#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/01/2220156.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220156_Fobs loop_ _publ_author_name 'Bon, V. V.' 'Dudko, A. V.' 'Kozachkova, A. N.' 'Pekhnyo, V. I.' _publ_section_title ; 1-Ammonio-1-phosphonopentane-1-phosphonic acid ; _journal_coeditor_code EZ2151 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2436 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.938 _cell_angle_gamma 90.000 _cell_length_a 14.5502 _cell_length_b 7.1896 _cell_length_c 9.4855 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7461 _[local]_cod_data_source_file ez2151Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 82 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 153.84 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4658.04 4736.64 44.84 o 3 0 0 10732.69 10602.68 124.37 o 4 0 0 556.89 491.61 7.05 o 5 0 0 1663.43 1599.14 23.08 o 6 0 0 260.34 229.13 5.25 o 7 0 0 64.90 98.31 3.53 o 8 0 0 831.27 877.47 12.65 o 9 0 0 3260.74 3197.34 38.05 o 10 0 0 2666.45 2556.55 31.56 o 11 0 0 65.57 70.01 3.68 o 12 0 0 730.80 691.72 11.74 o 13 0 0 53.96 62.35 4.84 o 14 0 0 661.82 645.85 14.47 o 15 0 0 813.77 821.64 17.32 o 16 0 0 1372.43 1376.95 27.65 o 17 0 0 175.30 178.75 10.60 o 18 0 0 23.63 26.01 7.07 o 19 0 0 407.78 426.56 22.26 o 1 1 0 1542.23 1624.20 11.30 o 2 1 0 0.19 -0.63 0.63 o 3 1 0 14863.97 15036.88 107.25 o 4 1 0 2093.37 2061.51 16.68 o 5 1 0 1591.77 1709.03 14.69 o 6 1 0 1438.30 1515.78 13.89 o 7 1 0 296.62 313.85 4.91 o 8 1 0 444.02 437.38 5.47 o 9 1 0 116.82 130.07 3.03 o 10 1 0 1396.86 1390.82 13.44 o 11 1 0 2513.61 2415.71 22.77 o 12 1 0 1713.94 1667.09 17.27 o 13 1 0 930.98 922.66 12.51 o 14 1 0 252.49 245.57 5.95 o 15 1 0 84.45 80.43 4.54 o 16 1 0 18.15 14.11 3.41 o 17 1 0 40.92 51.44 5.19 o 18 1 0 93.29 98.90 7.38 o 19 1 0 186.90 193.10 9.71 o 0 2 0 4231.32 4246.13 44.30 o 1 2 0 4691.02 4829.92 34.09 o 2 2 0 1921.50 2050.64 16.86 o 3 2 0 392.62 407.82 4.18 o 4 2 0 4609.20 4459.87 36.29 o 5 2 0 185.77 265.87 5.72 o 6 2 0 3165.72 3560.56 30.66 o 7 2 0 2343.42 2346.38 20.74 o 8 2 0 375.04 359.05 5.30 o 9 2 0 657.96 682.22 8.53 o 10 2 0 266.88 298.47 5.49 o 11 2 0 789.38 748.72 10.51 o 12 2 0 560.94 547.36 8.50 o 13 2 0 109.06 113.37 4.60 o 14 2 0 1429.76 1400.02 18.22 o 15 2 0 15.82 17.24 