#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220112.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220112_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Jebas, Samuel Robinson' 'Girish, K. S.' 'Kalluraya, B.' _publ_section_title ; 4-[(4-Chlorophenyl)(5-hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)methyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ; _journal_coeditor_code CI2705 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2301 _journal_page_last o2302 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.994 _cell_angle_gamma 90.000 _cell_length_a 10.8809 _cell_length_b 11.2046 _cell_length_c 18.9376 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7072 _[local]_cod_data_source_file ci2705Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ksg2_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 220.20 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14353.00 15465.20 311.94 o 2 0 0 878.58 895.20 22.53 o 3 0 0 5077.39 4884.59 85.33 o 4 0 0 212.32 226.39 16.80 o 5 0 0 136.58 106.33 15.41 o 6 0 0 6317.54 6615.86 194.95 o 7 0 0 251.45 279.07 30.47 o 8 0 0 6383.76 6169.29 128.88 o 9 0 0 3300.19 3272.33 89.25 o 10 0 0 57.02 41.81 32.50 o 11 0 0 494.36 534.14 62.72 o 12 0 0 1.62 30.32 30.92 o 13 0 0 40.86 34.87 36.16 o 14 0 0 57.13 37.55 39.72 o 15 0 0 351.93 356.46 73.31 o 1 1 0 4921.66 4949.33 64.36 o 2 1 0 11.07 10.95 6.09 o 3 1 0 81.75 99.83 8.61 o 4 1 0 201.82 220.18 11.46 o 5 1 0 1185.91 1175.12 26.49 o 6 1 0 39.58 53.64 9.97 o 7 1 0 175.04 162.40 15.32 o 8 1 0 380.10 380.10 35.67 o 9 1 0 2271.36 2215.05 49.96 o 10 1 0 228.96 233.06 24.93 o 11 1 0 195.12 207.07 25.43 o 12 1 0 175.88 241.29 36.26 o 13 1 0 219.96 229.63 37.64 o 14 1 0 51.72 101.72 32.83 o 15 1 0 177.25 149.28 38.44 o 1 2 0 4758.62 4944.88 51.97 o 2 2 0 34745.38 36183.29 374.93 o 3 2 0 713.55 845.54 20.00 o 4 2 0 12125.80 12834.58 144.37 o 5 2 0 53.90 40.50 12.63 o 6 2 0 544.79 467.87 24.23 o 7 2 0 122.13 92.51 13.64 o 8 2 0 1.41 -9.01 9.01 o 9 2 0 232.45 252.23 25.32 o 10 2 0 54.48 71.37 18.86 o 11 2 0 158.65 145.82 30.67 o 12 2 0 27.11 63.40 24.72 o 13 2 0 563.78 590.86 53.02 o 14 2 0 47.43 57.79 29.51 o 15 2 0 37.13 17.18 26.18 o 1 3 0 13910.59 13885.60 135.90 o 2 3 0 10139.71 10213.73 86.59 o 3 3 0 201.87 222.53 9.51 o 4 3 0 170.87 