#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/01/2220136.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220136_Fobs loop_ _publ_author_name 'Wang, Zhigang' _publ_section_title ; 1,4-Diphenylbutane-1,4-dione ; _journal_coeditor_code CV2479 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2423 _journal_volume 64 _journal_year 2008 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.3781 _cell_length_b 14.1607 _cell_length_c 5.3186 _exptl_crystal_F_000 252.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file cv2479Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' t in P2(1)2(1)2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 75.18 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 259.99 243.19 38.89 o 4 0 0 3.08 2.38 0.52 o 6 0 0 28.33 26.95 4.76 o 8 0 0 7.19 8.58 2.27 o 10 0 0 24.73 31.71 3.62 o 1 1 0 618.37 655.64 47.89 o 2 1 0 5056.89 4993.64 363.69 o 3 1 0 79.15 78.26 7.33 o 4 1 0 2.98 2.86 0.35 o 5 1 0 8.93 8.52 0.64 o 6 1 0 44.44 43.57 4.09 o 7 1 0 0.35 0.26 0.34 o 8 1 0 3.92 4.97 0.68 o 9 1 0 3.46 7.44 1.42 o 10 1 0 11.86 19.55 2.17 o 0 2 0 453.64 518.62 89.10 o 1 2 0 1.57 2.03 0.14 o 2 2 0 5.42 2.90 0.80 o 3 2 0 5.60 5.28 0.58 o 4 2 0 73.95 66.95 4.31 o 5 2 0 19.87 20.29 1.06 o 6 2 0 3.35 3.20 0.49 o 7 2 0 23.69 25.59 2.09 o 8 2 0 3.47 3.20 0.74 o 9 2 0 3.83 5.90 1.33 o 10 2 0 1.80 2.18 1.84 o 1 3 0 992.60 1041.78 42.33 o 2 3 0 389.88 403.20 30.13 o 3 3 0 3.95 3.41 0.80 o 4 3 0 10.40 10.46 1.03 o 5 3 0 282.01 305.89 27.60 o 6 3 0 78.69 78.23 6.74 o 7 3 0 0.08 0.04 0.33 o 8 3 0 0.26 0.66 0.51 o 9 3 0 1.75 1.00 0.81 o 10 3 0 0.04 -0.08 1.30 o 0 4 0 8.03 11.57 1.37 o 1 4 0 325.61 318.76 13.78 o 2 4 0 91.33 105.14 7.72 o 3 4 0 34.81 38.41 2.65 o 4 4 0 175.15 216.56 22.04 o 5 4 0 25.18 28.69 4.58 o 6 4 0 38.84 32.98 4.58 o 7 4 0 42.60 39.23 2.90 o 8 4 0 11.60 11.74 1.17 o 9 4 0 0.11 0.10 0.76 o 10 4 0 0.20 -0.69 1.41 o 1 5 0 78.06 92.87 6.40 o 2 5 0 100.42 110.56 8.27 o 3 5 0 116.29 141.99 10.04 o 4 5 0 67.09 77.53 6.50 o 5 5 0 7.63 5.45 1.54 o 6 5 0 18.51 9.52 3.92 o 7 5 0 2.26 2.33 0.46 o 8 5 0 0.12 0.21 0.51 o 9 5 0 0.64 -0.39 1.14 o 0 6 0 242.12 229.97 7.58 o 1 6 0 978.49 1092.39 64.02 o 2 6 0 252.91 269.95 9.70 o 3 6 0 34.73 40.82 3.03 o 4 6 0 3.76 3.74 0.37 o 5 6 0 12.09 11.14 1.34 o 6 6 0 0.10 0.20 0.28 o 7 6 0 0.09 0.32 0.31 o 8 6 0 3.00 4.04 1.44 o 9 6 0 0.01 -0.12 1.17 o 1 7 0 718.24 803.97 51.90 o 2 7 0 7.42 7.80 2.02 