#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220142.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220142_Fobs loop_ _publ_author_name 'Yang, Jin-hui' 'Chen, Yan-xue' 'Wang, Shao-hui' 'Wang, Jian-lei' _publ_section_title ; N-(2-Formamidoethyl)formamide ; _journal_coeditor_code DN2396 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2418 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7138 _cell_length_b 6.6714 _cell_length_c 9.3162 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file dn2396Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R80915E1 in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 44.32 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 254.55 252.78 11.31 o 6 0 0 121.09 130.16 3.00 o 8 0 0 0.01 0.54 1.49 o 10 0 0 158.57 166.01 6.43 o 2 1 0 447.89 434.91 11.09 o 4 1 0 12.51 13.33 0.51 o 6 1 0 245.40 245.56 4.10 o 8 1 0 7.27 7.47 0.62 o 10 1 0 3.48 5.47 0.92 o 4 2 0 1.73 2.35 0.29 o 6 2 0 38.27 41.17 1.24 o 8 2 0 31.46 35.33 1.28 o 10 2 0 85.69 88.79 3.72 o 2 3 0 572.53 582.74 8.09 o 4 3 0 18.97 17.37 0.52 o 6 3 0 604.67 613.37 11.05 o 8 3 0 2.57 2.18 0.58 o 0 4 0 1305.71 1301.75 37.93 o 2 4 0 1470.94 1520.17 40.83 o 4 4 0 78.99 77.31 1.57 o 6 4 0 1.13 1.20 0.51 o 8 4 0 201.23 216.66 6.92 o 2 5 0 82.57 77.83 1.80 o 4 5 0 147.64 149.27 2.02 o 6 5 0 149.47 146.16 3.03 o 8 5 0 26.07 29.97 1.38 o 0 6 0 100.74 96.19 3.70 o 2 6 0 238.29 245.99 5.93 o 4 6 0 29.85 30.14 1.35 o 6 6 0 5.34 4.92 1.42 o 2 7 0 0.42 2.21 0.81 o 4 7 0 142.04 155.26 4.93 o 1 1 1 1549.78 1488.60 34.48 o 3 1 1 16.27 16.71 0.37 o 4 1 1 864.33 918.43 4.33 o 5 1 1 728.90 769.68 9.14 o 6 1 1 2.42 0.60 0.24 o 7 1 1 394.46 391.47 5.77 o 8 1 1 6.40 5.02 0.41 o 9 1 1 0.09 1.10 0.69 o 10 1 1 82.48 87.49 1.90 o 0 2 1 161.45 149.81 1.31 o 1 2 1 1133.71 1097.73 38.93 o 2 2 1 15.99 16.08 0.31 o 3 2 1 18.88 18.56 0.60 o 4 2 1 37.05 41.75 0.76 o 5 2 1 255.85 276.43 3.85 o 6 2 1 0.17 0.31 0.30 o 7 2 1 232.85 234.72 3.08 o 8 2 1 5.22 4.90 0.44 o 9 2 1 0.04 0.22 0.33 o 1 3 1 161.92 151.74 1.90 o 2 3 1 1220.12 1202.44 17.82 o 3 3 1 82.10 81.62 