141.49 11.10 o 5 3 0 69.19 67.25 8.90 o 6 3 0 15.25 4.84 7.68 o 7 3 0 474.60 459.56 20.70 o 8 3 0 1.95 -12.07 12.07 o 9 3 0 445.06 356.43 28.16 o 10 3 0 7.65 3.61 14.58 o 11 3 0 221.97 215.14 27.65 o 12 3 0 28.69 29.45 31.00 o 13 3 0 3.22 14.19 20.19 o 14 3 0 68.76 102.30 31.08 o 0 4 0 6562.71 6203.27 291.09 o 1 4 0 284.81 301.59 13.42 o 2 4 0 26.73 29.57 5.47 o 3 4 0 989.92 999.35 19.38 o 4 4 0 1397.14 1522.31 25.05 o 5 4 0 2241.59 2340.37 68.74 o 6 4 0 618.27 653.65 25.60 o 7 4 0 163.76 124.32 17.96 o 8 4 0 1291.42 1187.61 43.87 o 9 4 0 8.76 52.26 16.93 o 10 4 0 108.30 89.31 24.79 o 11 4 0 123.46 132.59 23.90 o 12 4 0 282.37 289.13 32.38 o 13 4 0 25.18 25.56 20.86 o 14 4 0 13.09 -5.86 23.14 o 1 5 0 262.60 260.64 16.74 o 2 5 0 451.94 482.84 12.85 o 3 5 0 258.78 241.43 9.66 o 4 5 0 203.80 210.91 12.26 o 5 5 0 85.62 84.46 10.28 o 6 5 0 44.38 35.19 11.81 o 7 5 0 49.20 44.65 14.23 o 8 5 0 2.72 -3.84 12.87 o 9 5 0 785.99 743.08 39.69 o 10 5 0 0.74 -7.77 13.37 o 11 5 0 113.12 95.43 22.36 o 12 5 0 54.20 71.13 22.30 o 13 5 0 569.55 664.99 49.11 o 14 5 0 12.30 12.51 23.95 o 0 6 0 2616.47 2445.78 61.66 o 1 6 0 47.98 52.94 7.28 o 2 6 0 4145.93 4360.81 52.50 o 3 6 0 517.55 525.75 14.44 o 4 6 0 1505.71 1504.47 28.60 o 5 6 0 991.97 935.64 35.62 o 6 6 0 1616.17 1638.86 49.48 o 7 6 0 144.81 151.33 30.21 o 8 6 0 781.73 768.78 39.27 o 9 6 0 145.22 201.12 25.44 o 10 6 0 301.35 293.47 30.79 o 11 6 0 1289.14 1326.48 55.55 o 12 6 0 10.10 17.27 19.06 o 13 6 0 0.28 7.30 18.58 o 14 6 0 680.99 744.65 89.35 o 1 7 0 65.61 74.96 10.56 o 2 7 0 78.11 61.43 8.34 o 3 7 0 87.24 86.44 10.57 o 4 7 0 384.94 453.80 26.33 o 5 7 0 396.52 444.30 28.36 o 6 7 0 150.01 155.27 29.32 o 7 7 0 3235.76 2971.41 73.60 o 8 7 0 998.97 873.87 41.63 o 9 7 0 138.81 145.18 24.84 o 10 7 0 212.31 213.01 41.23 o 11 7 0 172.52 139.94 26.92 o 12 7 0 23.02 49.23 27.56 o 13 7 0 35.46 38.66 31.17 o 0 8 0 1469.06 1423.60 46.85 o 1 8 0 649.97 620.05 22.62 o 2 8 0 4510.83 4491.77 58.88 o 3 8 0 505.63 544.04 18.83 o 4 8 0 15.65 21.58 12.97 o 5 8 0 416.12 470.03 30.89 o 6 8 0 1058.23 1001.72 41.97 o 7 8 0 1939.46 2067.08 62.42 o 8 8 0 36.09 30.63 17.35 o 9 8 0 741.80 696.74 42.50 o 10 8 0 24.94 24.44 18.11 o 11 8 0 70.16 38.86 20.73 o 12 8 0 60.14 87.25 23.44 o 13 8 0 34.79 54.70 25.76 o 1 9 0 9.13 -1.89 6.07 o 2 9 0 