#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220161.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220161_Fobs loop_ _publ_author_name 'Baryala, Yamna' 'Salem, Moussa' 'Essassi, El Mokhtar' 'Reuter, Hans' 'Izaaryene, Maher' _publ_section_title ; Dimethyl 3-acetyl-3-(1,3-benzothiazol-2-yl)pentanedioate ; _journal_coeditor_code FJ2155 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2290 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.011 _cell_angle_gamma 90.000 _cell_length_a 14.4075 _cell_length_b 8.8089 _cell_length_c 13.8968 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file fj2155Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AZ003_0ma in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 243.24 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 722.12 685.32 5.99 o 2 0 0 43.12 38.43 0.52 o 3 0 0 2553.85 2477.97 11.82 o 4 0 0 927.39 860.10 4.50 o 5 0 0 85.34 128.87 1.35 o 6 0 0 0.40 4.33 0.52 o 7 0 0 5420.97 5440.65 25.95 o 8 0 0 4990.21 4853.86 26.00 o 9 0 0 297.94 324.53 2.93 o 10 0 0 21.80 22.01 1.23 o 11 0 0 221.60 179.56 3.09 o 12 0 0 970.16 962.54 8.64 o 13 0 0 5.75 4.90 1.73 o 14 0 0 18.80 20.03 3.08 o 15 0 0 380.37 395.08 11.34 o 16 0 0 19.07 28.22 6.81 o 1 1 0 3264.10 3278.69 11.81 o 2 1 0 2271.25 2244.24 7.86 o 3 1 0 14.31 11.14 0.31 o 4 1 0 958.33 1013.34 3.63 o 5 1 0 15.79 18.07 0.42 o 6 1 0 2090.83 2157.02 7.83 o 7 1 0 488.80 531.17 2.47 o 8 1 0 472.31 464.82 2.39 o 9 1 0 652.78 653.40 3.45 o 10 1 0 302.86 278.13 2.19 o 11 1 0 172.72 181.34 2.06 o 12 1 0 18.64 23.17 1.27 o 13 1 0 421.87 445.72 4.52 o 14 1 0 38.60 40.35 2.14 o 15 1 0 61.14 63.93 3.33 o 16 1 0 260.31 243.75 7.38 o 0 2 0 14415.57 13786.44 67.45 o 1 2 0 2330.94 2176.09 7.80 o 2 2 0 584.76 597.32 2.41 o 3 2 0 546.23 569.38 2.39 o 4 2 0 111.22 95.36 0.79 o 5 2 0 799.03 885.64 3.49 o 6 2 0 431.09 491.04 2.30 o 7 2 0 526.06 570.40 2.83 o 8 2 0 24.54 28.14 0.73 o 9 2 0 328.89 357.60 2.31 o 10 2 0 16.24 16.83 0.85 o 11 2 0 113.70 121.40 1.82 o 12 2 0 84.34 77.56 1.83 o 13 2 0 22.64 20.85 1.62 o 14 2 0 0.60 0.22 1.58 o 15 2 0 5.94 4.33 2.30 o 16 2 0 0.41 0.42 2.76 o 1 3 0 657.01 666.82 2.72 o 2 3 0 3521.45 3629.47 13.09 o 3 3 0 286.41 299.34 