3.39 o 16 2 0 19.17 26.29 3.88 o 17 2 0 3.59 6.61 4.66 o 18 2 0 15.95 18.96 4.91 o 1 3 0 14273.68 14697.26 111.63 o 2 3 0 2951.55 2952.09 28.64 o 3 3 0 1359.08 1414.58 13.31 o 4 3 0 386.25 434.83 5.72 o 5 3 0 791.38 861.45 9.16 o 6 3 0 182.71 213.13 3.97 o 7 3 0 450.89 464.20 6.97 o 8 3 0 1327.27 1301.86 14.65 o 9 3 0 1.32 -1.71 1.71 o 10 3 0 81.52 88.97 3.75 o 11 3 0 1684.41 1642.44 19.30 o 12 3 0 123.84 130.28 5.50 o 13 3 0 317.05 320.15 9.06 o 14 3 0 2.46 -2.55 2.55 o 15 3 0 596.01 597.51 12.76 o 16 3 0 338.54 366.82 10.36 o 17 3 0 1274.57 1297.23 22.85 o 18 3 0 779.95 799.86 18.61 o 0 4 0 2650.02 2761.20 35.48 o 1 4 0 3.56 21.43 1.98 o 2 4 0 195.67 199.89 3.69 o 3 4 0 1052.56 1040.23 11.20 o 4 4 0 3404.43 3319.26 37.23 o 5 4 0 2739.68 2739.36 24.64 o 6 4 0 0.96 5.71 1.85 o 7 4 0 1461.37 1449.35 15.82 o 8 4 0 995.17 999.42 12.90 o 9 4 0 311.08 305.29 6.20 o 10 4 0 737.80 699.88 16.23 o 11 4 0 204.98 198.88 5.59 o 12 4 0 54.85 50.60 3.86 o 13 4 0 138.96 144.39 6.89 o 14 4 0 453.39 450.84 11.74 o 15 4 0 59.35 67.80 5.48 o 16 4 0 16.89 13.62 4.61 o 17 4 0 492.72 475.79 13.35 o 1 5 0 0.32 -0.46 1.20 o 2 5 0 1350.44 1421.39 14.72 o 3 5 0 3767.72 3712.54 35.00 o 4 5 0 174.56 189.44 5.92 o 5 5 0 1014.96 1055.95 12.96 o 6 5 0 3872.07 3725.79 37.35 o 7 5 0 1067.25 1048.00 19.45 o 8 5 0 142.86 151.68 5.53 o 9 5 0 0.68 -2.64 2.64 o 10 5 0 43.72 50.00 4.30 o 11 5 0 794.87 789.26 16.94 o 12 5 0 123.99 113.00 6.77 o 13 5 0 403.24 410.80 14.71 o 14 5 0 133.86 119.53 7.39 o 15 5 0 727.55 767.39 16.80 o 16 5 0 235.81 261.78 10.50 o 0 6 0 3524.12 3510.46 52.14 o 1 6 0 280.77 304.80 13.28 o 2 6 0 12.82 25.78 3.06 o 3 6 0 972.60 928.54 14.38 o 4 6 0 88.32 87.59 4.26 o 5 6 0 63.22 57.67 4.15 o 6 6 0 349.03 332.47 7.85 o 7 6 0 527.71 528.15 12.59 o 8 6 0 4.54 6.62 3.15 o 9 6 0 862.41 877.28 15.57 o 10 6 0 569.83 557.58 12.16 o 11 6 0 2.01 1.53 4.35 o 12 6 0 32.04 31.71 5.56 o 13 6 0 4.80 4.36 4.69 o 14 6 0 163.01 175.39 9.53 o 15 6 0 297.09 325.66 12.65 o 1 7 0 6.63 -0.51 3.10 o 2 7 0 35.27 44.70 4.86 o 3 7 0 803.77 789.05 16.89 o 4 7 0 1230.39 1242.27 19.88 o 5 7 0 3.39 11.81 3.41 o 6 7 0 1004.05 1008.38 16.63 o 7 7 0 289.74 296.98 10.40 o 8 7 0 392.69 399.13 10.89 o 9 7 0 199.39 193.61 8.29 o 10 7 0 0.18 -2.87 3.34 o 11 7 0 21.01 15.46 4.79 o 12 7 0 641.92 659.80 