#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220276.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220276_Fobs loop_ _publ_author_name 'Bartholom\"a, Mark Daniel' 'Ouellette, Wayne' 'Zubieta, Jon' _publ_section_title ; 2-(1,3-Dioxoisoindolin-2-yl)ethyl 4-methylbenzenesulfonate ; _journal_coeditor_code LH2734 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2395 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.121 _cell_angle_gamma 90.000 _cell_length_a 13.6817 _cell_length_b 12.5642 _cell_length_c 19.3194 _exptl_crystal_F_000 1440.00 _reflns_d_resolution_high 0.7550 _[local]_cod_data_source_file lh2734Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c2c in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 525.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14744.91 15451.91 202.89 o 4 0 0 108.29 202.86 5.74 o 6 0 0 9159.76 9348.04 103.45 o 8 0 0 21062.29 21180.43 226.78 o 10 0 0 820.93 880.14 27.14 o 12 0 0 38.07 39.32 8.40 o 14 0 0 984.98 961.00 33.96 o 16 0 0 2948.59 2922.92 70.18 o 1 1 0 16661.08 17062.28 118.97 o 3 1 0 6578.18 7248.30 55.90 o 5 1 0 4997.00 5333.25 43.43 o 7 1 0 3328.35 3986.56 35.12 o 9 1 0 702.87 798.89 12.09 o 11 1 0 1289.09 1150.30 25.11 o 13 1 0 211.07 225.83 11.92 o 15 1 0 956.14 922.70 24.44 o 17 1 0 587.38 616.02 20.98 o 0 2 0 93609.37 79463.44 7950.31 o 2 2 0 112.93 114.73 2.78 o 4 2 0 41.71 11.47 1.90 o 6 2 0 7390.52 7774.43 62.47 o 8 2 0 2198.17 2127.19 22.30 o 10 2 0 2017.28 2009.91 31.77 o 12 2 0 1905.92 1758.14 31.47 o 14 2 0 1216.10 1226.23 27.55 o 16 2 0 981.65 967.09 25.91 o 1 3 0 313.40 399.19 5.68 o 3 3 0 3731.35 3581.35 30.41 o 5 3 0 358.94 329.67 6.37 o 7 3 0 668.70 818.11 11.73 o 9 3 0 41.58 67.87 7.69 o 11 3 0 2661.16 2526.39 56.10 o 13 3 0 12.48 12.08 5.01 o 15 3 0 37.41 43.85 6.87 o 17 3 0 299.72 326.88 15.20 o 0 4 0 8610.48 8601.36 94.48 o 2 4 0 7373.92 7946.67 68.58 o 4 4 0 2617.83 2692.60 25.35 o 6 4 0 3155.62 3373.18 31.62 o 8 4 0 3.24 12.22 3.27 o 10 4 0 32.23 16.14 4.82 o 12 4 0 87.69 96.06 8.24 o 14 4 0 178.14 194.85 11.89 o 16 4 0 11.00 50.22 6.95 o 1 5 0 236.44 260.89 6.42 o 3 5 0 6273.54 7075.77 52.79 o 5 5 0 885.31 1009.68 13.43 o 7 5 0 210.87 202.83 10.21 o 9 5 0 195.29 169.91 6.40 o 11 5 0 0.22 -2.09 3.55 o 13 5 0 68.97 71.24 7.76 o 15 5 0 729.32 686.39 21.08 o 0 6 0 28.11 23.88 3.42 o 2 6 0 583.38 467.47 8.01 o 4 6 0 2037.98 2320.57 23.98 o 6 6 0 444.74 