#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220191.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220191_Fobs loop_ _publ_author_name 'Hittle, Jennifer L.' 'LaDuca, Robert L.' _publ_section_title ; Poly[di-\m~3~-chlorido-[\m~2~-(3-pyridyl)(4-pyridyl)methanone-\k^2^N:N']dicopper(I)] ; _journal_coeditor_code HB2839 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1599 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.462 _cell_angle_gamma 90.000 _cell_length_a 3.7765 _cell_length_b 25.9349 _cell_length_c 12.3392 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file hb2839Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21c in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 198.82 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6208.54 5539.83 81.80 o 2 0 0 4024.63 4126.28 72.27 o 3 0 0 557.97 533.65 14.69 o 4 0 0 4.94 91.32 63.93 o 1 1 0 15514.62 15010.58 154.46 o 2 1 0 9463.32 9388.16 200.52 o 3 1 0 454.82 426.05 9.13 o 4 1 0 8.85 3.97 14.29 o 0 2 0 851.49 1022.44 22.63 o 1 2 0 2964.81 2776.66 29.78 o 2 2 0 100.59 92.52 4.76 o 3 2 0 321.82 301.37 7.94 o 4 2 0 126.21 123.09 15.88 o 1 3 0 0.88 2.38 1.59 o 2 3 0 12080.14 12573.40 160.41 o 3 3 0 9.04 4.76 4.37 o 4 3 0 54.49 37.72 13.10 o 0 4 0 25989.89 29141.66 471.71 o 1 4 0 10404.50 10471.75 108.40 o 2 4 0 2330.22 2314.48 32.16 o 3 4 0 1279.97 1231.69 17.47 o 4 4 0 39.81 0.00 25.41 o 1 5 0 13896.42 13463.62 138.97 o 2 5 0 450.95 544.37 63.53 o 3 5 0 606.82 593.61 11.12 o 4 5 0 322.84 349.02 16.68 o 0 6 0 14070.39 14948.24 240.62 o 1 6 0 9200.57 8775.10 91.32 o 2 6 0 182.31 221.16 6.75 o 3 6 0 415.63 360.93 8.74 o 4 6 0 2.15 9.53 18.26 o 1 7 0 45.37 39.31 2.38 o 2 7 0 4964.61 5320.65 50.43 o 3 7 0 61.29 58.77 6.35 o 4 7 0 2.12 0.00 14.69 o 0 8 0 804.21 928.73 19.46 o 1 8 0 12069.37 12162.04 134.60 o 2 8 0 3126.62 3051.03 32.16 o 3 8 0 1885.92 1798.70 27.40 o 4 8 0 64.30 86.56 15.09 o 1 9 0 24030.22 24021.53 244.59 o 2 9 0 144.14 206.08 9.93 o 3 9 0 43.53 41.29 6.35 o 4 9 0 624.18 758.79 24.22 o 0 10 0 4330.90 4854.10 105.22 o 1 10 0 2481.33 2545.57 28.19 o 2 10 0 4.13 0.00 5.16 o 3 10 0 1735.10 1654.56 25.81 o 4 10 0 92.62 92.12 14.69 o 1 11 0 9538.43 9857.89 102.44 o 2 11 0 1812.78 1855.87 24.62 o 3 11 0 991.65 