#------------------------------------------------------------------------------ #$Date: 2016-04-03 03:55:59 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181124 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/03/2220326.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220326_Fobs loop_ _publ_author_name 'Yuan, Yan-Qin' 'Guo, Sheng-Rong' 'Wang, Li-Jin' _publ_section_title ; [4-(Methylsulfonyl)phenyl]acetic acid ; _journal_coeditor_code RZ2263 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2435 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.102 _cell_angle_gamma 90.000 _cell_length_a 19.0857 _cell_length_b 4.9711 _cell_length_c 10.7236 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file rz2263Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' t in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 133.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 272.59 0.01 0.03 o 2 0 0 4.97 4.20 0.33 o 3 0 0 3009.03 2783.75 40.81 o 4 0 0 2134.72 2190.69 28.81 o 5 0 0 3690.69 3573.61 46.58 o 6 0 0 2730.74 2869.79 37.82 o 7 0 0 7.38 6.25 0.68 o 8 0 0 138.95 120.01 3.69 o 9 0 0 375.49 382.47 6.78 o 10 0 0 1465.08 1575.94 22.31 o 11 0 0 480.13 518.68 8.91 o 12 0 0 96.45 99.26 3.09 o 13 0 0 1573.22 1612.13 23.52 o 14 0 0 341.42 335.01 7.01 o 15 0 0 0.13 1.00 0.77 o 16 0 0 1254.20 1262.12 19.82 o 17 0 0 41.07 37.88 4.03 o 18 0 0 4.43 4.43 1.14 o 19 0 0 89.47 86.35 3.68 o 20 0 0 16.54 20.89 2.84 o 21 0 0 7.36 11.55 2.40 o 1 1 0 576.13 605.54 7.01 o 3 1 0 402.80 426.24 4.47 o 4 1 0 763.85 776.53 7.03 o 5 1 0 138.51 163.78 2.09 o 6 1 0 0.12 5.42 0.38 o 7 1 0 226.78 214.23 2.34 o 8 1 0 730.25 822.32 7.27 o 9 1 0 143.30 153.60 1.97 o 10 1 0 40.35 39.65 1.10 o 11 1 0 118.88 114.82 1.84 o 12 1 0 408.11 392.85 7.59 o 13 1 0 12.54 13.39 0.78 o 14 1 0 115.24 99.64 2.73 o 15 1 0 100.81 93.13 2.73 o 16 1 0 249.26 244.84 4.94 o 17 1 0 9.26 10.06 1.13 o 18 1 0 35.37 29.17 1.75 o 19 1 0 10.19 10.49 1.26 o 20 1 0 83.75 70.12 2.76 o 21 1 0 15.44 20.16 1.72 o 0 2 0 1.60 0.94 0.40 o 1 2 0 722.00 722.40 7.70 o 2 2 0 123.99 122.26 1.98 o 3 2 0 73.58 67.30 2.10 o 5 2 0 43.35 38.36 0.92 o 6 2 0 2.80 3.01 0.36 o 7 2 0 255.02 285.29 3.39 o 8 2 0 1147.36 1250.97 11.54 o 9 2 0 266.13 