1.56 o 4 3 0 823.46 727.08 3.14 o 5 3 0 457.11 483.75 2.32 o 6 3 0 31.66 60.46 0.79 o 7 3 0 813.63 883.04 3.89 o 8 3 0 172.57 155.50 1.44 o 9 3 0 62.00 65.66 1.13 o 10 3 0 190.50 170.06 1.92 o 11 3 0 278.84 278.42 3.05 o 12 3 0 88.80 92.35 2.05 o 13 3 0 156.17 145.64 3.13 o 14 3 0 11.30 10.22 2.00 o 15 3 0 124.17 132.02 4.42 o 16 3 0 263.70 277.75 8.07 o 0 4 0 18260.40 19329.49 93.80 o 1 4 0 1359.68 1344.52 5.27 o 2 4 0 1146.33 1238.16 5.13 o 3 4 0 0.24 4.30 0.41 o 4 4 0 190.76 222.36 1.45 o 5 4 0 183.92 154.00 1.22 o 6 4 0 0.16 -0.33 0.47 o 7 4 0 1607.56 1558.32 6.56 o 8 4 0 538.07 483.93 3.00 o 9 4 0 33.09 33.57 0.99 o 10 4 0 47.83 55.02 1.42 o 11 4 0 529.82 511.59 4.38 o 12 4 0 7.97 14.81 1.46 o 13 4 0 0.80 5.10 1.83 o 14 4 0 19.19 17.64 2.43 o 15 4 0 160.92 162.56 6.27 o 1 5 0 1098.51 1147.13 4.73 o 2 5 0 336.64 340.82 1.96 o 3 5 0 1150.84 1095.38 4.94 o 4 5 0 1189.75 1324.02 5.61 o 5 5 0 209.19 264.60 1.81 o 6 5 0 762.09 699.47 3.56 o 7 5 0 1158.39 1110.99 5.06 o 8 5 0 290.03 294.52 2.31 o 9 5 0 739.11 733.12 4.95 o 10 5 0 201.71 198.42 2.61 o 11 5 0 123.93 136.88 2.58 o 12 5 0 46.93 54.20 2.24 o 13 5 0 155.64 140.54 5.56 o 14 5 0 142.33 161.15 5.69 o 15 5 0 175.47 185.23 7.38 o 0 6 0 57.74 48.58 1.12 o 1 6 0 264.88 269.59 1.91 o 2 6 0 7.66 23.65 0.73 o 3 6 0 22.48 24.88 0.77 o 4 6 0 140.07 147.54 1.53 o 5 6 0 394.90 353.38 2.43 o 6 6 0 159.30 157.81 1.71 o 7 6 0 1744.08 1625.62 8.67 o 8 6 0 247.14 239.41 2.65 o 9 6 0 125.58 128.93 2.20 o 10 6 0 10.50 11.22 1.37 o 11 6 0 28.33 28.92 1.84 o 12 6 0 9.94 8.50 2.01 o 13 6 0 163.68 170.54 4.85 o 14 6 0 18.78 17.83 3.91 o 1 7 0 273.02 267.53 2.09 o 2 7 0 9.04 7.40 0.74 o 3 7 0 16.31 16.09 0.81 o 4 7 0 0.93 4.50 0.82 o 5 7 0 0.67 4.34 1.00 o 6 7 0 517.63 499.27 4.45 o 7 7 0 1541.84 1468.10 10.35 o 8 7 0 0.06 0.21 1.13 o 9 7 0 71.57 77.71 2.35 o 10 7 0 143.51 143.61 3.43 o 11 7 0 1.64 0.11 1.74 o 12 7 0 27.14 38.39 4.06 o 13 7 0 0.54 3.24 4.25 o 0 8 0 14.71 28.88 2.04 o 1 8 0 676.51 687.43 5.39 o 2 8 0 126.25 119.17 2.03 o 3 8 0 43.47 45.23 1.47 o 4 8 0 27.13 25.22 1.45 o 5 8 0 179.87 191.41 2.95 o 6 8 0 6.01 5.95 1.44 o 7 8 0 741.53 741.04 7.17 o 8 8 0 194.62 207.24 4.65 o 9 8 0 11.85 13.57 2.10 o 10 8 