#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/01/2220198.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220198_Fobs loop_ _publ_author_name 'Khaldei, Hamid' 'Mohd Ali, Hapipah' 'Ng, Seik Weng' _publ_section_title ; Benzyl N'-(4,6-dimethoxy-2-methyl-3-phenyl-1H-indol-7-ylmethylene)hydrazinecarbodithioate ; _journal_coeditor_code HB2850 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2442 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.461 _cell_angle_beta 103.960 _cell_angle_gamma 93.944 _cell_length_a 10.0913 _cell_length_b 12.8541 _cell_length_c 18.9232 _exptl_crystal_F_000 1000.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file hb2850Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 350.65 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5.34 1.43 1.60 o 2 0 0 12260.04 13730.76 195.25 o 3 0 0 714.74 839.34 27.05 o 4 0 0 2259.96 2242.63 56.72 o 5 0 0 57.28 49.35 8.18 o 6 0 0 346.15 390.44 26.60 o 7 0 0 664.52 663.98 23.29 o 8 0 0 524.92 584.55 36.37 o 9 0 0 724.18 647.75 41.64 o 10 0 0 12.97 17.49 24.78 o 11 0 0 122.01 109.46 25.03 o 12 0 0 194.44 264.15 36.02 o -12 1 0 374.75 362.92 39.80 o -11 1 0 169.64 133.04 26.47 o -10 1 0 132.07 152.64 51.63 o -9 1 0 1.82 -6.02 12.78 o -8 1 0 127.57 128.68 20.86 o -7 1 0 825.54 831.88 27.69 o -6 1 0 396.87 366.90 19.73 o -5 1 0 1065.35 1104.06 37.95 o -4 1 0 2865.57 2868.11 67.00 o -3 1 0 103.89 85.04 6.24 o -2 1 0 100.07 115.68 5.70 o -1 1 0 383.50 370.90 8.09 o 1 1 0 304.76 286.55 11.55 o 2 1 0 2630.58 2720.77 58.16 o 3 1 0 92.52 132.55 7.25 o 4 1 0 1368.21 1253.11 26.53 o 5 1 0 1237.63 1320.04 40.64 o 6 1 0 4972.49 4977.57 85.77 o 7 1 0 1708.48 1688.79 58.78 o 8 1 0 0.23 -14.13 9.42 o 9 1 0 3.69 -16.87 11.25 o 10 1 0 23.14 13.56 16.35 o 11 1 0 0.19 21.70 28.28 o 12 1 0 17.19 24.53 36.52 o -12 2 0 10.83 -2.58 17.61 o -11 2 0 262.62 264.95 32.69 o -10 2 0 20.91 10.47 14.90 o -9 2 0 247.82 252.98 31.20 o -8 2 0 31.55 29.43 9.76 o -7 2 0 15.90 14.48 8.03 o -6 2 0 1958.88 2136.73 61.06 o -5 2 0 422.92 446.28 22.70 o -4 2 0 20.18 38.66 6.90 o -3 2 0 3392.01 3367.51 49.54 o -2 2 0 2222.60 2388.21 34.72 o -1 2 0 40.16 45.40 4.11 o 0 2 0 1239.55 1330.62 22.80 o 1 2 0 796.22 730.53 15.77 o 2 2 0 29932.18 31882.41 390.12 