17.75 o 13 7 0 125.05 128.77 8.34 o 0 8 0 14.83 4.76 6.99 o 1 8 0 518.50 498.12 15.16 o 2 8 0 318.38 338.68 13.09 o 3 8 0 23.96 17.63 4.91 o 4 8 0 778.46 776.54 27.65 o 5 8 0 1291.29 1321.85 23.54 o 6 8 0 39.62 59.78 9.13 o 7 8 0 882.67 831.58 21.05 o 8 8 0 483.20 492.47 14.64 o 9 8 0 1.25 9.41 4.67 o 10 8 0 55.69 55.29 7.59 o 1 9 0 334.76 343.59 13.96 o 2 9 0 1237.28 1175.11 26.44 o 3 9 0 227.25 228.88 14.20 o 4 9 0 49.97 49.20 7.02 o 5 9 0 5.94 1.72 5.02 o 6 9 0 48.64 42.90 9.00 o -19 1 1 62.92 64.62 7.11 o -18 1 1 86.06 94.61 7.05 o -17 1 1 36.24 31.16 5.02 o -16 1 1 57.91 59.63 4.56 o -15 1 1 92.05 93.48 4.75 o -14 1 1 150.29 156.92 5.16 o -13 1 1 795.54 770.27 10.74 o -12 1 1 606.82 569.01 8.17 o -11 1 1 48.85 58.55 2.92 o -10 1 1 32.42 33.41 2.26 o -9 1 1 1.34 2.78 1.39 o -8 1 1 59.37 104.08 3.46 o -7 1 1 1.69 14.36 1.64 o -6 1 1 2164.79 2300.31 21.24 o -5 1 1 257.51 322.03 4.31 o -4 1 1 652.97 540.33 5.42 o -3 1 1 1315.42 1278.31 9.94 o -2 1 1 4296.13 4468.31 32.75 o 0 1 1 4020.39 3922.90 28.70 o 1 1 1 1907.88 1975.73 13.94 o 3 1 1 1812.09 1939.80 15.92 o 4 1 1 581.49 643.61 6.32 o 5 1 1 354.52 410.28 4.58 o 6 1 1 102.54 84.65 2.15 o 7 1 1 394.19 367.87 5.12 o 8 1 1 6.89 5.83 1.43 o 9 1 1 9.08 8.75 1.61 o 10 1 1 660.69 641.13 7.86 o 11 1 1 3295.72 3286.34 30.17 o 12 1 1 906.32 866.07 11.64 o 13 1 1 57.46 60.42 3.84 o 14 1 1 13.31 13.34 2.68 o 15 1 1 24.48 29.58 3.77 o 16 1 1 153.54 159.03 6.97 o 17 1 1 148.20 145.59 7.33 o 18 1 1 38.07 47.97 5.70 o -19 2 1 173.71 184.45 10.24 o -18 2 1 331.93 350.96 11.90 o -17 2 1 65.73 80.22 7.63 o -16 2 1 539.96 540.94 11.36 o -15 2 1 193.35 211.59 6.50 o -14 2 1 346.11 343.71 7.62 o -13 2 1 283.47 274.05 6.14 o -12 2 1 286.01 264.82 5.56 o -11 2 1 223.31 214.02 5.10 o -10 2 1 118.75 111.02 4.39 o -9 2 1 593.15 654.55 11.93 o -8 2 1 304.00 345.62 5.41 o -7 2 1 250.38 229.17 6.19 o -6 2 1 4542.42 4719.41 42.89 o -5 2 1 2272.59 2342.07 20.11 o -4 2 1 2.81 6.08 1.02 o -3 2 1 2076.33 2347.73 19.68 o -1 2 1 8476.87 8774.84 65.23 o 0 2 1 1094.66 1221.19 10.55 o 1 2 1 2252.40 2221.80 18.16 o 2 2 1 677.00 703.07 6.59 o 3 2 1 1595.07 1617.51 14.24 o 4 2 1 2511.95 2658.79 23.13 o 5 2 1 58.31 69.49 2.06 o 6 2 1 41.46 49.54 2.31 o 7 2 1 493.19 535.09 6.54 o 8 2 1 480.12 459.52 6.12 o 9 2 1 195.22 181.47 5.09 o 10 2 1 