#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:55:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181122 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/01/2220125.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220125_Fobs loop_ _publ_author_name 'Natarajan, S.' 'Sudhapriya, V.' 'Vijayakumar, V.' 'Shoba, N.' 'Suresh, J.' 'Lakshman, P. L. Nilantha' _publ_section_title ; 2,4,6,8-Tetrakis(4-fluorophenyl)-3,7-diazabicyclo[3.3.1]nonan-9-one ; _journal_coeditor_code CI2727 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2496 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 133.249 _cell_angle_gamma 90.000 _cell_length_a 37.1521 _cell_length_b 7.1458 _cell_length_c 26.2165 _exptl_crystal_F_000 2144.00 _reflns_d_resolution_high 0.8415 _cod_data_source_file ci2727Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4fbd in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 474.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 12046.21 11439.18 53.34 o 6 0 0 615.55 614.16 19.04 o 8 0 0 12698.42 12750.25 80.67 o 10 0 0 1327.32 1388.15 36.58 o 12 0 0 5237.92 5904.69 70.43 o 14 0 0 8172.24 8357.68 90.64 o 16 0 0 11425.56 11468.98 115.75 o 18 0 0 141.76 157.03 22.95 o 20 0 0 192.17 183.77 24.45 o 22 0 0 179.13 187.94 26.41 o 24 0 0 0.44 -21.98 38.21 o 26 0 0 871.34 900.50 39.19 o 28 0 0 90.49 112.36 28.37 o 30 0 0 24.88 6.39 47.80 o 32 0 0 16.69 6.98 52.63 o 1 1 0 45128.48 40804.34 436.66 o 3 1 0 3324.05 3088.75 48.26 o 5 1 0 49819.06 44749.18 560.85 o 7 1 0 28569.02 26450.76 411.48 o 9 1 0 10886.74 10232.18 57.55 o 11 1 0 25018.41 23955.90 94.23 o 13 1 0 20.84 37.68 23.31 o 15 1 0 6508.55 6681.05 115.26 o 17 1 0 32.81 41.96 21.10 o 19 1 0 5072.06 5301.61 178.84 o 21 1 0 159.99 241.85 35.67 o 23 1 0 0.43 20.86 26.80 o 25 1 0 365.81 347.22 24.72 o 27 1 0 127.12 144.93 20.70 o 29 1 0 0.10 -9.83 51.16 o 31 1 0 356.35 408.98 27.55 o 0 2 0 3367.84 3417.27 45.06 o 2 2 0 86.51 104.53 15.46 o 4 2 0 79437.33 73715.42 194.00 o 6 2 0 13368.08 12785.99 89.21 o 8 2 0 42235.95 40750.04 167.27 o 10 2 0 33.34 3.72 25.89 o 12 2 0 5879.47 5798.92 77.34 o 14 2 0 34.26 19.37 28.89 o 16 2 0 1491.80 1532.53 46.23 o 18 2 0 45.59 64.62 35.67 o 20 2 0 128.76 74.47 26.48 o 22 2 0 605.96 643.83 33.45 o 24 2 0 1077.97 1114.66 40.17 o 26 2 0 37.69 -16.69 46.30 o 28 2 0 1024.55 996.56 43.76 o 30 2 0 7.01 17.93 48.84 o 1 3 0 4465.11 4833.59 63.52 o 3 3 0 7608.25 7086.58 76.43 o 5 3 0 1151.09 1235.30 34.43 o 7 3 0 2839.76 2951.53 55.56 o 9 3 0 18.02 21.45 17.22 o 11 3 0 3232.84 3158.77 65.34 o 13 3 0 0.20 2.15 32.54 o 15 3 0 3508.70 3517.37 76.17 o 17 3 0 788.42 708.98 32.74 o 19 3 0 3883.46 3620.86 87.51 o 21 3 0 3.97 20.15 42.65 o 23 3 0 0.46 1.70 43.89 o 25 3 0 46.50 56.80 48.84 o 27 3 0 19.55 -16.43 50.15 o 29 3 0 141.90 206.20 34.76 o 0 4 0 38711.28 40152.83 201.18 o 2 4 0 1557.20 1624.94 42.45 o 4 4 0 3062.46 3151.66 63.78 o 6 4 0 309.38 224.98 23.35 o 8 4 0 577.31 400.46 25.17 o 10 4 0 13.36 -18.06 33.19 o 12 4 0 94.08 47.34 37.30 o 14 4 0 65.94 83.93 25.24 o 16 4 0 277.53 294.17 30.00 o 18 4 0 230.22 179.01 30.39 o 20 4 0 742.79 729.32 37.17 o 22 4 0 403.74 426.48 35.87 o 24 4 0 130.55 88.30 49.63 o 26 4 0 22.12 47.28 49.56 o 28 4 0 6.22 27.71 48.32 o 1 5 0 284.92 298.99 25.69 o 3 5 0 72.80 26.41 39.52 o 5 5 0 2810.42 2978.66 74.86 o 7 5 0 270.91 274.93 28.82 o 9 5 0 63.99 68.34 25.43 o 11 5 0 80.06 100.62 27.26 o 13 5 0 75.09 58.56 27.85 o 15 5 0 296.95 263.78 31.82 o 17 5 0 24.28 49.10 43.10 o 19 5 0 55.69 58.10 47.34 o 21 5 0 628.57 547.91 37.89 o 23 5 0 6.48 -35.61 50.86 o 25 5 0 7.06 9.06 51.19 o 0 6 0 79.70 173.33 28.04 o 2 6 0 23.33 75.71 41.87 o 4 6 0 140.53 58.49 47.08 o 6 6 0 6.80 81.64 42.84 o 8 6 0 0.39 -40.95 45.97 o 10 6 0 50.80 24.72 45.06 o 12 6 0 62.14 -3.46 46.37 o 14 6 0 8.11 -27.32 46.69 o 16 6 0 215.86 229.22 34.76 o 18 6 0 1.53 22.17 50.41 o 20 6 0 24.86 40.56 50.47 o 22 6 0 4.05 -36.52 51.00 o 1 7 0 265.52 292.67 34.95 o 3 7 0 3841.93 3735.24 103.95 o 5 7 0 1049.40 962.65 44.21 o 7 7 0 5.01 13.24 48.06 o 9 7 0 299.63 282.82 35.61 o 11 7 0 188.22 224.13 35.80 o 13 7 0 0.00 -39.39 51.00 o 15 7 0 11.09 -50.34 53.34 o 17 7 0 14.71 27.26 53.93 o 0 8 0 17.35 60.91 53.73 o 2 8 0 54.03 69.58 56.99 o 4 8 0 5.07 -37.17 54.13 o 6 8 0 333.45 308.38 41.21 o 8 8 0 353.07 305.19 41.08 o 10 8 0 8.55 -37.24 55.36 o -31 1 1 195.01 260.61 41.47 o -29 1 1 118.72 150.59 21.67 o -27 1 1 105.43 110.76 20.74 o -25 1 1 29.03 -29.07 33.88 o -23 1 1 121.92 102.88 45.32 o -21 1 1 127.29 130.55 17.96 o -19 1 1 592.75 632.52 20.70 o -17 1 1 164.59 166.43 15.41 o -15 1 1 1377.25 1385.23 44.08 o -13 1 1 7534.27 7159.52 56.82 o -11 1 1 7836.83 7242.95 51.83 o -9 1 1 59822.95 54058.99 526.48 o -7 1 1 907.96 957.56 63.35 o -5 1 1 145386.70 124172.90 2526.61 o -3 1 1 11658.15 10675.19 230.23 o -1 1 1 832.59 857.12 36.84 o 1 1 1 660.25 604.89 12.43 o 3 1 1 1299.58 1292.19 115.33 o 5 1 1 916.66 768.70 29.48 o 7 1 1 64458.64 59162.61 628.93 o 9 1 1 2735.51 2603.52 37.63 o 11 1 1 2092.57 1960.69 52.69 o 13 1 1 1853.00 1770.36 34.08 o 15 1 1 2058.11 1981.40 54.29 o 17 1 1 624.72 673.09 26.28 o 19 1 1 1046.43 1090.82 57.09 o 21 1 1 627.60 629.24 32.44 o 23 1 1 686.07 764.48 25.06 o 25 1 1 260.84 299.04 22.39 o 27 1 1 0.61 -44.87 44.87 o 29 1 1 10.11 -2.60 34.11 o -32 2 1 1.35 53.60 49.04 o -30 2 1 23.94 87.90 45.45 o -28 2 1 638.11 700.24 38.67 o -26 2 1 23.10 1.76 43.04 o -24 2 1 247.06 251.06 30.71 o -22 2 1 25.79 34.37 39.58 o -20 2 1 428.75 385.01 29.02 o -18 2 1 246.98 215.85 24.98 o -16 2 1 345.79 315.82 23.61 o -14 2 1 1380.82 1381.57 39.84 o -12 2 1 8118.34 8026.28 86.54 o -10 2 1 6159.49 6243.66 72.84 o -8 2 1 9611.33 9368.59 80.80 o -6 2 1 74.74 35.54 26.67 o -4 2 1 321.95 325.86 17.22 o -2 2 1 4048.85 4133.49 49.95 o 0 2 1 5608.15 5454.93 258.37 o 2 2 1 12038.87 11567.25 78.38 o 4 2 1 0.09 13.17 24.39 o 6 2 1 2240.30 2179.49 44.47 o 8 2 1 311.72 360.88 18.32 o 10 2 1 767.91 700.76 21.58 o 12 2 1 312.33 345.62 21.06 o 14 2 1 4165.20 4041.41 73.69 o 16 2 1 33.67 59.80 23.54 o 18 2 1 201.28 145.81 25.30 o 20 2 1 650.87 630.98 33.65 o 22 2 1 339.71 332.58 32.15 o 24 2 1 31.86 78.91 46.17 o 26 2 1 10.38 89.27 28.82 o 28 2 1 168.01 182.46 33.45 o 30 2 1 1.30 -9.33 50.08 o -31 3 1 9.53 28.37 52.10 o -29 3 1 923.95 918.76 45.52 o -27 3 1 12.17 5.93 44.80 o -25 3 1 62.01 38.08 46.50 o -23 3 1 1261.52 1144.07 41.34 o -21 3 1 15.12 -2.93 39.39 o -19 3 1 1411.54 1380.78 42.19 o -17 3 1 388.89 363.16 28.17 o -15 3 1 618.84 701.67 28.89 o -13 3 1 899.30 933.96 28.50 o -11 3 1 2813.64 2964.57 60.97 o -9 3 1 303.60 320.71 19.04 o -7 3 1 888.56 821.14 24.26 o -5 3 1 18556.70 18614.58 120.38 o -3 3 1 17725.81 17959.59 116.14 o -1 3 1 5204.14 5410.98 67.43 o 1 3 1 3444.89 3170.64 53.86 o 3 3 1 4002.02 3869.31 59.08 o 5 3 1 188.83 162.18 17.41 o 7 3 1 6463.72 6783.15 80.80 o 9 3 1 4413.78 4085.69 68.73 o 11 3 1 280.72 202.35 22.37 o 13 3 1 2167.16 2101.30 60.58 