827.21 785.98 23.91 o 3 9 0 220.56 222.02 14.93 o 4 9 0 187.93 184.48 21.44 o 5 9 0 481.15 481.41 31.48 o 6 9 0 518.93 457.24 32.83 o 7 9 0 45.54 22.28 21.50 o 8 9 0 450.22 477.16 36.43 o 9 9 0 41.93 29.39 19.09 o 10 9 0 82.46 60.16 21.31 o 11 9 0 552.12 631.39 42.14 o 12 9 0 8.09 23.01 20.10 o 0 10 0 0.31 -5.11 8.23 o 1 10 0 12.87 4.82 6.66 o 2 10 0 1.36 8.50 6.58 o 3 10 0 0.02 8.29 7.90 o 4 10 0 977.93 979.93 53.50 o 5 10 0 111.59 113.89 24.46 o 6 10 0 563.49 581.15 37.31 o 7 10 0 318.05 317.79 31.67 o 8 10 0 100.40 97.40 22.73 o 9 10 0 104.75 106.40 23.03 o 10 10 0 5.31 7.22 17.08 o 11 10 0 27.04 10.75 19.65 o 1 11 0 31.92 20.09 7.98 o 2 11 0 192.09 164.50 17.29 o 3 11 0 3.24 6.47 10.60 o 4 11 0 43.89 45.32 16.92 o 5 11 0 103.21 114.71 22.99 o 6 11 0 61.69 37.60 23.50 o 7 11 0 2.15 17.43 15.95 o 8 11 0 35.41 25.92 17.39 o 9 11 0 30.45 44.43 23.23 o 10 11 0 172.73 169.33 32.13 o 0 12 0 685.90 717.58 35.01 o 1 12 0 47.41 39.76 9.29 o 2 12 0 698.81 641.72 36.69 o 3 12 0 39.92 32.05 14.49 o 4 12 0 254.33 240.94 24.92 o 5 12 0 4.34 -15.47 16.80 o 6 12 0 192.86 273.46 35.62 o 7 12 0 191.62 209.81 35.29 o 8 12 0 65.63 56.82 35.82 o 9 12 0 6.10 -4.64 20.80 o 1 13 0 13.40 5.69 10.97 o 2 13 0 725.40 747.31 57.38 o 3 13 0 0.04 28.87 16.54 o 4 13 0 51.16 43.30 26.64 o 5 13 0 23.86 54.37 22.76 o 6 13 0 11.04 35.14 23.56 o 7 13 0 6.41 13.80 23.72 o 8 13 0 278.63 281.28 39.40 o 0 14 0 319.01 417.30 69.75 o 1 14 0 17.21 40.86 23.04 o 2 14 0 1032.80 1150.31 59.29 o 3 14 0 6.55 31.58 32.51 o 4 14 0 424.44 380.12 52.89 o 5 14 0 2.64 12.84 36.18 o 6 14 0 14.41 13.16 32.37 o 7 14 0 284.33 244.67 49.67 o 1 15 0 1.10 24.49 44.62 o 2 15 0 104.01 140.81 31.85 o 3 15 0 36.41 53.87 27.85 o 4 15 0 471.70 428.39 45.65 o -15 1 1 22.41 8.40 26.80 o -14 1 1 33.24 28.82 25.27 o -13 1 1 2.57 18.88 22.93 o -12 1 1 50.75 66.67 26.66 o -11 1 1 1.67 8.30 17.54 o -10 1 1 2178.56 2053.20 59.59 o -9 1 1 53.94 53.19 14.30 o -8 1 1 535.61 558.35 26.42 o -7 1 1 350.67 366.88 21.66 o -6 1 1 113.00 140.78 12.09 o -5 1 1 54.22 41.57 8.08 o -4 1 1 953.21 1028.05 19.50 o -3 1 1 356.81 337.47 11.04 o -2 1 1 3255.76 3277.40 42.01 o -1 1 1 0.04 -0.49 2.69 o 0 1 1 661.46 651.14 16.51 o 1 1 1 1110.45 1036.17 16.47 o 2 1 1 13897.69 14510.91 196.89 o 3 1 1 19.00 -1.04 5.70 o 4 1 1 2793.01 2866.32 46.66 o 5 