o 3 7 0 7.22 8.43 0.84 o 4 7 0 96.10 101.66 7.11 o 5 7 0 0.59 0.73 0.28 o 6 7 0 10.99 11.22 2.31 o 7 7 0 0.03 0.10 0.43 o 8 7 0 0.97 1.71 0.75 o 9 7 0 5.17 5.71 2.12 o 0 8 0 41.17 36.42 1.44 o 1 8 0 14.66 16.39 0.72 o 2 8 0 46.28 48.61 2.93 o 3 8 0 11.91 12.30 0.62 o 4 8 0 0.78 0.77 0.26 o 5 8 0 5.37 5.23 0.67 o 6 8 0 2.41 2.25 0.58 o 7 8 0 0.68 0.58 0.55 o 8 8 0 1.12 1.39 0.70 o 9 8 0 2.93 2.48 1.35 o 1 9 0 48.89 42.58 1.56 o 2 9 0 0.15 0.68 0.24 o 3 9 0 28.40 31.34 2.66 o 4 9 0 3.53 3.79 0.51 o 5 9 0 3.51 3.70 0.68 o 6 9 0 59.92 56.40 5.41 o 7 9 0 19.46 17.13 2.80 o 8 9 0 28.78 27.27 5.01 o 0 10 0 59.21 57.08 2.99 o 1 10 0 35.17 30.98 1.09 o 2 10 0 35.73 31.55 1.13 o 3 10 0 133.52 123.01 5.75 o 4 10 0 177.21 168.45 7.34 o 5 10 0 0.30 0.51 0.48 o 6 10 0 53.02 53.42 3.83 o 7 10 0 14.02 14.20 3.46 o 8 10 0 5.74 5.70 1.68 o 1 11 0 8.96 7.89 0.69 o 2 11 0 26.67 22.22 1.25 o 3 11 0 24.96 24.28 1.36 o 4 11 0 3.81 4.44 0.78 o 5 11 0 89.24 80.13 4.63 o 6 11 0 27.31 26.33 1.93 o 7 11 0 4.14 4.77 1.10 o 8 11 0 6.13 6.26 1.56 o 0 12 0 6.33 5.55 0.96 o 1 12 0 0.28 0.32 0.37 o 2 12 0 6.32 6.32 0.86 o 3 12 0 37.98 35.37 1.68 o 4 12 0 1.72 1.79 0.60 o 5 12 0 2.32 3.35 0.79 o 6 12 0 0.17 -0.12 0.49 o 7 12 0 0.05 0.50 0.57 o 1 13 0 13.79 11.37 1.11 o 2 13 0 7.56 6.24 0.90 o 3 13 0 10.71 7.04 0.98 o 4 13 0 0.37 0.95 0.56 o 5 13 0 1.95 2.81 0.75 o 6 13 0 0.31 0.70 0.56 o 0 14 0 31.14 28.93 2.90 o 1 14 0 1.55 1.56 0.72 o 2 14 0 5.57 6.42 1.24 o 3 14 0 0.64 0.92 0.53 o 4 14 0 2.50 2.86 0.77 o 5 14 0 2.38 2.38 0.71 o 6 14 0 0.31 0.42 0.57 o 1 15 0 0.81 1.07 0.72 o 2 15 0 2.60 3.49 0.97 o 3 15 0 5.38 4.07 1.07 o 4 15 0 0.81 0.96 0.59 o 5 15 0 1.01 1.55 0.68 o 0 16 0 0.04 -0.78 0.90 o 1 16 0 0.33 1.09 0.85 o 2 16 0 2.61 4.01 1.06 o 3 16 0 4.24 4.46 1.10 o 4 16 0 0.31 1.57 1.00 o 1 17 0 1.38 0.08 0.91 o 2 17 0 0.14 0.66 0.61 o 0 0 1 263.12 89.62 114.81 o 1 0 1 4089.59 3831.63 158.41 o 2 0 1 5651.62 2914.86 1415.44 o 3 0 1 1050.03 1067.17 72.64 o 4 0 1 123.03 121.89 11.25 o 5 0 1 12.84 14.75 1.81 o 6 0 1 0.33 0.93 0.33 o 7 0 1 0.25 0.55 0.40 o 8 0 1 24.47 25.58 1.99 o 9 0 1 20.07 24.44 2.27 o 10 0 1 1.28 1.48 1.14 o 0 1 1 164.89 179.04 5.67 o 1 1 1 2109.59 2102.25 49.37 o 2 1 1 572.04 625.80 28.69 o 3 1 1 405.43 447.63 25.08 o 4 1 1 584.99 587.68 34.52 o 5 1 1 4.24 3.30 0.30 o 6 1 1 4.58 5.46 0.50 o 7 1 1 6.29 7.03 0.68 o 8 1 1 19.21 21.10 1.38 o 9 1 1 7.56 9.65 0.86 o 10 1 1 3.75 5.72 1.03 o 