138.51 152.43 4.21 o 11 2 1 266.52 248.72 5.44 o 12 2 1 179.76 163.36 4.99 o 13 2 1 17.22 11.28 2.45 o 14 2 1 132.72 138.78 5.48 o 15 2 1 138.10 137.93 5.73 o 16 2 1 117.68 120.80 6.72 o 17 2 1 84.38 92.10 6.66 o 18 2 1 30.62 27.11 5.47 o -18 3 1 147.99 155.29 8.28 o -17 3 1 13.39 12.66 4.40 o -16 3 1 59.44 57.56 5.19 o -15 3 1 5.29 5.93 3.20 o -14 3 1 173.42 178.21 6.03 o -13 3 1 194.75 183.29 6.17 o -12 3 1 187.72 152.13 4.73 o -11 3 1 37.37 35.08 2.98 o -10 3 1 8.56 3.10 1.85 o -9 3 1 3.29 4.40 1.64 o -8 3 1 308.78 268.86 5.83 o -7 3 1 589.81 632.01 8.74 o -6 3 1 507.91 541.19 7.50 o -5 3 1 657.58 608.40 8.05 o -4 3 1 461.73 463.19 5.58 o -3 3 1 1054.01 1130.18 11.77 o -2 3 1 579.88 677.07 8.11 o -1 3 1 533.58 535.17 6.86 o 0 3 1 4548.64 4932.73 41.25 o 1 3 1 2757.90 3008.07 24.53 o 2 3 1 43.40 50.88 1.79 o 3 3 1 362.03 417.89 5.75 o 4 3 1 52.76 63.62 2.66 o 5 3 1 64.32 78.55 2.40 o 6 3 1 381.46 414.16 5.81 o 7 3 1 59.19 69.16 2.98 o 8 3 1 190.49 173.51 4.65 o 9 3 1 284.76 282.76 5.57 o 10 3 1 860.08 824.08 11.59 o 11 3 1 14.86 23.34 2.75 o 12 3 1 6.57 6.75 2.67 o 13 3 1 153.15 137.52 5.49 o 14 3 1 13.64 10.76 3.12 o 15 3 1 1.51 3.36 3.25 o 16 3 1 89.64 98.90 6.94 o 17 3 1 63.99 64.84 6.71 o 18 3 1 3.10 5.79 4.69 o -17 4 1 255.11 234.69 11.84 o -16 4 1 198.50 200.11 8.79 o -15 4 1 31.68 28.21 4.70 o -14 4 1 22.53 18.65 4.24 o -13 4 1 19.80 10.13 3.12 o -12 4 1 24.78 19.95 3.18 o -11 4 1 91.85 73.51 4.21 o -10 4 1 237.68 242.34 6.47 o -9 4 1 11.27 13.72 2.36 o -8 4 1 470.33 432.71 7.52 o -7 4 1 44.79 38.78 2.30 o -6 4 1 81.40 86.83 3.42 o -5 4 1 3223.22 3215.54 28.49 o -4 4 1 3054.42 3086.98 27.20 o -3 4 1 6.07 5.07 1.43 o -2 4 1 252.51 245.26 4.45 o -1 4 1 117.16 108.92 2.37 o 0 4 1 635.60 650.43 7.11 o 1 4 1 933.61 940.21 9.45 o 2 4 1 63.01 50.99 2.23 o 3 4 1 1448.15 1533.87 16.53 o 4 4 1 2164.02 2156.02 23.33 o 5 4 1 2591.54 2579.59 26.21 o 6 4 1 720.89 694.13 9.55 o 7 4 1 61.63 62.12 2.50 o 8 4 1 257.39 268.29 7.22 o 9 4 1 529.50 511.97 8.47 o 10 4 1 1590.50 1530.02 18.94 o 11 4 1 733.67 705.32 15.06 o 12 4 1 198.42 197.72 7.05 o 13 4 1 564.23 553.88 11.14 o 14 4 1 239.55 215.95 8.23 o 15 4 1 176.97 181.20 7.96 o 16 4 1 104.11 96.62 7.08 o 17 4 1 68.16 68.03 7.09 o -16 5 1 0.31 7.52 5.65 o -15 5 1 256.60 277.71 13.92 o -14 5 1 80.90 83.92 6.99 o -13 