#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/03/2220320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220320_Fobs loop_ _publ_author_name 'Bon, V. V.' 'Dudko, A. V.' 'Kozachkova, A. N.' 'Pekhnyo, V. I.' _publ_section_title ; Ammonium 1-ammonioethane-1,1-diylbis(hydrogenphosphonate) dihydrate ; _journal_coeditor_code RK2118 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2340 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.957 _cell_angle_gamma 90.000 _cell_length_a 8.8922 _cell_length_b 6.9390 _cell_length_c 18.9576 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.7974 _[local]_cod_data_source_file rk2118Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 901 in P2(1)/n New: P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 218.04 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7594.13 7556.54 76.30 o 2 0 0 222.80 265.49 12.26 o 3 0 0 929.17 1029.39 19.13 o 4 0 0 452.69 444.95 15.61 o 5 0 0 877.46 868.13 26.45 o 6 0 0 5379.65 5394.63 86.30 o 7 0 0 248.97 273.46 23.15 o 8 0 0 354.79 400.99 42.41 o 9 0 0 169.16 194.47 47.42 o 3 1 0 5397.47 5561.49 48.88 o 4 1 0 2044.42 2047.51 25.30 o 5 1 0 329.56 318.89 11.27 o 6 1 0 9.71 0.46 6.46 o 7 1 0 16.16 20.22 8.60 o 8 1 0 587.32 650.82 31.69 o 9 1 0 805.11 788.32 64.65 o 0 2 0 4944.34 4631.89 48.57 o 1 2 0 4308.62 4316.95 33.23 o 2 2 0 7911.10 7552.80 56.67 o 3 2 0 1605.58 1667.55 27.29 o 4 2 0 1175.72 1187.11 21.49 o 5 2 0 405.93 382.36 11.38 o 6 2 0 1390.98 1294.92 27.23 o 7 2 0 572.95 569.49 20.15 o 8 2 0 1627.05 1630.66 34.71 o 9 2 0 74.69 67.40 21.45 o 1 3 0 1404.63 1490.78 18.84 o 2 3 0 20.71 12.29 4.03 o 3 3 0 195.37 168.99 6.90 o 4 3 0 2913.23 2844.18 37.75 o 5 3 0 47.24 33.89 7.22 o 6 3 0 305.80 282.16 17.41 o 7 3 0 398.69 377.96 17.26 o 8 3 0 321.48 385.46 33.10 o 9 3 0 161.11 122.35 30.46 o 0 4 0 11189.58 11159.76 172.28 o 1 4 0 279.70 299.10 11.29 o 2 4 0 45.98 38.45 5.41 o 3 4 0 207.64 218.87 10.10 o 4 4 0 2774.80 2688.68 34.05 o 5 4 0 213.30 188.49 12.41 o 6 4 0 1826.07 1757.12 32.99 o 7 4 0 215.98 208.69 15.57 o 8 4 0 99.76 125.10 26.74 o 1 5 0 65.13 55.72 7.76 o 2 5 0 780.13 758.91 21.21 o 3 5 0 104.51 108.16 8.91 o 4 5 0 997.97 987.20 24.87 o 5 5 0 929.21 896.87 24.58 o 6 5 0 161.44 179.84 18.44 o 7 5 0 0.38 5.48 21.18 o 8 5 0 351.61 441.36 74.77 o 0 