576.69 10.50 o 8 6 0 955.35 871.76 14.07 o 10 6 0 1121.10 1082.15 25.76 o 12 6 0 374.22 347.29 13.60 o 14 6 0 271.76 267.28 13.33 o 16 6 0 14.76 45.64 5.80 o 1 7 0 4156.24 5082.78 44.19 o 3 7 0 660.24 689.30 9.80 o 5 7 0 3310.50 3636.35 35.22 o 7 7 0 177.40 200.05 6.85 o 9 7 0 1813.53 1722.87 27.10 o 11 7 0 841.96 819.50 20.68 o 13 7 0 417.06 405.31 15.36 o 15 7 0 25.93 65.97 7.26 o 0 8 0 1228.52 1094.67 20.05 o 2 8 0 1788.52 1568.93 18.57 o 4 8 0 3486.35 3249.46 32.82 o 6 8 0 359.71 325.82 8.53 o 8 8 0 7254.60 7043.89 63.31 o 10 8 0 318.68 325.72 12.12 o 12 8 0 3294.99 3212.08 49.01 o 14 8 0 186.99 211.96 13.89 o 1 9 0 2.16 0.60 3.40 o 3 9 0 140.45 127.54 6.60 o 5 9 0 1912.26 1898.73 32.51 o 7 9 0 5112.17 5190.34 54.91 o 9 9 0 117.10 129.82 7.36 o 11 9 0 2.93 22.46 5.23 o 13 9 0 43.01 72.04 8.36 o 0 10 0 2.11 -2.10 5.51 o 2 10 0 218.20 214.53 10.28 o 4 10 0 4331.80 4222.38 146.71 o 6 10 0 3165.32 3067.28 60.22 o 8 10 0 3643.83 3355.36 57.62 o 10 10 0 504.84 536.41 15.88 o 12 10 0 2078.99 2045.95 44.06 o 1 11 0 250.75 236.57 11.30 o 3 11 0 156.71 141.14 9.31 o 5 11 0 3641.14 3473.26 48.42 o 7 11 0 1020.26 949.23 21.93 o 9 11 0 321.11 305.41 11.94 o 11 11 0 1.00 45.65 16.77 o 0 12 0 24.56 20.09 7.27 o 2 12 0 197.03 258.94 12.18 o 4 12 0 36.03 29.85 5.71 o 6 12 0 1140.69 1029.13 29.32 o 8 12 0 96.62 112.43 8.59 o 10 12 0 90.85 135.88 13.18 o 1 13 0 49.60 38.06 6.20 o 3 13 0 669.20 628.83 18.67 o 5 13 0 137.41 148.54 10.13 o 7 13 0 27.41 43.99 9.51 o 9 13 0 21.67 48.68 5.64 o 0 14 0 20.77 26.52 8.21 o 2 14 0 21.79 15.84 5.21 o 4 14 0 395.71 367.29 14.63 o 6 14 0 24.88 78.11 7.72 o 8 14 0 23.00 61.46 9.65 o 1 15 0 46.14 76.00 11.78 o 3 15 0 441.46 439.97 16.27 o 5 15 0 84.79 153.09 16.43 o 7 15 0 274.67 302.80 17.06 o 0 16 0 292.13 319.53 23.92 o 2 16 0 1.38 25.08 8.30 o 4 16 0 805.38 839.70 23.44 o -17 1 1 20.42 45.07 6.98 o -15 1 1 52.14 57.18 7.72 o -13 1 1 277.19 279.39 12.65 o -11 1 1 875.51 761.94 18.62 o -9 1 1 48.80 30.19 4.79 o -7 1 1 2742.52 2877.50 26.41 o -5 1 1 113.00 138.10 7.08 o -3 1 1 76.27 61.49 2.08 o -1 1 1 148.61 132.64 2.69 o 1 1 1 14416.62 15047.98 113.23 o 3 1 1 36118.41 38624.91 283.80 o 5 1 1 7206.08 7399.71 58.64 o 7 1 1 5626.16 5660.94 47.76 o 9 1 1 63.52 118.80 10.09 o 11 1 1 1327.97 1227.66 24.40 o 13 1 1 0.04 1.37 4.17 o 15 1 1 324.53 306.37 14.52 o 17 1 1 0.41 12.00 5.25 o -16 2 1 81.49 109.55 9.77 o -14 2 1 4.69 