0 2 1 212.25 214.48 10.67 o 1 2 1 333.95 345.81 9.09 o 2 2 1 502.21 566.49 24.94 o 3 2 1 172.06 185.52 9.32 o 4 2 1 48.55 43.68 1.63 o 5 2 1 17.17 19.32 1.05 o 6 2 1 11.41 9.17 0.82 o 7 2 1 16.75 18.79 1.43 o 8 2 1 15.07 17.80 1.32 o 9 2 1 3.55 4.65 0.63 o 10 2 1 5.02 7.18 1.35 o 0 3 1 211.23 242.38 19.56 o 1 3 1 388.28 397.49 14.39 o 2 3 1 19.50 20.25 0.77 o 3 3 1 497.01 572.94 28.71 o 4 3 1 70.58 76.91 3.22 o 5 3 1 40.78 37.00 1.36 o 6 3 1 27.85 27.43 1.73 o 7 3 1 12.78 11.07 1.77 o 8 3 1 12.42 12.32 1.00 o 9 3 1 0.76 1.25 0.50 o 10 3 1 2.09 3.85 1.13 o 0 4 1 2.31 2.25 0.21 o 1 4 1 120.40 119.35 6.45 o 2 4 1 83.23 84.99 3.97 o 3 4 1 90.56 96.14 4.82 o 4 4 1 49.74 47.26 2.14 o 5 4 1 100.12 107.48 3.79 o 6 4 1 24.09 28.93 1.84 o 7 4 1 4.82 5.60 0.58 o 8 4 1 5.93 6.05 0.73 o 9 4 1 3.57 3.36 0.65 o 0 5 1 460.62 542.03 31.35 o 1 5 1 269.85 292.39 15.94 o 2 5 1 18.96 22.88 0.97 o 3 5 1 76.13 83.81 3.17 o 4 5 1 55.37 61.54 2.51 o 5 5 1 11.35 11.22 0.47 o 6 5 1 0.06 0.26 0.22 o 7 5 1 4.50 5.59 0.61 o 8 5 1 1.29 1.25 0.41 o 9 5 1 2.48 2.37 0.52 o 0 6 1 322.41 373.09 20.89 o 1 6 1 63.98 59.89 2.62 o 2 6 1 507.75 577.01 27.24 o 3 6 1 11.07 9.82 0.87 o 4 6 1 47.03 49.27 2.32 o 5 6 1 25.03 24.14 1.05 o 6 6 1 1.20 0.98 0.29 o 7 6 1 0.09 -0.08 0.31 o 8 6 1 2.48 2.19 0.49 o 9 6 1 1.10 0.99 0.45 o 0 7 1 277.61 299.35 14.49 o 1 7 1 127.89 134.66 6.02 o 2 7 1 11.70 9.70 0.78 o 3 7 1 126.41 123.48 4.00 o 4 7 1 28.77 28.46 1.18 o 5 7 1 7.91 9.03 0.52 o 6 7 1 11.11 11.19 0.69 o 7 7 1 4.61 5.19 0.62 o 8 7 1 0.67 0.72 0.41 o 9 7 1 1.38 1.67 0.56 o 0 8 1 7.03 7.52 0.49 o 1 8 1 18.75 20.14 0.80 o 2 8 1 7.45 9.39 0.68 o 3 8 1 85.51 77.05 4.79 o 4 8 1 48.36 49.91 2.46 o 5 8 1 8.96 9.13 0.55 o 6 8 1 0.06 0.43 0.30 o 7 8 1 7.87 8.14 0.74 o 8 8 1 5.06 4.94 0.73 o 9 8 1 2.50 2.07 0.69 o 0 9 1 2.70 2.85 0.36 o 1 9 1 31.17 33.27 1.39 o 2 9 1 8.57 8.63 0.48 o 3 9 1 32.40 30.64 1.68 o 4 9 1 20.16 19.53 1.34 o 5 9 1 57.21 57.06 2.47 o 6 9 1 27.42 25.37 1.89 o 7 9 1 37.50 32.68 1.70 o 8 9 1 4.09 3.44 0.69 o 0 10 1 47.25 44.12 4.65 o 1 10 1 70.35 66.79 3.03 o 2 10 1 90.77 91.36 4.61 o 3 10 1 7.97 7.87 0.67 o 4 10 1 91.53 89.26 4.28 o 5 10 1 62.81 56.97 3.32 o 6 10 1 19.61 18.01 1.09 o 7 10 1 4.68 5.22 0.73 o 8 10 1 0.84 1.54 0.53 o 0 11 1 9.97 10.36 0.85 o 1 11 1 54.25 49.15 2.10 o 2 11 1 75.84 72.19 2.87 o 3 11 1 38.98 36.03 1.52 o 4 11 1 15.45 13.69 1.41 o 5 11 1 10.52 11.55 0.90 o 6 11 1 3.10 2.86 0.56 