6 0 1820.30 1697.38 54.20 o 1 6 0 7.72 6.08 7.62 o 2 6 0 238.29 255.29 15.63 o 3 6 0 31.29 33.85 9.30 o 4 6 0 3.60 7.89 10.34 o 5 6 0 685.59 707.99 39.91 o 6 6 0 981.88 1022.33 49.54 o 7 6 0 263.62 344.56 50.49 o 1 7 0 1690.97 1637.88 32.01 o 2 7 0 0.44 -4.67 8.17 o 3 7 0 7.24 4.91 12.02 o 4 7 0 166.63 183.90 36.32 o 5 7 0 173.57 184.77 29.82 o 0 8 0 633.83 729.56 34.61 o 1 8 0 6.23 45.35 19.97 o 2 8 0 1026.84 1048.00 73.74 o 3 8 0 7.52 -3.26 19.18 o -9 1 1 129.67 182.91 26.15 o -8 1 1 493.41 519.89 21.24 o -7 1 1 809.30 778.35 21.54 o -6 1 1 1264.11 1242.84 26.12 o -5 1 1 2786.91 2759.05 32.93 o -4 1 1 376.00 400.72 10.90 o -3 1 1 825.32 972.93 13.43 o -2 1 1 1714.77 1698.85 14.50 o -1 1 1 2485.34 2677.23 17.79 o 0 1 1 6246.98 6380.14 43.48 o 1 1 1 1143.21 1145.74 11.62 o 2 1 1 2713.38 2585.37 23.61 o 3 1 1 324.18 349.83 8.09 o 4 1 1 539.39 533.23 12.25 o 5 1 1 1298.99 1297.62 21.24 o 6 1 1 1367.91 1331.92 25.86 o 7 1 1 17.31 11.97 9.93 o 8 1 1 658.27 694.68 36.22 o 9 1 1 6.26 3.59 27.49 o -9 2 1 3.84 -6.68 13.55 o -8 2 1 13.01 22.63 14.67 o -7 2 1 136.78 131.75 12.31 o -6 2 1 985.43 986.01 18.43 o -5 2 1 9.17 14.35 4.67 o -4 2 1 266.26 257.61 8.47 o -3 2 1 39.45 52.03 4.29 o -2 2 1 102.86 130.62 4.85 o -1 2 1 979.87 1042.71 11.76 o 0 2 1 1837.77 1801.21 16.65 o 1 2 1 1728.64 1846.40 15.78 o 2 2 1 398.63 401.65 9.62 o 3 2 1 361.57 347.93 11.15 o 4 2 1 37.64 33.21 7.08 o 5 2 1 0.78 1.23 7.08 o 6 2 1 38.78 31.51 9.22 o 7 2 1 114.18 109.51 12.12 o 8 2 1 48.88 70.67 19.53 o 9 2 1 45.24 42.17 24.47 o -9 3 1 37.25 25.35 19.28 o -8 3 1 96.09 129.77 18.80 o -7 3 1 3246.42 3137.16 50.03 o -6 3 1 208.14 192.19 12.91 o -5 3 1 241.45 234.48 12.43 o -4 3 1 1852.75 1828.67 22.89 o -3 3 1 1788.62 1716.08 21.56 o -2 3 1 4252.17 4362.40 36.41 o -1 3 1 9810.28 10230.88 112.61 o 0 3 1 2691.07 2593.59 26.35 o 1 3 1 404.08 491.28 10.57 o 2 3 1 189.10 186.47 6.95 o 3 3 1 0.88 -4.65 4.65 o 4 3 1 4228.77 4179.84 49.58 o 5 3 1 161.70 158.67 11.61 o 6 3 1 588.37 591.29 19.75 o 7 3 1 1.81 18.85 9.15 o 8 3 1 31.01 38.90 12.62 o 9 3 1 189.75 227.38 68.22 o -8 4 1 436.66 531.11 37.82 o -7 4 1 224.30 262.61 16.76 o -6 4 1 3.11 2.26 8.23 o -5 4 1 248.34 239.80 13.18 o -4 4 1 128.41 131.38 7.87 o -3 4 1 366.56 366.67 11.58 o -2 4 1 932.01 931.71 17.38 o -1 4 1 57.04 65.38 7.80 o 0 4 