-15 3 1 2060.53 1809.21 522.20 o
-13 3 1 3462.98 3923.78 464.20 o
-11 3 1 4670.46 5595.08 461.10 o
-9 3 1 3566.96 3955.53 722.53 o
-7 3 1 4972.96 5672.16 373.82 o
-5 3 1 4595.32 4641.98 640.79 o
-3 3 1 4420.07 5808.91 999.49 o
-1 3 1 2432.15 2771.20 248.80 o
1 3 1 1291.29 1037.74 248.66 o
3 3 1 616.18 1373.40 256.63 o
5 3 1 1247.00 698.19 1573.14 o
7 3 1 1730.33 1937.13 381.63 o
9 3 1 1572.60 1414.94 407.84 o
11 3 1 2870.86 2830.09 451.13 o
13 3 1 1244.66 882.97 1549.38 o
15 3 1 1448.03 1236.13 1027.08 o
17 3 1 1569.29 1637.77 2875.82 o
-16 4 1 457.10 1288.44 2000.86 o
-14 4 1 459.20 727.09 485.39 o
-12 4 1 670.33 246.72 537.06 o
-10 4 1 556.96 212.28 680.68 o
-8 4 1 448.81 705.67 668.93 o
-6 4 1 3960.81 4215.86 414.60 o
-4 4 1 867.26 877.62 416.69 o
-2 4 1 3165.79 4223.16 340.29 o
0 4 1 6162.03 6801.08 782.14 o
2 4 1 8573.45 8968.26 461.89 o
4 4 1 2296.07 2473.48 381.70 o
6 4 1 4432.22 3740.40 460.64 o
8 4 1 2299.61 2546.14 534.26 o
10 4 1 671.66 -66.94 447.21 o
12 4 1 649.97 156.17 633.18 o
14 4 1 1745.71 2299.12 605.77 o
16 4 1 217.53 -557.39 2411.46 o
-15 5 1 1145.34 250.39 1026.99 o
-13 5 1 5449.86 5128.13 652.13 o
-11 5 1 15731.15 16582.67 695.21 o
-9 5 1 6548.18 6767.88 523.44 o
-7 5 1 4860.95 4353.56 477.69 o
-5 5 1 17725.34 17372.38 1439.10 o
-3 5 1 4028.27 4379.58 484.66 o
-1 5 1 46.38 -623.09 700.20 o
1 5 1 1393.94 1428.02 410.83 o
3 5 1 1748.67 2131.06 774.85 o
5 5 1 3368.73 3966.59 440.45 o
7 5 1 1453.31 2166.74 798.23 o
9 5 1 448.89 924.89 627.84 o
11 5 1 5368.22 5985.27 609.56 o
13 5 1 8356.71 9816.07 791.23 o
-12 6 1 205.54 699.47 779.94 o
-10 6 1 192.93 -1373.33 1373.33 o
-8 6 1 218.82 -745.77 1073.59 o
-6 6 1 4980.93 4471.53 599.20 o
-4 6 1 1698.15 2187.73 810.01 o
-2 6 1 3642.83 3757.06 477.50 o
0 6 1 9802.16 9296.70 573.28 o
2 6 1 11930.03 10610.91 595.07 o
4 6 1 3090.70 1775.86 2043.34 o
6 6 1 5945.35 5817.59 581.69 o
8 6 1 3864.63 3158.69 604.72 o
10 6 1 741.53 789.68 591.22 o
12 6 1 308.36 -482.78 915.22 o
-9 7 1 763.45 -317.96 1340.05 o
-7 7 1 577.65 409.70 968.18 o
-5 7 1 87.43 -711.26 1061.95 o
-3 7 1 15.50 -1135.27 1135.27 o
-1 7 1 360.79 -375.97 712.86 o
1 7 1 314.86 -622.57 1261.19 o
3 7 1 162.33 -286.16 1198.94 o
5 7 1 158.80 -1608.21 1660.43 o
7 7 1 32.52 -1240.21 1293.66 o
-20 0 2 10529.29 10419.33 747.26 o
-18 0 2 5.49 -667.48 667.48 o
-16 0 2 25883.74 23624.37 1193.39 o
-14 0 2 116.08 -309.88 1812.97 o
-12 0 2 3806.77 3247.06 401.35 o
-10 0 2 12407.99 12319.22 445.69 o
