#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/03/2220325.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220325_Fobs loop_ _publ_author_name 'Pavlov\'a, Anna' '\N,N')(maleato-\k^2^O^1^,O^1'^)nickel(II) 7.34-hydrate ; _journal_coeditor_code RZ2262 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1536 _journal_page_last m1537 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.767 _cell_angle_gamma 90.000 _cell_length_a 20.7108 _cell_length_b 17.4754 _cell_length_c 15.6460 _exptl_crystal_F_000 2587.28 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file rz2262Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ap154 in I 2/a after co-editor comments' _shelx_refln_list_code 4 _shelx_F_calc_maximum 407.28 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1318.71 1884.99 201.55 o 4 0 0 314.50 251.88 148.41 o 6 0 0 73.09 319.35 121.24 o 8 0 0 646.88 407.94 102.45 o 10 0 0 7511.07 7636.13 116.53 o 12 0 0 589.07 525.68 89.19 o 14 0 0 1723.24 1704.18 96.63 o 16 0 0 11913.08 12153.98 311.56 o 18 0 0 13390.83 13740.73 221.53 o 20 0 0 18367.38 18730.15 299.96 o 22 0 0 2003.40 2120.45 114.32 o 24 0 0 6055.34 5987.50 190.73 o 1 1 0 18943.78 23148.61 307.98 o 3 1 0 349.02 307.00 109.26 o 5 1 0 43.56 99.86 93.39 o 7 1 0 14525.12 15620.07 119.01 o 9 1 0 1114.69 1253.91 71.20 o 11 1 0 41281.94 42019.18 428.46 o 13 1 0 621.66 723.79 66.95 o 15 1 0 3123.71 3050.27 71.27 o 17 1 0 1078.75 1066.47 64.87 o 19 1 0 16.52 24.66 66.10 o 21 1 0 4657.38 4684.58 87.98 o 23 1 0 1.26 11.10 87.51 o 0 2 0 64233.79 71646.38 439.59 o 2 2 0 102.40 95.60 122.22 o 4 2 0 90187.49 94073.16 4488.56 o 6 2 0 4478.66 4671.22 92.24 o 8 2 0 503.09 488.14 77.62 o 10 2 0 4044.11 3972.15 76.44 o 12 2 0 1407.53 1223.33 70.26 o 14 2 0 6586.78 6404.81 95.09 o 16 2 0 5394.14 5462.09 119.36 o 18 2 0 2764.65 2763.48 76.27 o 20 2 0 19666.21 20112.55 427.29 o 22 2 0 1019.31 951.22 75.53 o 24 2 0 2426.10 2468.66 86.82 o 1 3 0 28847.62 32184.70 245.34 o 3 3 0 60094.32 63611.34 2059.33 o 5 3 0 45.09 104.34 88.16 o 7 3 0 41923.29 41412.09 400.01 o 9 3 0 15715.27 15624.52 209.51 o 11 3 0 1775.39 2054.08 74.46 o 13 3 0 8573.62 8282.70 159.64 o 15 3 0 8859.07 9049.29 231.65 o 17 3 0 6662.11 6809.63 97.61 o 19 3 0 1400.26 1475.86 76.33 o 21 3 0 4466.70 4432.68 93.10 o 23 3 0 459.61 484.69 86.85 o 0 4 0 2961.86 2586.44 141.20 o 2 4 0 63447.96 66726.29 1994.24 o 4 4 0 1788.47 