1 0.46 2.80 5.28 o 1 4 1 819.81 789.11 15.56 o 2 4 1 45.17 40.98 5.86 o 3 4 1 219.74 220.16 9.06 o 4 4 1 272.41 281.60 15.87 o 5 4 1 657.93 653.23 22.42 o 6 4 1 35.12 34.12 10.88 o 7 4 1 34.85 25.05 18.22 o 8 4 1 42.63 40.43 19.43 o -8 5 1 0.10 7.89 20.00 o -7 5 1 8.96 2.56 14.50 o -6 5 1 1003.22 959.59 39.36 o -5 5 1 4274.69 4229.73 86.73 o -4 5 1 11.34 5.35 7.84 o -3 5 1 78.52 72.12 9.09 o -2 5 1 1111.28 1080.54 23.30 o -1 5 1 763.17 712.22 18.33 o 0 5 1 1133.15 1125.25 28.84 o 1 5 1 368.42 344.82 14.17 o 2 5 1 2916.52 2865.43 36.36 o 3 5 1 153.77 149.96 11.46 o 4 5 1 580.99 596.08 20.65 o 5 5 1 635.67 607.18 21.84 o 6 5 1 269.83 262.72 23.14 o 7 5 1 400.05 451.44 37.24 o -7 6 1 495.41 531.82 48.46 o -6 6 1 296.81 275.52 26.30 o -5 6 1 280.12 300.71 25.89 o -4 6 1 1.15 -0.45 8.44 o -3 6 1 3.23 4.53 7.15 o -2 6 1 22.04 15.50 8.28 o -1 6 1 314.02 328.81 14.49 o 0 6 1 527.33 506.72 18.77 o 1 6 1 130.27 134.19 11.25 o 2 6 1 852.45 770.23 22.81 o 3 6 1 795.05 808.97 29.07 o 4 6 1 1118.70 1117.08 37.34 o 5 6 1 27.57 43.63 13.24 o 6 6 1 0.10 31.47 16.98 o -6 7 1 2.82 -6.95 20.86 o -5 7 1 32.85 83.98 21.58 o -4 7 1 578.62 585.98 57.06 o -3 7 1 536.78 540.04 27.09 o -2 7 1 256.28 294.56 17.24 o -1 7 1 156.32 157.56 13.32 o 0 7 1 713.00 726.79 21.87 o 1 7 1 164.92 174.11 14.09 o 2 7 1 45.56 53.33 10.49 o 3 7 1 105.41 99.41 18.58 o 4 7 1 493.64 533.60 35.49 o 5 7 1 1.95 -16.89 18.63 o -4 8 1 13.74 23.81 23.47 o -3 8 1 51.60 102.39 49.86 o -2 8 1 0.48 8.28 15.62 o -1 8 1 35.71 35.71 12.15 o 0 8 1 32.82 82.91 15.65 o 1 8 1 1536.02 1487.32 62.41 o 2 8 1 271.63 336.41 61.52 o 3 8 1 207.04 275.76 27.72 o -10 0 2 101.64 141.07 51.88 o -9 0 2 287.17 246.65 31.58 o -8 0 2 30.39 48.62 25.32 o -7 0 2 3206.85 3161.04 62.70 o -6 0 2 15.50 8.12 10.70 o -5 0 2 241.02 258.04 15.89 o -4 0 2 7966.31 8633.10 100.64 o -3 0 2 47543.51 46616.73 407.76 o -2 0 2 464.76 475.05 10.39 o -1 0 2 11028.86 11122.77 104.14 o 0 0 2 1540.15 1524.90 18.03 o 2 0 2 8666.49 8638.19 84.29 o 3 0 2 5615.33 5388.14 67.06 o 4 0 2 459.99 453.38 16.45 o 5 0 2 3051.63 2889.31 54.48 o 6 0 2 2493.08 2344.98 51.36 o 7 0 2 1227.01 1249.34 38.43 o 8 0 2 445.07 429.67 65.46 o 9 0 2 5.99 1.02 21.68 o -10 1 2 18.46 5.09 32.58 o -9 1 2 80.38 110.79 22.01 o -8 1 2 143.06 172.28 14.43 o -7 1 2 145.03 167.31 12.62 