o 3 2 0 473.48 432.77 20.46 o 4 2 0 10961.92 11838.93 226.16 o 5 2 0 265.84 277.79 21.28 o 6 2 0 786.05 919.49 39.73 o 7 2 0 282.22 272.52 25.40 o 8 2 0 533.03 561.98 37.19 o 9 2 0 1459.45 1400.52 61.03 o 10 2 0 1.79 -2.23 14.58 o 11 2 0 228.21 214.36 33.12 o 12 2 0 32.04 43.84 23.76 o -12 3 0 123.29 140.03 28.96 o -11 3 0 755.27 723.23 47.47 o -10 3 0 12.73 13.35 14.76 o -9 3 0 70.27 111.22 20.68 o -8 3 0 292.44 290.38 19.70 o -7 3 0 0.04 -5.96 8.82 o -6 3 0 7.68 3.71 6.81 o -5 3 0 161.71 157.86 16.54 o -4 3 0 5196.23 5237.81 75.25 o -3 3 0 402.98 391.09 12.29 o -2 3 0 332.86 378.12 13.03 o -1 3 0 0.02 6.67 4.05 o 0 3 0 1115.76 1082.47 21.71 o 1 3 0 3713.38 3939.39 75.14 o 2 3 0 87.13 117.86 11.10 o 3 3 0 238.42 236.84 23.48 o 4 3 0 523.22 793.43 48.71 o 5 3 0 982.77 1083.13 49.23 o 6 3 0 92.45 86.51 15.82 o 7 3 0 929.21 827.86 41.43 o 8 3 0 1266.88 1341.08 57.11 o 9 3 0 1046.25 1075.55 53.96 o 10 3 0 87.62 79.56 21.80 o 11 3 0 3.68 -5.41 16.99 o 12 3 0 0.41 -5.94 18.70 o -12 4 0 5.01 17.03 16.64 o -11 4 0 18.87 17.72 17.17 o -10 4 0 1627.31 1530.92 63.11 o -9 4 0 150.56 146.19 17.27 o -8 4 0 857.93 858.23 32.20 o -7 4 0 21.61 14.13 8.73 o -6 4 0 3999.28 4439.84 71.05 o -5 4 0 68.88 82.45 8.56 o -4 4 0 3296.82 3340.44 52.15 o -3 4 0 194.37 193.06 11.18 o -2 4 0 547.60 489.72 15.78 o -1 4 0 1374.45 1468.96 29.48 o 0 4 0 303.85 294.19 11.81 o 1 4 0 266.23 246.47 13.07 o 2 4 0 9735.03 9846.45 187.08 o 3 4 0 3611.87 3853.37 66.53 o 4 4 0 230.74 185.48 17.77 o 5 4 0 961.59 1029.07 41.01 o 6 4 0 51.52 53.09 15.63 o 7 4 0 33.66 52.40 25.30 o 8 4 0 823.42 683.64 124.79 o 9 4 0 12.95 0.27 14.12 o 10 4 0 18.91 42.23 19.88 o 11 4 0 362.05 369.55 40.49 o 12 4 0 40.40 6.87 19.95 o -12 5 0 82.19 52.39 23.09 o -11 5 0 1.01 -1.78 13.08 o -10 5 0 1315.60 1332.82 46.82 o -9 5 0 89.35 87.88 15.18 o -8 5 0 207.00 197.92 15.44 o -7 5 0 541.80 609.87 25.91 o -6 5 0 2380.99 2430.99 67.39 o -5 5 0 301.95 301.93 20.19 o -4 5 0 735.04 701.11 38.76 o -3 5 0 161.20 181.98 11.66 o -2 5 0 3321.37 2945.40 52.81 o -1 5 0 272.30 274.73 14.54 o 0 5 0 4872.49 4944.87 80.18 o 1 5 0 182.23 203.96 11.11 o 2 5 0 2.39 2.81 7.05 o 3 5 0 120.28 148.22 13.01 o 4 5 0 139.32 137.51 9.10 o 5 5 0 0.25 5.15 9.60 o 6 5 0 343.61 272.29 44.04 