1.22 o 4 3 1 337.79 345.40 2.81 o 5 3 1 68.61 71.99 1.15 o 6 3 1 10.11 7.62 0.44 o 7 3 1 97.07 102.00 1.75 o 8 3 1 4.62 4.16 0.53 o 9 3 1 33.54 36.07 0.96 o 0 4 1 68.30 73.37 5.65 o 1 4 1 572.15 531.63 5.95 o 2 4 1 40.93 40.39 0.65 o 3 4 1 32.38 31.63 0.63 o 4 4 1 25.58 25.16 0.51 o 5 4 1 58.34 60.20 0.89 o 6 4 1 0.93 1.15 0.27 o 7 4 1 125.14 121.86 1.44 o 8 4 1 9.08 8.81 0.56 o 1 5 1 216.14 221.55 5.55 o 2 5 1 251.63 244.03 5.44 o 3 5 1 4.71 4.17 0.30 o 4 5 1 106.04 107.35 1.11 o 5 5 1 4.10 3.19 0.55 o 6 5 1 26.03 26.48 0.77 o 7 5 1 0.29 0.56 0.41 o 8 5 1 1.40 1.64 0.68 o 0 6 1 11.62 12.37 1.45 o 1 6 1 94.19 93.39 2.54 o 2 6 1 27.63 29.56 1.06 o 3 6 1 94.80 100.96 3.10 o 4 6 1 13.27 12.22 0.72 o 5 6 1 9.97 11.99 0.99 o 6 6 1 1.41 1.45 0.66 o 1 7 1 51.26 51.70 1.77 o 2 7 1 61.04 60.28 1.81 o 3 7 1 17.12 18.07 0.83 o 4 7 1 16.62 15.85 1.34 o 0 0 2 9.64 3.51 0.44 o 3 0 2 1426.86 1462.73 23.82 o 4 0 2 1099.48 1046.12 78.13 o 5 0 2 620.67 573.20 6.36 o 6 0 2 1.67 2.40 0.41 o 7 0 2 0.16 0.23 0.27 o 8 0 2 641.30 559.03 15.89 o 9 0 2 51.86 49.29 2.77 o 10 0 2 133.67 140.16 6.02 o 1 1 2 76.63 69.39 1.22 o 2 1 2 234.76 225.81 1.43 o 3 1 2 12.20 11.62 0.31 o 4 1 2 31.54 33.50 0.74 o 5 1 2 50.04 58.50 0.94 o 6 1 2 144.48 143.07 2.19 o 7 1 2 5.25 4.89 0.42 o 8 1 2 13.74 14.90 0.61 o 9 1 2 0.27 0.60 0.57 o 10 1 2 2.81 4.11 0.84 o 0 2 2 1041.68 994.24 9.84 o 1 2 2 450.63 400.66 3.73 o 2 2 2 255.28 226.65 1.83 o 3 2 2 706.07 686.02 4.98 o 4 2 2 310.02 311.02 3.36 o 5 2 2 513.22 495.64 5.98 o 6 2 2 2.70 3.04 0.36 o 7 2 2 1.11 1.60 0.37 o 8 2 2 335.92 324.77 3.96 o 9 2 2 26.59 29.04 1.10 o 1 3 2 122.68 121.23 1.59 o 2 3 2 334.79 338.28 4.74 o 3 3 2 86.05 85.89 1.36 o 4 3 2 2.69 2.73 0.23 o 5 3 2 126.19 125.21 2.26 o 6 3 2 326.16 327.54 2.89 o 7 3 2 43.83 47.24 1.18 o 8 3 2 19.45 20.76 0.68 o 9 3 2 0.45 0.97 0.45 o 0 4 2 1963.99 1951.37 54.52 o 1 4 2 9.26 9.46 0.39 o 2 4 2 14.97 18.59 0.44 o 3 4 2 256.80 245.82 3.69 o 4 4 2 2.11 2.28 0.24 o 5 4 2 171.31 170.04 2.39 o 6 4 2 1.24 1.28 0.38 o 7 4 2 39.96 39.57 0.97 o 8 4 2 44.45 44.55 1.05 o 1 5 2 13.43 13.33 