o -6 1 2 0.54 7.83 6.84 o -5 1 2 312.26 298.26 10.90 o -4 1 2 2912.03 2931.69 35.28 o -3 1 2 5266.10 4960.38 40.54 o -2 1 2 1249.70 1241.87 11.35 o -1 1 2 4277.76 4453.15 32.58 o 0 1 2 4106.20 4082.89 34.54 o 1 1 2 778.18 792.97 8.80 o 2 1 2 678.23 673.89 10.79 o 3 1 2 139.70 165.58 6.59 o 4 1 2 1.93 -4.39 4.39 o 5 1 2 327.22 323.38 12.50 o 6 1 2 179.55 163.64 11.62 o 7 1 2 525.69 540.61 21.37 o 8 1 2 1522.33 1497.57 35.63 o 9 1 2 859.00 1007.74 103.39 o -9 2 2 894.53 948.03 46.09 o -8 2 2 345.73 340.47 17.46 o -7 2 2 909.45 821.05 23.53 o -6 2 2 0.57 -6.46 6.46 o -5 2 2 5000.46 4791.70 51.82 o -4 2 2 303.76 303.94 9.58 o -3 2 2 2381.31 2414.21 22.02 o -2 2 2 59.95 35.94 3.33 o -1 2 2 8396.03 8379.18 59.11 o 0 2 2 9084.69 8938.16 63.32 o 1 2 2 722.63 593.38 8.63 o 2 2 2 3547.68 3927.95 37.57 o 3 2 2 491.74 468.79 12.48 o 4 2 2 2276.65 2301.58 30.92 o 5 2 2 7420.87 6926.28 74.57 o 6 2 2 127.12 129.80 11.99 o 7 2 2 138.73 135.03 13.34 o 8 2 2 495.33 612.24 46.04 o 9 2 2 323.27 300.07 25.56 o -9 3 2 2.39 2.98 17.94 o -8 3 2 19.10 19.97 14.94 o -7 3 2 84.09 108.85 12.83 o -6 3 2 1.86 -7.57 7.57 o -5 3 2 890.70 843.04 17.34 o -4 3 2 630.51 621.37 13.43 o -3 3 2 248.68 233.14 7.21 o -2 3 2 100.35 100.38 5.12 o -1 3 2 1182.85 1156.07 15.28 o 0 3 2 2678.54 2869.45 29.42 o 1 3 2 2126.02 2203.25 23.99 o 2 3 2 0.94 -0.42 3.76 o 3 3 2 63.28 63.31 7.34 o 4 3 2 78.37 81.82 8.36 o 5 3 2 40.56 37.49 8.86 o 6 3 2 106.55 107.37 11.51 o 7 3 2 98.11 132.31 13.78 o 8 3 2 329.24 357.66 25.37 o -9 4 2 73.35 165.59 45.35 o -8 4 2 453.51 423.76 62.96 o -7 4 2 1824.65 1842.31 39.45 o -6 4 2 14.10 17.97 8.47 o -5 4 2 200.47 211.73 10.61 o -4 4 2 1687.51 1618.91 23.72 o -3 4 2 3696.30 3650.00 38.79 o -2 4 2 39.91 37.68 5.93 o -1 4 2 574.93 583.84 14.83 o 0 4 2 17.51 9.45 5.71 o 1 4 2 153.67 152.53 8.29 o 2 4 2 2405.55 2392.71 28.71 o 3 4 2 4793.83 4607.46 50.68 o 4 4 2 1621.33 1527.02 27.49 o 5 4 2 43.09 42.59 8.62 o 6 4 2 175.94 187.61 16.36 o 7 4 2 31.65 36.32 11.88 o 8 4 2 400.89 578.63 83.27 o -8 5 2 11.27 58.74 30.34 o -7 5 2 97.81 153.49 18.78 o -6 5 2 1141.75 1163.20 34.88 o -5 5 2 17.09 14.07 8.72 o -4 5 2 113.47 112.61 9.80 o -3 5 2 32.76 41.43 8.30 o -2 5 2 8.25 22.30 7.61 o -1 5 2 156.33 158.13 11.52 o 0 5 2 2.73 4.06 7.57 o 1 5 2 4760.22 4756.67 56.84 o 2 5 2 0.16 0.08 