1819.28 102.46 o 6 4 0 6384.62 6800.76 92.36 o 8 4 0 14279.17 15260.05 112.47 o 10 4 0 978.22 768.84 69.51 o 12 4 0 20.00 45.62 65.93 o 14 4 0 27.13 116.73 74.89 o 16 4 0 26.08 -2.53 78.11 o 18 4 0 3977.36 3985.86 88.01 o 20 4 0 102.05 106.33 81.92 o 22 4 0 743.75 785.88 88.93 o 1 5 0 9761.79 9996.62 108.39 o 3 5 0 38186.74 38539.12 440.85 o 5 5 0 514.22 479.79 75.90 o 7 5 0 1284.07 1430.17 69.67 o 9 5 0 1300.08 1670.17 81.75 o 11 5 0 1614.59 1714.90 82.77 o 13 5 0 6128.84 6539.57 82.45 o 15 5 0 4.93 -8.93 74.65 o 17 5 0 11336.66 11408.11 155.04 o 19 5 0 989.20 951.60 71.19 o 21 5 0 5945.41 6045.52 101.46 o 23 5 0 44.47 101.38 92.93 o 0 6 0 905.30 675.90 110.50 o 2 6 0 31938.74 33688.45 287.53 o 4 6 0 41244.95 42191.70 278.50 o 6 6 0 23875.88 25187.79 318.45 o 8 6 0 63947.96 63067.42 2815.82 o 10 6 0 4354.77 4584.28 75.78 o 12 6 0 22935.83 22486.40 187.36 o 14 6 0 37.53 42.33 65.06 o 16 6 0 1185.39 1323.84 70.23 o 18 6 0 249.32 229.57 69.88 o 20 6 0 696.16 686.56 72.53 o 22 6 0 5973.54 5881.30 103.69 o 1 7 0 55.95 76.56 70.74 o 3 7 0 1833.02 2002.32 72.53 o 5 7 0 8273.71 8965.22 106.56 o 7 7 0 12809.67 13170.81 105.87 o 9 7 0 781.35 705.62 73.18 o 11 7 0 861.56 858.13 76.49 o 13 7 0 365.70 393.24 65.70 o 15 7 0 5904.17 5998.66 72.16 o 17 7 0 3226.42 3486.55 111.36 o 19 7 0 155.97 160.07 72.14 o 21 7 0 2124.65 2133.35 80.34 o 0 8 0 8506.34 8661.33 141.31 o 2 8 0 24598.44 25749.23 243.02 o 4 8 0 38.78 99.52 65.37 o 6 8 0 465.44 611.81 63.27 o 8 8 0 14093.98 13869.88 98.04 o 10 8 0 298.98 349.05 73.31 o 12 8 0 3767.67 3526.29 73.24 o 14 8 0 747.51 787.29 68.60 o 16 8 0 14265.32 14620.48 227.81 o 18 8 0 1358.01 1362.41 88.57 o 20 8 0 1273.78 1288.47 102.19 o 22 8 0 2145.49 2054.75 91.87 o 1 9 0 3247.77 2995.52 67.81 o 3 9 0 12269.05 10967.72 102.39 o 5 9 0 36035.29 35565.20 418.38 o 7 9 0 3081.73 3137.45 81.54 o 9 9 0 5828.32 5810.82 102.56 o 11 9 0 6414.91 6451.32 77.64 o 13 9 0 2649.68 2681.36 84.92 o 15 9 0 848.60 781.05 77.09 o 17 9 0 3273.22 3425.66 85.48 o 19 9 0 2714.77 2555.72 114.67 o 21 9 0 4336.17 4455.46 277.32 o 0 10 0 4126.45 4511.99 101.64 o 2 10 0 1116.17 1566.28 65.27 o 4 10 0 798.87 867.61 66.36 o 6 10 0 940.47 949.83 58.45 o 8 10 0 4575.30 4666.54 136.06 o 10 10 0 5144.69 5056.62 77.35 o 12 10 0 2310.73 2289.51 81.83 o 14 10 0 637.59 766.14 92.88 o 16 10 0 71.17 117.36 77.26 o 18 10 0 293.38 247.57 76.61 o 20 10 0 547.37 451.87 