299.96 3.66 o 10 2 0 0.88 0.12 0.25 o 11 2 0 19.82 20.74 0.99 o 12 2 0 30.12 34.05 2.23 o 13 2 0 28.92 20.06 1.11 o 14 2 0 44.57 35.66 1.42 o 15 2 0 46.49 45.57 1.94 o 16 2 0 26.31 19.92 2.00 o 17 2 0 7.84 10.86 1.21 o 18 2 0 151.37 136.55 5.77 o 19 2 0 3.50 3.70 0.92 o 20 2 0 40.56 49.03 3.39 o 1 3 0 41.85 37.18 1.19 o 2 3 0 2.11 4.55 0.41 o 3 3 0 823.14 864.78 8.37 o 4 3 0 50.06 42.32 1.09 o 5 3 0 72.57 76.82 2.19 o 6 3 0 37.25 33.76 1.10 o 7 3 0 69.41 62.99 1.45 o 8 3 0 3.41 6.15 0.56 o 9 3 0 214.75 211.05 3.09 o 10 3 0 0.16 0.87 0.46 o 11 3 0 29.65 32.57 1.34 o 12 3 0 0.31 1.50 0.51 o 13 3 0 2.87 2.36 0.72 o 14 3 0 1.97 3.04 0.79 o 15 3 0 1.50 2.32 0.76 o 16 3 0 37.79 37.53 2.38 o 17 3 0 1.76 4.61 1.83 o 18 3 0 2.46 2.61 1.58 o 0 4 0 425.35 454.60 11.48 o 1 4 0 374.21 353.57 7.96 o 2 4 0 0.01 0.45 0.45 o 3 4 0 5.62 4.60 1.03 o 4 4 0 161.28 158.18 3.36 o 5 4 0 314.41 316.87 5.80 o 6 4 0 98.78 102.67 3.88 o 7 4 0 71.05 74.68 3.50 o 8 4 0 2.19 1.77 0.70 o 9 4 0 246.05 257.80 6.63 o 10 4 0 34.05 33.47 2.37 o 11 4 0 0.24 -0.35 0.95 o 12 4 0 54.22 65.95 4.16 o 13 4 0 77.01 83.53 3.70 o 14 4 0 53.19 59.53 6.24 o 15 4 0 0.93 2.54 1.42 o 16 4 0 50.50 51.97 4.34 o 1 5 0 56.82 54.09 3.11 o 2 5 0 587.74 602.21 12.56 o 3 5 0 121.18 123.16 6.50 o 4 5 0 0.78 0.92 0.82 o 5 5 0 95.22 99.83 11.05 o 6 5 0 8.17 6.13 1.44 o 7 5 0 137.94 142.31 4.01 o 8 5 0 22.52 23.58 2.24 o 9 5 0 24.63 25.75 5.60 o 10 5 0 9.09 12.72 1.84 o 11 5 0 204.06 236.01 8.02 o -21 1 1 6.12 7.49 1.17 o -20 1 1 84.87 81.69 2.90 o -19 1 1 0.91 2.00 0.66 o -18 1 1 98.93 96.33 2.61 o -17 1 1 1.10 1.41 0.56 o -16 1 1 70.13 66.33 2.02 o -15 1 1 0.21 0.17 0.41 o -14 1 1 251.44 237.68 3.91 o -13 1 1 147.63 156.56 2.92 o -12 1 1 114.65 116.16 2.18 o -11 1 1 14.77 15.76 0.72 o -10 1 1 299.00 346.93 3.98 o -9 1 1 1620.73 1753.12 15.43 o -8 1 1 619.58 674.93 5.88 o -7 1 1 660.33 718.19 6.13 o -6 1 1 937.74 1039.22 8.46 o -5 1 1 259.75 262.15 2.52 o -4 1 1 1353.46 1430.35 11.26 o -3 1 1 824.22 848.40 8.39 o -1 1 1 704.37 752.06 9.73 o 0 1 1 691.52 760.31 7.64 o 1 1 1 6538.28 5264.05 46.42 o 3 1 1 3362.60 3309.81 28.18 o 4 1 1 11541.30 9117.09 79.89 o 5 1 1 1297.76 1411.54 14.76 o 6 1 1 5663.82 5732.68 48.65 o 7 1 1 1414.20 1678.01 14.85 o 8 1 1 