0.71 o 2 5 2 46.22 49.08 0.99 o 3 5 2 84.49 81.76 1.11 o 4 5 2 51.95 55.99 1.25 o 5 5 2 64.37 58.63 1.47 o 6 5 2 41.84 39.09 0.93 o 7 5 2 32.32 33.49 1.01 o 0 6 2 1020.51 1065.87 48.72 o 1 6 2 6.88 7.45 0.66 o 2 6 2 43.58 42.34 1.61 o 3 6 2 64.83 62.98 1.37 o 4 6 2 9.99 8.00 0.71 o 5 6 2 65.07 62.36 2.40 o 6 6 2 0.73 0.68 0.60 o 1 7 2 0.02 0.43 0.48 o 2 7 2 0.97 1.06 0.54 o 3 7 2 26.48 24.34 1.02 o 4 7 2 83.78 99.04 3.59 o 2 1 3 55.76 53.12 0.75 o 3 1 3 301.98 324.17 3.60 o 4 1 3 25.36 33.51 0.73 o 5 1 3 3.24 4.03 0.28 o 6 1 3 525.85 502.90 11.18 o 7 1 3 125.47 136.83 1.84 o 8 1 3 64.08 68.92 1.79 o 9 1 3 161.42 151.77 6.71 o 0 2 3 768.42 827.25 10.03 o 1 2 3 203.53 200.92 2.16 o 2 2 3 41.42 42.53 0.62 o 3 2 3 78.23 82.87 0.97 o 4 2 3 32.62 35.94 0.66 o 5 2 3 150.99 156.00 2.06 o 6 2 3 21.18 21.98 0.64 o 7 2 3 150.64 153.48 3.85 o 8 2 3 40.90 35.79 0.98 o 9 2 3 3.50 4.64 0.60 o 1 3 3 91.35 100.61 1.42 o 2 3 3 143.39 130.89 2.12 o 3 3 3 392.40 386.76 4.56 o 4 3 3 1.80 1.72 0.29 o 5 3 3 15.80 16.53 0.63 o 6 3 3 120.78 120.83 3.18 o 7 3 3 191.82 196.32 3.13 o 8 3 3 37.28 41.99 1.17 o 9 3 3 28.71 26.10 0.91 o 0 4 3 460.59 429.55 9.98 o 1 4 3 80.12 82.66 1.41 o 2 4 3 98.51 89.68 1.53 o 3 4 3 4.54 4.67 0.31 o 4 4 3 9.62 7.92 0.44 o 5 4 3 30.19 29.47 0.69 o 6 4 3 16.41 14.32 0.70 o 7 4 3 82.23 78.70 1.74 o 8 4 3 66.33 65.30 1.32 o 1 5 3 22.04 20.38 1.06 o 2 5 3 214.24 220.96 5.71 o 3 5 3 190.62 185.32 2.96 o 4 5 3 16.06 15.60 0.56 o 5 5 3 60.89 56.61 1.11 o 6 5 3 3.41 3.62 0.58 o 7 5 3 177.35 187.35 3.34 o 0 6 3 56.07 47.44 2.87 o 1 6 3 0.82 1.10 0.53 o 2 6 3 69.30 65.99 2.12 o 3 6 3 16.72 19.60 0.85 o 4 6 3 0.01 0.26 0.28 o 5 6 3 22.92 23.51 1.09 o 6 6 3 10.28 9.30 0.79 o 1 7 3 1.49 1.10 0.59 o 2 7 3 108.32 111.93 3.02 o 3 7 3 14.75 13.29 0.84 o 4 7 3 67.63 67.16 2.42 o 1 0 4 1029.39 1190.19 22.13 o 2 0 4 8.94 14.00 0.50 o 3 0 4 371.37 324.92 4.59 o 4 0 4 6.83 6.31 0.41 o 5 0 4 788.48 776.21 8.57 o 6 0 4 18.15 17.05 0.92 o 7 0 4 464.86 457.45 8.12 o 8 0 4 3.03 1.72 0.77 o 9 0 4 26.35 22.35 1.95 o 1 1 4 52.14 54.01 1.59 o 2 1 4 35.45 35.57 0.74 o 3 1 4 