o 7 5 0 719.64 679.70 43.91 o 8 5 0 167.32 158.59 28.67 o 9 5 0 396.18 397.93 37.18 o 10 5 0 228.43 278.99 35.22 o 11 5 0 291.67 289.26 38.99 o -12 6 0 233.04 261.13 47.35 o -11 6 0 38.25 15.70 23.35 o -10 6 0 28.10 28.75 18.02 o -9 6 0 23.80 29.05 10.75 o -8 6 0 2164.75 2235.14 82.63 o -7 6 0 91.19 81.69 12.99 o -6 6 0 5648.78 5523.90 98.70 o -5 6 0 60.07 41.01 11.10 o -4 6 0 3031.76 3029.87 71.25 o -3 6 0 118.96 135.12 11.15 o -2 6 0 15.39 5.00 6.77 o -1 6 0 34.77 29.67 6.98 o 0 6 0 249.78 314.66 14.46 o 1 6 0 24.81 35.10 11.42 o 2 6 0 815.04 874.50 112.08 o 3 6 0 1348.59 1476.78 45.29 o 4 6 0 879.80 798.75 24.33 o 5 6 0 216.96 225.24 22.79 o 6 6 0 538.02 495.99 33.63 o 7 6 0 546.09 535.33 53.57 o 8 6 0 198.87 192.16 36.78 o 9 6 0 36.06 14.61 15.52 o 10 6 0 9.52 6.53 24.78 o 11 6 0 43.88 59.37 24.56 o -11 7 0 0.24 -0.78 24.00 o -10 7 0 5.35 -16.53 13.62 o -9 7 0 22.40 27.18 10.91 o -8 7 0 323.30 368.74 23.92 o -7 7 0 68.26 68.27 12.95 o -6 7 0 1960.95 1982.43 59.66 o -5 7 0 76.23 72.83 13.37 o -4 7 0 457.83 374.07 22.25 o -3 7 0 285.13 289.96 15.93 o -2 7 0 9597.27 10102.31 153.42 o -1 7 0 538.95 525.85 19.62 o 0 7 0 4391.06 4266.49 75.64 o 1 7 0 80.98 56.75 20.04 o 2 7 0 178.55 192.51 25.04 o 3 7 0 451.16 515.02 20.74 o 4 7 0 607.50 622.34 22.92 o 5 7 0 173.65 159.17 21.64 o 6 7 0 564.87 485.37 34.32 o 7 7 0 3.28 5.99 12.70 o 8 7 0 132.97 81.61 27.24 o 9 7 0 29.70 24.08 23.87 o 10 7 0 6.18 -11.14 16.15 o 11 7 0 438.23 553.45 50.61 o -11 8 0 15.69 2.21 25.17 o -10 8 0 271.55 237.85 29.80 o -9 8 0 13.69 16.89 12.53 o -8 8 0 435.62 464.85 39.11 o -7 8 0 55.06 56.93 13.39 o -6 8 0 1903.72 1989.92 61.17 o -5 8 0 2.23 4.41 9.47 o -4 8 0 676.76 664.78 30.11 o -3 8 0 102.58 116.39 14.59 o -2 8 0 1781.12 1979.84 79.58 o -1 8 0 239.34 263.59 18.71 o 0 8 0 579.30 624.03 28.60 o 1 8 0 228.77 240.17 19.35 o 2 8 0 982.28 818.81 43.00 o 3 8 0 557.76 572.72 27.70 o 4 8 0 9.03 1.00 7.92 o 5 8 0 123.50 138.08 22.77 o 6 8 0 707.64 716.83 41.89 o 7 8 0 4.79 -5.81 18.29 o 8 8 0 204.75 211.70 30.74 o 9 8 0 30.65 23.64 19.47 o 10 8 0 3.87 8.85 20.09 o -11 9 0 61.43 99.76 32.95 o -10 9 0 487.81 536.71 40.28 o -9 9 0 134.10 139.65 19.91 o -8 9 0 488.24 614.80 41.85 o -7 9 0 53.45 29.56 13.68 o -6 9 0 3474.60 3726.87 