0 2.51 -0.14 2.38 o 11 8 0 7.24 8.69 4.23 o 12 8 0 671.40 709.74 18.28 o 1 9 0 0.96 3.26 1.71 o 2 9 0 51.70 47.31 2.19 o 3 9 0 1151.64 1125.79 11.81 o 4 9 0 1264.19 1226.69 10.89 o 5 9 0 30.37 25.60 1.99 o 6 9 0 12.49 14.84 2.02 o 7 9 0 109.57 126.88 4.22 o 8 9 0 467.75 499.27 10.47 o 9 9 0 235.29 245.84 8.58 o 10 9 0 26.42 31.62 3.75 o 0 10 0 750.63 755.11 16.88 o 1 10 0 25.91 17.63 2.71 o 2 10 0 296.40 302.79 6.23 o 3 10 0 83.67 90.08 3.58 o 4 10 0 35.95 34.14 3.35 o 5 10 0 3.93 7.43 2.75 o 6 10 0 63.32 75.01 4.46 o 7 10 0 88.73 112.05 6.59 o 8 10 0 16.01 14.78 3.92 o 1 11 0 75.60 82.00 5.52 o 2 11 0 0.42 0.98 3.78 o 3 11 0 108.50 102.23 6.53 o 4 11 0 0.02 -0.88 3.92 o 5 11 0 12.63 12.81 4.45 o -17 1 1 75.10 75.07 5.36 o -16 1 1 13.26 13.27 2.70 o -15 1 1 60.91 57.33 2.42 o -14 1 1 1244.81 1249.78 9.38 o -13 1 1 7.35 13.10 1.15 o -12 1 1 3110.15 3095.61 16.51 o -11 1 1 749.94 709.79 4.35 o -10 1 1 184.59 194.95 1.75 o -9 1 1 216.10 223.38 1.70 o -8 1 1 818.92 955.44 4.30 o -7 1 1 1433.22 1479.19 5.85 o -6 1 1 60.14 71.21 0.69 o -5 1 1 263.99 257.13 1.28 o -4 1 1 9922.07 10038.38 35.49 o -3 1 1 647.71 698.66 2.69 o -2 1 1 9365.37 9371.34 34.73 o -1 1 1 249.34 229.45 1.03 o 0 1 1 1061.15 1058.74 3.78 o 1 1 1 4182.11 4262.26 14.71 o 2 1 1 10297.11 10260.63 35.57 o 3 1 1 13881.56 13965.73 45.53 o 4 1 1 7333.63 7426.63 24.38 o 5 1 1 3779.28 3741.41 12.87 o 6 1 1 918.37 932.13 3.73 o 7 1 1 669.67 587.68 2.76 o 8 1 1 1683.36 1559.44 6.42 o 9 1 1 0.91 1.63 0.66 o 10 1 1 142.62 151.20 1.69 o 11 1 1 0.51 0.14 0.91 o 12 1 1 66.66 66.65 1.80 o 13 1 1 575.01 575.47 5.96 o 14 1 1 49.90 52.20 2.95 o 15 1 1 25.87 24.13 3.12 o 16 1 1 15.18 9.92 4.01 o -17 2 1 91.68 112.06 5.46 o -16 2 1 544.74 530.35 9.35 o -15 2 1 139.00 136.44 3.45 o -14 2 1 359.10 352.37 4.58 o -13 2 1 128.38 121.66 2.22 o -12 2 1 378.35 364.62 3.34 o -11 2 1 225.09 191.51 2.13 o -10 2 1 498.86 500.97 3.12 o -9 2 1 4.49 7.79 0.65 o -8 2 1 1763.97 1740.45 7.28 o -7 2 1 13.31 15.41 0.52 o -6 2 1 135.63 115.84 0.93 o -5 2 1 1858.96 1845.54 6.78 o -4 2 1 1292.88 1263.92 4.96 o -3 2 1 3895.98 3855.14 14.30 o -2 2 1 7.99 -0.46 0.31 o -1 2 1 5313.78 5120.41 18.92 o 0 2 1 1255.10 1178.38 4.17 o 1 2 1 1651.89 