o 7 11 1 12.20 11.57 1.02 o 0 12 1 8.44 7.75 0.81 o 1 12 1 30.66 26.61 1.33 o 2 12 1 12.02 11.30 0.88 o 3 12 1 17.92 18.98 0.82 o 4 12 1 10.22 8.63 0.67 o 5 12 1 2.37 3.20 0.60 o 6 12 1 0.25 0.40 0.40 o 7 12 1 1.24 1.98 0.52 o 0 13 1 9.17 8.84 1.04 o 1 13 1 17.05 15.27 1.00 o 2 13 1 0.42 0.27 0.29 o 3 13 1 3.06 3.81 0.58 o 4 13 1 1.94 2.23 0.44 o 5 13 1 5.29 5.32 0.70 o 6 13 1 0.93 1.02 0.46 o 0 14 1 4.66 5.44 0.92 o 1 14 1 4.01 3.66 0.62 o 2 14 1 1.80 1.66 0.49 o 3 14 1 9.81 11.84 1.32 o 4 14 1 0.70 0.92 0.42 o 5 14 1 1.51 1.40 0.54 o 0 15 1 1.66 0.97 0.62 o 1 15 1 3.04 2.47 0.57 o 2 15 1 4.35 4.49 0.72 o 3 15 1 0.19 0.17 0.41 o 4 15 1 0.46 1.01 0.45 o 5 15 1 2.38 2.77 0.66 o 0 16 1 0.58 1.54 0.85 o 1 16 1 0.49 0.64 0.51 o 2 16 1 2.64 3.80 0.81 o 3 16 1 0.26 0.70 0.49 o 0 17 1 7.68 9.86 1.62 o 1 17 1 1.21 1.92 0.71 o 0 0 2 10.19 8.53 0.75 o 1 0 2 34.15 30.11 0.81 o 2 0 2 79.42 79.25 2.85 o 3 0 2 438.68 449.41 21.68 o 4 0 2 550.25 603.14 90.04 o 5 0 2 83.92 44.66 24.94 o 6 0 2 44.86 39.78 3.98 o 7 0 2 1.30 1.25 0.53 o 8 0 2 11.00 12.21 1.28 o 9 0 2 0.33 0.00 0.58 o 0 1 2 34.35 29.84 0.79 o 1 1 2 63.77 57.53 0.91 o 2 1 2 101.16 104.66 3.16 o 3 1 2 423.08 489.92 17.44 o 4 1 2 192.15 209.56 10.83 o 5 1 2 47.63 47.92 2.45 o 6 1 2 158.94 161.67 8.76 o 7 1 2 13.57 10.50 2.13 o 8 1 2 10.27 9.82 1.19 o 9 1 2 7.33 7.45 0.84 o 0 2 2 482.20 462.32 9.54 o 1 2 2 479.05 486.97 9.79 o 2 2 2 384.46 403.40 13.79 o 3 2 2 99.77 107.69 4.16 o 4 2 2 34.02 27.91 1.68 o 5 2 2 0.09 0.24 0.21 o 6 2 2 82.90 79.47 4.96 o 7 2 2 21.07 23.42 1.85 o 8 2 2 31.68 30.03 2.78 o 9 2 2 2.38 3.21 0.67 o 0 3 2 35.63 37.41 1.13 o 1 3 2 105.04 115.98 2.65 o 2 3 2 277.69 285.37 9.22 o 3 3 2 38.07 43.27 1.50 o 4 3 2 89.38 106.09 5.58 o 5 3 2 2.49 2.86 0.38 o 6 3 2 13.48 13.31 0.84 o 7 3 2 1.95 1.90 0.48 o 8 3 2 2.59 3.33 0.60 o 9 3 2 8.88 8.58 0.91 o 0 4 2 88.03 87.35 6.18 o 1 4 2 36.48 37.64 1.24 o 2 4 2 92.81 98.38 3.65 o 3 4 2 45.25 48.88 1.79 o 4 4 2 19.90 21.04 1.16 o 5 4 2 9.54 7.51 1.20 o 6 4 2 0.02 0.82 0.30 o 7 4 2 6.28 7.07 0.75 o 8 4 2 2.19 2.19 0.53 o 9 4 2 0.33 0.61 0.43 o 0 5 2 165.34 149.82 27.24 o 1 5 2 147.78 165.30 7.64 o 2 5 2 6.10 5.46 0.34 o 3 5 2 51.61 58.62 2.85 o 4 5 2 67.63 67.89 3.85 o 5 5 2 0.53 0.40 0.22 o 6 5 2 1.69 1.67 0.42 o 7 5 2 9.27 9.81 0.97 o 8 5 2 3.21 3.27 0.61 o 9 5 2 3.48 3.39 0.64 o 0 6 2 14.29 16.55 0.89 o 1 6 2 152.85 168.85 8.16 o 2 6 2 123.62 134.22 6.31 o 3 6 2 