2.65 4.68 o -12 2 1 480.87 516.09 16.05 o -10 2 1 189.55 199.79 9.82 o -8 2 1 13.39 10.79 1.96 o -6 2 1 1425.73 1420.20 15.34 o -4 2 1 8436.75 8497.76 65.88 o -2 2 1 5754.56 5740.75 44.67 o 0 2 1 18081.20 18838.06 152.91 o 2 2 1 4332.27 4689.64 37.26 o 4 2 1 3984.34 4225.83 35.41 o 6 2 1 3063.74 3395.00 30.85 o 8 2 1 661.08 640.04 10.26 o 10 2 1 1039.65 1044.14 37.21 o 12 2 1 87.86 88.31 7.92 o 14 2 1 64.33 78.37 8.31 o 16 2 1 26.90 43.36 6.87 o -17 3 1 1163.27 1109.54 28.69 o -15 3 1 87.62 99.86 9.22 o -13 3 1 106.90 111.18 9.02 o -11 3 1 312.37 286.80 12.39 o -9 3 1 11102.85 11405.52 91.62 o -7 3 1 4934.47 5220.28 50.46 o -5 3 1 311.54 338.92 6.31 o -3 3 1 271.34 163.01 3.70 o -1 3 1 37097.55 37192.53 275.09 o 1 3 1 617.94 466.27 6.32 o 3 3 1 1133.76 967.76 11.14 o 5 3 1 125.87 90.78 3.71 o 7 3 1 13404.04 13245.73 103.90 o 9 3 1 145.42 175.48 6.37 o 11 3 1 1055.14 930.59 21.02 o 13 3 1 1155.67 1117.31 25.32 o 15 3 1 27.56 40.55 6.90 o -16 4 1 263.92 264.53 13.57 o -14 4 1 596.00 606.24 18.91 o -12 4 1 7.95 0.31 4.13 o -10 4 1 6602.93 6301.19 90.32 o -8 4 1 895.37 1027.61 17.99 o -6 4 1 123.20 109.59 4.34 o -4 4 1 6.57 1.08 1.43 o -2 4 1 5759.75 5693.97 46.15 o 0 4 1 304.21 321.51 5.16 o 2 4 1 17.03 8.29 1.62 o 4 4 1 131.16 162.54 6.40 o 6 4 1 1208.08 1161.24 14.79 o 8 4 1 3130.16 3183.53 32.02 o 10 4 1 8.39 -3.24 3.53 o 12 4 1 146.78 172.63 10.35 o 14 4 1 303.23 277.97 13.07 o 16 4 1 3.05 34.91 5.47 o -15 5 1 782.08 716.35 21.55 o -13 5 1 83.05 98.93 8.84 o -11 5 1 1197.79 1217.43 25.02 o -9 5 1 5427.90 5416.60 55.56 o -7 5 1 347.27 399.32 8.46 o -5 5 1 39.33 8.99 2.11 o -3 5 1 2500.94 2918.09 27.22 o -1 5 1 13654.02 14055.92 116.80 o 1 5 1 3515.21 3304.20 29.34 o 3 5 1 2412.49 2385.53 23.24 o 5 5 1 114.79 131.04 5.03 o 7 5 1 3168.86 2903.59 29.69 o 9 5 1 5254.49 5239.11 79.31 o 11 5 1 1383.71 1294.02 25.98 o 13 5 1 1267.47 1147.19 26.13 o 15 5 1 1109.09 1122.18 27.71 o -16 6 1 78.85 111.62 9.31 o -14 6 1 0.81 12.47 4.74 o -12 6 1 1956.02 1916.50 34.42 o -10 6 1 1879.33 1674.75 32.18 o -8 6 1 47.94 51.95 4.08 o -6 6 1 1477.03 1698.08 20.16 o -4 6 1 614.03 640.65 9.33 o -2 6 1 18.23 -1.46 1.76 o 0 6 1 1741.02 1700.26 17.81 o 2 6 1 76.66 67.74 3.00 o 4 6 1 40.17 53.23 3.70 o 6 6 1 2599.95 2872.44 29.43 o 8 6 1 714.08 687.39 12.60 o 10 6 1 438.52 379.57 13.29 o 12 6 1 244.42 239.03 11.72 o 14 6 1 0.28 12.94 8.23 o -15 7 1 160.82 234.49 12.56 o -13 7 1 655.14 648.56 19.45 o -11 7 1 446.98 409.42 14.57 o -9 7 1 169.98 147.86 6.50 o -7 7 1 1091.15 1080.48 16.00 o -5 7 1 639.29 588.06 10.71 o -3 7 1 3332.88 3651.26 34.40 o -1 7 1 1283.32 1377.19 16.09 o 1 7 1 13371.90 14610.30 113.43 o 3 7 1 1020.07 1047.69 14.11 o 5 7 1 597.97 712.28 11.87 o 7 7 1 110.56 102.20 5.44 o 9 7 1 2070.69 2009.32 28.41 o 11 7 1 38.31 41.51 6.14 o 13 7 1 92.81 123.26 9.48 o 15 7 1 1813.49 1794.64 36.49 o -14 8 1 2.84 22.27 5.85 o -12 8 1 535.05 522.21 16.95 o -10 8 1 143.73 156.91 7.68 o -8 8 1 343.06 283.30 8.56 o -6 8 1 2577.63 2430.06 27.33 o -4 8 1 318.58 348.16 7.81 o -2 8 1 1505.78 1624.52 19.00 o 0 8 1 799.84 831.78 11.71 o 2 8 1 346.87 232.77 5.18 o 4 8 1 746.87 766.20 12.51 o 6 8 1 1911.03 1852.43 22.72 o 8 8 1 389.84 416.13 10.42 o 10 8 1 86.17 96.71 9.95 o 12 8 1 1384.97 1352.74 33.58 o 14 8 1 29.49 60.96 15.97 o -13 9 1 300.29 309.79 15.18 o -11 9 1 494.57 506.99 19.20 o -9 9 1 911.70 936.93 18.15 o -7 9 1 474.68 490.34 14.53 o -5 9 1 1458.18 1220.49 17.75 o -3 9 1 324.58 387.60 9.91 o -1 9 1 97.42 147.72 12.63 o 1 9 1 59.50 144.35 6.42 o 3 9 1 1855.97 1730.29 24.26 o 5 9 1 343.06 306.93 9.91 o 7 9 1 105.31 98.75 6.78 o 9 9 1 1229.62 1120.65 20.36 o 11 9 1 67.09 92.04 11.30 o 13 9 1 270.52 307.16 15.53 o -14 10 1 0.62 26.50 9.15 o -12 10 1 5.25 34.52 5.59 o -10 10 1 1423.62 1429.70 27.48 o -8 10 1 628.53 583.87 14.28 o -6 10 1 2507.38 2319.62 35.94 o -4 10 1 601.34 521.06 15.40 o -2 10 1 391.44 403.83 13.33 o 0 10 1 278.26 271.89 11.18 o 2 10 1 1919.30 1578.34 69.09 o 4 10 1 3.69 0.58 3.35 o 6 10 1 63.11 68.03 9.59 o 8 10 1 3392.18 3243.37 40.43 o 10 10 1 974.83 972.73 22.16 o 12 10 1 476.40 545.25 20.51 o -13 11 1 122.06 196.80 16.08 o -11 11 1 1471.76 1565.13 46.17 o -9 11 1 964.47 888.78 20.85 o -7 11 1 2627.89 2518.98 39.40 o -5 11 1 6624.72 6256.60 74.42 o -3 11 1 3401.90 3299.90 46.45 o -1 11 1 3149.87 2908.74 56.06 o 1 11 1 1871.56 1727.33 30.09 o 3 11 1 1868.20 1703.93 32.46 o 5 11 1 142.85 114.81 8.86 o 7 11 1 3.35 23.51 4.95 o 9 11 1 3205.58 3064.32 43.82 o 11 11 1 649.83 642.10 21.90 o -12 12 1 248.74 296.85 18.49 o -10 12 1 1.29 23.38 10.67 o -8 12 1 79.69 111.56 8.59 o -6 12 1 672.77 763.30 20.26 o -4 12 1 22.12 30.73 6.17 o -2 12 1 2224.16 1897.96 33.27 o 0 12 1 240.58 233.44 11.45 o 2 12 1 516.55 491.36 15.75 o 4 12 1 161.30 149.52 9.80 o 6 12 1 715.38 686.53 19.01 o 8 12 1 328.78 