o 15 3 1 1756.77 1767.94 51.91 o 17 3 1 58.98 20.28 37.43 o 19 3 1 4495.41 4101.27 93.25 o 21 3 1 4.35 -6.52 42.52 o 23 3 1 1063.84 1070.38 41.93 o 25 3 1 4.49 23.74 47.47 o 27 3 1 8.59 -49.04 49.04 o 29 3 1 3.79 -9.33 50.60 o -28 4 1 0.00 -6.65 49.76 o -26 4 1 161.55 90.97 52.23 o -24 4 1 860.32 795.84 40.63 o -22 4 1 79.61 106.23 29.08 o -20 4 1 348.05 365.64 31.43 o -18 4 1 471.24 491.95 31.11 o -16 4 1 219.08 122.34 27.19 o -14 4 1 11.05 10.11 37.43 o -12 4 1 604.97 585.53 28.43 o -10 4 1 1097.68 1099.07 31.43 o -8 4 1 775.45 885.05 28.37 o -6 4 1 54.01 -12.59 31.95 o -4 4 1 1700.58 1875.09 52.95 o -2 4 1 9810.98 10366.39 105.97 o 0 4 1 1.69 18.88 21.00 o 2 4 1 1739.93 1618.94 43.17 o 4 4 1 22.53 6.78 30.32 o 6 4 1 5329.66 5058.70 81.19 o 8 4 1 277.75 253.22 24.06 o 10 4 1 167.30 125.47 24.52 o 12 4 1 76.56 78.97 24.72 o 14 4 1 129.13 35.61 43.37 o 16 4 1 1536.11 1503.71 43.50 o 18 4 1 187.50 144.90 30.45 o 20 4 1 107.19 112.16 30.13 o 22 4 1 1067.84 1153.59 44.41 o 24 4 1 34.43 34.76 50.54 o 26 4 1 284.38 236.72 38.34 o -25 5 1 72.26 87.25 52.82 o -23 5 1 115.32 95.14 50.73 o -21 5 1 403.75 368.05 36.26 o -19 5 1 15.42 30.13 29.41 o -17 5 1 1114.93 1076.38 42.26 o -15 5 1 234.83 222.57 30.78 o -13 5 1 137.17 134.20 28.24 o -11 5 1 233.24 270.63 29.48 o -9 5 1 37.89 41.60 39.45 o -7 5 1 1329.17 1232.76 39.58 o -5 5 1 135.35 118.82 27.32 o -3 5 1 248.60 234.30 26.61 o -1 5 1 34.46 -28.56 38.93 o 1 5 1 49.39 -6.00 36.78 o 3 5 1 2820.32 2746.57 71.21 o 5 5 1 1618.96 1548.83 46.10 o 7 5 1 578.41 592.05 30.71 o 9 5 1 175.28 169.68 27.39 o 11 5 1 240.92 195.50 30.26 o 13 5 1 249.82 250.93 30.78 o 15 5 1 22.93 9.91 45.26 o 17 5 1 954.50 1009.60 40.82 o 19 5 1 88.81 78.97 47.41 o 21 5 1 0.82 64.36 47.34 o 23 5 1 438.79 424.46 38.87 o 25 5 1 45.86 38.15 34.69 o -22 6 1 12.32 -53.54 53.54 o -20 6 1 87.14 4.17 48.52 o -18 6 1 260.60 172.48 36.13 o -16 6 1 892.96 896.40 42.52 o -14 6 1 2.26 -33.78 43.76 o -12 6 1 896.05 839.34 41.21 o -10 6 1 69.68 -3.26 48.00 o -8 6 1 364.01 280.08 32.87 o -6 6 1 37.16 7.63 45.06 o -4 6 1 0.76 -4.50 43.82 o -2 6 1 33.98 79.95 27.91 o 0 6 1 191.25 160.75 28.95 o 2 6 1 54.71 49.30 29.15 o 4 6 1 50.87 34.43 28.95 o 6 6 1 26.91 23.48 45.13 o 8 6 1 64.27 62.67 43.89 o 10 6 1 232.65 208.15 31.82 o 12 6 1 123.83 91.49 47.73 o 