#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/02/2220271.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220271_Fobs loop_ _publ_author_name 'Yamaguchi, Toshiki' 'Masaoka, Shigeyuki' 'Sakai, Ken' _publ_section_title ; Diaqua(1,4,7,10,13-pentaoxacyclopentadecane)iron(II) bis(\m-cis-1,2-dicyano-1,2-ethylenedithiolato)bis[(cis-1,2-dicyano-1,2-ethylenedithiolato)ferrate(III)] 1,4,7,10,13-pentaoxacyclopentadecane disolvate ; _journal_coeditor_code LH2727 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1557 _journal_page_last m1558 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.600 _cell_angle_gamma 90.000 _cell_length_a 13.3763 _cell_length_b 15.7392 _cell_length_c 30.0695 _exptl_crystal_F_000 2952.00 _reflns_d_resolution_high 0.7800 _[local]_cod_data_source_file lh2727Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mnt2 in P2(1)/c 2008/09/24 21:38:41 003 KENX' _shelx_refln_list_code 4 _shelx_F_calc_maximum 918.50 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9237.99 9858.58 236.39 o 3 0 0 8861.12 8611.62 179.92 o 4 0 0 73095.17 78997.35 1580.63 o 5 0 0 2396.72 2319.46 82.62 o 6 0 0 46792.91 47262.41 750.65 o 7 0 0 77136.03 82423.65 1281.61 o 8 0 0 475.69 570.79 59.08 o 9 0 0 193.03 195.48 62.38 o 10 0 0 11073.25 11094.87 286.17 o 11 0 0 7775.09 7890.30 234.95 o 12 0 0 32653.07 32503.22 699.15 o 13 0 0 10293.78 10401.23 344.43 o 14 0 0 3029.33 3120.27 211.60 o 15 0 0 2.16 -116.77 116.77 o 16 0 0 9196.76 9091.96 569.17 o 17 0 0 0.65 12.85 224.91 o 2 1 0 9426.24 10365.07 122.09 o 3 1 0 32804.91 34572.99 384.56 o 4 1 0 6395.84 6662.60 133.89 o 5 1 0 3667.06 3620.19 74.28 o 6 1 0 21570.92 21862.38 259.29 o 7 1 0 1894.60 2135.36 59.40 o 8 1 0 2178.34 2220.13 63.34 o 9 1 0 5684.78 5684.81 102.47 o 10 1 0 2794.20 2865.79 82.65 o 11 1 0 3928.62 3930.65 115.09 o 12 1 0 41.64 20.98 55.71 o 13 1 0 1714.66 1753.08 100.24 o 14 1 0 230.74 106.56 74.44 o 15 1 0 31.90 -78.15 104.55 o 16 1 0 45.76 27.28 134.22 o 17 1 0 319.27 466.38 152.84 o 0 2 0 155792.80 168715.34 2694.72 o 1 2 0 28433.65 30299.72 378.52 o 2 2 0 1.98 17.66 16.71 o 3 2 0 408.57 403.13 24.58 o 4 2 0 3199.12 3009.26 57.90 o 5 2 0 6245.36 5877.35 90.78 o 6 2 0 100964.62 106497.48 1218.99 o 7 2 0 137.56 94.11 28.64 o 8 2 0 5153.11 5589.02 97.03 o 9 2 0 3.43 -4.47 33.29 o 10 2 0 2320.67 2297.93 77.73 o 11 2 0 40.32 -22.96 51.25 o 12 2 0 19640.95 19430.31 356.10 o 13 2 0 2327.49 