1012.51 18.66 o 4 11 0 83.60 61.15 14.69 o 0 12 0 963.31 920.00 23.43 o 1 12 0 6939.15 6945.43 73.06 o 2 12 0 127.90 96.88 5.96 o 3 12 0 1342.70 1291.25 22.24 o 4 12 0 1.77 5.56 14.29 o 1 13 0 6179.91 6285.11 66.71 o 2 13 0 1355.54 1436.97 24.62 o 3 13 0 344.78 310.90 11.12 o 4 13 0 39.56 39.31 15.09 o 0 14 0 12980.58 12836.66 237.05 o 1 14 0 4933.29 5000.22 54.00 o 2 14 0 304.40 330.36 9.13 o 3 14 0 57.69 75.04 7.94 o 4 14 0 247.50 276.75 21.84 o 1 15 0 3448.97 3494.55 38.91 o 2 15 0 200.58 363.31 33.35 o 3 15 0 405.16 409.37 12.71 o 4 15 0 25.82 32.96 18.26 o 0 16 0 3240.29 3312.70 65.12 o 1 16 0 1792.81 1852.70 22.63 o 2 16 0 210.03 209.65 8.74 o 3 16 0 547.15 581.70 14.69 o 4 16 0 295.16 207.66 23.43 o 1 17 0 1454.16 1483.83 20.65 o 2 17 0 5280.33 5464.38 71.07 o 3 17 0 782.51 763.55 17.07 o 4 17 0 22.86 27.00 19.46 o 0 18 0 13932.16 14243.05 304.15 o 1 18 0 835.28 838.20 15.49 o 2 18 0 2049.97 2111.58 31.77 o 3 18 0 113.27 134.21 9.93 o 4 18 0 101.96 112.77 49.63 o 1 19 0 13.43 9.13 4.76 o 2 19 0 758.61 1164.19 50.82 o 3 19 0 47.24 43.68 8.34 o 0 20 0 13290.31 13451.31 289.06 o 1 20 0 116.53 111.57 6.75 o 2 20 0 503.38 486.01 14.29 o 3 20 0 293.27 268.41 13.50 o 1 21 0 15.76 12.31 5.96 o 2 21 0 3187.34 3350.82 47.25 o 3 21 0 26.49 19.46 9.53 o 0 22 0 696.03 738.14 25.01 o 1 22 0 426.25 454.24 13.10 o 2 22 0 571.46 609.49 15.49 o 3 22 0 112.06 103.63 11.51 o 1 23 0 12.56 9.13 6.75 o 2 23 0 708.76 798.49 26.21 o 3 23 0 75.74 89.74 11.91 o 0 24 0 6529.15 6289.48 141.75 o 1 24 0 20.97 22.24 7.15 o 2 24 0 765.07 712.33 21.84 o 3 24 0 51.96 62.74 13.10 o 1 25 0 1054.09 1132.42 23.03 o 2 25 0 70.84 97.28 18.66 o 3 25 0 344.76 309.71 17.87 o 0 26 0 203.78 159.22 17.47 o 1 26 0 2292.37 2175.11 36.93 o 2 26 0 1601.31 1556.09 34.15 o 3 26 0 258.35 295.81 25.41 o 1 27 0 1348.90 1404.02 27.40 o 2 27 0 287.76 287.87 15.09 o 3 27 0 397.98 349.02 38.12 o 0 28 0 2.18 0.00 14.69 o 1 28 0 613.76 597.58 17.47 o 2 28 0 340.09 335.92 16.28 o 1 29 0 1102.15 1066.51 23.82 o 2 29 0 17.78 25.01 12.71 o 0 30 0 65.49 77.03 18.66 o 1 30 0 18.56 23.03 9.53 o 2 30 0 221.90 182.65 17.87 o 1 31 0 290.43 310.50 16.68 o 2 31 0 162.52 84.18 31.77 o 0 32 0 167.69 203.69 23.43 o 1 32 0 302.41 294.62 17.07 o 1 33 0 266.06 270.80 