1573.76 5.61 o 2 2 1 23.12 33.16 0.52 o 3 2 1 9971.62 10390.20 36.44 o 4 2 1 1852.04 1892.82 6.84 o 5 2 1 741.06 699.46 2.95 o 6 2 1 150.18 126.25 1.05 o 7 2 1 225.65 206.43 1.51 o 8 2 1 43.85 47.51 0.92 o 9 2 1 85.25 70.07 1.16 o 10 2 1 1794.82 1731.65 8.64 o 11 2 1 397.15 423.69 3.70 o 12 2 1 738.47 721.36 6.37 o 13 2 1 96.38 83.67 2.73 o 14 2 1 11.75 13.54 2.17 o 15 2 1 150.30 153.89 4.77 o 16 2 1 98.21 104.79 8.60 o -16 3 1 62.25 59.22 4.09 o -15 3 1 4.32 -2.46 2.01 o -14 3 1 96.80 93.55 2.64 o -13 3 1 161.43 166.62 2.91 o -12 3 1 1470.03 1417.27 9.50 o -11 3 1 893.97 818.46 5.27 o -10 3 1 10.75 10.63 0.82 o -9 3 1 42.45 35.46 0.86 o -8 3 1 391.81 446.26 2.43 o -7 3 1 988.50 949.32 4.16 o -6 3 1 115.52 133.30 1.09 o -5 3 1 1468.79 1526.99 6.14 o -4 3 1 3013.27 3017.12 11.28 o -3 3 1 44.12 50.24 0.66 o -2 3 1 1.34 3.49 0.38 o -1 3 1 38.06 38.23 0.54 o 0 3 1 244.93 247.84 1.27 o 1 3 1 184.56 156.87 0.99 o 2 3 1 130.22 109.67 1.19 o 3 3 1 3.32 12.55 0.44 o 4 3 1 3837.09 4322.53 15.51 o 5 3 1 552.68 576.93 2.60 o 6 3 1 2540.50 2621.88 9.98 o 7 3 1 807.15 800.12 3.77 o 8 3 1 1601.91 1617.85 6.97 o 9 3 1 330.62 294.53 2.41 o 10 3 1 5.53 2.89 0.92 o 11 3 1 213.35 191.39 2.67 o 12 3 1 175.88 178.18 3.14 o 13 3 1 18.45 15.65 1.96 o 14 3 1 175.94 168.53 4.55 o 15 3 1 515.03 498.04 9.94 o -16 4 1 69.17 73.19 4.79 o -15 4 1 224.14 230.16 5.29 o -14 4 1 41.78 45.85 2.46 o -13 4 1 31.52 32.66 1.78 o -12 4 1 1.56 0.76 1.18 o -11 4 1 0.77 -0.08 0.97 o -10 4 1 4.53 3.27 0.83 o -9 4 1 60.82 71.39 1.15 o -8 4 1 148.16 159.20 1.42 o -7 4 1 74.72 67.04 0.93 o -6 4 1 12.04 10.44 0.55 o -5 4 1 263.12 326.30 1.82 o -4 4 1 540.32 517.58 2.53 o -3 4 1 16.26 20.53 0.54 o -2 4 1 1903.09 2185.34 8.55 o -1 4 1 265.99 263.89 1.46 o 0 4 1 16.35 12.65 0.43 o 1 4 1 409.73 380.71 1.88 o 2 4 1 636.40 788.80 3.34 o 3 4 1 1.87 2.48 0.39 o 4 4 1 141.36 115.68 1.08 o 5 4 1 312.35 326.37 2.01 o 6 4 1 172.77 193.31 1.55 o 7 4 1 608.98 613.49 3.16 o 8 4 1 324.77 304.67 2.21 o 9 4 1 52.19 48.12 1.16 o 10 4 1 137.49 122.51 2.10 o 11 4 1 157.48 148.37 2.61 o 12 4 1 7.74 8.28 1.59 o 13 4 1 29.98 15.89 2.16 o 14 4 1 4.84 5.07 2.76 o 15 4 1 28.73 22.63 4.24 o -15 5 1 2.73 -1.38 2.89 o -14 5 1 150.16 