385.26 14.32 o 10 12 1 34.54 60.29 7.43 o -9 13 1 334.19 357.77 18.69 o -7 13 1 189.88 256.94 12.42 o -5 13 1 2107.26 2132.37 37.31 o -3 13 1 173.11 179.02 10.90 o -1 13 1 1686.65 1497.00 29.67 o 1 13 1 740.71 729.23 20.03 o 3 13 1 1727.85 1630.71 31.43 o 5 13 1 1769.63 1619.28 31.63 o 7 13 1 1065.56 975.18 23.83 o 9 13 1 1145.13 1269.58 27.85 o -8 14 1 291.98 322.08 13.69 o -6 14 1 334.76 375.46 14.73 o -4 14 1 24.64 33.27 6.52 o -2 14 1 1502.57 1374.64 29.25 o 0 14 1 13.16 15.14 4.43 o 2 14 1 101.41 112.85 9.27 o 4 14 1 44.89 73.73 7.51 o 6 14 1 402.15 403.57 15.26 o 8 14 1 209.50 246.77 23.50 o -7 15 1 585.02 646.83 20.04 o -5 15 1 787.62 844.12 26.61 o -3 15 1 266.35 288.25 13.34 o -1 15 1 1001.51 1011.24 25.36 o 1 15 1 787.07 785.06 22.02 o 3 15 1 346.08 369.55 14.94 o 5 15 1 631.67 678.30 20.54 o 7 15 1 928.46 992.51 29.49 o -4 16 1 271.11 350.78 14.83 o -2 16 1 667.34 729.59 21.65 o 0 16 1 606.15 707.40 25.36 o 2 16 1 60.84 127.32 15.78 o 4 16 1 24.15 55.15 6.16 o -16 0 2 1929.23 1810.59 52.01 o -14 0 2 2.40 7.21 7.21 o -12 0 2 9887.90 10136.42 156.49 o -10 0 2 13729.49 14284.75 204.03 o -8 0 2 3223.90 3250.54 57.55 o -6 0 2 6706.82 6452.19 255.88 o -4 0 2 2991.47 3365.71 51.55 o -2 0 2 25240.36 26586.00 438.11 o 0 0 2 14512.10 14490.44 388.04 o 2 0 2 0.67 17.36 3.99 o 4 0 2 16625.38 17169.65 181.55 o 6 0 2 226.50 174.21 22.16 o 8 0 2 2384.08 2420.04 34.97 o 10 0 2 213.09 175.07 13.13 o 12 0 2 3470.91 3357.20 85.49 o 14 0 2 1077.35 1014.93 35.37 o 16 0 2 4.43 27.80 8.71 o -17 1 2 49.76 87.05 8.93 o -15 1 2 384.02 382.93 15.52 o -13 1 2 1705.05 1556.37 30.04 o -11 1 2 3209.58 3013.26 83.97 o -9 1 2 1306.92 1097.11 20.72 o -7 1 2 1916.86 1899.59 21.48 o -5 1 2 1969.83 1849.33 23.72 o -3 1 2 36504.63 37588.38 257.62 o -1 1 2 11836.17 12147.13 112.39 o 1 1 2 1989.09 2215.14 20.45 o 3 1 2 252216.13 185240.14 1919.51 o 5 1 2 2760.80 3005.71 27.11 o 7 1 2 4611.60 4732.31 41.46 o 9 1 2 1855.59 2121.92 32.19 o 11 1 2 1002.29 992.54 21.73 o 13 1 2 52.76 39.20 6.23 o 15 1 2 254.77 274.05 15.06 o -16 2 2 1836.33 1732.94 35.83 o -14 2 2 5.56 2.79 4.65 o -12 2 2 1608.56 1532.21 28.83 o -10 2 2 637.93 604.38 15.74 o -8 2 2 384.50 328.69 8.06 o -6 2 2 1677.81 1677.89 16.99 o -4 2 2 346.63 238.22 4.36 o -2 2 2 13245.21 13437.70 100.48 o 0 2 2 42085.35 43167.53 353.81 o 2 2 2 44730.48 45929.25 341.04 o 4 2 2 389.35 351.37 6.26 o 6 2 2 67.53 177.68 5.50 o 8 