43.28 o -5 1 1 65.84 48.04 20.65 o -4 1 1 15.56 23.82 10.72 o -3 1 1 256.63 227.12 6.75 o -2 1 1 26900.73 29496.23 328.77 o -1 1 1 7059.78 6531.69 67.90 o 0 1 1 1208.44 1210.65 16.28 o 1 1 1 7158.53 7074.08 64.72 o 2 1 1 5687.57 6013.52 104.43 o 3 1 1 483.66 431.61 9.53 o 4 1 1 612.73 439.55 25.41 o -5 2 1 150.42 128.65 33.35 o -4 2 1 2315.28 2735.37 48.44 o -3 2 1 293.68 270.80 7.94 o -2 2 1 51.59 65.52 4.76 o -1 2 1 88.11 90.93 2.78 o 0 2 1 19132.93 21057.45 273.18 o 1 2 1 257.02 109.19 2.38 o 2 2 1 117.87 78.62 9.13 o 3 2 1 565.95 555.49 10.72 o 4 2 1 121.41 22.24 25.41 o -4 3 1 220.98 222.36 13.10 o -3 3 1 743.77 774.67 13.50 o -2 3 1 3428.60 3553.32 72.27 o -1 3 1 4003.78 4119.93 43.68 o 0 3 1 3252.48 3249.96 42.49 o 1 3 1 11210.14 10550.37 102.05 o 2 3 1 891.87 990.67 51.22 o 3 3 1 26.10 32.16 4.76 o 4 3 1 1.39 2.78 12.31 o -4 4 1 126.56 102.84 13.50 o -3 4 1 1840.87 1787.98 24.62 o -2 4 1 654.77 637.29 15.49 o -1 4 1 11337.92 11126.11 122.69 o 0 4 1 8664.97 9346.07 121.10 o 1 4 1 556.67 631.33 7.54 o 2 4 1 2762.36 2802.47 33.35 o 3 4 1 201.45 183.05 7.54 o 4 4 1 1.19 0.00 16.28 o -4 5 1 125.12 117.53 14.29 o -3 5 1 1.76 3.18 4.76 o -2 5 1 16914.40 17692.74 185.03 o -1 5 1 207.34 272.78 5.16 o 0 5 1 2345.26 2410.17 32.16 o 1 5 1 743.22 779.04 9.13 o 2 5 1 435.91 401.83 7.15 o 3 5 1 17.87 7.94 5.16 o 4 5 1 584.36 622.60 25.81 o -4 6 1 608.69 657.14 23.82 o -3 6 1 3356.50 3407.99 42.09 o -2 6 1 17.81 28.59 4.76 o -1 6 1 9657.85 9428.27 104.82 o 0 6 1 14157.79 15321.08 197.34 o 1 6 1 1943.48 2148.11 22.24 o 2 6 1 1922.97 1826.89 22.63 o 3 6 1 4.14 1.59 5.56 o 4 6 1 340.80 384.75 25.81 o -4 7 1 123.53 137.78 13.50 o -3 7 1 3302.61 3373.05 42.09 o -2 7 1 3.50 6.75 18.66 o -1 7 1 12405.35 12821.96 141.75 o 0 7 1 212.96 176.69 3.97 o 1 7 1 16747.48 16508.70 159.62 o 2 7 1 266.46 250.15 11.91 o 3 7 1 16.35 9.93 5.56 o 4 7 1 687.58 909.27 31.37 o -4 8 1 36.82 46.06 12.31 o -3 8 1 1529.59 1574.75 22.63 o -2 8 1 0.94 9.13 12.31 o -1 8 1 7856.12 7761.00 86.96 o 0 8 1 7314.41 7603.76 98.87 o 1 8 1 26.99 12.31 1.99 o 2 8 1 2265.00 2342.67 25.81 o 3 8 1 84.39 97.28 8.34 o 4 8 1 4.63 11.12 14.29 o -4 9 1 452.32 457.42 21.04 o -3 9 1 1534.98 1523.53 22.24 o -2 9 1 1825.53 1988.49 26.21 o -1 9 1 4391.81 4621.82 