14 6 1 797.43 841.16 41.80 o 16 6 1 83.67 15.91 49.69 o 18 6 1 5.75 63.32 31.63 o 20 6 1 5.01 26.41 51.13 o -19 7 1 42.41 86.21 50.47 o -17 7 1 81.58 48.84 55.63 o -15 7 1 96.09 111.12 34.95 o -13 7 1 162.61 229.35 36.06 o -11 7 1 297.42 332.90 36.65 o -9 7 1 63.47 11.41 53.41 o -7 7 1 298.03 318.56 37.69 o -5 7 1 9.97 58.43 51.45 o -3 7 1 23.97 -52.10 52.10 o -1 7 1 12.87 -10.89 49.63 o 1 7 1 4.27 -5.48 50.47 o 3 7 1 7.81 23.80 47.54 o 5 7 1 0.94 76.17 45.91 o 7 7 1 85.77 142.75 32.21 o 9 7 1 3.05 88.04 46.37 o 11 7 1 3.12 -53.21 53.21 o 13 7 1 66.72 98.99 33.45 o 15 7 1 14.89 -4.50 52.82 o 17 7 1 9.80 11.67 54.06 o -10 8 1 43.96 57.45 60.97 o -8 8 1 82.29 106.16 36.19 o -6 8 1 38.14 30.98 57.19 o -4 8 1 81.00 -8.74 60.39 o -2 8 1 270.41 223.41 41.08 o 0 8 1 2.69 -38.82 38.82 o 2 8 1 0.10 -34.95 54.39 o 4 8 1 24.40 -53.80 53.80 o 6 8 1 3.04 -51.78 55.76 o 8 8 1 37.19 90.97 35.74 o -34 0 2 2.69 0.00 50.41 o -32 0 2 31.74 -2.15 48.91 o -30 0 2 196.08 252.76 32.15 o -28 0 2 567.58 615.73 35.02 o -26 0 2 484.26 484.98 32.74 o -24 0 2 847.12 950.91 34.76 o -22 0 2 113.14 138.57 23.35 o -20 0 2 1629.86 1507.23 45.65 o -18 0 2 80.36 99.97 19.82 o -16 0 2 190.30 268.93 18.32 o -14 0 2 18648.79 20251.64 126.97 o -12 0 2 5919.20 5868.69 64.89 o -10 0 2 223840.78 212434.73 324.04 o -8 0 2 225573.69 200931.28 273.04 o -6 0 2 5636.67 5552.94 41.54 o -4 0 2 115.78 94.75 8.67 o 0 0 2 3914.61 3850.75 19.97 o 2 0 2 3690.56 3617.47 34.69 o 4 0 2 52511.50 50086.74 136.49 o 6 0 2 5465.48 5558.88 56.67 o 8 0 2 26398.01 25840.38 128.01 o 10 0 2 12631.90 13202.88 102.71 o 12 0 2 3211.12 3153.42 60.06 o 14 0 2 1094.51 1065.49 34.50 o 16 0 2 208.19 274.60 23.54 o 18 0 2 538.04 597.34 30.13 o 20 0 2 3309.80 3201.42 83.21 o 22 0 2 1753.52 1908.54 54.71 o 24 0 2 0.04 29.15 26.74 o 26 0 2 77.03 144.18 29.28 o 28 0 2 389.56 438.48 36.71 o 30 0 2 51.00 79.10 48.91 o -33 1 2 179.54 155.69 43.63 o -31 1 2 0.04 28.12 31.86 o -29 1 2 407.39 429.22 24.45 o -27 1 2 429.99 525.57 23.12 o -25 1 2 172.86 141.08 36.91 o -23 1 2 58.42 44.26 33.75 o -21 1 2 3.24 -23.99 23.99 o -19 1 2 95.77 121.52 14.91 o -17 1 2 1411.61 1475.31 29.50 o -15 1 2 438.25 546.57 18.06 o -13 1 2 313.53 228.07 11.87 o -11 1 2 37.15 18.77 17.26 o -9 1 2 84377.29 77309.59 725.02 o -7 1 2 32476.60 29662.85 834.05 o -5 1 2 636.58 711.66 19.01 o -3 1 2 46080.07 41896.98 1970.04 o -1 1 2 2440.57 2271.91 186.96 o 1 1 2 122734.63 103313.58 2416.14 o 3 1 2 77194.25 68353.45 337.31 o 5 1 2 41238.00 37936.61 461.37 o 7 1 2 2808.80 2524.72 37.27 o 9 1 2 4318.53 3770.53 67.23 o 11 1 2 1512.12 1489.21 30.73 o 13 1 2 637.39 677.07 37.46 o 15 1 2 850.51 924.03 24.06 o 17 1 2 832.39 839.23 21.88 o 19 1 2 619.08 571.75 22.25 o 21 1 2 1116.74 1152.80 38.25 o 23 1 2 707.24 717.73 25.91 o 25 1 2 127.29 124.88 21.21 o 27 1 2 227.53 249.29 24.58 o 29 1 2 442.26 455.51 27.96 o -32 2 2 25.08 -6.72 47.34 o -30 2 2 12.00 28.82 47.34 o -28 2 2 172.87 154.94 31.43 o -26 2 2 38.84 -45.71 45.71 o -24 2 2 89.81 62.34 39.71 o -22 2 2 204.31 231.76 27.58 o -20 2 2 915.24 913.02 33.19 o -18 2 2 10630.01 10908.94 119.92 o -16 2 2 15196.12 14449.14 128.21 o -14 2 2 21345.85 21561.87 145.16 o -12 2 2 39504.65 39394.30 180.05 o -10 2 2 2825.63 2721.53 49.82 o -8 2 2 6568.81 6737.05 67.75 o -6 2 2 43050.16 42146.74 150.31 o -4 2 2 32366.75 31822.35 125.47 o -2 2 2 1371.68 1524.71 36.45 o 0 2 2 16936.87 16291.87 744.81 o 2 2 2 570.18 837.64 25.24 o 4 2 2 12215.66 11142.27 84.84 o 6 2 2 1066.74 1027.86 30.71 o 8 2 2 454.95 638.09 20.02 o 10 2 2 1341.11 1302.07 37.43 o 12 2 2 46.49 31.17 32.61 o 14 2 2 4468.42 4435.68 80.99 o 16 2 2 38.44 51.32 22.56 o 18 2 2 4.47 -16.37 36.13 o 20 2 2 533.52 535.58 32.87 o 22 2 2 42.72 -15.00 44.28 o 24 2 2 601.41 562.25 37.37 o 26 2 2 123.81 83.99 33.78 o 28 2 2 135.46 163.48 33.06 o -31 3 2 79.85 101.27 34.43 o -29 3 2 459.40 499.00 38.02 o -27 3 2 29.63 58.56 43.43 o -25 3 2 30.81 60.91 45.26 o -23 3 2 53.15 70.56 41.47 o -21 3 2 166.58 82.36 43.82 o -19 3 2 353.89 298.08 28.43 o -17 3 2 15.53 -36.52 36.52 o -15 3 2 3076.57 3184.27 70.30 o -13 3 2 491.50 449.76 25.04 o -11 3 2 1322.29 1290.01 39.19 o -9 3 2 3408.11 3624.19 61.82 o -7 3 2 4486.11 4689.28 65.99 o -5 3 2 5169.98 5353.59 67.82 o -3 3 2 15952.22 17321.11 114.45 o -1 3 2 3793.16 4075.45 60.71 o 1 3 2 7143.15 7218.31 76.17 o 3 3 2 99.40 101.47 16.50 o 5 3 2 264.94 223.15 17.80 o 7 3 2 1566.33 1668.04 47.80 o 9 3 2 4650.62 4540.01 75.06 o 11 3 2 749.16 777.45 29.41 o 13 3 2 1179.21 1149.22 34.24 o 15 3 2 33.89 -18.26 39.65 o 17 3 2 319.03 291.17 30.71 o 19 3 2 2317.06 2515.20 66.12 o 21 3 2 50.56 65.73 