7.01 o 3 5 2 66.58 82.17 8.39 o 4 5 2 556.43 499.11 25.61 o 5 5 2 0.05 3.58 8.10 o 6 5 2 0.15 20.99 10.15 o 7 5 2 375.13 451.34 49.81 o -7 6 2 167.67 180.05 24.44 o -6 6 2 21.08 19.62 14.80 o -5 6 2 155.20 171.76 18.68 o -4 6 2 227.90 213.19 14.92 o -3 6 2 756.35 758.53 21.72 o -2 6 2 74.47 66.71 9.79 o -1 6 2 411.61 401.55 17.80 o 0 6 2 50.00 55.77 10.84 o 1 6 2 60.49 76.64 10.68 o 2 6 2 458.96 468.15 17.61 o 3 6 2 52.49 47.66 11.99 o 4 6 2 869.05 823.35 40.66 o 5 6 2 573.12 533.39 27.66 o 6 6 2 215.83 252.18 36.13 o -6 7 2 18.69 78.56 42.21 o -5 7 2 265.09 266.43 29.60 o -4 7 2 570.16 585.95 33.20 o -3 7 2 63.93 71.63 15.08 o -2 7 2 849.08 788.24 24.47 o -1 7 2 0.28 -1.22 7.11 o 0 7 2 364.31 400.08 18.68 o 1 7 2 2.78 6.49 9.65 o 2 7 2 57.44 42.35 12.86 o 3 7 2 88.47 70.42 14.18 o 4 7 2 9.28 -3.91 29.36 o 5 7 2 4.99 -16.05 20.72 o -4 8 2 84.90 81.31 27.42 o -3 8 2 235.83 370.84 60.56 o -2 8 2 215.69 279.26 38.17 o -1 8 2 1510.87 1468.29 32.63 o 0 8 2 26.98 63.19 22.83 o 1 8 2 426.65 396.53 35.96 o 2 8 2 20.19 58.31 42.76 o 3 8 2 78.90 95.22 36.81 o -10 1 3 68.96 61.94 37.83 o -9 1 3 1148.63 1171.92 31.43 o -8 1 3 1173.81 1147.06 26.76 o -7 1 3 376.21 411.09 16.47 o -6 1 3 0.15 2.73 6.67 o -5 1 3 1111.78 1105.57 18.83 o -4 1 3 2645.48 2832.15 27.35 o -3 1 3 2174.77 2068.27 18.48 o -2 1 3 1222.18 1279.75 12.64 o -1 1 3 2384.03 2351.08 20.51 o 0 1 3 1825.98 1833.22 15.15 o 1 1 3 3026.85 3142.70 28.33 o 2 1 3 66.54 62.25 4.28 o 3 1 3 50.49 36.87 4.95 o 4 1 3 128.43 125.51 7.44 o 5 1 3 365.49 364.90 12.66 o 6 1 3 236.42 257.36 13.76 o 7 1 3 823.16 831.85 54.14 o 8 1 3 0.98 22.87 21.83 o 9 1 3 134.45 112.85 52.43 o -10 2 3 24.89 -5.75 38.21 o -9 2 3 0.46 9.18 15.51 o -8 2 3 328.51 328.74 18.09 o -7 2 3 1745.91 1638.20 28.78 o -6 2 3 210.09 223.10 10.83 o -5 2 3 200.97 222.53 9.29 o -4 2 3 30.61 34.44 4.43 o -3 2 3 218.61 267.20 6.58 o -2 2 3 2183.80 2341.49 26.76 o -1 2 3 0.03 -0.35 3.11 o 0 2 3 2936.74 2902.88 25.05 o 1 2 3 33.95 30.81 3.55 o 2 2 3 165.32 192.53 7.20 o 3 2 3 0.60 -2.62 5.05 o 4 2 3 300.40 294.03 12.44 o 5 2 3 851.69 842.23 21.45 o 6 2 3 137.46 142.94 12.40 o 7 2 3 0.02 -0.95 10.71 o 8 2 3 29.89 47.02 15.44 o -9 3 3 5.09 12.50 21.06 o -8 3 3 203.75 203.06 22.70 o -7 3 3 630.83 611.41 20.74 o -6 3 3 62.46 64.52 8.56 o -5 3 3 7917.93 7670.87 