5 1 380.92 388.87 11.31 o -12 5 1 75.15 81.47 5.62 o -11 5 1 88.99 80.47 7.35 o -10 5 1 28.16 25.44 3.70 o -9 5 1 65.93 81.88 5.01 o -8 5 1 963.84 895.59 13.73 o -7 5 1 1610.17 1593.42 20.53 o -6 5 1 14.12 27.55 3.46 o -5 5 1 1517.34 1430.57 16.57 o -4 5 1 153.30 127.22 4.22 o -3 5 1 7.72 7.35 2.09 o -2 5 1 2581.01 2617.74 26.69 o -1 5 1 890.58 902.92 11.48 o 0 5 1 1081.28 1160.21 19.11 o 1 5 1 1049.30 1063.78 11.75 o 2 5 1 1250.52 1155.42 13.10 o 3 5 1 1567.50 1479.21 16.75 o 4 5 1 4.41 11.37 2.26 o 5 5 1 1450.12 1429.39 16.79 o 6 5 1 1638.65 1610.71 19.32 o 7 5 1 811.98 822.76 12.04 o 8 5 1 136.54 140.24 5.85 o 9 5 1 26.24 23.07 3.28 o 10 5 1 295.40 314.61 9.14 o 11 5 1 82.78 91.03 5.75 o 12 5 1 0.46 -0.49 3.29 o 13 5 1 166.31 166.43 8.05 o 14 5 1 231.71 240.06 9.51 o 15 5 1 382.78 440.53 12.82 o 16 5 1 267.81 279.91 10.92 o -15 6 1 136.06 181.73 12.88 o -14 6 1 0.24 1.32 3.98 o -13 6 1 23.63 34.25 5.08 o -12 6 1 182.31 175.80 8.75 o -11 6 1 70.74 69.61 5.18 o -10 6 1 31.00 41.90 4.62 o -9 6 1 47.87 53.71 4.60 o -8 6 1 218.40 212.03 7.38 o -7 6 1 109.82 108.01 5.33 o -6 6 1 394.53 365.86 8.61 o -5 6 1 3.67 0.11 2.80 o -4 6 1 95.05 117.27 4.96 o -3 6 1 351.19 367.72 8.20 o -2 6 1 45.23 37.66 3.91 o -1 6 1 108.35 63.92 3.48 o 0 6 1 93.09 90.93 3.37 o 1 6 1 287.91 307.79 7.41 o 2 6 1 304.57 339.88 6.79 o 3 6 1 2.94 8.90 2.74 o 4 6 1 37.68 46.77 4.03 o 5 6 1 86.97 99.55 5.24 o 6 6 1 0.54 3.36 2.64 o 7 6 1 361.84 334.31 8.66 o 8 6 1 3.12 0.58 2.80 o 9 6 1 117.55 113.97 6.15 o 10 6 1 108.38 105.48 6.63 o 11 6 1 37.63 49.61 5.98 o 12 6 1 222.01 209.44 9.63 o 13 6 1 24.23 27.38 5.56 o 14 6 1 111.17 124.75 8.64 o -13 7 1 39.22 47.48 5.95 o -12 7 1 203.60 222.59 10.27 o -11 7 1 456.03 456.79 12.65 o -10 7 1 67.74 76.02 7.76 o -9 7 1 199.79 201.00 8.83 o -8 7 1 318.42 325.86 11.63 o -7 7 1 90.72 90.98 6.17 o -6 7 1 305.29 289.65 9.32 o -5 7 1 80.55 76.30 5.01 o -4 7 1 408.60 412.06 10.11 o -3 7 1 930.30 895.78 16.96 o -2 7 1 3.54 10.35 3.01 o -1 7 1 8.36 1.21 3.63 o 0 7 1 125.36 126.92 6.46 o 1 7 1 344.38 349.03 9.81 o 2 7 1 833.76 852.22 17.96 o 3 7 1 204.80 218.01 9.36 o 4 7 1 1.92 9.07 3.27 o 5 7 1 275.59 270.99 8.53 o 6 7 1 496.01 490.69 11.55 o 7 7 1 82.77 88.68 5.73 o 8 7 1 63.55 66.27 5.35 o 9 7 1 109.13 121.93 6.72 o 10 7 1 25.56 22.55 4.77 o 11 7 1 