8.10 9.32 0.49 o 4 6 2 48.52 43.90 1.95 o 5 6 2 7.47 8.17 0.53 o 6 6 2 6.56 6.78 0.61 o 7 6 2 3.49 3.53 0.57 o 8 6 2 0.38 -0.11 0.34 o 9 6 2 0.25 0.13 0.42 o 0 7 2 0.01 0.15 0.17 o 1 7 2 5.97 6.28 0.37 o 2 7 2 31.34 29.53 1.61 o 3 7 2 7.22 8.79 0.45 o 4 7 2 11.12 11.16 0.59 o 5 7 2 31.08 26.52 1.07 o 6 7 2 11.13 9.88 0.80 o 7 7 2 4.62 5.01 0.64 o 8 7 2 2.32 1.66 0.50 o 0 8 2 0.35 0.57 0.28 o 1 8 2 64.82 61.76 4.24 o 2 8 2 53.17 54.87 3.13 o 3 8 2 92.51 93.28 5.18 o 4 8 2 32.47 35.94 1.68 o 5 8 2 37.51 29.18 2.90 o 6 8 2 13.81 13.79 0.92 o 7 8 2 6.59 5.99 0.72 o 8 8 2 0.30 0.39 0.40 o 0 9 2 12.42 12.52 1.30 o 1 9 2 25.49 25.32 1.34 o 2 9 2 37.49 35.60 2.08 o 3 9 2 76.79 82.45 4.41 o 4 9 2 45.67 43.89 2.48 o 5 9 2 31.37 26.25 2.80 o 6 9 2 5.70 6.26 0.74 o 7 9 2 14.33 13.78 1.08 o 8 9 2 3.78 3.50 0.69 o 0 10 2 86.52 89.92 6.97 o 1 10 2 12.93 13.09 0.67 o 2 10 2 86.31 87.09 5.99 o 3 10 2 26.71 26.91 1.51 o 4 10 2 7.80 7.25 0.61 o 5 10 2 3.38 3.37 0.49 o 6 10 2 5.51 5.96 0.77 o 7 10 2 0.99 1.50 0.52 o 0 11 2 199.20 191.98 17.29 o 1 11 2 20.62 19.11 1.35 o 2 11 2 46.96 46.73 3.17 o 3 11 2 7.31 7.68 0.61 o 4 11 2 0.39 0.71 0.34 o 5 11 2 0.28 0.30 0.32 o 6 11 2 0.76 0.44 0.41 o 7 11 2 0.48 0.72 0.49 o 0 12 2 33.45 33.53 3.72 o 1 12 2 42.39 40.29 2.47 o 2 12 2 32.57 31.48 1.80 o 3 12 2 0.57 0.88 0.35 o 4 12 2 1.31 1.98 0.47 o 5 12 2 0.92 1.42 0.47 o 6 12 2 2.28 2.94 0.69 o 0 13 2 16.14 17.90 1.25 o 1 13 2 1.22 1.06 0.34 o 2 13 2 1.33 1.17 0.35 o 3 13 2 11.59 11.91 0.96 o 4 13 2 1.20 1.17 0.45 o 5 13 2 0.74 0.93 0.52 o 6 13 2 2.26 2.14 0.68 o 0 14 2 1.29 1.11 0.50 o 1 14 2 3.51 3.96 0.51 o 2 14 2 1.01 1.05 0.39 o 3 14 2 1.37 1.23 0.48 o 4 14 2 3.34 4.53 0.74 o 5 14 2 0.15 0.19 0.48 o 0 15 2 1.00 0.63 0.50 o 1 15 2 3.12 3.34 0.53 o 2 15 2 0.59 0.80 0.39 o 3 15 2 2.99 3.94 0.69 o 4 15 2 0.14 0.21 0.47 o 0 16 2 2.51 3.11 0.77 o 1 16 2 0.48 0.73 0.43 o 2 16 2 0.29 0.82 0.43 o 0 0 3 0.48 1.54 0.38 o 1 0 3 2.90 2.60 0.70 o 2 0 3 7.81 7.67 0.41 o 3 0 3 3.35 3.06 0.42 o 4 0 3 3.62 3.22 0.55 o 5 0 3 56.39 49.57 2.22 o 6 0 3 25.36 23.33 1.36 o 7 0 3 5.12 4.09 1.26 o 8 0 3 0.00 -0.10 0.57 o 9 0 3 2.94 1.65 0.89 o 0 1 3 233.54 216.46 5.35 o 1 1 3 34.62 32.50 2.43 o 2 1 3 37.39 37.54 3.20 o 3 1 3 19.03 15.12 1.71 o 4 1 3 25.67 19.11 2.65 o 5 1 3 126.71 87.66 15.84 o 6 1 3 3.52 2.69 0.51 o 7 1 3 43.15 37.07 2.18 o 8 1 3 4.15 4.83 0.78 o 9 1 3 3.26 2.67 0.68 o 0 2 3 165.44 161.40 3.06 o 1 2 3 