68.33 o -4 3 3 2131.50 2175.58 22.79 o -3 3 3 121.94 112.70 5.50 o -2 3 3 62.76 52.90 4.59 o -1 3 3 13.03 -0.81 3.56 o 0 3 3 1.35 4.42 3.90 o 1 3 3 5093.91 5271.10 44.83 o 2 3 3 2809.99 2854.66 30.29 o 3 3 3 319.86 323.35 12.06 o 4 3 3 92.65 76.73 8.73 o 5 3 3 318.66 315.97 14.53 o 6 3 3 30.94 42.01 10.16 o 7 3 3 624.45 624.38 26.28 o 8 3 3 99.16 102.68 20.67 o -9 4 3 77.29 166.92 44.65 o -8 4 3 466.99 538.72 35.95 o -7 4 3 587.58 613.28 25.11 o -6 4 3 1646.63 1641.89 31.27 o -5 4 3 187.56 204.96 11.30 o -4 4 3 149.06 147.64 8.97 o -3 4 3 6.59 3.04 4.45 o -2 4 3 21.82 32.80 6.58 o -1 4 3 103.49 103.65 8.25 o 0 4 3 134.67 129.93 8.63 o 1 4 3 633.23 666.00 14.98 o 2 4 3 71.61 97.93 7.50 o 3 4 3 410.62 412.98 16.81 o 4 4 3 389.79 386.59 14.47 o 5 4 3 527.14 478.38 21.46 o 6 4 3 18.28 21.12 11.86 o 7 4 3 281.27 317.18 31.56 o -8 5 3 1779.95 1745.11 58.16 o -7 5 3 33.87 39.16 18.15 o -6 5 3 8.35 10.87 11.91 o -5 5 3 427.32 409.16 15.25 o -4 5 3 531.89 499.45 16.09 o -3 5 3 3365.61 3279.59 42.78 o -2 5 3 2768.04 2672.07 41.03 o -1 5 3 292.60 277.92 13.07 o 0 5 3 3124.23 3052.34 47.99 o 1 5 3 2582.14 2462.91 36.32 o 2 5 3 234.25 224.80 11.30 o 3 5 3 547.36 527.57 21.56 o 4 5 3 0.22 -8.12 8.12 o 5 5 3 172.57 174.82 19.01 o 6 5 3 242.43 274.52 20.99 o 7 5 3 96.46 172.28 57.02 o -7 6 3 337.29 356.54 56.14 o -6 6 3 4.95 33.20 15.86 o -5 6 3 344.41 301.87 20.86 o -4 6 3 891.91 905.94 28.52 o -3 6 3 265.16 266.03 14.32 o -2 6 3 537.44 479.47 17.94 o -1 6 3 2.98 9.13 7.45 o 0 6 3 49.42 66.02 10.64 o 1 6 3 188.28 179.77 13.30 o 2 6 3 262.09 298.09 15.88 o 3 6 3 195.84 191.87 16.31 o 4 6 3 289.27 261.72 20.73 o 5 6 3 39.35 46.86 13.61 o 6 6 3 607.14 616.06 55.89 o -6 7 3 240.28 323.58 70.99 o -5 7 3 412.15 395.43 30.37 o -4 7 3 242.61 272.18 22.31 o -3 7 3 0.41 -3.90 9.72 o -2 7 3 610.38 624.30 20.30 o -1 7 3 1442.59 1413.39 32.95 o 0 7 3 1033.76 981.39 25.94 o 1 7 3 52.56 76.62 14.67 o 2 7 3 62.36 48.61 12.95 o 3 7 3 142.88 147.45 17.54 o 4 7 3 3.67 -3.89 12.58 o 5 7 3 64.39 55.66 27.27 o -4 8 3 224.50 418.62 122.06 o -3 8 3 565.08 623.64 34.33 o -2 8 3 756.52 810.87 27.31 o -1 8 3 46.07 113.68 29.46 o 0 8 3 356.27 352.89 20.16 o 1 8 3 4.79 11.24 14.43 o 2 8 3 28.26 44.82 17.21 o -10 0 4 186.01 195.56 63.50 o -9 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