112.34 o -5 9 0 9.05 10.86 10.53 o -4 9 0 957.22 949.58 37.88 o -3 9 0 20.19 32.70 14.92 o -2 9 0 635.30 656.87 40.28 o -1 9 0 23.86 22.65 9.39 o 0 9 0 408.64 465.98 26.20 o 1 9 0 0.80 6.09 8.69 o 2 9 0 3813.06 3707.34 93.63 o 3 9 0 2851.07 2797.03 61.96 o 4 9 0 0.12 -11.93 13.36 o 5 9 0 138.69 187.26 24.92 o 6 9 0 0.95 -17.26 11.51 o 7 9 0 2.68 -3.60 14.54 o 8 9 0 51.71 36.64 20.40 o 9 9 0 311.35 370.48 41.59 o 10 9 0 64.70 73.25 26.49 o -10 10 0 309.62 395.86 34.50 o -9 10 0 22.38 21.53 14.92 o -8 10 0 5.16 5.63 11.42 o -7 10 0 6.21 -8.32 12.11 o -6 10 0 1586.52 1558.96 55.52 o -5 10 0 64.90 67.68 15.68 o -4 10 0 3216.70 3156.22 81.98 o -3 10 0 28.43 25.21 16.73 o -2 10 0 16.92 24.83 15.44 o -1 10 0 104.03 89.18 14.80 o 0 10 0 1341.28 1315.95 46.92 o 1 10 0 4.34 17.25 11.14 o 2 10 0 186.20 170.43 16.34 o 3 10 0 193.90 202.99 17.88 o 4 10 0 662.55 659.76 54.74 o 5 10 0 0.11 -10.90 17.38 o 6 10 0 103.85 129.65 24.44 o 7 10 0 798.73 626.58 45.52 o 8 10 0 11.08 16.44 22.51 o 9 10 0 390.99 463.34 69.53 o -10 11 0 318.49 312.24 56.17 o -9 11 0 1.00 -9.70 13.77 o -8 11 0 40.09 19.29 13.74 o -7 11 0 75.11 49.43 18.42 o -6 11 0 14.11 2.46 19.20 o -5 11 0 1.54 -10.36 10.66 o -4 11 0 14.12 -4.44 10.47 o -3 11 0 24.30 8.13 18.36 o -2 11 0 438.53 425.55 28.21 o -1 11 0 23.82 28.25 12.31 o 0 11 0 1747.70 1684.45 56.93 o 1 11 0 842.51 794.31 39.39 o 2 11 0 1923.05 1928.14 52.41 o 3 11 0 84.38 70.70 14.31 o 4 11 0 15.63 15.12 14.06 o 5 11 0 51.64 42.03 23.87 o 6 11 0 261.66 239.72 42.16 o 7 11 0 150.66 109.74 34.51 o 8 11 0 86.31 105.95 58.63 o -9 12 0 51.00 38.14 34.25 o -8 12 0 413.50 412.38 60.58 o -7 12 0 110.32 108.83 18.67 o -6 12 0 51.58 65.29 23.03 o -5 12 0 35.75 43.26 16.54 o -4 12 0 312.32 348.02 28.39 o -3 12 0 3.85 -15.47 10.32 o -2 12 0 1549.82 1450.15 78.48 o -1 12 0 511.49 561.39 48.26 o 0 12 0 178.36 166.83 21.55 o 1 12 0 3.52 12.59 10.92 o 2 12 0 1604.05 1609.42 74.18 o 3 12 0 152.51 172.57 25.13 o 4 12 0 6.60 13.41 14.76 o 5 12 0 2.24 10.90 14.69 o 6 12 0 72.31 39.18 25.56 o 7 12 0 1.17 37.88 28.80 o 8 12 0 3.11 27.24 28.54 o -8 13 0 1819.85 2021.31 124.01 o -7 13 0 21.10 51.89 30.35 o -6 13 0 507.31 534.08 32.25 o -5 13 0 0.44 -4.07 18.23 o -4 13 0 0.37 2.63 13.30 o -3 13 0 207.55 170.84 