130.88 129.84 2.49 o 2 2 3 32.68 32.12 0.96 o 3 2 3 101.03 95.99 4.08 o 4 2 3 1.65 1.65 0.29 o 5 2 3 171.22 153.35 6.45 o 6 2 3 13.19 12.91 1.19 o 7 2 3 44.26 36.91 3.12 o 8 2 3 0.02 0.54 0.40 o 9 2 3 0.09 -0.24 0.42 o 0 3 3 11.17 13.09 0.51 o 1 3 3 91.63 95.15 1.43 o 2 3 3 29.63 26.76 0.91 o 3 3 3 28.12 22.73 1.54 o 4 3 3 39.34 37.15 2.09 o 5 3 3 30.67 30.13 1.85 o 6 3 3 4.27 4.26 0.62 o 7 3 3 20.69 19.05 1.25 o 8 3 3 0.80 1.44 0.45 o 9 3 3 0.69 0.75 0.45 o 0 4 3 55.29 63.75 2.36 o 1 4 3 4.50 3.89 0.25 o 2 4 3 31.24 33.52 1.48 o 3 4 3 0.61 0.65 0.25 o 4 4 3 26.13 22.83 1.59 o 5 4 3 3.09 3.00 0.47 o 6 4 3 9.21 7.77 0.71 o 7 4 3 0.43 0.54 0.41 o 8 4 3 1.06 0.37 0.37 o 0 5 3 51.91 56.60 3.06 o 1 5 3 23.60 26.18 1.07 o 2 5 3 18.56 20.11 0.99 o 3 5 3 39.85 39.58 1.91 o 4 5 3 11.42 10.95 0.66 o 5 5 3 1.28 1.06 0.41 o 6 5 3 17.38 13.30 0.97 o 7 5 3 0.16 0.46 0.43 o 8 5 3 4.57 4.74 0.85 o 0 6 3 45.79 43.96 3.12 o 1 6 3 36.81 39.21 1.88 o 2 6 3 12.89 13.36 0.56 o 3 6 3 4.74 4.76 0.40 o 4 6 3 18.20 17.09 1.35 o 5 6 3 9.39 11.13 0.74 o 6 6 3 5.13 5.06 0.59 o 7 6 3 0.12 0.01 0.37 o 8 6 3 0.58 0.82 0.45 o 0 7 3 0.23 0.24 0.25 o 1 7 3 33.09 31.71 1.33 o 2 7 3 15.54 14.61 0.80 o 3 7 3 1.01 1.39 0.31 o 4 7 3 0.73 0.52 0.27 o 5 7 3 10.82 10.54 0.68 o 6 7 3 0.87 1.13 0.39 o 7 7 3 2.00 2.12 0.53 o 8 7 3 4.79 3.84 0.66 o 0 8 3 17.73 11.45 4.90 o 1 8 3 106.02 106.64 5.11 o 2 8 3 20.68 21.57 1.16 o 3 8 3 38.40 38.51 2.44 o 4 8 3 32.71 30.35 2.54 o 5 8 3 5.57 6.06 0.57 o 6 8 3 18.89 19.47 1.15 o 7 8 3 0.91 0.93 0.47 o 0 9 3 52.29 46.33 3.63 o 1 9 3 41.43 42.79 2.03 o 2 9 3 56.27 53.47 3.35 o 3 9 3 27.30 28.99 1.38 o 4 9 3 5.95 5.73 0.64 o 5 9 3 2.41 2.98 0.50 o 6 9 3 6.08 5.30 0.78 o 7 9 3 0.40 1.34 0.53 o 0 10 3 32.68 32.58 2.79 o 1 10 3 17.89 17.84 0.78 o 2 10 3 1.75 2.51 0.43 o 3 10 3 4.25 4.52 0.65 o 4 10 3 6.92 7.76 0.79 o 5 10 3 3.62 3.97 0.70 o 6 10 3 0.22 0.28 0.56 o 7 10 3 0.33 0.82 0.49 o 0 11 3 0.85 0.91 0.44 o 1 11 3 40.39 37.93 3.66 o 2 11 3 25.54 26.47 1.73 o 3 11 3 7.82 7.76 0.68 o 4 11 3 8.90 9.68 0.95 o 5 11 3 2.62 3.41 0.70 o 6 11 3 0.99 1.09 0.69 o 0 12 3 21.75 24.88 2.51 o 1 12 3 19.68 17.25 1.50 o 2 12 3 5.48 5.47 0.65 o 3 12 3 10.01 11.44 0.91 o 4 12 3 12.56 15.45 1.05 o 5 12 3 2.14 2.42 0.65 o 0 13 3 5.64 5.89 0.86 o 1 13 3 0.66 0.68 0.32 o 2 13 3 11.34 11.97 1.17 o 3 13 3 0.31 0.39 0.37 o 4 13 3 2.54 2.43 0.58 o 5 13 3 2.25 2.18 0.65 o 0 14 3 2.07 3.09 0.70 o 1 14 3 0.87 