101.34 o 1 11 0 7709.02 7567.39 75.07 o 3 11 0 3480.63 3806.90 63.60 o 5 11 0 5753.54 5603.95 64.83 o 7 11 0 1837.99 1955.17 69.99 o 9 11 0 20073.49 20043.04 104.53 o 11 11 0 2134.38 2307.52 79.13 o 13 11 0 106.41 228.31 81.94 o 15 11 0 6778.07 6339.94 92.00 o 17 11 0 5557.24 5475.17 105.44 o 19 11 0 93.33 30.83 72.07 o 0 12 0 531.53 405.73 89.74 o 2 12 0 1315.50 1314.13 63.95 o 4 12 0 25790.09 25399.43 279.19 o 6 12 0 10.86 0.92 57.06 o 8 12 0 4071.16 4094.65 85.36 o 10 12 0 70.40 49.58 78.03 o 12 12 0 723.28 874.76 67.17 o 14 12 0 3353.23 3681.86 100.58 o 16 12 0 3197.78 3115.77 133.00 o 18 12 0 1457.35 1352.57 172.18 o 1 13 0 109.42 128.59 60.56 o 3 13 0 5.02 -15.01 60.40 o 5 13 0 1228.00 1274.05 65.16 o 7 13 0 1563.60 1453.79 63.50 o 9 13 0 2109.61 2074.55 81.72 o 11 13 0 4848.22 4982.91 99.78 o 13 13 0 513.91 442.96 69.33 o 15 13 0 603.57 709.07 78.86 o 17 13 0 1263.47 1269.32 102.91 o 19 13 0 14.90 41.15 104.98 o 0 14 0 11196.88 11139.72 336.41 o 2 14 0 170.78 173.81 63.63 o 4 14 0 81.14 152.18 61.94 o 6 14 0 2260.38 2226.03 87.87 o 8 14 0 8174.25 8438.51 136.87 o 10 14 0 1644.53 1734.71 71.01 o 12 14 0 341.99 304.93 69.11 o 14 14 0 609.54 596.13 99.70 o 16 14 0 2526.51 2706.10 101.94 o 18 14 0 1279.35 1006.05 86.67 o 1 15 0 7382.10 7422.73 105.07 o 3 15 0 1237.56 1390.25 65.71 o 5 15 0 1986.10 2044.75 68.78 o 7 15 0 2971.16 2869.78 70.43 o 9 15 0 22013.38 22482.32 352.29 o 11 15 0 6704.79 6417.89 194.03 o 13 15 0 5399.83 5195.93 126.22 o 15 15 0 34.15 60.43 79.23 o 0 16 0 1052.03 1010.53 93.98 o 2 16 0 780.11 764.64 67.40 o 4 16 0 3.33 79.57 65.44 o 6 16 0 3874.64 3894.16 74.58 o 8 16 0 1309.17 1431.48 85.39 o 10 16 0 153.27 123.55 83.36 o 12 16 0 715.55 679.35 74.84 o 14 16 0 483.76 389.21 100.63 o 1 17 0 438.57 475.31 66.56 o 3 17 0 2595.41 2688.57 72.06 o 5 17 0 4368.41 4401.49 91.88 o 7 17 0 8828.82 8489.54 253.36 o 9 17 0 3221.23 3186.82 115.34 o 11 17 0 662.86 803.95 88.69 o 13 17 0 8538.76 8010.57 164.29 o 0 18 0 569.69 616.82 81.34 o 2 18 0 776.18 764.92 70.18 o 4 18 0 2810.94 2794.43 67.81 o 6 18 0 56.63 95.48 71.22 o 8 18 0 4337.63 4369.83 94.56 o 10 18 0 389.54 445.06 88.13 o 12 18 0 1967.37 1893.82 86.26 o 1 19 0 107.30 183.46 63.73 o 3 19 0 72.56 85.95 71.55 o 5 19 0 134.68 121.67 71.94 o 7 19 0 271.54 208.61 78.18 o 9 19 0 675.26 588.78 79.22 o 0 20 0 837.54 898.11 108.11 o 2 20 0 23.93 35.89 73.99 o 4 20 0 725.12 747.71 