8.60 8.29 0.36 o 4 1 4 53.47 55.35 0.95 o 5 1 4 53.55 57.06 1.04 o 6 1 4 45.70 46.27 0.89 o 7 1 4 13.90 11.90 0.64 o 8 1 4 17.70 18.34 0.81 o 9 1 4 0.14 0.49 0.58 o 0 2 4 963.56 1011.43 7.24 o 1 2 4 440.52 429.98 3.39 o 2 2 4 7.64 4.79 0.21 o 3 2 4 358.91 358.58 3.26 o 4 2 4 19.52 17.66 0.55 o 5 2 4 658.39 672.99 11.12 o 6 2 4 23.86 22.00 0.62 o 7 2 4 287.06 287.78 4.25 o 8 2 4 3.21 3.86 0.77 o 9 2 4 15.24 15.96 0.86 o 1 3 4 143.50 143.00 3.28 o 2 3 4 53.18 55.36 1.32 o 3 3 4 44.87 44.84 0.89 o 4 3 4 92.84 95.00 1.41 o 5 3 4 179.61 178.04 2.15 o 6 3 4 100.21 98.37 1.80 o 7 3 4 77.94 79.38 1.63 o 8 3 4 39.41 37.36 1.10 o 0 4 4 11.72 13.98 0.90 o 1 4 4 2.01 0.96 0.42 o 2 4 4 138.03 128.34 2.06 o 3 4 4 180.96 187.96 2.44 o 4 4 4 72.17 63.78 1.00 o 5 4 4 583.11 584.76 7.21 o 6 4 4 12.33 11.86 0.64 o 7 4 4 37.44 35.23 1.09 o 8 4 4 34.90 35.02 1.01 o 1 5 4 11.19 12.47 1.05 o 2 5 4 0.13 -0.01 0.73 o 3 5 4 64.96 68.55 2.15 o 4 5 4 0.13 0.19 0.19 o 5 5 4 93.60 90.68 1.48 o 6 5 4 1.95 2.13 0.63 o 7 5 4 47.72 51.20 1.31 o 0 6 4 4.44 4.61 0.76 o 1 6 4 62.66 67.23 3.04 o 2 6 4 80.59 73.71 1.79 o 3 6 4 146.82 142.20 3.04 o 4 6 4 44.18 40.06 1.46 o 5 6 4 305.98 320.28 4.76 o 1 7 4 5.18 5.85 0.84 o 2 7 4 13.53 14.20 0.97 o 3 7 4 25.79 28.97 1.12 o 1 1 5 93.05 98.58 1.94 o 2 1 5 429.66 494.91 6.49 o 3 1 5 1113.83 1190.63 13.61 o 4 1 5 143.23 152.84 2.29 o 5 1 5 15.78 14.16 0.57 o 6 1 5 163.84 160.67 2.83 o 7 1 5 328.69 312.96 3.54 o 8 1 5 0.75 1.06 0.57 o 9 1 5 12.06 10.48 1.04 o 0 2 5 391.34 412.84 8.00 o 1 2 5 2.64 2.15 0.54 o 2 2 5 9.62 10.31 0.64 o 3 2 5 87.41 87.34 1.29 o 4 2 5 32.76 30.96 0.82 o 5 2 5 99.85 99.79 1.32 o 6 2 5 8.44 9.28 0.51 o 7 2 5 29.21 29.72 1.11 o 8 2 5 57.76 54.48 1.53 o 1 3 5 216.33 198.82 2.69 o 2 3 5 67.39 74.92 1.28 o 3 3 5 301.93 304.06 5.38 o 4 3 5 67.71 65.97 0.99 o 5 3 5 19.98 20.96 0.70 o 6 3 5 2.49 2.45 0.65 o 7 3 5 180.47 180.73 3.37 o 8 3 5 0.43 0.48 0.60 o 0 4 5 312.71 322.27 6.31 o 1 4 5 0.04 0.21 0.39 o 2 4 5 31.18 30.93 1.02 o 3 4 5 32.46 30.22 0.96 o 4 4 5 26.01 22.05 0.68 o 5 4 5 41.12 40.22 0.91 o 6 4 5 12.55 11.09 