53.21 o 0 9 1 238.84 181.46 4.37 o 1 9 1 94.39 59.56 3.18 o 2 9 1 88.01 118.32 5.16 o 3 9 1 256.21 213.22 10.32 o 4 9 1 25.74 20.25 13.50 o -4 10 1 386.65 403.42 20.25 o -3 10 1 4460.37 4492.37 54.00 o -2 10 1 368.01 379.99 8.34 o -1 10 1 39528.99 39706.32 467.34 o 0 10 1 621.14 813.19 12.71 o 1 10 1 5387.03 5458.82 57.97 o 2 10 1 1023.68 927.54 17.87 o 3 10 1 9.57 8.74 6.75 o 4 10 1 208.51 198.53 16.28 o -4 11 1 92.35 106.41 15.49 o -3 11 1 2092.55 2222.76 29.78 o -2 11 1 93.43 117.53 11.51 o -1 11 1 17771.29 18646.88 221.56 o 0 11 1 728.99 646.82 10.72 o 1 11 1 16405.89 17034.01 188.21 o 2 11 1 2.29 7.94 5.96 o 3 11 1 1114.12 1034.35 21.44 o 4 11 1 127.70 166.37 15.88 o -4 12 1 17.36 16.28 14.29 o -3 12 1 210.31 223.15 8.74 o -2 12 1 1.59 12.31 6.35 o -1 12 1 1003.07 1038.72 16.28 o 0 12 1 14030.85 14925.21 206.47 o 1 12 1 7314.25 7453.27 84.57 o 2 12 1 79.88 91.72 9.93 o 3 12 1 11.65 26.60 7.94 o 4 12 1 107.54 87.75 15.49 o -4 13 1 45.63 42.49 15.49 o -3 13 1 1841.10 1923.77 27.00 o -2 13 1 1566.16 1530.28 29.78 o -1 13 1 7518.53 7565.64 85.77 o 0 13 1 329.61 386.34 7.15 o 1 13 1 3941.53 4011.53 47.25 o 2 13 1 724.64 708.36 16.68 o 3 13 1 2085.02 2068.30 35.34 o 4 13 1 273.96 353.39 21.04 o -4 14 1 231.87 261.27 19.06 o -3 14 1 5242.34 5394.90 64.32 o -2 14 1 9.02 9.93 7.54 o -1 14 1 11363.28 11261.11 126.27 o 0 14 1 2248.19 2406.60 31.37 o 1 14 1 40.22 63.13 4.37 o 2 14 1 577.70 607.11 14.69 o 3 14 1 320.78 297.80 13.90 o 4 14 1 22.26 21.44 15.49 o -4 15 1 4.96 9.93 18.26 o -3 15 1 78.61 71.87 7.15 o -2 15 1 8490.85 8628.58 98.87 o -1 15 1 621.74 599.17 10.32 o 0 15 1 416.03 365.30 7.94 o 1 15 1 3342.29 3370.67 40.90 o 2 15 1 1265.65 1294.82 23.82 o 3 15 1 1786.75 1683.94 34.94 o 4 15 1 39.24 40.50 16.28 o -4 16 1 128.09 173.52 21.84 o -3 16 1 19.79 19.06 6.75 o -2 16 1 115.76 127.06 7.94 o -1 16 1 237.43 225.53 6.75 o 0 16 1 10492.91 10425.29 136.99 o 1 16 1 1750.60 1650.19 22.24 o 2 16 1 470.07 472.51 12.71 o 3 16 1 327.20 363.71 15.88 o 4 16 1 34.11 7.15 17.87 o -4 17 1 37.05 29.38 22.63 o -3 17 1 243.66 262.86 10.32 o -2 17 1 202.51 292.64 24.62 o -1 17 1 877.89 963.67 15.09 o 0 17 1 2470.17 2658.34 40.50 o 1 17 1 1509.47 1496.93 21.04 o 2 17 1 160.13 430.81 35.74 o 3 17 1 29.63 28.19 9.93 o 