1 1 66.00 61.69 9.40 o 6 1 1 1663.57 1826.00 37.41 o 7 1 1 69.89 54.14 11.49 o 8 1 1 172.21 181.05 24.99 o 9 1 1 400.21 413.06 24.70 o 10 1 1 140.12 138.79 21.43 o 11 1 1 2.31 0.66 14.48 o 12 1 1 95.21 67.41 35.62 o 13 1 1 175.42 159.98 34.64 o 14 1 1 0.33 31.56 26.72 o 15 1 1 25.66 69.78 31.87 o -15 2 1 69.06 68.94 51.05 o -14 2 1 29.20 49.08 27.43 o -13 2 1 289.38 277.20 40.44 o -12 2 1 220.25 226.28 35.69 o -11 2 1 27.31 23.82 17.19 o -10 2 1 183.90 198.42 24.36 o -9 2 1 1942.35 1947.17 56.53 o -8 2 1 664.08 674.54 25.96 o -7 2 1 1051.47 1094.33 29.66 o -6 2 1 22.00 9.28 7.29 o -5 2 1 2317.52 2446.14 35.42 o -4 2 1 423.44 331.42 12.69 o -3 2 1 717.52 807.42 19.12 o -2 2 1 12195.07 12436.06 289.16 o -1 2 1 48489.71 48728.29 498.61 o 0 2 1 7371.84 7430.37 82.94 o 1 2 1 7708.13 7756.82 70.36 o 2 2 1 4114.50 4218.85 53.97 o 3 2 1 6419.46 6726.44 81.04 o 4 2 1 60.98 72.59 8.83 o 5 2 1 968.39 946.92 24.28 o 6 2 1 895.92 738.85 23.28 o 7 2 1 1423.36 1372.98 34.47 o 8 2 1 1501.67 1339.82 36.77 o 9 2 1 190.88 181.44 22.12 o 10 2 1 364.20 327.76 29.26 o 11 2 1 284.42 319.56 30.07 o 12 2 1 37.73 23.33 20.81 o 13 2 1 395.42 463.65 48.90 o 14 2 1 8.20 25.81 37.99 o 15 2 1 1.97 -1.78 26.04 o -15 3 1 40.37 -41.46 94.31 o -14 3 1 92.16 82.57 28.03 o -13 3 1 133.79 112.19 33.17 o -12 3 1 662.53 634.20 41.29 o -11 3 1 68.75 85.46 20.69 o -10 3 1 1550.78 1317.54 69.56 o -9 3 1 378.42 398.68 29.64 o -8 3 1 8.44 9.37 12.63 o -7 3 1 1045.62 1072.80 28.79 o -6 3 1 82.93 53.42 9.36 o -5 3 1 1221.30 1395.50 29.09 o -4 3 1 1.06 6.78 6.70 o -3 3 1 2007.70 2118.66 35.10 o -2 3 1 3056.62 3092.78 33.95 o -1 3 1 20.37 1.23 6.20 o 0 3 1 33221.29 34188.22 393.72 o 1 3 1 303.91 305.07 10.08 o 2 3 1 213.48 251.75 9.78 o 3 3 1 18.31 13.27 6.15 o 4 3 1 1039.77 1195.24 26.10 o 5 3 1 548.19 635.95 20.08 o 6 3 1 1463.98 1503.16 33.49 o 7 3 1 383.62 420.11 21.04 o 8 3 1 373.12 354.50 26.42 o 9 3 1 180.96 188.40 23.35 o 10 3 1 54.34 29.02 17.00 o 11 3 1 232.66 273.04 28.95 o 12 3 1 0.04 19.09 16.98 o 13 3 1 7.06 -4.76 20.28 o 14 3 1 190.86 187.04 38.67 o -14 4 1 84.81 39.43 27.25 o -13 4 1 77.47 87.07 27.47 o -12 4 1 410.88 469.86 49.42 o -11 4 1 190.63 218.14 27.64 o -10 4 1 1747.64 1629.92 56.04 o -9 4 1 25.41 32.71 16.99 o -8 4 1 32.47 33.69 15.91 o -7 4 1 1371.16 1427.98 45.07 o -6 4 1 