1542.28 1716.40 15.27 o 9 1 1 286.44 294.20 3.52 o 10 1 1 1025.85 1089.31 10.30 o 11 1 1 1.72 2.48 0.38 o 12 1 1 38.12 44.38 1.73 o 13 1 1 131.48 140.32 4.37 o 14 1 1 6.16 6.69 1.09 o 15 1 1 131.01 127.21 3.34 o 16 1 1 6.47 6.56 1.02 o 17 1 1 340.82 353.85 6.57 o 18 1 1 5.55 4.64 1.00 o 19 1 1 3.93 2.37 0.97 o 20 1 1 13.45 11.36 1.74 o -20 2 1 84.44 84.34 3.82 o -19 2 1 71.83 60.07 3.16 o -18 2 1 1.93 2.74 1.02 o -17 2 1 3.36 3.89 0.87 o -16 2 1 267.87 268.78 5.42 o -15 2 1 25.86 24.33 1.40 o -14 2 1 2.55 2.33 0.55 o -13 2 1 93.40 98.98 2.26 o -12 2 1 70.17 67.46 1.93 o -11 2 1 377.39 397.80 7.06 o -10 2 1 677.01 693.40 6.98 o -9 2 1 113.04 106.54 1.78 o -8 2 1 177.32 177.38 2.43 o -7 2 1 1464.53 1544.36 13.81 o -6 2 1 487.04 526.87 5.34 o -5 2 1 115.04 159.85 2.55 o -3 2 1 734.18 746.48 7.93 o -2 2 1 710.56 683.80 7.34 o -1 2 1 179.07 218.52 2.93 o 0 2 1 848.52 916.59 9.52 o 1 2 1 622.03 665.81 6.29 o 2 2 1 241.04 202.59 3.36 o 5 2 1 562.84 630.41 6.26 o 6 2 1 1577.30 1787.53 15.88 o 7 2 1 725.13 699.87 6.99 o 8 2 1 1006.59 1094.42 10.80 o 9 2 1 13.55 10.58 1.22 o 10 2 1 27.04 32.42 1.05 o 11 2 1 249.53 243.66 4.96 o 12 2 1 189.82 194.82 3.46 o 13 2 1 215.98 205.62 3.66 o 14 2 1 10.08 7.35 0.84 o 15 2 1 5.03 3.14 0.78 o 16 2 1 46.35 43.82 2.03 o 17 2 1 117.37 111.01 3.33 o 18 2 1 0.36 1.20 0.67 o 19 2 1 131.71 131.53 3.88 o -19 3 1 14.71 19.92 2.12 o -18 3 1 178.07 193.60 5.86 o -17 3 1 25.95 27.74 2.36 o -16 3 1 1.95 3.43 1.06 o -15 3 1 31.00 31.20 2.14 o -14 3 1 166.64 172.99 4.09 o -13 3 1 72.57 74.97 2.81 o -12 3 1 463.09 443.63 8.85 o -11 3 1 157.81 160.00 8.00 o -10 3 1 48.70 49.14 2.36 o -9 3 1 526.31 541.78 5.97 o -8 3 1 99.69 91.60 1.80 o -7 3 1 154.14 164.04 3.66 o -6 3 1 61.55 65.10 1.42 o -3 3 1 13.00 15.62 0.83 o -2 3 1 99.82 129.01 2.36 o -1 3 1 135.67 125.73 2.33 o 0 3 1 10.98 5.98 0.57 o 1 3 1 280.33 319.09 4.30 o 2 3 1 1.24 0.88 0.27 o 3 3 1 159.77 157.23 2.52 o 5 3 1 156.26 127.08 5.53 o 6 3 1 288.24 296.75 3.75 o 7 3 1 26.57 26.17 0.97 o 8 3 1 14.05 16.84 0.84 o 9 3 1 596.32 589.25 6.51 o 10 3 1 224.56 215.27 7.29 o 11 3 1 7.93 6.03 0.97 o 12 3 1 20.91 18.89 1.18 o 13 3 1 4.56 5.80 0.80 o 14 3 1 6.56 11.25 1.03 o 15 3 1 110.35 97.69 3.09 o 16 3 1 1.67 3.71 1.53 o 17 