#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:55:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181124 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/03/2220324.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220324_Fobs loop_ _publ_author_name 'Wang, Juxian' 'Liu, Mingliang' 'Cao, Jue' 'Wang, Yucheng' _publ_section_title ; tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate ; _journal_coeditor_code RZ2260 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2294 _journal_volume 64 _journal_year 2008 _space_group_IT_number 88 _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.8134 _cell_length_b 22.8134 _cell_length_c 12.0742 _exptl_crystal_F_000 2464.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file rz2260Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080108c in I4(1)/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 333.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+3/4, x+1/4, z+1/4' 'y+3/4, -x+3/4, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+5/4, x+3/4, z+3/4' 'y+5/4, -x+5/4, z+5/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-3/4, -x-1/4, -z-1/4' '-y-3/4, x-3/4, -z-3/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y-1/4, -x+1/4, -z+1/4' '-y-1/4, x-1/4, -z-1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 109944.76 97193.48 7057.76 o 2 2 0 68360.73 65723.12 1543.62 o -2 4 0 68640.16 63161.11 1560.08 o 0 4 0 8894.35 8299.55 86.06 o 2 4 0 7044.68 6681.53 190.04 o 4 4 0 2334.49 2015.02 62.87 o -4 6 0 33752.26 33424.49 659.24 o -2 6 0 1142.50 1037.89 28.09 o 0 6 0 12161.99 12832.62 272.15 o 2 6 0 289.72 313.02 21.26 o 4 6 0 540.09 734.56 42.45 o 6 6 0 47301.79 50473.75 286.17 o -6 8 0 3494.26 3775.04 95.02 o -4 8 0 16631.19 16571.91 288.15 o -2 8 0 23980.53 22903.43 666.31 o 0 8 0 17212.45 17267.80 371.04 o 4 8 0 6518.39 6050.77 72.52 o 6 8 0 2.93 6.52 16.50 o 8 8 0 8737.63 9078.91 118.24 o -8 10 0 960.37 791.13 33.06 o -6 10 0 1981.89 1804.00 81.64 o -4 10 0 28641.63 32238.70 575.83 o -2 10 0 138.85 214.94 23.92 o 0 10 0 33785.52 35292.01 219.47 o 2 10 0 18700.78 19704.99 318.42 o 4 10 0 600.18 696.45 42.14 o 8 10 0 14949.38 16808.04 143.23 o 10 10 0 1317.96 1481.37 45.77 o -10 12 0 228.81 202.63 33.55 o -8 12 0 3948.01 4165.55 68.22 o -6 12 0 20734.89 23026.06 202.02 o -4 12 0 1506.92 1520.22 52.17 o -2 12 0 926.47 962.93 53.40 o 0 12 0 2253.95 2478.05 62.48 o 2 12 0 71.81 47.24 20.76 o 4 12 0 664.83 550.05 32.36 o 6 12 0 539.28 406.36 29.92 o 8 12 0 9550.46 10117.29 118.26 o 10 12 0 1201.49 1204.55 45.39 o 12 12 0 125.56 174.38 35.01 o -12 14 0 2.45 -12.36 29.84 o -10 14 