0.71 o 7 4 5 3.23 2.58 0.70 o 1 5 5 280.31 280.83 5.15 o 2 5 5 4.21 4.78 0.67 o 3 5 5 5.07 6.73 0.83 o 4 5 5 11.82 12.15 0.68 o 5 5 5 11.19 13.29 0.77 o 6 5 5 64.49 64.47 2.03 o 0 6 5 16.14 19.07 1.88 o 1 6 5 1.61 0.84 0.56 o 2 6 5 58.07 62.02 2.15 o 3 6 5 6.25 6.98 0.76 o 4 6 5 0.47 0.62 0.59 o 1 7 5 42.78 43.79 1.74 o 0 0 6 69.16 71.87 3.59 o 1 0 6 114.51 143.77 3.79 o 2 0 6 62.90 62.55 1.90 o 3 0 6 471.41 446.56 7.64 o 4 0 6 49.32 54.40 1.50 o 5 0 6 952.98 907.94 8.55 o 6 0 6 72.31 73.73 1.81 o 7 0 6 14.88 14.04 0.86 o 8 0 6 32.22 36.88 1.90 o 1 1 6 35.79 35.38 1.29 o 2 1 6 0.45 0.34 0.29 o 3 1 6 4.41 4.95 0.42 o 4 1 6 60.80 58.71 1.16 o 5 1 6 19.53 19.69 0.69 o 6 1 6 3.48 3.65 0.52 o 7 1 6 10.27 8.83 0.69 o 8 1 6 18.37 18.18 1.09 o 0 2 6 46.81 53.57 2.10 o 1 2 6 30.70 37.68 1.50 o 2 2 6 8.25 7.77 0.78 o 3 2 6 430.91 411.99 4.95 o 4 2 6 37.97 42.81 0.99 o 5 2 6 609.59 589.38 7.84 o 6 2 6 39.94 41.40 0.93 o 7 2 6 0.81 1.13 0.47 o 8 2 6 44.73 49.37 1.32 o 1 3 6 145.95 152.17 3.16 o 2 3 6 0.11 0.36 0.39 o 3 3 6 17.95 18.30 0.81 o 4 3 6 204.90 201.75 3.01 o 5 3 6 96.06 97.27 1.76 o 6 3 6 3.12 3.12 0.56 o 7 3 6 39.12 39.48 1.21 o 0 4 6 0.55 0.50 1.07 o 1 4 6 6.56 6.26 0.59 o 2 4 6 105.09 101.00 2.22 o 3 4 6 326.00 328.92 5.29 o 4 4 6 3.13 3.62 0.76 o 5 4 6 177.44 182.66 3.16 o 6 4 6 14.59 13.55 0.84 o 1 5 6 20.27 22.51 1.49 o 2 5 6 10.51 8.57 0.84 o 3 5 6 52.47 54.18 1.94 o 4 5 6 39.41 35.74 1.16 o 5 5 6 57.62 55.91 1.64 o 0 6 6 1.57 2.58 1.06 o 1 6 6 26.12 29.07 1.78 o 2 6 6 151.98 152.72 3.86 o 3 6 6 119.82 124.75 3.42 o 1 1 7 215.78 226.29 4.67 o 2 1 7 252.76 247.56 6.14 o 3 1 7 0.09 0.50 0.31 o 4 1 7 31.25 26.37 0.77 o 5 1 7 195.40 192.06 3.10 o 6 1 7 119.16 110.81 1.51 o 7 1 7 362.21 371.09 3.83 o 0 2 7 169.02 172.83 5.99 o 1 2 7 37.59 34.02 1.43 o 2 2 7 3.12 2.90 0.72 o 3 2 7 89.83 84.94 1.81 o 4 2 7 20.46 19.77 0.79 o 5 2 7 43.79 46.65 1.02 o 6 2 7 0.13 0.34 0.36 o 7 2 7 4.63 4.61 0.72 o 1 3 7 44.31 44.33 1.69 o 2 3 7 48.05 46.17 1.84 o 3 3 7 55.30 51.93 2.03 o 4 3 7 76.71 69.22 1.66 o 5 3 7 80.02 77.17 1.66 o 6 3 7 1.56 1.35 0.44 o 7 3 