94.69 105.04 7.71 o 12 7 1 152.68 146.83 9.67 o 13 7 1 10.73 22.54 15.65 o -10 8 1 0.25 4.83 4.26 o -9 8 1 67.08 73.44 9.80 o -8 8 1 195.85 196.17 11.45 o -7 8 1 88.22 95.31 7.61 o -6 8 1 3.83 4.43 4.01 o -5 8 1 20.46 20.35 4.51 o -4 8 1 13.90 20.09 4.94 o -3 8 1 245.37 244.79 11.10 o -2 8 1 99.79 97.89 7.21 o -1 8 1 199.21 201.84 9.20 o 0 8 1 532.46 509.22 16.12 o 1 8 1 418.21 409.97 17.31 o 2 8 1 237.41 241.89 10.26 o 3 8 1 0.62 -0.57 4.04 o 4 8 1 339.39 334.26 11.92 o 5 8 1 117.22 124.38 8.16 o 6 8 1 3.51 -0.31 5.33 o 7 8 1 75.12 73.79 7.06 o 8 8 1 225.96 219.10 10.54 o 9 8 1 179.46 194.35 11.51 o 10 8 1 16.15 18.89 7.48 o -6 9 1 38.65 41.05 7.08 o -5 9 1 56.25 68.77 7.14 o -4 9 1 82.12 81.25 10.47 o -3 9 1 49.43 44.53 7.27 o -2 9 1 6.02 3.68 5.61 o -1 9 1 1.27 0.01 5.29 o 0 9 1 18.12 17.08 6.13 o 1 9 1 29.11 20.10 7.57 o 2 9 1 204.10 198.33 11.49 o 3 9 1 138.27 132.05 9.09 o 4 9 1 76.60 72.95 8.13 o 5 9 1 0.01 -3.31 4.39 o 6 9 1 1.47 0.15 5.35 o -19 0 2 112.19 135.58 22.12 o -18 0 2 159.16 194.05 14.55 o -17 0 2 80.60 78.54 8.65 o -16 0 2 9.88 11.13 4.50 o -15 0 2 461.95 451.55 13.28 o -14 0 2 2153.70 2126.47 32.88 o -13 0 2 2055.40 1993.80 28.97 o -12 0 2 5907.26 5750.71 75.89 o -11 0 2 3817.07 3760.72 51.38 o -10 0 2 14.23 23.48 2.98 o -9 0 2 532.55 569.88 11.05 o -8 0 2 1799.90 1672.12 25.76 o -7 0 2 1768.20 1931.41 26.62 o -6 0 2 712.65 813.68 12.62 o -5 0 2 3803.01 4257.03 50.03 o -4 0 2 635.56 746.61 9.12 o -3 0 2 385.55 343.51 4.55 o -2 0 2 23665.33 23455.93 335.28 o -1 0 2 5244.63 5533.37 53.68 o 0 0 2 3073.04 2859.37 25.12 o 1 0 2 159.32 161.93 2.36 o 2 0 2 371.43 319.94 6.56 o 3 0 2 118.57 127.66 4.41 o 4 0 2 278.86 232.16 5.06 o 5 0 2 13561.98 13883.35 148.77 o 6 0 2 1114.60 1140.36 14.84 o 7 0 2 1155.75 1110.08 15.23 o 8 0 2 13923.20 13873.02 151.11 o 9 0 2 727.48 767.16 12.23 o 10 0 2 663.03 667.14 11.98 o 11 0 2 1910.77 1793.31 25.60 o 12 0 2 371.76 348.35 8.62 o 13 0 2 305.86 277.57 10.48 o 14 0 2 1873.99 1795.05 32.83 o 15 0 2 809.11 814.67 19.81 o 16 0 2 18.49 16.79 5.31 o 17 0 2 252.90 248.64 19.90 o 18 0 2 101.89 114.74 11.60 o -19 1 2 41.42 43.46 8.54 o -18 1 2 161.33 166.70 8.97 o -17 1 2 524.49 517.40 12.53 o -16 1 2 105.62 113.14 5.48 o -15 1 2 294.15 297.25 7.34 o -14 1 2 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