0 180.78 208.19 34.14 o -8 14 0 6429.97 6664.95 222.55 o -6 14 0 12.25 24.60 42.06 o -4 14 0 4243.47 4553.85 144.54 o -2 14 0 495.00 512.54 37.48 o 0 14 0 4008.94 4132.76 188.99 o 2 14 0 259.41 278.46 28.28 o 4 14 0 997.88 1006.73 42.52 o 6 14 0 1557.14 1610.72 52.64 o 8 14 0 989.14 1054.79 45.76 o 10 14 0 1719.53 1687.48 56.85 o 12 14 0 682.09 739.23 52.98 o 14 14 0 2913.45 2895.72 92.14 o -14 16 0 1047.34 1174.27 82.43 o -12 16 0 639.99 574.56 62.12 o -10 16 0 2469.05 2078.62 95.09 o -8 16 0 3065.80 2889.98 135.33 o -6 16 0 2184.10 2304.71 121.36 o -4 16 0 5567.85 5364.65 169.27 o -2 16 0 772.38 611.81 57.41 o 0 16 0 1511.44 1465.07 84.45 o 2 16 0 57.09 18.84 25.29 o 4 16 0 62.52 37.65 25.94 o 6 16 0 5559.17 4975.01 94.08 o 8 16 0 2662.19 2599.92 79.87 o 10 16 0 241.07 217.18 38.35 o 12 16 0 561.09 437.22 47.57 o 14 16 0 346.39 376.41 69.53 o 16 16 0 2410.88 2363.02 111.39 o -16 18 0 12.79 -63.95 59.78 o -14 18 0 291.66 303.33 57.88 o -12 18 0 50.16 40.17 44.75 o -10 18 0 108.46 56.09 42.04 o -8 18 0 1097.41 932.19 94.44 o -6 18 0 587.77 560.50 78.23 o -4 18 0 1595.15 1442.40 107.48 o -2 18 0 877.81 840.78 72.81 o 0 18 0 307.69 266.85 53.00 o 2 18 0 135.72 91.83 46.00 o 4 18 0 272.72 307.24 43.40 o 6 18 0 1011.30 998.78 52.37 o 8 18 0 9319.77 9474.00 140.03 o 10 18 0 6357.09 6990.74 180.14 o 12 18 0 135.49 65.82 40.75 o 14 18 0 341.72 478.44 63.38 o 16 18 0 2868.79 2934.44 134.08 o 18 18 0 446.74 544.91 88.87 o -18 20 0 65.62 169.91 73.88 o -16 20 0 156.69 131.88 101.06 o -14 20 0 151.71 178.40 80.07 o -12 20 0 108.28 133.65 70.84 o -10 20 0 357.61 262.27 74.32 o -8 20 0 47.66 -44.42 54.25 o -6 20 0 384.33 337.64 79.53 o -4 20 0 1304.88 1311.27 140.79 o -2 20 0 2827.37 2867.80 120.66 o 0 20 0 681.06 655.96 72.15 o 2 20 0 96.51 117.53 52.45 o 4 20 0 3176.60 3018.23 118.21 o 6 20 0 1858.06 1853.84 95.36 o 8 20 0 280.72 221.61 70.90 o 10 20 0 97.91 36.00 48.01 o 12 20 0 98.05 129.95 52.62 o 14 20 0 148.46 172.32 54.70 o 16 20 0 467.55 567.12 92.36 o 18 20 0 2.88 74.07 72.32 o -14 22 0 2.71 10.79 71.00 o -12 22 0 52.96 65.48 76.73 o -10 22 0 46.95 109.18 70.95 o -8 22 0 1494.01 1571.36 128.16 o -6 22 0 371.24 374.47 80.20 o -4 22 0 1060.40 1189.60 165.51 o -2 22 0 480.39 401.31 64.93 o 0 22 0 1.46 26.61 52.02 o 2 22 0 2251.73 2420.37 114.30 o 4 22 0 27.59 3.67 50.68 o 6 22 0 427.53 357.18 62.38 o 8 22 0 1253.91 1331.46 118.80 o 10 22 0 5.09 88.83 85.41 o 12 22 0 1.31 5.12 61.17 o -12 24 0 17.53 -80.40 70.88 o -10 24 0 225.35 256.37 75.55 o -8 24 0 249.61 303.41 80.27 o -6 24 0 7.83 -81.00 62.89 o -4 24 0 111.29 88.86 65.86 o -2 24 0 2741.09 2808.76 159.78 o 0 