35.15 o -2 13 0 0.10 -8.17 16.86 o -1 13 0 25.67 22.44 20.24 o 0 13 0 291.79 257.92 28.57 o 1 13 0 746.67 695.77 33.59 o 2 13 0 67.62 60.07 14.76 o 3 13 0 55.54 31.56 16.77 o 4 13 0 585.97 642.63 44.45 o 5 13 0 901.49 959.72 102.16 o 6 13 0 185.04 230.16 33.10 o 7 13 0 4.06 -12.60 17.24 o -7 14 0 6.59 13.23 30.35 o -6 14 0 109.09 107.93 39.05 o -5 14 0 69.20 71.61 35.41 o -4 14 0 41.14 29.20 14.49 o -3 14 0 1.54 -16.90 14.42 o -2 14 0 311.13 318.22 47.61 o -1 14 0 3.55 -0.59 13.80 o 0 14 0 904.43 939.34 49.48 o 1 14 0 86.37 106.63 23.02 o 2 14 0 173.53 146.33 37.49 o 3 14 0 85.78 82.13 23.20 o 4 14 0 13.32 -4.95 17.02 o 5 14 0 70.21 52.78 21.71 o 6 14 0 2.23 2.49 18.67 o -6 15 0 265.29 369.45 63.04 o -5 15 0 7.59 1.04 25.68 o -4 15 0 582.95 613.19 71.09 o -3 15 0 0.14 -7.13 15.83 o -2 15 0 188.91 213.78 30.61 o -1 15 0 3.98 36.53 19.34 o 0 15 0 15.28 6.40 16.60 o 1 15 0 118.07 77.03 22.46 o 2 15 0 31.46 23.35 28.15 o 3 15 0 102.47 133.48 41.51 o 4 15 0 18.79 21.92 29.45 o -4 16 0 35.06 17.38 33.21 o -3 16 0 49.21 37.88 31.65 o -2 16 0 43.56 78.35 37.75 o -1 16 0 19.26 54.87 34.12 o 0 16 0 640.04 779.90 51.89 o 1 16 0 807.31 924.52 79.13 o 2 16 0 301.42 376.45 56.43 o -2 -16 1 619.22 808.16 74.98 o -1 -16 1 360.52 370.28 38.48 o 0 -16 1 458.45 445.85 59.02 o 1 -16 1 193.24 145.68 41.51 o 2 -16 1 17.82 7.65 26.46 o 3 -16 1 0.19 -18.29 23.22 o 4 -16 1 755.59 769.38 81.46 o -4 -15 1 11.00 15.26 28.28 o -3 -15 1 43.88 25.30 28.15 o -2 -15 1 159.02 244.26 45.27 o -1 -15 1 26.75 31.02 18.41 o 0 -15 1 0.66 -8.83 15.62 o 1 -15 1 1.02 -6.33 21.92 o 2 -15 1 47.53 35.28 27.11 o 3 -15 1 81.76 52.02 31.26 o 4 -15 1 45.05 29.71 29.32 o 5 -15 1 5.39 19.59 28.41 o 6 -15 1 957.04 1130.52 98.98 o -6 -14 1 1.40 1.34 18.37 o -5 -14 1 22.24 22.25 19.61 o -4 -14 1 42.71 52.29 21.27 o -3 -14 1 0.15 -19.98 13.35 o -2 -14 1 29.02 25.79 13.39 o -1 -14 1 258.60 209.14 27.85 o 0 -14 1 1575.88 1753.65 124.86 o 1 -14 1 82.79 51.83 18.65 o 2 -14 1 975.72 1006.80 51.58 o 3 -14 1 156.97 179.01 56.69 o 4 -14 1 94.09 112.99 38.27 o 5 -14 1 0.06 9.08 26.20 o 6 -14 1 72.83 88.86 39.44 o 7 -14 1 70.27 123.88 43.85 o -7 -13 1 205.03 217.92 52.93 o -6 -13 1 93.83 112.04 26.23 o -5 -13 1 27.87 19.87 19.07 o -4 -13 1 551.31 680.94 