4 17 1 77.70 48.44 19.85 o -4 18 1 641.35 514.20 48.04 o -3 18 1 959.13 999.41 18.66 o -2 18 1 36.45 76.24 13.10 o -1 18 1 134.55 154.85 6.35 o 0 18 1 6660.78 6904.13 116.74 o 1 18 1 1538.39 1426.65 22.24 o 2 18 1 79.35 244.19 21.44 o 3 18 1 0.07 2.38 9.53 o 4 18 1 8.63 109.99 40.50 o -3 19 1 352.32 382.77 13.50 o -2 19 1 9990.93 9914.67 124.28 o -1 19 1 161.86 160.02 6.75 o 0 19 1 706.80 759.58 18.66 o 1 19 1 1014.53 969.63 17.47 o 2 19 1 996.75 1044.28 20.25 o 3 19 1 1112.92 1138.38 32.56 o -3 20 1 5.44 5.16 7.94 o -2 20 1 257.98 278.34 12.31 o -1 20 1 248.18 235.86 7.94 o 0 20 1 1975.50 1963.87 38.12 o 1 20 1 14.90 19.85 5.56 o 2 20 1 3863.00 3908.29 54.40 o 3 20 1 808.88 806.44 27.40 o -3 21 1 31.63 25.41 8.74 o -2 21 1 6.79 83.38 18.66 o -1 21 1 3.79 9.13 5.96 o 0 21 1 962.50 1031.97 21.44 o 1 21 1 2033.94 2063.54 30.57 o 2 21 1 1819.65 1938.86 38.52 o 3 21 1 3.07 23.82 11.12 o -3 22 1 0.51 1.19 9.53 o -2 22 1 57.20 57.18 11.91 o -1 22 1 382.69 392.70 12.71 o 0 22 1 4435.07 4527.31 73.06 o 1 22 1 256.49 270.00 10.72 o 2 22 1 225.25 306.14 16.68 o 3 22 1 1.58 12.31 10.72 o -3 23 1 21.35 27.40 11.12 o -2 23 1 2673.16 2658.34 42.09 o -1 23 1 626.07 667.46 16.28 o 0 23 1 3556.91 3645.83 60.35 o 1 23 1 197.78 186.62 9.93 o 2 23 1 8.89 66.31 18.26 o 3 23 1 118.53 125.07 13.90 o -3 24 1 398.02 389.52 18.66 o -2 24 1 207.75 223.15 15.09 o -1 24 1 1536.11 1555.69 28.19 o 0 24 1 8.26 54.79 8.74 o 1 24 1 42.25 55.99 7.94 o 2 24 1 4458.14 4257.31 59.56 o 3 24 1 176.06 149.69 15.09 o -3 25 1 283.26 299.78 18.26 o -2 25 1 1668.56 1550.93 30.57 o -1 25 1 569.94 541.20 15.49 o 0 25 1 867.81 921.98 23.43 o 1 25 1 1674.62 1654.96 29.78 o 2 25 1 436.60 434.78 18.26 o 3 25 1 78.80 54.00 13.90 o -3 26 1 0.24 11.91 25.81 o -2 26 1 89.26 109.19 17.87 o -1 26 1 7.61 28.59 7.94 o 0 26 1 960.58 869.17 25.81 o 1 26 1 952.02 940.64 21.04 o 2 26 1 34.54 43.28 13.90 o 3 26 1 6.13 26.60 19.06 o -3 27 1 460.10 459.80 43.68 o -2 27 1 91.32 88.15 14.29 o -1 27 1 1775.23 1712.14 31.37 o 0 27 1 1243.81 1252.34 32.96 o 1 27 1 1392.50 1298.00 25.81 o 2 27 1 1249.72 1157.44 28.99 o -2 28 1 8.33 12.71 14.69 o -1 28 1 2229.71 2171.14 37.72 o 0 28 1 64.84 62.34 11.12 o 1 28 1 33.01 34.54 8.74 o 2 28 1 1395.13 1376.62 32.56 o -2 29 1 