24 0 165.19 54.46 55.78 o 2 24 0 1994.09 1852.77 111.90 o 4 24 0 19.70 19.53 52.51 o 6 24 0 2177.63 2577.37 155.86 o 8 24 0 186.00 245.24 87.99 o 10 24 0 483.45 607.93 100.89 o 12 24 0 353.95 413.29 137.03 o -6 26 0 225.10 216.75 84.72 o -4 26 0 0.43 -21.45 65.32 o -2 26 0 32.90 97.95 78.87 o 0 26 0 500.94 451.18 78.00 o 2 26 0 16.68 70.88 61.78 o 4 26 0 121.84 128.62 61.85 o 6 26 0 922.61 1103.26 182.71 o 0 1 1 12631.93 12622.06 167.15 o -1 2 1 21067.79 21359.69 225.93 o 1 2 1 2062.37 2203.04 25.07 o -2 3 1 0.01 63.75 7.66 o 0 3 1 24370.54 22447.59 317.18 o 2 3 1 62119.17 61058.98 348.40 o -3 4 1 38312.03 36793.95 560.42 o -1 4 1 111120.26 104752.99 960.42 o 1 4 1 22002.96 21238.33 273.06 o 3 4 1 7097.42 7146.20 103.22 o -4 5 1 10871.63 11420.18 125.47 o -2 5 1 33839.04 33464.49 530.54 o 0 5 1 8088.05 7261.58 105.42 o 2 5 1 225.34 199.54 14.13 o 4 5 1 2.19 5.15 8.20 o -5 6 1 27911.29 28095.85 231.92 o -3 6 1 430.06 493.36 26.79 o -1 6 1 126.49 135.99 13.87 o 1 6 1 29329.92 27366.21 210.90 o 3 6 1 19500.86 19523.99 209.40 o 5 6 1 11406.31 12511.71 90.92 o -6 7 1 8508.28 8908.28 103.76 o -4 7 1 3995.04 4091.20 51.94 o -2 7 1 2337.24 1914.67 40.62 o 4 7 1 1942.00 1978.66 28.77 o 6 7 1 7.08 32.53 11.22 o -7 8 1 4332.98 4486.28 54.92 o -5 8 1 7660.05 8115.80 88.45 o -3 8 1 194.93 292.30 22.68 o -1 8 1 4198.02 4309.71 69.28 o 1 8 1 3968.07 4011.26 44.93 o 3 8 1 759.66 748.72 20.11 o 5 8 1 13.19 6.57 11.23 o 7 8 1 15413.38 15069.89 169.64 o -8 9 1 2435.65 2673.90 37.63 o -6 9 1 4150.19 4098.15 54.40 o -4 9 1 241.23 246.50 22.91 o -2 9 1 1294.49 1357.87 28.98 o 0 9 1 427.40 414.01 16.36 o 2 9 1 497.33 328.23 15.56 o 4 9 1 12816.58 13019.75 158.80 o 6 9 1 3115.28 3044.04 43.78 o 8 9 1 12771.01 14238.96 89.09 o -9 10 1 420.18 507.82 21.45 o -7 10 1 2.91 54.39 18.69 o -5 10 1 1517.50 1322.47 37.33 o -3 10 1 22981.60 23138.59 285.86 o -1 10 1 319.00 411.12 19.92 o 1 10 1 4807.74 5240.39 50.51 o 3 10 1 975.73 1110.60 26.25 o 5 10 1 908.19 910.10 25.45 o 7 10 1 2405.54 2436.68 39.03 o 9 10 1 498.31 647.41 23.77 o -10 11 1 54.90 78.78 18.39 o -8 11 1 2806.81 3292.88 50.57 o -6 11 1 1.05 -21.01 15.81 o -4 11 1 6738.39 6543.54 83.35 o -2 11 1 3696.98 3885.42 50.92 o 0 11 1 14686.22 14602.38 115.27 o 2 11 1 212.61 215.63 16.64 o 4 11 1 4740.91 4852.18 53.45 o 6 11 1 152.57 154.92 17.56 o 8 11 1 1.57 4.80 14.23 o 10 11 1 1233.42 1272.15 31.82 o -11 12 1 152.17 188.32 21.81 o -9 12 1 1306.99 1162.53 33.46 o -7 12 1 3063.78 2802.94 55.92 o -5 12 1 3637.02 3437.91 87.87 o -3 12 1 9187.22 9001.77 114.73 o -1 12 1 33.58 10.96 14.88 o 1 12 1 13302.69 14235.01 139.76 o 3 12 1 9052.36 