1.07 0.42 o 2 14 3 3.21 3.72 0.57 o 3 14 3 0.88 1.35 0.42 o 0 15 3 0.04 0.28 0.48 o 1 15 3 1.49 1.86 0.49 o 2 15 3 2.60 2.97 0.55 o 0 0 4 0.58 0.28 0.33 o 1 0 4 10.98 9.50 0.82 o 2 0 4 7.97 6.55 0.65 o 3 0 4 6.87 6.09 0.64 o 4 0 4 0.19 0.62 0.53 o 5 0 4 0.00 0.22 0.51 o 6 0 4 0.40 0.67 0.64 o 7 0 4 3.05 2.90 0.99 o 8 0 4 0.00 0.01 0.61 o 0 1 4 51.18 45.08 1.23 o 1 1 4 37.84 32.61 1.16 o 2 1 4 46.27 37.73 2.13 o 3 1 4 10.57 12.54 0.65 o 4 1 4 2.68 1.84 0.46 o 5 1 4 7.29 7.00 0.73 o 6 1 4 3.76 2.48 0.62 o 7 1 4 3.57 4.12 0.77 o 8 1 4 7.14 6.23 0.87 o 0 2 4 0.29 0.17 0.20 o 1 2 4 6.39 4.49 0.58 o 2 2 4 37.85 34.28 1.08 o 3 2 4 126.33 124.37 5.93 o 4 2 4 41.82 37.23 1.31 o 5 2 4 2.71 1.64 0.45 o 6 2 4 15.68 11.94 1.29 o 7 2 4 5.04 4.55 0.82 o 8 2 4 1.53 0.86 0.43 o 0 3 4 25.37 26.15 0.81 o 1 3 4 32.03 29.43 0.80 o 2 3 4 13.76 13.75 0.68 o 3 3 4 18.18 17.48 0.82 o 4 3 4 35.14 32.94 1.15 o 5 3 4 25.45 25.25 1.07 o 6 3 4 6.31 5.96 0.70 o 7 3 4 3.33 3.70 0.62 o 0 4 4 9.28 8.62 0.71 o 1 4 4 3.24 3.20 0.36 o 2 4 4 8.05 10.12 0.59 o 3 4 4 42.31 40.08 2.05 o 4 4 4 0.69 0.47 0.30 o 5 4 4 0.87 0.54 0.35 o 6 4 4 0.50 0.61 0.38 o 7 4 4 3.95 2.87 0.65 o 0 5 4 4.02 4.33 0.58 o 1 5 4 4.14 4.06 0.41 o 2 5 4 1.89 2.07 0.37 o 3 5 4 0.14 0.55 0.26 o 4 5 4 8.24 8.62 0.62 o 5 5 4 12.22 10.99 0.79 o 6 5 4 1.98 1.39 0.46 o 7 5 4 2.64 2.07 0.56 o 0 6 4 9.12 9.84 0.81 o 1 6 4 0.57 0.68 0.26 o 2 6 4 14.77 15.28 0.78 o 3 6 4 1.64 1.45 0.37 o 4 6 4 7.54 6.84 0.57 o 5 6 4 0.74 0.73 0.36 o 6 6 4 1.49 2.14 0.48 o 7 6 4 2.37 2.86 0.62 o 0 7 4 44.31 41.31 2.88 o 1 7 4 1.35 1.62 0.32 o 2 7 4 14.29 13.81 0.86 o 3 7 4 6.31 5.77 0.65 o 4 7 4 3.09 3.66 0.52 o 5 7 4 3.48 3.56 0.58 o 6 7 4 0.39 0.39 0.37 o 7 7 4 0.91 1.18 0.56 o 0 8 4 24.23 24.61 2.08 o 1 8 4 45.64 39.58 3.12 o 2 8 4 35.94 35.18 2.29 o 3 8 4 3.75 4.42 0.58 o 4 8 4 5.11 6.39 0.69 o 5 8 4 2.00 2.05 0.49 o 6 8 4 0.08 0.03 0.37 o 0 9 4 21.16 20.85 1.92 o 1 9 4 13.31 13.20 0.82 o 2 9 4 14.56 16.61 1.00 o 3 9 4 14.16 15.07 0.99 o 4 9 4 4.53 5.25 0.68 o 5 9 4 1.04 1.22 0.50 o 6 9 4 0.09 0.22 0.48 o 0 10 4 2.84 3.64 0.80 o 1 10 4 5.20 5.71 0.61 o 2 10 4 1.15 1.23 0.42 o 3 10 4 1.49 0.69 0.42 o 4 10 4 1.91 1.56 0.53 o 5 10 4 2.57 2.85 0.64 o 0 11 4 0.70 0.82 0.56 o 1 11 4 4.03 4.93 0.60 o 2 11 4 1.76 1.91 0.50 o 3 11 4 2.24 2.39 0.53 o 4 11 4 14.09 20.19 1.64 o 0 12 4 0.95 1.22 0.61 o 1 12 4 1.00 1.00 0.39 o 2 12 4 1.47 1.63 0.48 o 3 12 4 13.32 13.82 