2532.20 154.11 o 14 2 0 465.85 598.20 115.27 o 15 2 0 200.65 14.38 86.15 o 16 2 0 9588.75 9779.12 302.21 o 17 2 0 137.97 68.13 147.62 o 1 3 0 1554.65 1474.65 54.96 o 2 3 0 10026.06 10388.12 152.48 o 3 3 0 14535.34 15283.18 182.95 o 4 3 0 6386.50 6670.60 101.16 o 5 3 0 25.37 -5.12 22.74 o 6 3 0 22223.09 22236.47 282.77 o 7 3 0 8175.94 8231.91 119.22 o 8 3 0 69.95 6.14 30.37 o 9 3 0 2674.26 2813.60 73.67 o 10 3 0 3028.88 3252.55 87.16 o 11 3 0 12650.22 12461.42 243.93 o 12 3 0 255.42 212.69 76.45 o 13 3 0 450.65 439.07 86.18 o 14 3 0 142.85 99.11 83.87 o 15 3 0 251.56 257.20 93.29 o 16 3 0 1318.82 1297.88 128.12 o 0 4 0 164.81 135.38 52.88 o 1 4 0 46329.39 49723.73 588.97 o 2 4 0 75.87 142.82 37.48 o 3 4 0 26304.17 26977.53 408.63 o 4 4 0 2765.18 3042.79 60.28 o 5 4 0 1408.70 1458.64 46.12 o 6 4 0 2568.92 2487.45 61.16 o 7 4 0 30053.53 29721.06 503.76 o 8 4 0 18.56 16.34 31.07 o 9 4 0 414.43 446.12 41.86 o 10 4 0 3003.74 2937.43 92.98 o 11 4 0 6451.28 6147.42 181.96 o 12 4 0 2970.15 2948.83 140.32 o 13 4 0 7.73 -42.18 76.42 o 14 4 0 3286.29 3076.28 146.66 o 15 4 0 11.36 -88.85 88.85 o 16 4 0 1846.67 2095.41 146.85 o 1 5 0 51687.46 54847.75 610.31 o 2 5 0 13125.25 13279.97 180.27 o 3 5 0 5339.07 5529.38 109.35 o 4 5 0 632.82 756.01 37.69 o 5 5 0 888.83 998.50 48.30 o 6 5 0 874.76 994.78 42.46 o 7 5 0 1120.63 1206.73 50.48 o 8 5 0 80.83 55.93 37.61 o 9 5 0 56.57 -22.97 47.97 o 10 5 0 283.49 244.65 61.17 o 11 5 0 261.11 156.76 76.34 o 12 5 0 1120.32 1056.31 98.54 o 13 5 0 1401.61 1490.67 113.85 o 14 5 0 215.55 114.16 91.21 o 15 5 0 554.40 500.58 106.50 o 16 5 0 143.57 46.46 102.37 o 0 6 0 2483.36 3963.67 113.68 o 1 6 0 1758.85 1766.84 55.33 o 2 6 0 35698.97 36650.73 420.85 o 3 6 0 920.91 1095.45 57.24 o 4 6 0 2551.31 2487.15 83.21 o 5 6 0 1813.11 1884.33 64.52 o 6 6 0 387.94 342.54 32.86 o 7 6 0 7237.55 6893.31 147.97 o 8 6 0 2322.57 2464.49 88.82 o 9 6 0 16897.93 17131.52 264.17 o 10 6 0 4307.91 4338.07 157.58 o 11 6 0 36.28 -32.97 73.18 o 12 6 0 9.68 3.13 78.48 o 13 6 0 20.07 29.46 87.06 o 14 6 0 5256.10 5380.51 197.13 o 15 6 0 151.69 48.04 99.80 o 16 6 0 361.42 343.15 113.88 o 1 7 0 1402.92 1560.53 56.03 o 2 7 0 27933.38 28963.25 370.40 o 3 7 0 25658.98 26881.23 372.70 o 4 7 0 1790.73 2156.00 82.35 o 5 7 0 1400.74 1210.70 66.68 o 6 7 0 1606.81 1752.47 77.75 o 7 7 0 288.67 343.91 61.60 o 8 7 0 4276.46 4239.03 115.19 o 9 7 0 328.10 185.37 59.22 o 10 7 0 2340.45 