3 1 28.43 31.66 3.46 o 18 3 1 50.50 49.37 4.15 o -16 4 1 38.58 39.98 3.84 o -15 4 1 4.85 9.57 2.23 o -14 4 1 1.20 3.95 1.16 o -13 4 1 10.43 12.68 1.76 o -12 4 1 22.92 30.96 2.64 o -11 4 1 180.16 185.51 6.56 o -10 4 1 171.41 173.68 7.86 o -9 4 1 17.22 18.12 2.99 o -8 4 1 3.27 4.64 0.87 o -7 4 1 144.10 152.25 3.75 o -6 4 1 118.80 113.66 3.16 o -5 4 1 331.97 337.06 6.08 o -4 4 1 18.00 23.95 2.59 o -3 4 1 0.40 1.26 0.62 o -2 4 1 138.75 118.83 5.93 o -1 4 1 68.71 73.01 2.45 o 0 4 1 20.33 13.03 1.17 o 1 4 1 24.15 26.22 1.21 o 2 4 1 73.17 70.89 1.98 o 3 4 1 183.87 193.40 4.16 o 5 4 1 83.29 81.53 2.22 o 6 4 1 419.47 429.11 9.94 o 7 4 1 2.78 4.97 0.79 o 8 4 1 159.76 162.25 4.34 o 9 4 1 91.58 82.39 3.44 o 10 4 1 1.54 1.92 0.97 o 11 4 1 129.53 129.94 4.59 o 12 4 1 5.72 6.80 1.37 o 13 4 1 0.27 2.02 0.97 o 14 4 1 1.51 1.36 1.02 o 15 4 1 23.94 26.41 2.36 o -12 5 1 2.41 5.61 1.49 o -11 5 1 3.94 6.34 1.45 o -10 5 1 2.27 4.26 1.62 o -9 5 1 7.65 9.59 1.62 o -8 5 1 12.36 15.46 1.90 o -7 5 1 5.92 9.48 1.27 o -6 5 1 22.21 22.90 2.54 o -5 5 1 2.56 5.41 1.06 o -4 5 1 0.00 0.45 0.66 o -3 5 1 101.92 115.01 3.53 o -2 5 1 1.66 0.52 1.00 o -1 5 1 3.22 1.53 1.08 o 0 5 1 81.50 85.64 4.25 o 1 5 1 6.80 5.70 1.45 o 2 5 1 56.39 55.00 3.16 o 3 5 1 37.34 33.78 2.59 o 4 5 1 4.12 3.76 1.19 o 5 5 1 19.34 20.35 2.14 o 6 5 1 5.91 9.18 1.62 o 7 5 1 1.78 1.77 1.03 o 8 5 1 26.24 33.00 3.95 o 9 5 1 9.85 14.06 2.85 o 10 5 1 0.52 4.48 1.87 o 11 5 1 0.17 2.84 1.18 o -22 0 2 13.93 16.64 1.90 o -21 0 2 99.09 85.11 3.71 o -20 0 2 3.53 2.39 0.90 o -19 0 2 17.43 10.07 1.46 o -18 0 2 0.05 -0.11 0.57 o -17 0 2 420.49 431.99 8.74 o -16 0 2 1044.17 1027.56 16.44 o -15 0 2 136.01 134.54 5.95 o -14 0 2 2.56 3.55 0.80 o -13 0 2 9.91 11.94 1.16 o -12 0 2 107.34 117.11 3.26 o -11 0 2 35.68 46.75 1.88 o -10 0 2 130.20 146.75 3.53 o -9 0 2 14.20 8.09 0.51 o -8 0 2 173.51 226.71 3.24 o -7 0 2 430.34 486.57 6.25 o -6 0 2 538.66 606.97 7.25 o -5 0 2 11206.84 8609.13 96.45 o -4 0 2 1.32 -0.35 0.41 o -3 0 2 17731.51 12624.06 236.98 o -2 0 2 3.40 0.25 0.27 o -1 0 2 10583.53 7580.96 145.20 o 0 0 2 6232.17 5521.98 103.44 o 1 0 2 1473.15 1443.50 27.24 o 2 0 2 53.24 45.78 1.84 o 3 0 2 819.74 857.65 17.09 o 4 0 2 4291.44 4387.71 80.87 o 5 0 2 1180.00 1170.35 