284.91 265.21 26.82 o -5 4 1 1205.71 1294.73 35.35 o -4 4 1 1278.08 1221.83 27.44 o -3 4 1 11591.77 12372.74 126.07 o -2 4 1 4110.12 4384.57 47.97 o -1 4 1 5529.44 5825.48 76.03 o 0 4 1 172.63 232.87 10.77 o 1 4 1 8629.55 8937.12 85.51 o 2 4 1 1187.68 1116.49 17.81 o 3 4 1 6720.81 7045.63 105.77 o 4 4 1 123.49 74.80 9.57 o 5 4 1 3050.79 3074.98 65.54 o 6 4 1 80.56 84.62 11.55 o 7 4 1 651.22 643.44 31.36 o 8 4 1 263.62 247.53 26.61 o 9 4 1 463.77 488.25 32.56 o 10 4 1 605.05 594.18 44.90 o 11 4 1 263.71 231.24 28.91 o 12 4 1 116.50 107.94 24.21 o 13 4 1 229.48 229.57 31.91 o 14 4 1 13.04 2.10 24.51 o -14 5 1 241.83 231.46 44.27 o -13 5 1 33.29 65.74 23.03 o -12 5 1 226.82 220.58 30.06 o -11 5 1 110.48 133.61 24.28 o -10 5 1 4.21 4.94 18.74 o -9 5 1 53.19 28.74 15.78 o -8 5 1 2123.98 1832.40 55.63 o -7 5 1 94.51 78.46 17.11 o -6 5 1 0.25 -9.70 9.70 o -5 5 1 1238.65 1245.98 29.80 o -4 5 1 2582.68 2723.84 39.08 o -3 5 1 436.65 498.21 13.42 o -2 5 1 3645.36 3706.69 44.51 o -1 5 1 122.63 106.30 9.29 o 0 5 1 408.89 388.99 14.69 o 1 5 1 970.65 1135.07 21.53 o 2 5 1 65.51 65.11 7.42 o 3 5 1 16.15 29.11 8.33 o 4 5 1 1366.46 1363.45 24.98 o 5 5 1 918.49 896.47 32.05 o 6 5 1 32.73 59.46 13.74 o 7 5 1 10.63 1.22 12.34 o 8 5 1 301.70 273.53 25.73 o 9 5 1 3.49 26.09 18.02 o 10 5 1 0.41 -1.08 15.09 o 11 5 1 17.98 18.42 17.03 o 12 5 1 141.70 98.41 21.53 o 13 5 1 228.51 205.30 31.80 o 14 5 1 0.02 3.36 24.34 o -14 6 1 169.27 201.99 33.36 o -13 6 1 81.65 120.91 27.80 o -12 6 1 72.83 47.33 20.95 o -11 6 1 18.73 21.27 17.56 o -10 6 1 0.02 13.09 16.98 o -9 6 1 112.06 120.57 36.55 o -8 6 1 1533.43 1390.14 89.00 o -7 6 1 793.56 700.05 35.02 o -6 6 1 9.23 12.34 11.74 o -5 6 1 146.67 184.56 24.48 o -4 6 1 951.58 1068.17 39.38 o -3 6 1 2991.02 3042.56 37.30 o -2 6 1 461.29 476.31 15.21 o -1 6 1 17.86 38.97 8.33 o 0 6 1 296.80 288.45 14.18 o 1 6 1 608.03 568.96 18.76 o 2 6 1 2887.46 2995.76 37.63 o 3 6 1 195.06 173.21 10.43 o 4 6 1 83.12 90.18 11.04 o 5 6 1 1683.84 1705.44 38.13 o 6 6 1 684.25 656.42 35.07 o 7 6 1 492.99 526.61 31.71 o 8 6 1 175.65 150.19 28.03 o 9 6 1 57.08 65.04 17.78 o 10 6 1 26.04 40.68 17.65 o 11 6 1 2.00 11.93 16.08 o 12 6 1 19.43 40.75 18.15 o 13 6 1 0.88 33.36 19.51 o 14 6 1 296.58 280.97 65.94 o -13 7 1 4.23 29.05 23.12 o -12 7 1 62.20 67.29 35.40 o -11 7 1 