2256.29 104.14 o 11 7 0 2064.78 2084.03 126.55 o 12 7 0 290.10 105.17 87.26 o 13 7 0 2311.63 2355.88 143.80 o 14 7 0 8.58 -89.31 89.31 o 15 7 0 230.93 87.69 105.73 o 16 7 0 1369.28 1313.31 146.15 o 0 8 0 1030.91 769.53 85.20 o 1 8 0 6949.43 6415.59 124.11 o 2 8 0 18.50 -10.11 28.69 o 3 8 0 96.37 80.86 33.35 o 4 8 0 649.27 597.82 61.28 o 5 8 0 8940.00 8418.06 164.87 o 6 8 0 6731.36 6674.91 155.17 o 7 8 0 5314.35 4958.11 138.48 o 8 8 0 1455.82 1629.64 83.31 o 9 8 0 6808.54 6772.09 152.58 o 10 8 0 13.17 -55.21 64.09 o 11 8 0 4095.80 3717.35 158.73 o 12 8 0 41.27 35.71 88.50 o 13 8 0 146.01 105.46 98.03 o 14 8 0 248.31 274.90 108.14 o 15 8 0 178.71 -27.18 104.86 o 1 9 0 644.95 921.53 59.23 o 2 9 0 2261.98 2046.11 64.97 o 3 9 0 22978.89 22960.64 337.81 o 4 9 0 916.41 1087.15 73.93 o 5 9 0 8733.21 8204.14 170.60 o 6 9 0 1773.91 1757.15 94.62 o 7 9 0 45.99 17.47 66.35 o 8 9 0 20264.19 19748.69 308.31 o 9 9 0 1384.66 1465.55 86.95 o 10 9 0 1941.32 1759.97 103.42 o 11 9 0 3260.25 3037.33 152.60 o 12 9 0 97.71 -90.38 90.38 o 13 9 0 5803.25 5571.18 213.86 o 14 9 0 4.08 -101.54 101.54 o 15 9 0 120.47 76.76 113.22 o 0 10 0 7194.06 7139.56 185.43 o 1 10 0 57930.34 58210.99 670.52 o 2 10 0 9273.15 9368.49 184.15 o 3 10 0 904.29 1017.91 76.80 o 4 10 0 8369.35 7903.99 170.22 o 5 10 0 12206.48 11970.63 235.19 o 6 10 0 1054.87 949.69 88.05 o 7 10 0 806.79 760.38 79.08 o 8 10 0 1025.74 1072.22 84.50 o 9 10 0 4487.93 4623.73 161.37 o 10 10 0 2300.46 2523.92 122.01 o 11 10 0 4778.87 4867.58 190.46 o 12 10 0 4805.32 4691.26 193.83 o 13 10 0 4944.35 4984.05 206.20 o 14 10 0 9.52 -47.95 110.63 o 1 11 0 46.53 4.33 81.58 o 2 11 0 8874.65 8512.68 195.98 o 3 11 0 20892.68 20759.33 588.04 o 4 11 0 21.97 -23.76 72.34 o 5 11 0 305.23 391.56 130.41 o 6 11 0 259.91 153.51 70.09 o 7 11 0 337.07 263.78 73.54 o 8 11 0 1238.07 1364.29 92.87 o 9 11 0 7088.94 7235.56 174.59 o 10 11 0 882.09 862.66 100.86 o 11 11 0 1020.49 951.90 122.96 o 12 11 0 767.16 946.48 124.01 o 13 11 0 2466.65 2840.93 171.17 o 14 11 0 27.30 -37.22 111.35 o 0 12 0 710.73 745.56 107.66 o 1 12 0 5062.53 4939.59 158.60 o 2 12 0 500.06 461.61 100.05 o 3 12 0 20.92 -39.74 75.59 o 4 12 0 18.86 19.04 78.81 o 5 12 0 505.72 418.62 75.76 o 6 12 0 168.53 99.30 71.25 o 7 12 0 1159.97 1135.56 90.76 o 8 12 0 2706.92 2762.04 117.75 o 9 12 0 2707.34 2806.68 121.43 o 10 12 0 542.07 607.74 98.43 o 11 12 0 4056.84 4201.78 192.27 o 12 12 