29.21 o 23 3 2 176.81 151.75 33.32 o 25 3 2 301.48 257.32 36.06 o 27 3 2 224.51 187.16 36.26 o -30 4 2 3.74 -35.15 53.73 o -28 4 2 7.02 62.15 49.76 o -26 4 2 5.73 51.78 46.63 o -24 4 2 109.57 92.73 48.91 o -22 4 2 103.33 157.49 27.91 o -20 4 2 56.01 39.39 27.26 o -18 4 2 13.04 4.24 26.28 o -16 4 2 28.29 23.61 38.21 o -14 4 2 185.79 172.94 25.50 o -12 4 2 21.04 -2.28 34.56 o -10 4 2 6321.05 6627.17 94.49 o -8 4 2 1577.17 1781.18 52.95 o -6 4 2 1095.97 1071.62 29.21 o -4 4 2 361.52 475.13 23.02 o -2 4 2 1072.97 1235.30 36.19 o 0 4 2 170.54 169.45 23.22 o 2 4 2 151.46 199.68 19.63 o 4 4 2 324.04 395.83 23.28 o 6 4 2 2046.09 2115.46 58.30 o 8 4 2 397.84 380.90 24.78 o 10 4 2 207.43 158.99 25.56 o 12 4 2 429.98 487.13 29.67 o 14 4 2 676.67 680.35 33.84 o 16 4 2 428.16 427.33 33.39 o 18 4 2 57.26 41.67 43.82 o 20 4 2 22.85 23.35 46.82 o 22 4 2 32.51 52.95 45.65 o 24 4 2 555.14 544.38 39.58 o 26 4 2 40.37 46.95 34.24 o -27 5 2 28.71 -20.61 52.50 o -25 5 2 245.09 231.63 36.52 o -23 5 2 1.04 -48.00 48.00 o -21 5 2 157.13 109.75 32.87 o 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28 11.83 -9.68 48.97 o -31 1 28 121.36 137.91 22.48 o -29 1 28 51.92 22.97 32.73 o -27 1 28 11.94 -6.37 31.67 o -25 1 28 57.32 58.67 32.42 o -23 1 28 29.90 16.27 30.82 o -21 1 28 2.29 -5.87 31.37 o -19 1 28 0.11 -5.57 38.64 o -17 1 28 51.38 73.37 26.24 o -15 1 28 1.69 17.68 40.43 o -38 2 28 186.73 182.40 37.95 o -36 2 28 421.49 396.42 38.02 o -34 2 28 136.10 95.60 54.52 o -32 2 28 419.35 376.33 37.37 o -30 2 28 0.56 17.15 45.58 o -28 2 28 367.94 344.71 36.39 o -26 2 28 7.24 12.78 48.91 o -24 2 28 69.91 59.47 49.04 o -22 2 28 384.10 438.22 38.80 o -20 2 28 222.99 329.77 34.89 o -18 2 28 132.59 196.48 33.65 o -16 2 28 40.25 51.58 51.58 o -35 3 28 53.78 84.51 50.80 o -33 3 28 387.97 548.36 40.76 o -31 3 28 140.28 184.29 36.13 o -29 3 28 104.01 89.08 35.61 o -27 3 28 240.04 331.47 36.32 o -25 3 28 0.24 13.56 47.87 o -23 3 28 123.68 74.47 54.58 o -21 3 28 0.68 6.85 47.15 o -19 3 28 10.08 35.02 48.00 o -39 1 29 31.38 -22.15 40.63 o -37 1 29 4.39 10.22 35.74 o -35 1 29 3.74 11.24 37.99 o -33 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194.67 225.11 24.94 o -32 2 30 112.43 30.39 51.26 o -30 2 30 89.85 88.88 56.80 o -28 2 30 36.53 60.26 53.02 o -26 2 30 60.83 96.32 52.04 o