7.02 39.31 14.29 o -1 29 1 43.24 54.00 9.93 o 0 29 1 133.92 137.38 13.50 o 1 29 1 449.71 504.67 16.28 o 2 29 1 168.68 104.82 17.87 o -2 30 1 91.75 88.55 18.26 o -1 30 1 268.43 290.65 14.69 o 0 30 1 182.01 221.56 15.49 o 1 30 1 2611.28 2522.15 42.88 o 2 30 1 70.74 55.19 17.07 o -1 31 1 251.85 230.30 15.09 o 0 31 1 3.47 8.34 14.69 o 1 31 1 512.38 526.90 19.85 o 2 31 1 55.03 63.13 25.81 o -1 32 1 457.80 456.23 23.03 o 0 32 1 252.20 274.37 17.87 o 1 32 1 1142.29 1072.86 28.19 o -1 33 1 577.19 740.92 54.00 o 0 33 1 4.53 0.00 22.24 o 1 33 1 61.64 124.28 32.96 o 0 34 1 21.42 56.78 36.53 o -4 0 2 5938.29 6714.34 214.02 o -3 0 2 656.13 676.20 15.88 o -2 0 2 649.96 547.15 15.09 o -1 0 2 14584.54 14179.52 206.47 o 0 0 2 25581.51 25831.34 470.92 o 1 0 2 17163.77 15017.72 258.09 o 2 0 2 249.16 234.27 7.94 o 3 0 2 2064.36 1952.76 41.69 o 4 0 2 166.43 74.65 29.38 o -4 1 2 362.15 355.37 19.06 o -3 1 2 104.16 79.02 5.16 o -2 1 2 17171.84 18316.52 205.28 o -1 1 2 3870.72 4287.49 45.27 o 0 1 2 12104.48 11573.60 149.30 o 1 1 2 1569.55 1371.85 18.66 o 2 1 2 4167.75 4216.02 51.22 o 3 1 2 1692.63 1666.87 26.21 o 4 1 2 894.11 667.46 29.38 o -4 2 2 430.81 456.23 15.09 o -3 2 2 228.36 201.71 7.15 o -2 2 2 2194.03 2380.79 27.40 o -1 2 2 28499.21 27814.28 285.49 o 0 2 2 12848.41 12779.08 164.78 o 1 2 2 6749.85 6216.02 65.12 o 2 2 2 1454.03 1486.21 24.62 o 3 2 2 125.47 157.24 8.34 o 4 2 2 62.27 57.97 13.50 o -4 3 2 4.77 33.75 10.72 o -3 3 2 598.94 553.51 11.12 o -2 3 2 16678.04 16950.23 190.59 o -1 3 2 1164.00 877.91 10.72 o 0 3 2 153.93 121.10 2.78 o 1 3 2 1615.06 1584.68 17.87 o 2 3 2 317.26 305.34 7.15 o 3 3 2 4089.49 3931.72 53.21 o 4 3 2 2740.11 3015.30 81.00 o -4 4 2 2734.00 3076.45 44.07 o -3 4 2 995.29 1015.29 16.28 o -2 4 2 2481.47 2386.35 36.93 o -1 4 2 9.68 16.28 1.59 o 0 4 2 4725.59 4937.88 64.32 o 1 4 2 112.57 45.66 2.38 o 2 4 2 2.65 0.00 5.56 o 3 4 2 85.06 86.56 7.15 o 4 4 2 1136.65 1333.34 36.93 o -4 5 2 0.84 12.31 13.50 o -3 5 2 3281.51 3201.92 39.71 o -2 5 2 77.20 80.21 5.16 o -1 5 2 3991.29 4019.47 45.66 o 0 5 2 1144.21 918.01 13.10 o 1 5 2 169.58 193.37 3.97 o 2 5 2 558.30 479.65 14.69 o 3 5 2 9.95 13.10 6.75 o 4 5 2 150.00 158.83 17.47 o -4 6 2 740.23 860.83 27.40 o -3 6 2 521.93 510.62 11.12 o -2 6 2 406.81 