143.39 4.24 o -13 5 1 41.83 47.94 2.41 o -12 5 1 911.19 868.90 8.08 o -11 5 1 62.51 58.86 1.74 o -10 5 1 78.70 78.62 1.62 o -9 5 1 537.00 515.39 3.36 o -8 5 1 51.58 45.13 0.95 o -7 5 1 348.99 358.83 2.27 o -6 5 1 620.27 607.27 3.26 o -5 5 1 17.26 19.49 0.68 o -4 5 1 514.37 501.76 2.71 o -3 5 1 213.43 247.25 1.70 o -2 5 1 7.75 16.97 0.57 o -1 5 1 29.11 26.88 0.60 o 0 5 1 9.94 20.25 0.52 o 1 5 1 55.99 39.26 0.66 o 2 5 1 4.37 0.29 0.48 o 3 5 1 783.55 724.42 3.41 o 4 5 1 706.48 665.15 3.28 o 5 5 1 118.05 100.51 1.19 o 6 5 1 68.19 74.84 1.14 o 7 5 1 199.48 226.50 1.85 o 8 5 1 334.81 324.78 2.67 o 9 5 1 140.52 114.65 1.95 o 10 5 1 103.02 101.61 2.16 o 11 5 1 47.40 48.92 2.14 o 12 5 1 3.65 4.77 1.64 o 13 5 1 67.54 66.56 3.42 o 14 5 1 121.57 120.50 7.01 o -14 6 1 220.47 229.23 6.97 o -13 6 1 83.30 97.02 6.15 o -12 6 1 0.03 1.49 1.63 o -11 6 1 12.78 11.76 1.50 o -10 6 1 135.73 127.27 2.31 o -9 6 1 17.74 19.17 1.13 o -8 6 1 151.43 146.48 1.91 o -7 6 1 0.18 0.58 0.77 o -6 6 1 6.76 6.01 0.77 o -5 6 1 2162.18 2038.89 9.24 o -4 6 1 1131.08 1132.12 5.59 o -3 6 1 786.31 817.86 4.05 o -2 6 1 18.59 2.52 0.60 o -1 6 1 266.59 273.87 1.88 o 0 6 1 129.03 139.32 1.28 o 1 6 1 53.02 56.11 0.87 o 2 6 1 445.41 514.86 2.93 o 3 6 1 1801.74 1699.08 7.40 o 4 6 1 2750.85 2617.83 10.64 o 5 6 1 408.55 408.96 2.64 o 6 6 1 3.26 3.08 0.81 o 7 6 1 123.36 136.39 2.01 o 8 6 1 30.93 36.64 1.35 o 9 6 1 3.10 1.95 1.23 o 10 6 1 642.61 598.50 6.40 o 11 6 1 869.91 863.18 8.56 o 12 6 1 338.93 328.71 6.66 o 13 6 1 99.18 107.97 6.47 o -13 7 1 379.37 396.92 12.86 o -12 7 1 150.65 158.13 5.59 o -11 7 1 63.57 56.88 2.82 o -10 7 1 47.64 58.34 2.61 o -9 7 1 233.92 248.74 4.35 o -8 7 1 11.83 14.65 1.32 o -7 7 1 811.19 761.79 7.40 o -6 7 1 22.62 23.14 1.13 o -5 7 1 2490.31 2476.02 13.39 o -4 7 1 1084.00 1010.65 5.33 o -3 7 1 144.41 149.60 1.62 o -2 7 1 162.14 156.89 1.59 o -1 7 1 147.94 134.77 1.49 o 0 7 1 1084.16 1043.96 5.11 o 1 7 1 664.67 606.06 3.39 o 2 7 1 141.77 122.87 1.45 o 3 7 1 385.20 372.25 2.79 o 4 7 1 1740.65 1744.07 8.96 o 5 7 1 94.41 88.06 1.81 o 6 7 1 2335.10 2340.53 14.26 o 7 7 1 133.18 127.46 2.29 o 8 7 1 330.60 338.27 4.08 o 9 7 1 10.42 12.54 1.72 o 10 7 1 32.99 32.87 2.20 o 11 7 1 81.43 