9638.52 123.67 o 5 12 1 6436.73 6432.97 71.92 o 7 12 1 1039.88 916.08 28.15 o 9 12 1 96.73 87.71 16.66 o 11 12 1 1037.35 954.48 33.44 o -12 13 1 3797.63 3756.25 68.80 o -10 13 1 84.60 110.41 21.97 o -8 13 1 591.54 546.95 29.20 o -6 13 1 110.17 82.60 18.71 o -4 13 1 67.32 86.84 22.43 o -2 13 1 10994.46 11333.29 164.53 o 0 13 1 51.43 55.10 20.35 o 2 13 1 1731.69 1514.24 33.55 o 4 13 1 872.71 840.48 27.72 o 6 13 1 160.19 180.18 19.00 o 8 13 1 494.30 502.11 24.54 o 10 13 1 890.16 897.54 33.43 o 12 13 1 901.15 928.38 38.54 o -13 14 1 1.60 3.86 25.71 o -11 14 1 360.35 419.86 34.16 o -9 14 1 342.08 289.60 27.56 o -7 14 1 815.14 703.14 40.74 o -5 14 1 1013.87 834.94 38.21 o -3 14 1 1207.72 1262.48 45.32 o -1 14 1 2316.77 2344.05 45.01 o 1 14 1 377.97 333.05 19.94 o 3 14 1 745.19 671.40 27.13 o 5 14 1 676.43 716.53 27.41 o 7 14 1 18.11 9.51 16.19 o 9 14 1 1657.88 1833.54 41.28 o 11 14 1 73.02 87.63 21.36 o 13 14 1 159.07 150.30 26.14 o -14 15 1 1528.86 1526.53 56.58 o -12 15 1 651.20 693.18 40.72 o -10 15 1 7.42 -23.81 23.65 o -8 15 1 11.82 1.12 36.54 o -6 15 1 321.35 285.90 43.95 o -4 15 1 1805.92 1899.90 65.49 o -2 15 1 362.71 289.28 29.33 o 0 15 1 2014.25 1995.53 58.28 o 2 15 1 214.13 157.44 19.32 o 4 15 1 155.12 156.00 20.05 o 6 15 1 120.08 100.96 19.28 o 8 15 1 382.57 351.38 24.51 o 10 15 1 0.07 4.67 20.21 o 12 15 1 0.78 0.64 22.87 o 14 15 1 86.63 24.67 26.95 o -15 16 1 1.40 27.33 35.29 o -13 16 1 195.70 177.23 34.60 o -11 16 1 39.15 23.44 26.89 o -9 16 1 146.85 125.12 30.57 o -7 16 1 1020.15 842.13 59.55 o -5 16 1 634.58 609.45 45.39 o -3 16 1 14.33 25.18 30.43 o -1 16 1 0.15 -17.49 21.99 o 1 16 1 106.61 88.88 24.45 o 3 16 1 7800.56 7952.76 123.05 o 5 16 1 98.68 97.11 20.79 o 7 16 1 65.21 53.55 19.53 o 9 16 1 28.57 10.42 20.77 o 11 16 1 921.56 861.71 40.56 o 13 16 1 1585.36 1639.91 58.57 o 15 16 1 2.48 42.05 32.82 o -16 17 1 156.23 128.90 43.22 o -14 17 1 1181.51 1077.53 63.10 o -12 17 1 63.31 34.24 36.68 o -10 17 1 330.34 303.37 37.30 o -8 17 1 141.01 143.54 46.91 o -6 17 1 1944.56 1951.72 81.80 o -4 17 1 871.25 932.22 56.13 o -2 17 1 236.20 248.22 41.44 o 0 17 1 314.83 259.08 34.60 o 2 17 1 52.70 63.25 24.75 o 4 17 1 417.74 376.85 27.11 o 6 17 1 3233.33 3258.34 56.98 o 8 17 1 1388.41 1338.58 40.30 o 10 17 1 430.32 373.54 33.21 o 12 17 1 520.49 445.78 35.33 o 14 17 1 2.86 25.90 29.48 o 16 17 1 145.33 193.61 44.12 o -17 18 1 301.03 276.93 47.62 o -15 18 1 455.21 529.59 53.76 o -13 18 1 104.62 54.91 38.27 o -11 18 1 1552.12 1546.40 72.67 o -9 18 1 904.98 891.36 55.91 o -7 18 1 1706.47 1627.26 80.40 o -5 18 1 4323.99 4547.20 190.66 o -3 18 1 154.09 196.02 37.84 o -1 18 1 49.99 18.60 32.54 o 1 18 1 403.78 423.58 39.34 o 3 18 1 1081.49 1023.04 42.53 o 5 18 1 0.24 -12.50 24.40 o 7 18 1 687.66 645.54 34.92 o 9 18 1 56.40 40.12 27.04 o 11 18 1 3.52 -19.81 26.30 o 13 18 1 327.05 364.87 38.09 o 15 18 1 337.98 402.71 48.52 o 17 18 1 369.67 383.09 50.01 o -18 19 1 245.84 308.26 59.15 o -16 19 1 0.21 -2.49 37.47 o -14 19 1 15.19 8.27 36.69 o -12 19 1 114.36 112.60 41.54 o -10 19 1 317.59 271.04 54.00 o -8 19 1 469.62 383.30 52.55 o -6 19 1 1370.25 1272.70 75.75 o -4 19 1 2144.37 2036.25 88.65 o -2 19 1 221.43 239.99 41.45 o 0 19 1 3986.13 4083.89 102.08 o 2 19 1 0.91 12.74 29.41 o 4 19 1 2974.76 3084.40 74.39 o 6 19 1 4.62 -39.51 26.34 o 8 19 1 1.70 -21.85 29.28 o 10 19 1 78.31 46.33 31.79 o 12 19 1 787.38 827.04 52.66 o 14 19 1 619.98 683.20 55.74 o 16 19 1 175.80 173.24 44.18 o 18 19 1 0.34 58.37 47.38 o -17 20 1 87.13 110.81 51.23 o -15 20 1 127.17 200.78 55.46 o -13 20 1 800.95 819.29 63.10 o -11 20 1 15.74 46.96 38.51 o -9 20 1 1017.17 961.44 75.45 o -7 20 1 346.38 411.42 59.14 o -5 20 1 72.82 73.45 42.88 o -3 20 1 127.21 80.39 40.88 o -1 20 1 1032.51 1056.39 58.59 o 1 20 1 920.04 880.12 55.25 o 3 20 1 749.82 693.60 49.20 o 5 20 1 71.89 52.68 33.88 o 7 20 1 1713.24 1754.46 61.46 o 9 20 1 400.36 412.25 43.40 o 11 20 1 187.05 172.65 36.47 o 13 20 1 70.39 186.90 56.38 o 15 20 1 48.60 79.70 45.50 o 17 20 1 187.43 238.60 55.78 o -16 21 1 49.27 89.06 54.81 o -14 21 1 306.20 361.52 59.63 o -12 21 1 939.25 969.51 67.95 o -10 21 1 27.23 22.05 45.82 o -8 21 1 77.53 23.56 44.98 o -6 21 1 197.78 129.60 46.15 o -4 21 1 946.94 905.65 68.25 o -2 21 1 314.53 340.05 50.26 o 0 21 1 2643.06 2669.16 83.05 o 2 21 1 2014.60 1958.82 72.48 o 4 21 1 43.07 57.09 36.80 o 6 21 1 36.44 4.73 34.95 o 8 21 1 1776.13 1795.69 90.01 o 10 21 1 1369.05 1377.66 71.99 o 12 21 1 877.73 1030.86 65.50 o 14 21 1 0.06 17.18 43.52 o 16 21 1 50.39 107.91 49.05 o -15 22 1 20.65 41.41 50.44 o -13 22 1 1.40 7.12 47.91 o -11 22 1 487.48 516.74 66.06 o -9 22 1 10.39 -14.77 48.14 o -7 22 1 21.55 -7.62 47.60 o -5 22 1 752.96 690.49 66.21 o -3 22 1 813.00 736.89 60.79 o -1 22 1 1055.20 1087.86 66.45 o 1 22 1 714.06 685.28 55.11 o 3 22 1 390.95 390.07 45.51 o 5 22 1 2489.00 2564.06 81.93 o 7 22 1 253.16 209.61 47.99 o 9 22 1 51.71 71.50 48.48 o 11 22 1 27.68 30.15 51.74 o 13 22 1 120.53 152.99 59.82 o 15 22 1 322.19 287.72 77.31 o -14 23 1 33.57 11.22 49.13 o -12 23 1 280.39 230.14 57.30 o -10 23 1 610.94 619.39 66.24 o -8 23 1 11.35 11.65 45.11 o -6 23 1 149.00 184.82 52.63 o -4 23 1 0.10 -19.36 42.22 o -2 23 1 6.16 -27.18 40.52 o 0 23 1 1.22 12.78 42.69 o 2 23 1 307.40 295.98 