418.50 14.29 o -1 6 2 12315.65 12073.90 133.41 o 0 6 2 678.74 630.14 9.93 o 1 6 2 425.78 340.68 5.56 o 2 6 2 1610.87 1544.58 23.43 o 3 6 2 737.80 708.36 16.28 o 4 6 2 3.92 61.15 23.03 o -4 7 2 53.73 55.19 15.09 o -3 7 2 12.61 13.90 5.16 o -2 7 2 2460.59 2572.18 32.16 o -1 7 2 361.97 445.50 7.54 o 0 7 2 759.51 642.05 9.93 o 1 7 2 1706.21 1668.06 19.06 o 2 7 2 550.41 575.34 13.10 o 3 7 2 456.76 446.70 15.09 o 4 7 2 855.89 842.17 25.01 o -4 8 2 309.24 316.46 19.06 o -3 8 2 3368.80 3519.17 43.68 o -2 8 2 48.17 97.68 11.51 o -1 8 2 9046.80 8432.43 94.50 o 0 8 2 296.35 237.44 5.16 o 1 8 2 73.67 44.47 2.78 o 2 8 2 2576.13 2405.41 28.19 o 3 8 2 1525.66 1510.43 30.97 o 4 8 2 1449.00 1685.14 44.07 o -4 9 2 205.27 179.87 19.85 o -3 9 2 6932.93 6880.71 86.56 o -2 9 2 166.95 170.74 6.35 o -1 9 2 256.22 265.24 5.96 o 0 9 2 1614.34 1309.51 19.06 o 1 9 2 2381.20 2255.32 25.41 o 2 9 2 2372.89 2329.17 29.38 o 3 9 2 245.90 272.78 12.71 o 4 9 2 603.11 667.46 23.03 o -4 10 2 0.58 0.00 14.69 o -3 10 2 677.25 677.79 14.29 o -2 10 2 814.29 886.64 16.28 o -1 10 2 1937.53 1851.51 23.03 o 0 10 2 101.13 106.02 3.97 o 1 10 2 1323.52 1257.10 16.68 o 2 10 2 1848.35 1933.30 25.41 o 3 10 2 7.56 14.69 7.94 o 4 10 2 576.48 655.15 23.03 o -4 11 2 175.05 179.87 17.87 o -3 11 2 465.76 448.28 11.91 o -2 11 2 329.76 278.74 7.54 o -1 11 2 5733.91 6062.76 69.09 o 0 11 2 550.42 498.31 9.13 o 1 11 2 242.35 312.89 6.75 o 2 11 2 2581.99 2453.85 33.75 o 3 11 2 2270.81 2097.69 40.10 o 4 11 2 22.78 21.04 16.28 o -4 12 2 141.40 133.02 17.07 o -3 12 2 3701.04 3787.98 50.82 o -2 12 2 1158.89 1263.46 21.84 o -1 12 2 14889.42 14720.72 163.59 o 0 12 2 4445.69 4570.59 61.15 o 1 12 2 37.76 47.65 3.97 o 2 12 2 644.15 596.79 14.69 o 3 12 2 2855.29 2812.00 50.82 o 4 12 2 303.36 307.33 19.06 o -4 13 2 45.79 24.62 15.88 o -3 13 2 1017.98 1087.56 21.84 o -2 13 2 1025.62 996.23 20.65 o -1 13 2 1569.44 1608.11 19.46 o 0 13 2 2265.39 2203.70 31.37 o 1 13 2 345.36 441.93 8.74 o 2 13 2 8.73 89.74 13.90 o 3 13 2 31.98 32.16 9.13 o 4 13 2 4.09 14.29 15.09 o -4 14 2 923.97 999.81 32.56 o -3 14 2 449.65 457.42 13.90 o -2 14 2 612.46 640.46 16.28 o -1 14 2 0.23 6.35 2.78 o 0 14 2 1087.55 989.48 15.88 o 1 14 2 13494.17 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