4.18 19.86 19.76 o -10 7 1 20.25 22.52 17.82 o -9 7 1 816.18 713.22 41.60 o -8 7 1 127.10 82.74 31.41 o -7 7 1 4.84 -5.51 12.73 o -6 7 1 948.62 1027.10 41.03 o -5 7 1 1140.90 1171.13 53.85 o -4 7 1 0.22 6.61 7.38 o -3 7 1 1239.57 1243.90 23.56 o -2 7 1 18.76 27.97 10.50 o -1 7 1 288.88 296.81 15.91 o 0 7 1 713.96 707.29 23.21 o 1 7 1 2009.86 2092.05 52.12 o 2 7 1 1057.06 1013.86 21.65 o 3 7 1 235.34 188.54 11.22 o 4 7 1 627.58 646.44 23.13 o 5 7 1 1528.52 1393.28 58.40 o 6 7 1 18.34 29.91 14.67 o 7 7 1 120.42 151.93 24.46 o 8 7 1 451.19 474.88 33.35 o 9 7 1 342.34 325.15 31.08 o 10 7 1 56.82 58.66 35.49 o 11 7 1 4.44 28.55 17.07 o 12 7 1 0.13 20.69 18.73 o 13 7 1 57.84 62.39 23.04 o -13 8 1 178.02 171.92 29.10 o -12 8 1 26.51 25.52 22.21 o -11 8 1 113.49 128.15 27.35 o -10 8 1 38.72 10.15 16.51 o -9 8 1 155.61 135.74 24.48 o -8 8 1 51.19 35.51 17.95 o -7 8 1 411.47 423.59 31.68 o -6 8 1 24.93 9.51 12.32 o -5 8 1 237.26 221.44 23.71 o -4 8 1 33.21 26.79 11.24 o -3 8 1 3550.18 3501.12 45.58 o -2 8 1 71.74 61.41 9.04 o -1 8 1 59.69 40.60 14.00 o 0 8 1 176.61 167.33 14.72 o 1 8 1 162.20 169.58 11.14 o 2 8 1 38.49 39.32 8.36 o 3 8 1 218.02 215.03 12.86 o 4 8 1 68.22 56.49 11.50 o 5 8 1 470.15 457.83 80.33 o 6 8 1 386.50 350.56 27.71 o 7 8 1 28.90 21.53 18.65 o 8 8 1 20.41 20.51 25.07 o 9 8 1 0.03 23.11 16.81 o 10 8 1 6.77 39.84 17.56 o 11 8 1 112.63 98.80 22.87 o 12 8 1 76.22 87.06 24.20 o 13 8 1 17.23 23.32 21.19 o -12 9 1 881.97 881.17 49.72 o -11 9 1 44.17 42.15 24.02 o -10 9 1 4.81 28.33 19.61 o -9 9 1 58.87 68.73 29.91 o -8 9 1 18.24 18.06 18.00 o -7 9 1 6.91 -0.40 14.82 o -6 9 1 268.10 278.69 27.65 o -5 9 1 57.33 31.46 15.36 o -4 9 1 24.46 21.39 12.82 o -3 9 1 1147.76 1217.96 28.92 o -2 9 1 308.75 331.24 17.23 o -1 9 1 1012.56 1006.46 29.82 o 0 9 1 233.38 206.45 14.34 o 1 9 1 124.58 149.20 12.01 o 2 9 1 34.87 43.02 9.05 o 3 9 1 67.41 59.92 9.42 o 4 9 1 0.09 6.67 10.48 o 5 9 1 8.71 13.07 11.92 o 6 9 1 108.06 88.44 25.04 o 7 9 1 97.70 99.33 18.22 o 8 9 1 137.28 120.85 21.07 o 9 9 1 0.43 17.05 15.50 o 10 9 1 34.75 14.16 18.03 o 11 9 1 58.54 120.18 25.26 o 12 9 1 0.01 20.48 20.14 o -11 10 1 200.69 233.57 30.69 o -10 10 1 189.72 180.74 29.89 o -9 10 1 239.55 246.08 31.04 o -8 10 1 130.07 149.01 25.48 o -7 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