#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220284.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220284_Fobs loop_ _publ_author_name 'Lin, Chia-Her' 'Kuo, Ting-Shen' 'Tong, Hung-Chun' 'Chen Hsu, Chih-Yung' 'Lo, Yih-Hsing' _publ_section_title ; Azido(1,1-diphenylmethanimine-\kN)[hydridotris(pyrazolyl-\kN^2^)borato](triphenylphosphine-{\kP})ruthenium(II) diethyl ether solvate ; _journal_coeditor_code NC2120 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1511 _journal_page_last m1512 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.445 _cell_angle_beta 81.716 _cell_angle_gamma 88.040 _cell_length_a 11.7387 _cell_length_b 13.0535 _cell_length_c 14.7187 _exptl_crystal_F_000 904.00 _reflns_d_resolution_high 0.8397 _[local]_cod_data_source_file nc2120Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a8770_0m in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 219.68 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2177.89 2363.16 32.01 o 2 0 0 8218.41 9018.02 103.82 o 3 0 0 3.72 -19.91 19.91 o 4 0 0 3119.14 3172.56 49.61 o 5 0 0 2313.82 2395.47 47.21 o 6 0 0 9921.44 9871.79 147.40 o 7 0 0 286.09 281.89 27.69 o 8 0 0 8553.15 8556.55 315.54 o 9 0 0 1523.18 1472.05 93.20 o 10 0 0 587.10 711.48 94.34 o 11 0 0 549.80 454.57 87.91 o 12 0 0 221.66 177.51 79.03 o 13 0 0 39.90 16.26 75.46 o -13 1 0 44.42 -66.86 70.85 o -12 1 0 50.65 -3.38 69.82 o -11 1 0 24.28 28.90 61.64 o -10 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1104.26 66.25 o 5 7 0 632.07 665.61 44.32 o 6 7 0 254.11 200.91 37.07 o 7 7 0 47.98 51.95 35.32 o 8 7 0 82.76 66.57 37.17 o 9 7 0 256.98 233.90 46.46 o 10 7 0 738.96 937.80 195.17 o 11 7 0 47.96 74.98 57.57 o 12 7 0 235.39 249.82 79.26 o -11 8 0 75.75 137.10 147.67 o -10 8 0 209.88 274.48 143.30 o -9 8 0 115.90 80.54 79.31 o -8 8 0 42.54 6.42 86.78 o -7 8 0 517.54 485.49 85.08 o -6 8 0 800.98 853.85 214.06 o -5 8 0 380.08 362.71 112.52 o -4 8 0 2820.15 2761.60 93.02 o -3 8 0 791.57 669.12 54.02 o -2 8 0 205.10 201.60 39.19 o -1 8 0 807.16 875.90 60.73 o 0 8 0 302.97 232.35 26.19 o 1 8 0 3.11 -20.27 20.27 o 2 8 0 1545.24 1510.53 43.14 o 3 8 0 657.27 550.65 78.83 o 4 8 0 1107.09 1034.90 58.33 o 5 8 0 764.03 694.92 50.00 o 6 8 0 12.34 -1.16 37.05 o 7 8 0 487.58 466.62 46.54 o 8 8 0 528.16 531.18 52.53 o 9 8 0 101.54 4.62 85.21 o 10 8 0 606.84 640.59 105.74 o 11 8 0 267.12 307.53 113.91 o -11 9 0 651.99 874.47 181.03 o -10 9 0 13.92 -103.96 138.72 o -9 9 0 0.62 0.92 105.01 o -8 9 0 2.55 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