-8 0 2 3585.63 3425.52 273.94 o
-6 0 2 72271.96 72594.48 1038.73 o
-4 0 2 341.15 791.72 205.41 o
-2 0 2 69867.13 70606.14 1005.26 o
0 0 2 22146.45 21997.73 365.43 o
2 0 2 210452.11 202865.61 2191.96 o
4 0 2 19863.77 20013.31 423.57 o
6 0 2 112703.16 106410.86 4129.61 o
8 0 2 18910.68 17775.47 1045.69 o
10 0 2 36316.39 36270.50 834.98 o
12 0 2 6.67 -1138.20 1138.20 o
14 0 2 22551.38 22806.87 1817.21 o
16 0 2 30.34 363.76 580.81 o
-19 1 2 9265.78 8010.39 714.51 o
-17 1 2 5.33 -1085.42 1085.42 o
-15 1 2 15496.37 14430.41 608.17 o
-13 1 2 1848.09 1779.42 1050.82 o
-11 1 2 59541.45 57850.98 1804.85 o
-9 1 2 795.38 505.82 410.84 o
-7 1 2 79489.49 82855.84 3243.32 o
-5 1 2 2330.64 2810.16 205.78 o
-3 1 2 140032.23 149748.44 1770.21 o
-1 1 2 20386.09 20797.01 345.81 o
1 1 2 34374.13 34376.48 484.56 o
3 1 2 7046.28 6975.26 282.90 o
5 1 2 18205.91 19555.49 472.75 o
7 1 2 20679.86 20867.20 564.53 o
9 1 2 10704.75 11142.82 549.57 o
11 1 2 14268.86 14777.25 677.51 o
13 1 2 64.52 581.96 577.02 o
15 1 2 13871.90 14650.48 723.65 o
17 1 2 346.66 -86.06 1343.65 o
-20 2 2 1546.66 -1101.11 1437.89 o
-18 2 2 2047.47 2220.50 939.18 o
-16 2 2 3425.75 2245.76 1526.77 o
-14 2 2 4947.12 5603.54 593.41 o
-12 2 2 5282.40 5679.79 1034.36 o
-10 2 2 9609.39 9239.71 477.44 o
-8 2 2 7410.60 7019.01 353.11 o
-6 2 2 5564.93 5237.17 296.44 o
-4 2 2 32012.97 31437.75 1153.22 o
-2 2 2 1669.29 1240.00 194.00 o
0 2 2 28572.80 28262.01 1801.81 o
2 2 2 5147.18 5403.64 273.04 o
4 2 2 11803.26 11220.80 690.11 o
6 2 2 5122.79 5412.23 946.47 o
8 2 2 14887.73 15491.71 579.49 o
10 2 2 990.86 776.47 868.57 o
12 2 2 7880.25 6681.94 658.48 o
14 2 2 717.94 1152.64 506.01 o
16 2 2 3987.71 3068.18 654.65 o
-19 3 2 218.11 1212.39 815.55 o
-17 3 2 25112.53 25536.59 897.20 o
-15 3 2 0.84 -721.64 721.64 o
-13 3 2 25642.76 26051.01 797.77 o
-11 3 2 9345.93 8885.14 551.09 o
-9 3 2 60079.18 59852.44 972.32 o
-7 3 2 2006.92 2791.03 309.32 o
-5 3 2 79900.45 78570.28 1128.17 o
-3 3 2 5981.00 5537.91 341.22 o
-1 3 2 38566.27 38281.86 633.24 o
1 3 2 1095.83 1024.97 268.93 o
3 3 2 59113.34 54174.81 835.69 o
5 3 2 12616.08 12332.62 504.21 o
7 3 2 222.55 -265.81 735.02 o
9 3 2 8154.41 8501.87 1399.66 o
11 3 2 1261.21 653.53 558.49 o
13 3 2 22454.02 21016.71 810.76 o
15 3 2 246.67 353.69 588.43 o
-18 4 2 4654.74 4585.52 739.06 o
-16 4 2 160.04 -362.24 1332.12 o
-14 4 2 7836.18 7464.03 589.55 o
-12 4 2 4027.76 3977.47 464.26 o
-10 4 2 9960.53 9671.42 812.01 o