1.05 o 4 12 4 1.65 1.73 0.55 o 0 13 4 0.46 0.60 0.51 o 1 13 4 0.92 1.26 0.43 o 2 13 4 1.00 1.63 0.49 o 0 0 5 0.08 0.60 0.75 o 1 0 5 4.26 5.35 0.79 o 2 0 5 1.23 0.96 0.48 o 3 0 5 5.77 3.96 0.97 o 4 0 5 5.55 5.60 1.17 o 5 0 5 4.69 4.37 1.12 o 6 0 5 4.11 5.26 1.20 o 0 1 5 11.87 16.16 1.47 o 1 1 5 15.48 15.52 1.01 o 2 1 5 7.79 7.81 0.60 o 3 1 5 0.95 1.24 0.51 o 4 1 5 0.50 0.39 0.44 o 5 1 5 3.19 4.62 0.80 o 6 1 5 2.10 2.89 0.68 o 0 2 5 5.49 5.27 1.06 o 1 2 5 50.64 51.51 1.38 o 2 2 5 8.94 8.96 0.93 o 3 2 5 10.67 8.44 1.52 o 4 2 5 5.26 5.98 0.85 o 5 2 5 1.43 2.41 0.63 o 6 2 5 0.19 0.29 0.46 o 0 3 5 2.19 2.99 0.86 o 1 3 5 36.55 36.83 1.71 o 2 3 5 16.65 14.30 1.53 o 3 3 5 19.27 19.00 0.90 o 4 3 5 3.28 3.26 0.55 o 5 3 5 0.05 0.41 0.42 o 6 3 5 0.50 1.18 0.54 o 0 4 5 1.79 2.27 0.77 o 1 4 5 27.00 25.95 1.07 o 2 4 5 6.08 5.89 0.72 o 3 4 5 0.12 0.06 0.30 o 4 4 5 2.70 2.01 0.48 o 5 4 5 0.01 0.14 0.44 o 6 4 5 3.56 3.40 0.68 o 0 5 5 2.35 1.41 0.73 o 1 5 5 0.43 0.30 0.37 o 2 5 5 0.60 1.09 0.36 o 3 5 5 0.80 1.00 0.38 o 4 5 5 3.52 3.16 0.56 o 5 5 5 2.70 3.27 0.58 o 6 5 5 0.92 1.20 0.49 o 0 6 5 2.12 3.17 1.29 o 1 6 5 1.48 1.85 0.49 o 2 6 5 0.91 1.78 0.46 o 3 6 5 4.63 4.30 0.58 o 4 6 5 1.19 1.47 0.45 o 5 6 5 1.54 1.43 0.45 o 0 7 5 6.40 8.73 1.43 o 1 7 5 4.60 5.09 0.70 o 2 7 5 6.90 8.75 0.91 o 3 7 5 1.54 2.49 0.54 o 4 7 5 4.73 5.32 0.71 o 5 7 5 0.73 1.04 0.45 o 0 8 5 3.83 6.20 1.26 o 1 8 5 10.56 11.75 1.01 o 2 8 5 6.10 7.40 0.84 o 3 8 5 4.60 5.26 0.70 o 4 8 5 3.19 4.54 0.74 o 0 9 5 7.63 10.44 1.90 o 1 9 5 1.23 1.55 0.51 o 2 9 5 5.80 7.95 0.91 o 3 9 5 2.07 1.33 0.45 o 4 9 5 1.76 2.34 0.68 o 0 10 5 6.90 7.63 1.35 o 1 10 5 0.25 0.28 0.39 o 2 10 5 4.32 3.85 0.74 o 3 10 5 0.96 0.94 0.49 o 0 11 5 0.90 0.88 0.69 o 1 11 5 0.22 0.75 0.48 o 0 0 6 0.98 0.36 0.93 o 1 0 6 0.79 0.99 1.05 o 3 0 6 0.26 0.66 1.05 o 4 0 6 6.18 8.10 1.53 o 0 1 6 0.02 -0.30 0.84 o 1 1 6 0.13 0.16 0.52 o 2 1 6 0.95 1.41 0.64 o 3 1 6 3.11 4.61 1.65 o 4 1 6 1.50 1.90 0.66 o 0 2 6 9.60 12.45 1.65 o 1 2 6 8.17 10.14 1.25 o 2 2 6 3.64 4.66 0.95 o 3 2 6 1.47 4.01 1.06 o 4 2 6 0.17 -0.08 0.51 o 0 3 6 21.03 20.55 2.01 o 1 3 6 1.34 1.15 0.53 o 2 3 6 8.28 11.86 1.34 o 3 3 6 4.36 5.21 1.13 o 0 4 6 13.47 15.78 1.86 o 1 4 6 4.30 6.28 0.89 o 2 4 6 5.65 4.79 0.92 o 3 4 6 0.40 0.66 0.53 o 0 5 6 3.43 3.21 0.95 o 1 5 6 0.86 0.67 0.48 o 2 5 6 0.39 0.34 0.61 o 0 6 6 0.01 -0.13 0.53 o 1 6 6 1.19 1.81 0.55 o 2 6 6 0.18 0.99 0.53 o 0 7 6 0.93 1.56 0.99 o