0 1119.04 1236.59 137.77 o 13 12 0 5.71 -109.02 109.02 o 1 13 0 652.77 592.16 114.24 o 2 13 0 4845.97 4827.37 166.84 o 3 13 0 3838.82 3978.46 134.06 o 4 13 0 200.51 250.09 73.20 o 5 13 0 580.45 610.05 82.55 o 6 13 0 5472.12 5272.74 153.04 o 7 13 0 1093.34 1234.35 97.05 o 8 13 0 7828.75 7337.10 183.85 o 9 13 0 1150.47 1180.06 102.12 o 10 13 0 3243.03 3371.08 149.93 o 11 13 0 239.39 452.25 115.36 o 12 13 0 10314.89 10482.84 310.10 o 13 13 0 3.69 24.30 117.09 o 0 14 0 79.15 280.70 155.46 o 1 14 0 249.49 113.09 108.38 o 2 14 0 812.38 866.83 122.70 o 3 14 0 723.27 689.49 100.75 o 4 14 0 3871.28 3841.94 137.10 o 5 14 0 181.21 72.42 74.39 o 6 14 0 1055.77 1072.25 98.39 o 7 14 0 5607.64 5277.07 161.60 o 8 14 0 737.93 707.77 95.19 o 9 14 0 2039.79 2083.36 122.29 o 10 14 0 1.13 75.89 154.75 o 11 14 0 87.38 190.62 173.75 o 12 14 0 18.54 131.91 137.41 o 1 15 0 1888.29 1933.74 162.45 o 2 15 0 888.97 966.30 147.74 o 3 15 0 1972.24 2079.69 154.61 o 4 15 0 1512.57 1592.49 127.81 o 5 15 0 378.13 415.21 87.92 o 6 15 0 2270.84 2492.29 125.64 o 7 15 0 196.79 149.81 112.52 o 8 15 0 645.61 679.82 105.45 o 9 15 0 767.75 925.67 101.78 o 10 15 0 25.73 129.59 133.03 o 11 15 0 3284.49 3674.22 246.19 o 0 16 0 5073.49 4930.23 309.46 o 1 16 0 2696.32 2822.31 177.45 o 2 16 0 545.90 481.83 131.01 o 3 16 0 1.07 58.17 119.03 o 4 16 0 126.05 152.54 119.52 o 5 16 0 6739.27 7140.83 219.24 o 6 16 0 144.31 218.94 131.23 o 7 16 0 263.42 209.54 110.78 o 8 16 0 449.69 542.37 122.41 o 9 16 0 595.47 873.42 137.52 o 10 16 0 177.53 167.16 132.43 o 1 17 0 1208.32 1311.99 155.89 o 2 17 0 0.42 -109.25 120.40 o 3 17 0 1638.85 1449.04 158.25 o 4 17 0 0.99 -117.76 120.56 o 5 17 0 1640.08 1811.60 211.45 o 6 17 0 882.22 969.52 218.63 o 7 17 0 358.88 299.44 118.59 o 8 17 0 154.06 502.29 198.76 o 9 17 0 1691.50 1868.64 290.79 o 0 18 0 327.32 249.29 195.03 o 1 18 0 1167.15 1666.86 169.80 o 2 18 0 2348.71 2600.68 215.97 o 3 18 0 602.47 681.08 148.04 o 4 18 0 3100.71 3245.52 203.95 o 5 18 0 10498.87 10026.05 445.35 o 6 18 0 196.72 217.76 213.25 o 7 18 0 3441.55 3855.64 216.05 o 1 19 0 12.09 123.90 142.97 o 2 19 0 3165.95 3129.73 210.62 o 3 19 0 2603.27 2581.57 196.53 o 4 19 0 283.65 119.53 171.59 o 5 19 0 826.04 1152.33 166.73 o 0 20 0 864.05 763.55 239.59 o 1 20 0 1929.09 2199.08 199.53 o 2 20 0 2713.62 3034.59 306.35 o -17 1 1 35.77 317.61 147.55 o -16 1 1 5483.36 5375.15 276.60 o -15 1 1 619.47 444.15 118.56 o -14 1 1 145.76 146.42 86.22 o -13 1 1 2566.09 2516.61 115.46 o -12 1 1 14528.82 15018.50 265.29 o -11 1 1 2323.90 2373.56 94.97 o -10 1 1 1353.42 1578.86 63.49 o -9 1 1 4151.10 4043.81 86.03 o -8 1 1 10142.31 10776.74 152.11 o -7 1 1 27.50 31.23 29.46 o -6 1 1 62130.05 61977.84 864.80 o -5 1 1 19012.38 19623.35 428.34 o -4 1 1 294834.53 316044.19 4035.83 o -3 1 1 71062.95 72899.09 791.97 o -2 1 1 24397.43 24528.92 359.23 o -1 1 1 30088.23 30501.03 409.83 o 1 1 1 3690.52 3860.66 59.76 o 2 1 1 14005.19 14430.29 164.08 o 3 1 1 43258.01 44375.54 514.63 o 4 1 1 91504.48 96366.54 1092.93 o 5 1 1 1047.70 1186.33 40.31 o 6 1 1 20.02 -22.43 23.79 o 7 1 1 26349.36 27939.95 326.75 o 8 1 1 23788.68 23778.04 410.64 o 9 1 1 4581.71 4456.80 88.86 o 10 1 1 4532.73 4756.51 120.25 o 11 1 1 4135.26 4188.92 119.71 o 12 1 1 14369.51 14518.82 259.58 o 13 1 1 858.12 957.66 77.89 o 14 1 1 79.07 -17.73 70.06 o 15 1 1 411.09 135.04 96.15 o 16 1 1 3044.16 3131.79 228.07 o 17 1 1 144.91 170.40 259.34 o -17 2 1 469.36 775.55 264.39 o -16 2 1 2122.69 2352.36 162.07 o -15 2 1 3571.69 3675.35 160.47 o -14 2 1 398.90 423.59 109.95 o -13 2 1 32.05 -76.04 86.59 o -12 2 1 491.05 474.65 68.95 o -11 2 1 229.56 150.64 55.07 o -10 2 1 8.88 -7.15 37.81 o -9 2 1 7217.05 7196.87 119.30 o -8 2 1 8375.43 7991.74 122.94 o -7 2 1 17134.84 17793.58 234.53 o -6 2 1 16406.05 16839.66 210.25 o -5 2 1 2106.12 2385.54 57.42 o -4 2 1 50942.75 51686.95 625.52 o -3 2 1 95341.00 101915.13 1100.70 o -2 2 1 91154.20 96421.07 1176.88 o -1 2 1 36948.75 40023.88 498.59 o 0 2 1 57209.69 60009.76 779.69 o 1 2 1 1923.74 1928.64 46.99 o 2 2 1 5.59 42.42 17.39 o 3 2 1 24126.67 25529.15 435.96 o 4 2 1 999.70 1336.49 43.73 o 5 2 1 22405.13 22335.49 259.89 o 6 2 1 5431.47 6130.12 94.22 o 7 2 1 4105.95 4222.24 78.75 o 8 2 1 15282.06 15091.13 196.83 o 9 2 1 801.24 759.29 44.66 o 10 2 1 3242.62 3384.37 103.44 o 11 2 1 3359.70 3377.54 109.51 o 12 2 1 785.92 1094.66 84.44 o 13 2 1 356.85 346.66 88.82 o 14 2 1 128.62 47.36 97.90 o 15 2 1 12.26 -82.68 82.68 o 16 2 1 45.69 56.61 105.09 o 17 2 1 131.88 118.27 116.67 o -16 3 1 1922.40 2247.47 147.48 o -15 3 1 304.91 233.77 94.43 o -14 3 1 366.59 395.44 90.95 o -13 3 1 53.23 -73.26 73.90 o -12 3 1 4991.99 4980.26 163.63 o -11 3 1 82.08 19.09 55.46 o -10 3 1 2385.25 2446.57 74.38 o -9 3 1 1378.64 1557.23 56.90 o -8 3 1 22159.85 22914.91 295.16 o -7 3 1 12776.92 12668.50 221.20 o -6 3 1 