-8 4 2 4071.46 5020.71 628.58 o
-6 4 2 667.78 415.73 435.25 o
-4 4 2 34164.52 33228.59 1300.52 o
-2 4 2 70.96 -617.12 617.12 o
0 4 2 60724.46 58373.37 1114.97 o
2 4 2 7168.74 6790.14 455.44 o
4 4 2 25374.60 25373.16 715.73 o
6 4 2 1958.14 2452.94 446.16 o
8 4 2 40532.40 39542.34 857.47 o
10 4 2 486.44 864.73 1103.14 o
12 4 2 11409.72 11508.10 703.51 o
14 4 2 590.32 -420.50 836.42 o
-15 5 2 410.06 -1446.94 1446.94 o
-13 5 2 7661.69 8267.29 864.03 o
-11 5 2 2361.76 2265.40 497.30 o
-9 5 2 9111.32 8700.59 835.16 o
-7 5 2 1107.64 478.05 997.71 o
-5 5 2 7838.51 7274.14 553.00 o
-3 5 2 3797.55 3927.03 464.29 o
-1 5 2 15467.40 14821.84 789.87 o
1 5 2 2363.48 2297.37 451.09 o
3 5 2 4656.91 4844.92 628.61 o
5 5 2 5194.09 5254.00 490.02 o
7 5 2 2950.23 3601.88 514.02 o
9 5 2 8615.95 8647.74 656.22 o
11 5 2 595.35 787.62 868.44 o
13 5 2 3379.90 -768.76 1660.10 o
-14 6 2 1341.87 -548.44 947.93 o
-12 6 2 171.43 -1086.36 1334.72 o
-10 6 2 1982.73 1883.93 537.85 o
-8 6 2 2098.09 2527.94 522.43 o
-6 6 2 11179.95 10511.76 1129.67 o
-4 6 2 598.59 734.40 856.72 o
-2 6 2 3296.18 3589.91 863.20 o
0 6 2 79.30 -217.73 1061.19 o
2 6 2 16061.23 16699.52 1219.47 o
4 6 2 390.67 102.70 1132.44 o
6 6 2 9926.06 9791.73 652.84 o
8 6 2 773.37 691.45 595.95 o
10 6 2 4541.04 4992.42 725.84 o
-9 7 2 978.13 578.58 1167.79 o
-7 7 2 9369.86 10048.65 759.14 o
-5 7 2 548.39 139.13 759.20 o
-3 7 2 14837.26 13914.48 1036.17 o
-1 7 2 421.81 -633.51 1304.72 o
1 7 2 4602.21 5352.17 1344.98 o
3 7 2 148.41 490.53 752.45 o
5 7 2 1920.65 2077.49 1537.82 o
7 7 2 3716.81 3986.04 730.74 o
-21 1 3 94.16 -357.14 1595.86 o
-19 1 3 443.91 718.56 593.27 o
-17 1 3 2809.29 3614.49 480.73 o
-15 1 3 6111.98 5710.06 494.08 o
-13 1 3 7788.18 8727.26 498.88 o
-11 1 3 19185.39 18200.85 921.81 o
-9 1 3 25686.92 25767.36 578.75 o
-7 1 3 37459.29 38191.45 2499.65 o
-5 1 3 36518.40 38970.82 1462.66 o
-3 1 3 33107.96 32466.63 1629.81 o
-1 1 3 25737.69 26515.03 733.21 o
1 1 3 23735.57 24160.62 449.17 o
3 1 3 9455.25 8981.98 350.03 o
5 1 3 2500.81 2855.25 446.34 o
7 1 3 80.34 -565.57 629.95 o
9 1 3 41.34 -332.95 521.50 o
11 1 3 447.26 677.84 516.36 o
13 1 3 1959.94 2247.29 510.07 o
15 1 3 1295.01 363.28 1255.91 o
-20 2 3 4640.38 4313.14 700.92 o
-18 2 3 1049.73 606.71 2535.19 o
-16 2 3 11193.64 10292.52 694.34 o
-14 2 3 11193.17 10204.09 644.76 o
-12 2 3 8.12 395.57 373.10 o
-10 2 3 1443.03 1499.62 340.37 o
-8 2 3 10907.45 10202.64 420.38 o
-6 2 3 4862.02 4500.95 311.78 o