2 2 825.21 793.88 12.10 o 10 2 2 292.24 239.21 10.43 o 12 2 2 9.85 11.85 4.88 o 14 2 2 928.36 909.27 23.57 o 16 2 2 184.66 256.09 13.61 o -17 3 2 557.21 612.96 20.66 o -15 3 2 26.58 37.42 6.77 o -13 3 2 686.20 601.53 19.80 o -11 3 2 3126.01 3021.00 70.85 o -9 3 2 8380.18 8694.83 80.21 o -7 3 2 3.98 15.77 3.10 o -5 3 2 80.67 45.91 2.60 o -3 3 2 5942.92 6429.37 51.01 o -1 3 2 33.12 44.57 2.14 o 1 3 2 4112.25 4161.55 34.14 o 3 3 2 1053.96 1246.06 13.43 o 5 3 2 775.40 938.69 12.25 o 7 3 2 1314.74 1329.53 16.61 o 9 3 2 379.53 406.33 8.97 o 11 3 2 1825.16 1698.41 30.17 o 13 3 2 13.15 25.97 5.86 o 15 3 2 153.28 178.78 11.59 o -16 4 2 695.43 631.86 24.71 o -14 4 2 0.01 0.71 4.70 o -12 4 2 60.97 71.95 7.35 o -10 4 2 231.13 242.03 10.53 o -8 4 2 169.23 206.55 5.76 o -6 4 2 418.90 461.13 8.27 o -4 4 2 32.83 30.51 2.26 o -2 4 2 1261.13 1291.19 13.76 o 0 4 2 154.62 125.55 4.26 o 2 4 2 45.04 68.55 2.88 o 4 4 2 572.07 568.32 8.89 o 6 4 2 228.71 258.65 6.67 o 8 4 2 320.54 308.19 8.03 o 10 4 2 82.15 102.02 7.83 o 12 4 2 251.00 244.15 11.65 o 14 4 2 454.07 437.51 18.04 o 16 4 2 98.07 137.89 9.94 o -15 5 2 2067.17 1961.82 37.99 o -13 5 2 656.42 614.20 18.61 o -11 5 2 354.11 360.32 13.28 o -9 5 2 116.94 135.84 5.96 o -7 5 2 3579.90 3856.22 36.28 o -5 5 2 14.23 32.06 2.68 o -3 5 2 9161.69 10818.50 84.47 o -1 5 2 17488.19 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o -6 0 24 15.88 25.35 8.54 o -4 0 24 896.41 978.08 35.35 o -2 0 24 9.39 28.38 8.12 o 0 0 24 176.10 154.76 15.34 o -9 1 24 2772.46 2836.67 70.98 o -7 1 24 1375.60 1445.95 30.75 o -5 1 24 331.91 340.53 14.52 o -3 1 24 2251.53 2287.58 41.04 o -1 1 24 206.88 291.47 14.29 o -10 2 24 9.42 31.87 9.85 o -8 2 24 62.34 99.89 8.46 o -6 2 24 109.07 162.66 10.68 o -4 2 24 53.96 81.34 8.00 o -2 2 24 49.08 88.73 9.55 o 0 2 24 21.10 39.81 10.16 o -9 3 24 133.96 189.93 17.35 o -7 3 24 906.96 916.25 23.83 o -5 3 24 193.04 222.71 11.88 o -3 3 24 37.64 64.95 8.86 o -1 3 24 17.26 29.71 7.25 o -8 4 24 239.55 300.81 15.37 o -6 4 24 276.62 294.25 15.55 o -4 4 24 3.49 21.01 6.39 o -2 4 24 296.92 299.40 17.20 o -7 5 24 15.44 50.53 7.64 o -5 5 24 0.01 28.74 6.76 o -3 5 24 371.75 407.07 19.06 o -7 1 25 464.30 571.94 18.81 o -5 1 25 176.72 205.78 12.21 o -3 1 25 1.73 35.48 7.38 o -8 2 25 1072.88 1127.76 27.01 o -6 2 25 11.25 44.30 8.73 o -4 2 25 1147.90 1194.94 28.67 o -7 3 25 43.79 76.46 8.68 o -5 3 25 134.83 146.49 12.35 o