91.46 4.95 o 12 7 1 200.68 195.44 6.25 o -12 8 1 60.20 59.19 5.75 o -11 8 1 522.20 529.97 10.34 o -10 8 1 52.85 51.77 3.49 o -9 8 1 30.48 38.71 2.50 o -8 8 1 859.98 861.82 8.49 o -7 8 1 61.63 62.84 2.06 o -6 8 1 4.73 2.82 1.30 o -5 8 1 268.11 271.11 3.35 o -4 8 1 876.70 804.57 6.66 o -3 8 1 777.05 699.24 5.58 o -2 8 1 788.73 736.24 5.45 o -1 8 1 726.38 667.64 5.12 o 0 8 1 252.11 218.20 2.99 o 1 8 1 214.40 181.73 2.87 o 2 8 1 27.18 25.93 1.21 o 3 8 1 209.57 217.65 2.85 o 4 8 1 101.70 116.80 2.36 o 5 8 1 96.84 103.47 2.43 o 6 8 1 14.52 16.15 1.53 o 7 8 1 179.67 175.04 3.90 o 8 8 1 0.61 3.03 2.17 o 9 8 1 28.99 37.74 3.00 o 10 8 1 11.01 11.81 3.21 o 11 8 1 23.60 20.62 3.44 o -11 9 1 16.88 19.62 4.79 o -10 9 1 58.71 69.37 7.77 o -9 9 1 20.74 18.02 3.06 o -8 9 1 214.01 229.13 5.63 o -7 9 1 227.87 250.18 4.79 o -6 9 1 13.86 9.13 1.71 o -5 9 1 19.83 19.51 1.70 o -4 9 1 93.25 72.58 2.31 o -3 9 1 419.13 362.17 5.05 o -2 9 1 117.86 116.71 3.45 o -1 9 1 32.99 29.47 2.16 o 0 9 1 349.29 325.27 5.23 o 1 9 1 74.51 63.87 2.55 o 2 9 1 15.94 15.95 2.05 o 3 9 1 27.66 33.70 1.96 o 4 9 1 8.32 9.20 1.90 o 5 9 1 157.72 161.74 3.61 o 6 9 1 242.02 248.32 4.81 o 7 9 1 25.79 19.51 3.26 o 8 9 1 23.03 16.40 3.79 o 9 9 1 44.90 54.54 4.72 o 10 9 1 1.24 -1.01 3.45 o -9 10 1 70.59 67.25 4.76 o -8 10 1 207.07 195.94 6.11 o -7 10 1 0.46 -2.99 3.24 o -6 10 1 103.23 108.01 5.29 o -5 10 1 145.12 156.31 4.78 o -4 10 1 362.74 367.75 10.25 o -3 10 1 698.37 675.19 10.13 o -2 10 1 12.53 10.47 2.31 o -1 10 1 284.03 260.42 5.90 o 0 10 1 453.10 448.78 8.58 o 1 10 1 40.42 40.22 3.28 o 2 10 1 380.80 371.50 6.73 o 3 10 1 157.43 161.34 5.14 o 4 10 1 375.07 395.65 9.75 o 5 10 1 60.39 70.30 4.08 o 6 10 1 100.70 116.49 5.52 o 7 10 1 406.07 397.32 10.29 o 8 10 1 87.22 98.31 5.73 o -5 11 1 830.05 908.14 16.30 o -4 11 1 258.90 262.67 7.80 o -3 11 1 51.81 60.32 5.36 o -2 11 1 0.23 0.58 3.67 o -1 11 1 134.93 129.46 7.12 o 0 11 1 218.70 206.25 6.96 o 1 11 1 720.83 762.77 13.28 o 2 11 1 130.89 172.08 9.67 o 3 11 1 91.76 91.85 6.18 o 4 11 1 70.07 73.06 6.42 o -17 0 2 92.33 94.99 6.67 o -16 0 2 103.13 96.20 4.65 o -15 0 2 245.39 237.95 5.17 o -14 0 2 415.36 414.91 5.42 o -13 0 2 115.01 119.10 2.56 o -12 0 2 337.45 