2074.63 2170.57 56.80 o -5 3 1 6992.39 6936.86 102.13 o -4 3 1 2057.15 1959.46 48.90 o -3 3 1 2146.05 2192.51 48.50 o -2 3 1 4785.81 4839.15 91.56 o -1 3 1 2643.74 2773.73 67.92 o 0 3 1 7412.20 7484.85 99.28 o 1 3 1 1364.76 1349.87 39.98 o 2 3 1 4147.35 3930.88 74.20 o 3 3 1 11385.54 11946.84 215.09 o 4 3 1 3955.59 4256.71 73.79 o 5 3 1 2156.46 2142.89 51.56 o 6 3 1 1304.62 1388.96 46.91 o 7 3 1 736.43 758.63 37.38 o 8 3 1 6025.97 5773.99 97.98 o 9 3 1 153.98 133.73 36.80 o 10 3 1 4342.90 4476.43 113.80 o 11 3 1 810.22 807.46 71.94 o 12 3 1 5722.28 5636.82 174.64 o 13 3 1 533.82 448.05 86.08 o 14 3 1 253.92 53.50 83.66 o 15 3 1 894.88 946.65 131.36 o 16 3 1 4652.79 5038.60 195.44 o -16 4 1 1450.60 1668.11 139.56 o -15 4 1 1877.63 1895.36 134.52 o -14 4 1 25.89 10.18 83.97 o -13 4 1 3488.68 3645.43 152.51 o -12 4 1 571.43 498.51 82.65 o -11 4 1 8.12 21.94 71.00 o -10 4 1 62.34 65.02 61.58 o -9 4 1 1289.64 1313.79 60.34 o -8 4 1 1206.44 1239.04 55.61 o -7 4 1 14771.89 15004.86 196.24 o -6 4 1 20195.64 20368.07 249.31 o -5 4 1 7478.28 7752.42 156.57 o -4 4 1 9139.16 9590.03 127.97 o -3 4 1 9831.51 9913.06 154.12 o -2 4 1 22636.68 23468.02 312.45 o -1 4 1 8200.94 8706.35 126.79 o 0 4 1 11846.15 11404.60 146.42 o 1 4 1 3958.57 3967.01 71.44 o 2 4 1 2642.25 2649.13 59.60 o 3 4 1 11101.75 11605.44 148.32 o 4 4 1 37.92 35.94 23.87 o 5 4 1 282.08 173.89 26.59 o 6 4 1 1233.81 1397.23 46.24 o 7 4 1 11.31 16.85 27.86 o 8 4 1 6574.35 6286.30 104.62 o 9 4 1 2204.78 2348.98 68.52 o 10 4 1 596.35 593.88 64.85 o 11 4 1 2276.93 2167.80 118.31 o 12 4 1 2074.22 2142.67 119.69 o 13 4 1 460.60 538.96 91.54 o 14 4 1 5530.26 5643.13 192.37 o 15 4 1 229.41 223.17 94.58 o 16 4 1 53.76 -33.70 97.48 o -16 5 1 971.04 866.21 126.31 o -15 5 1 209.38 69.23 94.22 o -14 5 1 821.71 892.06 106.87 o -13 5 1 411.17 442.60 90.89 o -12 5 1 169.26 136.78 79.12 o -11 5 1 1119.46 1255.38 99.35 o -10 5 1 917.00 910.01 68.32 o -9 5 1 472.13 540.09 57.96 o -8 5 1 2671.01 2676.27 81.59 o -7 5 1 3069.54 2955.95 70.62 o -6 5 1 537.35 504.52 32.98 o -5 5 1 23070.32 23298.95 278.15 o -4 5 1 4028.15 4122.10 105.10 o -3 5 1 7177.41 7161.61 128.34 o -2 5 1 68.41 111.32 38.78 o -1 5 1 6266.59 6366.90 107.07 o 0 5 1 25566.39 26892.60 313.59 o 1 5 1 44769.05 47025.71 526.85 o 2 5 1 16.34 -6.31 26.35 o 3 5 1 6090.30 6230.99 106.16 o 4 5 1 895.18 981.11 41.35 o 5 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