74.68 o 6 20 0 2705.21 2545.98 75.71 o -24 1 1 9980.23 9584.32 213.89 o -22 1 1 838.30 898.89 75.12 o -20 1 1 349.22 381.09 73.16 o -18 1 1 1554.47 1563.78 70.12 o -16 1 1 36028.98 36492.26 525.54 o -14 1 1 15452.79 15360.48 176.12 o -12 1 1 21706.89 21300.69 294.98 o -10 1 1 1417.84 1268.44 68.00 o -8 1 1 2813.56 2615.66 84.87 o -6 1 1 1235.14 1187.92 94.75 o -4 1 1 615.92 660.85 114.36 o -2 1 1 99760.65 114375.05 956.67 o 0 1 1 45884.69 51051.26 291.48 o 2 1 1 27814.91 31494.49 278.19 o 4 1 1 58923.04 62071.14 329.57 o 6 1 1 101.13 171.93 81.34 o 8 1 1 3868.13 3728.18 79.47 o 10 1 1 26559.83 25941.61 310.22 o 12 1 1 5668.51 5637.14 74.01 o 14 1 1 12850.71 12240.27 200.04 o 16 1 1 1444.03 1443.76 68.70 o 18 1 1 2902.79 2968.37 73.56 o 20 1 1 5653.05 5667.12 80.97 o 22 1 1 1166.15 1282.89 71.32 o 24 1 1 416.38 368.45 87.16 o -23 2 1 5854.67 5795.64 117.38 o -21 2 1 1243.90 1265.50 71.97 o -19 2 1 336.16 294.93 74.64 o -17 2 1 2666.95 2715.13 72.08 o -15 2 1 7170.61 6996.62 124.65 o -13 2 1 121.16 95.89 63.73 o -11 2 1 8433.29 8053.77 88.90 o -9 2 1 3075.07 3073.05 78.90 o -7 2 1 9418.17 10212.18 129.80 o -5 2 1 19718.56 20616.69 196.94 o -3 2 1 78928.74 85115.66 1545.99 o -1 2 1 2.36 35.94 115.75 o 1 2 1 35047.29 37626.10 489.36 o 3 2 1 7511.22 8037.03 166.78 o 5 2 1 53437.54 55302.95 468.04 o 7 2 1 1830.10 2125.66 116.35 o 9 2 1 17681.02 17025.00 108.10 o 11 2 1 2256.34 2148.66 69.62 o 13 2 1 31003.74 31604.66 312.35 o 15 2 1 6579.15 6334.80 75.05 o 17 2 1 6759.33 6753.98 100.69 o 19 2 1 2095.65 2260.00 73.35 o 21 2 1 1414.41 1384.52 74.83 o 23 2 1 5213.66 5143.12 187.32 o -24 3 1 1251.22 1239.72 95.37 o -22 3 1 26.73 57.09 77.33 o -20 3 1 1432.79 1402.68 77.35 o -18 3 1 2317.30 2338.40 68.74 o -16 3 1 231.88 213.87 63.58 o -14 3 1 3421.89 3587.63 75.38 o -12 3 1 8.35 -15.85 66.82 o -10 3 1 6517.66 7961.32 102.35 o -8 3 1 81.81 107.22 80.92 o -6 3 1 17494.05 17748.08 133.32 o -4 3 1 62840.88 65935.99 299.53 o -2 3 1 71.11 102.03 93.17 o 0 3 1 2968.14 3458.94 106.79 o 2 3 1 132.46 147.33 100.68 o 4 3 1 77715.43 83345.07 974.65 o 6 3 1 47256.68 50545.30 583.84 o 8 3 1 3902.77 3883.28 89.15 o 10 3 1 2921.06 3113.52 86.18 o 12 3 1 7437.76 8015.82 133.81 o 14 3 1 8239.19 8398.98 171.55 o 16 3 1 4556.75 4322.16 111.86 o 18 3 1 1408.18 1302.80 82.46 o 20 3 1 5069.91 4976.81 96.05 o 22 3 1 139.89 201.96 83.30 o -23 4 1 873.21 985.30 91.66 o -21 4 1 