345.59 3.92 o -11 0 2 1399.60 1389.92 10.11 o -10 0 2 1.83 0.34 0.79 o -9 0 2 27.14 30.27 0.95 o -8 0 2 316.66 304.31 2.48 o -7 0 2 509.67 458.39 3.10 o -6 0 2 933.18 991.30 5.66 o -5 0 2 3985.88 4040.60 22.55 o -4 0 2 29329.28 29023.25 152.41 o -3 0 2 2322.82 2449.80 12.75 o -2 0 2 357.09 287.79 2.04 o -1 0 2 7837.42 7924.16 41.00 o 0 0 2 3947.07 4036.85 21.61 o 1 0 2 805.67 747.80 4.01 o 2 0 2 3546.59 3620.84 18.87 o 3 0 2 15660.34 16462.57 78.17 o 4 0 2 1305.76 1194.85 6.24 o 5 0 2 4647.60 4935.17 23.51 o 6 0 2 38.99 17.07 0.81 o 7 0 2 196.76 240.80 2.29 o 8 0 2 277.03 270.42 2.64 o 9 0 2 7.03 12.34 1.08 o 10 0 2 2534.83 2387.04 17.20 o 11 0 2 1511.33 1440.27 13.66 o 12 0 2 558.91 533.28 8.56 o 13 0 2 61.53 55.93 3.64 o 14 0 2 199.87 225.29 7.92 o 15 0 2 603.84 602.87 17.37 o -17 1 2 359.89 388.10 8.72 o -16 1 2 26.05 27.06 2.32 o -15 1 2 154.43 149.34 2.88 o -14 1 2 232.33 234.00 3.05 o -13 1 2 87.75 87.83 1.69 o -12 1 2 99.99 94.80 1.49 o -11 1 2 177.42 173.33 1.79 o -10 1 2 445.31 474.84 2.71 o -9 1 2 1469.95 1519.47 6.45 o -8 1 2 2175.53 2162.93 8.76 o -7 1 2 0.12 3.64 0.38 o -6 1 2 52.45 49.24 0.57 o -5 1 2 319.45 336.21 1.61 o -4 1 2 221.74 185.15 1.08 o -3 1 2 5.00 6.95 0.33 o -2 1 2 9938.09 10003.98 39.76 o -1 1 2 3632.03 3808.25 13.70 o 0 1 2 702.20 719.61 2.60 o 1 1 2 88.16 90.93 0.69 o 2 1 2 0.08 0.44 0.32 o 3 1 2 1785.06 1832.11 6.69 o 4 1 2 107.72 94.12 0.85 o 5 1 2 1994.05 2163.34 7.79 o 6 1 2 695.87 622.77 2.81 o 7 1 2 1456.34 1545.05 6.11 o 8 1 2 2.77 4.73 0.66 o 9 1 2 7.83 10.76 0.76 o 10 1 2 20.37 24.66 1.11 o 11 1 2 208.59 213.61 2.72 o 12 1 2 10.96 9.84 1.54 o 13 1 2 225.36 220.62 4.62 o 14 1 2 59.06 55.58 3.48 o 15 1 2 0.00 2.05 3.68 o -17 2 2 32.47 28.08 3.31 o -16 2 2 18.30 18.40 2.51 o -15 2 2 31.04 25.81 1.98 o -14 2 2 253.35 259.14 3.49 o -13 2 2 0.05 -0.07 0.99 o -12 2 2 29.14 28.99 1.09 o -11 2 2 20.97 27.48 0.96 o -10 2 2 163.89 180.34 1.68 o -9 2 2 5.96 2.61 0.59 o -8 2 2 3117.32 3288.54 12.83 o -7 2 2 200.73 246.84 1.47 o -6 2 2 718.30 695.03 3.09 o -5 2 2 113.99 126.82 0.93 o -4 2 2 4.85 10.96 0.36 o -3 2 2 634.65 623.00 2.73 o -2 2 2 220.30 188.78 1.12 o -1 2 2 659.89 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