45.66 o 4 23 1 0.04 -29.13 37.15 o 6 23 1 0.00 24.19 42.87 o 8 23 1 23.64 -33.03 42.42 o 10 23 1 96.61 90.74 55.39 o 12 23 1 181.12 196.37 75.06 o 14 23 1 73.40 99.49 110.44 o -11 24 1 0.44 19.25 50.56 o -9 24 1 2.94 9.91 50.26 o -7 24 1 39.02 35.93 49.38 o -5 24 1 37.30 22.99 47.92 o -3 24 1 0.57 -4.30 49.56 o -1 24 1 75.82 76.00 44.20 o 1 24 1 114.88 47.75 41.01 o 3 24 1 474.61 462.50 50.80 o 5 24 1 424.38 488.96 57.70 o 7 24 1 25.28 -27.67 55.26 o 9 24 1 164.78 81.90 51.06 o 11 24 1 3.07 -80.80 89.17 o -10 25 1 0.69 -12.03 47.80 o -8 25 1 26.23 14.58 49.92 o -6 25 1 335.89 389.71 63.43 o -4 25 1 31.08 0.60 45.70 o -2 25 1 16.26 23.31 44.13 o 0 25 1 2.53 -18.64 44.74 o 2 25 1 182.81 185.07 46.20 o 4 25 1 14.25 37.99 40.02 o 6 25 1 3.51 -49.97 54.54 o 8 25 1 76.50 65.84 61.62 o 10 25 1 293.53 391.31 99.87 o -7 26 1 8.15 -3.45 50.64 o -5 26 1 96.82 140.19 57.73 o -3 26 1 25.01 -41.46 48.70 o -1 26 1 25.41 22.11 45.30 o 1 26 1 31.91 23.27 45.34 o 3 26 1 778.21 879.41 64.56 o 5 26 1 80.30 2.55 49.35 o 7 26 1 1.39 -41.63 55.47 o -2 27 1 58.34 100.73 70.89 o 0 27 1 3.73 43.49 52.20 o 2 27 1 7.97 -26.74 45.15 o 1 1 2 59137.94 58055.61 309.49 o 0 2 2 16254.38 16809.25 108.64 o 2 2 2 767.98 906.04 18.76 o -1 3 2 10789.34 11271.93 105.04 o 1 3 2 67538.13 67180.28 534.81 o 3 3 2 11262.97 12362.44 124.17 o -2 4 2 28204.74 27879.79 270.80 o 0 4 2 14372.83 15021.33 82.54 o 2 4 2 18554.39 19738.17 233.98 o 4 4 2 27657.16 26404.01 346.51 o -3 5 2 31.56 83.25 14.72 o -1 5 2 1842.18 1714.62 27.39 o 1 5 2 46370.35 44375.48 355.12 o 3 5 2 6.54 14.35 8.18 o 5 5 2 19698.82 20117.58 219.79 o -4 6 2 55526.85 55475.80 669.80 o -2 6 2 11189.59 10535.53 199.13 o 0 6 2 854.31 826.61 20.41 o 4 6 2 2162.13 1933.40 29.29 o 6 6 2 2751.87 2744.86 47.44 o -5 7 2 6894.06 6868.91 104.81 o -3 7 2 7308.76 7227.49 76.75 o -1 7 2 3678.63 3853.73 43.26 o 1 7 2 13257.76 13939.75 98.82 o 3 7 2 12115.37 13500.06 152.19 o 5 7 2 722.80 740.77 20.33 o 7 7 2 158.32 128.71 13.34 o -6 8 2 2908.04 2630.34 37.75 o -4 8 2 23109.80 22806.71 280.43 o -2 8 2 16463.84 16745.42 264.89 o 0 8 2 2132.57 2367.24 35.02 o 2 8 2 784.53 807.64 20.69 o 4 8 2 1134.16 1248.37 25.86 o 6 8 2 2548.30 2561.15 36.87 o 8 8 2 35.53 62.22 15.37 o -7 9 2 7171.67 8106.41 83.15 o -5 9 2 29466.06 29837.56 364.88 o -3 9 2 2943.90 2829.83 53.11 o -1 9 2 534.31 511.42 21.57 o 1 9 2 2417.15 2174.46 31.75 o 3 9 2 912.57 828.93 22.70 o 5 9 2 491.87 361.05 18.64 o 7 9 2 6796.95 7613.96 71.06 o 9 9 2 4708.77 5561.59 75.60 o -8 10 2 335.10 393.33 20.07 o -6 10 2 102.37 152.26 21.80 o -4 10 2 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