45.21 o -3 -13 1 13.41 3.42 13.65 o -2 -13 1 103.29 93.58 25.45 o -1 -13 1 446.80 464.79 28.40 o 0 -13 1 470.17 477.24 28.46 o 1 -13 1 126.54 140.40 23.43 o 2 -13 1 115.53 108.69 21.51 o 3 -13 1 158.44 149.19 24.38 o 4 -13 1 35.30 0.92 11.26 o 5 -13 1 0.63 -0.45 15.13 o 6 -13 1 1244.11 1339.76 94.57 o 7 -13 1 35.78 40.99 32.43 o 8 -13 1 83.60 154.11 46.57 o -8 -12 1 4.81 -14.53 26.07 o -7 -12 1 230.49 204.57 44.75 o -6 -12 1 7.89 36.45 24.13 o -5 -12 1 200.09 206.78 29.71 o -4 -12 1 85.85 61.92 19.81 o -3 -12 1 0.01 -2.87 10.58 o -2 -12 1 2763.83 2830.60 68.89 o -1 -12 1 1175.77 1191.19 41.23 o 0 -12 1 21.57 8.12 12.33 o 1 -12 1 133.08 128.65 22.45 o 2 -12 1 2808.79 2925.41 134.15 o 3 -12 1 328.00 356.77 33.21 o 4 -12 1 228.41 278.76 22.74 o 5 -12 1 52.30 38.96 13.23 o 6 -12 1 32.79 16.75 12.07 o 7 -12 1 211.60 186.54 44.23 o 8 -12 1 33.70 50.07 35.93 o 9 -12 1 111.36 87.56 40.47 o -9 -11 1 452.86 462.71 64.34 o -8 -11 1 385.92 473.48 60.58 o -7 -11 1 323.11 250.10 45.40 o -6 -11 1 13.22 20.24 21.92 o -5 -11 1 202.12 243.62 41.25 o -4 -11 1 252.20 208.06 56.95 o -3 -11 1 427.91 417.23 24.93 o -2 -11 1 3596.94 3655.98 101.40 o -1 -11 1 810.78 899.96 34.10 o 0 -11 1 67.22 74.06 13.10 o 1 -11 1 107.51 107.49 17.05 o 2 -11 1 240.82 159.82 27.76 o 3 -11 1 17.19 14.22 11.09 o 4 -11 1 516.01 573.35 32.47 o 5 -11 1 0.22 11.20 10.28 o 6 -11 1 590.09 547.10 29.55 o 7 -11 1 31.96 30.67 13.59 o 8 -11 1 22.58 25.36 19.87 o 9 -11 1 74.40 46.70 32.43 o 10 -11 1 319.96 461.03 62.78 o -9 -10 1 935.82 918.69 61.09 o -8 -10 1 767.35 825.35 54.47 o -7 -10 1 1378.80 1360.07 63.88 o -6 -10 1 17.14 27.63 22.18 o -5 -10 1 38.38 38.92 22.70 o -4 -10 1 1261.95 1184.09 72.00 o -3 -10 1 5.35 -8.29 11.07 o -2 -10 1 2607.80 2546.48 60.15 o -1 -10 1 28.43 37.53 10.21 o 0 -10 1 303.21 290.72 23.01 o 1 -10 1 7.12 9.41 9.79 o 2 -10 1 412.82 466.21 72.25 o 3 -10 1 224.27 238.71 20.54 o 4 -10 1 721.78 849.88 36.87 o 5 -10 1 36.46 36.87 12.57 o 6 -10 1 8.91 -0.06 9.88 o 7 -10 1 47.13 66.27 20.42 o 8 -10 1 451.45 476.35 29.64 o 9 -10 1 35.55 48.97 28.27 o 10 -10 1 116.09 118.05 38.53 o -10 -9 1 50.34 68.04 25.87 o -9 -9 1 761.78 773.38 54.27 o -8 -9 1 297.95 302.11 53.25 o -7 -9 1 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