7 246.22 248.85 3.87 o 0 4 7 148.60 162.21 6.07 o 1 4 7 75.04 71.49 2.72 o 2 4 7 0.97 0.92 0.72 o 3 4 7 79.06 76.68 1.87 o 4 4 7 22.86 20.82 1.05 o 5 4 7 21.77 21.44 0.97 o 6 4 7 0.90 0.79 0.50 o 1 5 7 0.15 0.73 0.99 o 2 5 7 0.19 0.51 1.01 o 3 5 7 173.60 169.79 3.99 o 4 5 7 57.47 56.47 1.96 o 0 6 7 4.20 4.25 1.54 o 1 6 7 61.24 62.82 2.47 o 0 0 8 811.70 865.07 16.38 o 1 0 8 146.38 161.65 4.43 o 2 0 8 853.32 925.55 15.84 o 3 0 8 183.90 184.85 5.75 o 4 0 8 4.78 3.10 1.00 o 5 0 8 25.69 26.32 1.32 o 6 0 8 0.83 1.25 0.63 o 7 0 8 86.16 83.43 2.06 o 1 1 8 19.82 20.15 1.22 o 2 1 8 1.13 1.64 0.44 o 3 1 8 7.00 7.10 0.97 o 4 1 8 46.89 45.59 1.45 o 5 1 8 1.42 1.83 0.59 o 6 1 8 0.37 0.38 0.39 o 7 1 8 3.06 2.83 1.06 o 0 2 8 688.59 695.47 11.74 o 1 2 8 77.63 85.85 2.55 o 2 2 8 485.74 498.12 10.56 o 3 2 8 73.04 81.50 2.24 o 4 2 8 9.89 7.44 0.70 o 5 2 8 85.89 85.49 1.96 o 6 2 8 0.09 0.46 0.47 o 1 3 8 55.20 59.44 2.00 o 2 3 8 7.63 8.53 1.12 o 3 3 8 22.30 19.34 1.02 o 4 3 8 199.43 212.64 4.52 o 5 3 8 7.74 9.59 0.77 o 6 3 8 7.83 7.92 0.72 o 0 4 8 471.23 491.33 15.32 o 1 4 8 12.46 12.24 1.27 o 2 4 8 58.18 56.35 2.25 o 3 4 8 2.96 3.22 1.00 o 4 4 8 22.89 20.40 1.18 o 1 5 8 0.34 1.43 1.07 o 2 5 8 24.61 23.86 1.57 o 1 1 9 24.34 25.83 1.38 o 2 1 9 90.14 81.19 2.26 o 3 1 9 386.20 398.64 12.20 o 4 1 9 232.60 217.79 5.09 o 5 1 9 49.02 47.90 1.50 o 0 2 9 32.51 36.36 2.83 o 1 2 9 28.37 30.66 1.89 o 2 2 9 72.94 68.15 2.29 o 3 2 9 53.42 50.98 2.25 o 4 2 9 3.41 3.33 0.92 o 5 2 9 13.96 14.86 1.00 o 1 3 9 56.72 54.70 2.69 o 2 3 9 139.58 131.50 5.04 o 3 3 9 97.45 95.17 2.79 o 4 3 9 32.44 28.40 1.41 o 0 4 9 2.92 5.55 1.64 o 1 4 9 56.15 58.15 2.41 o 2 4 9 48.25 44.64 2.11 o 3 4 9 60.81 58.24 1.75 o 0 0 10 253.94 269.58 10.43 o 1 0 10 136.42 132.02 5.58 o 2 0 10 0.09 0.47 1.16 o 3 0 10 131.40 127.96 4.61 o 4 0 10 4.03 3.53 3.13 o 1 1 10 18.77 17.48 1.39 o 2 1 10 0.50 0.83 0.65 o 3 1 10 21.52 22.13 1.57 o 4 1 10 17.12 18.37 1.18 o 0 2 10 192.33 202.60 6.02 o 1 2 10 125.80 118.64 3.49 o 2 2 10 16.27 16.57 1.23 o 3 2 10 38.62 36.42 1.77 o 1 3 10 35.02 34.92 1.97 o 2 3 10 4.24 6.77 1.53 o