21.73 64.05 85.05 o -19 4 1 3704.03 3643.92 101.53 o -17 4 1 311.41 322.17 78.72 o -15 4 1 4243.32 4242.48 86.48 o -13 4 1 8923.78 9336.41 170.39 o -11 4 1 23186.38 23246.77 155.80 o -9 4 1 2706.05 2849.02 80.20 o -7 4 1 30473.03 30213.18 670.12 o -5 4 1 77001.77 82554.37 262.34 o -3 4 1 81090.06 81845.94 3345.35 o -1 4 1 7162.35 7897.41 117.96 o 1 4 1 19279.87 21196.51 140.03 o 3 4 1 616.62 514.84 84.65 o 5 4 1 6103.69 5959.22 97.14 o 7 4 1 6246.63 7133.90 130.54 o 9 4 1 51897.79 53128.32 453.86 o 11 4 1 8859.56 9628.02 154.13 o 13 4 1 29912.53 29568.33 240.29 o 15 4 1 6244.15 6149.76 92.16 o 17 4 1 1187.96 1232.32 77.92 o 19 4 1 8519.50 8502.94 225.64 o 21 4 1 8040.63 8141.24 101.78 o 23 4 1 380.99 461.32 92.12 o -22 5 1 1578.00 1487.10 92.10 o -20 5 1 8498.59 8300.51 139.92 o -18 5 1 690.69 716.54 84.10 o -16 5 1 174.65 228.68 77.61 o -14 5 1 9559.29 9732.71 111.02 o -12 5 1 2800.62 2605.35 84.36 o -10 5 1 593.65 474.13 83.21 o -8 5 1 6283.41 6632.82 96.20 o -6 5 1 28771.99 30094.18 149.72 o -4 5 1 3524.21 3825.07 83.71 o -2 5 1 14171.34 14301.06 117.22 o 0 5 1 323.89 418.37 83.26 o 2 5 1 13689.45 14078.02 148.29 o 4 5 1 2937.18 3180.03 93.94 o 6 5 1 55616.10 57543.64 650.37 o 8 5 1 413.29 385.96 65.08 o 10 5 1 4838.50 4427.12 77.52 o 12 5 1 8803.94 9388.93 87.07 o 14 5 1 99.40 79.46 72.00 o 16 5 1 863.60 911.16 78.75 o 18 5 1 156.10 102.33 80.05 o 20 5 1 6.48 109.17 72.32 o 22 5 1 734.45 769.41 76.16 o -23 6 1 164.61 121.30 96.48 o -21 6 1 1869.81 1854.75 94.15 o -19 6 1 1286.78 1269.63 89.15 o -17 6 1 5090.20 5096.75 118.97 o -15 6 1 1674.20 1712.82 84.74 o -13 6 1 2402.66 2286.92 83.87 o -11 6 1 13911.12 14787.80 263.72 o -9 6 1 4043.97 4551.57 85.24 o -7 6 1 51107.02 53646.74 1351.59 o -5 6 1 6738.65 7460.99 88.44 o -3 6 1 1125.61 1180.57 71.87 o -1 6 1 59460.87 61431.17 368.04 o 1 6 1 780.54 703.82 70.02 o 3 6 1 717.44 763.12 73.35 o 5 6 1 135.41 181.18 76.28 o 7 6 1 1163.40 1083.33 80.73 o 9 6 1 994.65 1103.77 71.50 o 11 6 1 1801.29 1774.62 69.83 o 13 6 1 815.38 910.44 78.42 o 15 6 1 5154.80 5186.94 87.68 o 17 6 1 2757.48 2982.59 86.99 o 19 6 1 359.22 416.99 69.96 o 21 6 1 2173.25 2046.57 90.33 o 23 6 1 15.57 8.61 90.45 o -22 7 1 2496.39 2355.55 90.55 o -20 7 1 6910.41 6996.51 97.47 o -18 7 1 23.48 14.09 92.66 o -16 7 1 1692.10 1672.53 93.56 o -14 7 1 3609.00 3693.90 94.45 o -12 7 1 643.54 727.51 74.36 o -10 7 1 11559.21 11066.15 