-4 2 3 23943.73 24251.39 486.93 o
-2 2 3 1488.57 1665.35 225.53 o
0 2 3 20874.11 19308.80 467.40 o
2 2 3 71077.77 71135.84 988.11 o
4 2 3 20991.08 21976.86 589.69 o
6 2 3 10253.97 10165.28 474.39 o
8 2 3 37476.27 35663.10 1928.42 o
10 2 3 19541.98 19331.81 658.81 o
12 2 3 3174.78 2201.63 1444.42 o
14 2 3 7135.50 7204.01 673.02 o
-19 3 3 3.70 182.88 1173.40 o
-17 3 3 485.40 -394.62 710.53 o
-15 3 3 1337.94 1729.55 598.64 o
-13 3 3 261.37 -925.18 925.18 o
-11 3 3 7917.86 7518.71 776.37 o
-9 3 3 8020.81 7932.52 864.85 o
-7 3 3 3902.77 3663.36 361.39 o
-5 3 3 3746.75 3645.98 470.08 o
-3 3 3 15568.89 16192.83 480.14 o
-1 3 3 2053.48 1884.27 306.92 o
1 3 3 2276.25 2149.08 334.42 o
3 3 3 4101.18 3851.08 416.61 o
5 3 3 1323.09 1119.38 1162.17 o
7 3 3 1018.41 653.54 1167.89 o
9 3 3 24.10 -302.74 1443.30 o
11 3 3 189.13 -628.12 628.12 o
13 3 3 1061.60 -85.19 609.95 o
-18 4 3 102.96 4.81 1351.13 o
-16 4 3 1957.27 2041.61 539.88 o
-14 4 3 2225.89 1808.06 523.02 o
-12 4 3 1184.87 2123.85 385.34 o
-10 4 3 6.06 150.68 528.95 o
-8 4 3 2105.75 2365.73 419.22 o
-6 4 3 2937.32 3294.48 628.38 o
-4 4 3 4974.13 5566.37 415.57 o
-2 4 3 1279.66 2024.99 1203.27 o
0 4 3 220.35 993.21 1026.80 o
2 4 3 11073.51 9862.23 853.74 o
4 4 3 1030.09 315.87 686.65 o
6 4 3 166.35 -1496.16 1496.16 o
8 4 3 6581.83 7179.79 540.24 o
10 4 3 2866.45 3209.00 544.98 o
12 4 3 39.26 255.53 743.18 o
-17 5 3 5362.04 5463.02 770.39 o
-15 5 3 2426.80 1729.84 1626.06 o
-13 5 3 2243.15 1447.98 1115.34 o
-11 5 3 7292.68 6674.54 822.91 o
-9 5 3 17012.29 16755.32 654.26 o
-7 5 3 4301.61 4618.83 558.04 o
-5 5 3 16635.63 16082.84 582.88 o
-3 5 3 20858.81 21246.60 730.40 o
-1 5 3 8215.33 7865.18 572.25 o
1 5 3 1264.62 474.86 528.43 o
3 5 3 8389.01 8026.40 561.30 o
5 5 3 826.83 430.90 610.30 o
7 5 3 28.56 96.51 606.96 o
9 5 3 111.68 -266.98 684.85 o
11 5 3 147.96 584.83 634.07 o
-14 6 3 2299.28 2215.69 1056.59 o
-12 6 3 1105.76 522.45 775.14 o
-10 6 3 228.84 33.21 1020.92 o
-8 6 3 2.58 -201.75 655.71 o
-6 6 3 120.99 -722.77 1100.20 o
-4 6 3 727.80 1227.76 504.66 o
-2 6 3 1230.50 304.19 605.26 o
0 6 3 2178.52 1211.96 1103.61 o
2 6 3 3590.95 4242.42 2953.74 o
4 6 3 4653.33 5390.11 584.50 o
6 6 3 5598.39 6190.04 660.75 o
8 6 3 4215.21 4957.69 1403.53 o
-9 7 3 39.99 304.30 617.10 o
-7 7 3 6.67 919.39 1079.53 o
-5 7 3 511.84 -672.58 950.57 o
-3 7 3 15.97 -100.44 718.69 o
-1 7 3 336.06 -573.26 1364.98 o
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