113.80 o -8 7 1 5829.58 5940.81 96.02 o -6 7 1 27374.19 27582.19 309.95 o -4 7 1 31519.49 31330.17 257.75 o -2 7 1 9800.94 9581.83 92.31 o 0 7 1 9312.41 8700.94 89.80 o 2 7 1 3454.69 3003.89 75.26 o 4 7 1 36409.00 37707.60 413.27 o 6 7 1 22000.38 22622.43 242.89 o 8 7 1 208.27 425.31 76.46 o 10 7 1 8930.04 8356.34 85.09 o 12 7 1 1956.79 2078.99 64.19 o 14 7 1 3867.29 3669.66 63.68 o 16 7 1 9.03 43.62 78.64 o 18 7 1 2808.56 2921.54 90.07 o 20 7 1 33.74 -9.38 87.74 o 22 7 1 6626.52 6899.32 164.43 o -21 8 1 391.43 410.89 84.13 o -19 8 1 6485.48 6451.03 110.45 o -17 8 1 1928.89 2029.06 96.91 o -15 8 1 3394.16 3601.32 84.71 o -13 8 1 3.17 -39.67 73.32 o -11 8 1 2223.71 2217.37 81.65 o -9 8 1 1294.74 1308.18 61.29 o -7 8 1 1587.82 1263.45 80.08 o -5 8 1 2339.38 2289.21 64.79 o -3 8 1 87.82 150.78 57.50 o -1 8 1 14474.40 15118.12 229.05 o 1 8 1 22058.37 21687.07 232.95 o 3 8 1 149.41 249.29 60.00 o 5 8 1 43812.72 45586.16 559.55 o 7 8 1 5096.57 5593.72 87.31 o 9 8 1 3691.51 3372.52 73.97 o 11 8 1 982.56 851.30 68.66 o 13 8 1 1453.18 1489.01 75.23 o 15 8 1 1922.52 1909.31 77.50 o 17 8 1 13.87 62.57 74.91 o 19 8 1 797.90 789.49 82.48 o 21 8 1 1175.53 1172.58 89.25 o -22 9 1 274.80 270.20 86.65 o -20 9 1 49.08 68.57 101.06 o -18 9 1 1.69 4.92 95.14 o -16 9 1 314.54 309.82 74.84 o -14 9 1 2994.75 2987.50 81.14 o -12 9 1 4655.58 4560.22 97.59 o -10 9 1 1796.99 1898.44 70.50 o -8 9 1 3700.20 3686.62 85.70 o -6 9 1 1867.98 1811.70 70.79 o -4 9 1 15901.91 16378.02 184.58 o -2 9 1 7028.69 7619.98 75.90 o 0 9 1 1037.27 987.00 67.05 o 2 9 1 1495.82 1452.44 61.52 o 4 9 1 840.37 955.62 61.91 o 6 9 1 8129.66 7764.34 91.51 o 8 9 1 9973.23 9812.33 106.73 o 10 9 1 135.45 123.75 73.21 o 12 9 1 8.01 -2.61 69.24 o 14 9 1 6308.76 6217.86 86.91 o 16 9 1 274.23 314.33 77.49 o 18 9 1 131.03 139.10 83.07 o 20 9 1 124.14 112.10 90.61 o -21 10 1 3.88 -40.70 103.81 o -19 10 1 5933.06 5838.37 166.74 o -17 10 1 318.44 303.48 74.87 o -15 10 1 3446.04 3700.45 84.71 o -13 10 1 366.18 446.46 151.63 o -11 10 1 17018.11 16872.51 322.66 o -9 10 1 1865.77 2036.67 80.26 o -7 10 1 13106.02 12715.19 186.27 o -5 10 1 7003.64 7020.97 121.90 o -3 10 1 6091.49 5079.89 73.52 o -1 10 1 11.14 46.93 61.86 o 1 10 1 3286.74 2940.15 68.62 o 3 10 1 4381.25 4627.42 69.62 o 5 10 1 8212.15 7792.33 158.49 o 7 10 1 5119.22 5215.13 69.85 o 9 10 1 16141.12 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