23.30 o 6 0 2 1260.90 1312.26 26.18 o 7 0 2 408.88 481.57 11.39 o 8 0 2 2248.06 2266.32 43.97 o 9 0 2 3845.14 4252.42 79.92 o 10 0 2 2389.95 2412.25 47.24 o 11 0 2 206.36 187.36 6.53 o 12 0 2 7.34 5.00 1.43 o 13 0 2 1586.66 1598.94 33.59 o 14 0 2 551.24 560.70 14.86 o 15 0 2 0.45 0.05 1.14 o 16 0 2 209.18 219.79 8.36 o 17 0 2 111.84 94.10 5.37 o 18 0 2 8.72 10.15 2.25 o 19 0 2 185.99 179.00 8.00 o 20 0 2 0.96 2.25 1.60 o -22 1 2 0.00 0.75 0.52 o -21 1 2 73.29 80.40 2.75 o -20 1 2 27.78 28.37 1.57 o -19 1 2 172.67 162.90 3.54 o -18 1 2 0.54 1.36 0.72 o -17 1 2 72.50 63.75 2.96 o -16 1 2 64.79 67.43 1.98 o -15 1 2 370.22 342.92 6.06 o -14 1 2 583.79 580.87 7.22 o -13 1 2 372.04 378.89 10.47 o -12 1 2 124.53 115.96 1.99 o -11 1 2 126.12 121.43 2.24 o -10 1 2 24.51 36.53 0.97 o -9 1 2 39.87 43.26 1.01 o -8 1 2 314.01 307.60 3.42 o -7 1 2 774.59 803.63 6.76 o -6 1 2 1584.62 1566.08 12.41 o -5 1 2 927.50 999.44 8.11 o -4 1 2 85.02 81.55 1.54 o -3 1 2 4902.34 4411.34 84.18 o -2 1 2 72.37 81.63 2.57 o -1 1 2 12387.21 8340.35 290.78 o 0 1 2 100.92 130.58 2.46 o 1 1 2 4144.63 4066.09 68.68 o 3 1 2 1228.05 1427.60 16.21 o 4 1 2 376.00 364.01 4.97 o 5 1 2 59.74 58.52 1.32 o 6 1 2 37.22 49.57 1.87 o 7 1 2 2777.28 2939.57 25.34 o 8 1 2 5.69 4.79 0.50 o 9 1 2 32.34 34.64 1.16 o 10 1 2 282.42 274.27 3.98 o 11 1 2 203.89 185.17 3.14 o 12 1 2 473.15 453.41 8.64 o 13 1 2 52.32 51.19 2.49 o 14 1 2 66.74 75.36 3.13 o 15 1 2 726.07 720.47 12.88 o 16 1 2 2.99 4.31 1.78 o 17 1 2 41.66 34.77 2.31 o 18 1 2 18.92 22.71 2.11 o 19 1 2 41.49 38.26 2.62 o 20 1 2 41.13 37.48 2.64 o -21 2 2 1.76 0.01 0.84 o -20 2 2 38.61 41.47 3.20 o -19 2 2 8.98 9.26 1.54 o -18 2 2 26.61 24.01 2.79 o -17 2 2 4.60 5.54 1.23 o -16 2 2 3.90 6.15 0.96 o -15 2 2 2.31 2.76 0.69 o -14 2 2 101.20 104.41 2.39 o -13 2 2 237.31 235.11 5.35 o -12 2 2 12.14 8.64 0.68 o -11 2 2 54.31 42.68 1.20 o -10 2 2 153.45 147.04 2.29 o -9 2 2 256.14 274.20 3.02 o -8 2 2 651.53 705.23 6.30 o -7 2 2 709.93 782.97 6.82 o -6 2 2 3.63 3.87 0.31 o -5 2 2 34.12 34.45 0.89 o -4 2 2 0.32 1.07 0.54 o -3 2 2 80.89 102.61 3.91 o -2 2 2 316.73 359.98 4.29 o -1 2 2 126.77 155.89 2.31 o 0 2 2 20.50 21.79 0.75 o 1 2 2 239.22 252.70 8.40 o 2 2 2 13.04 9.81 0.79 o 5 2 2 0.29 0.01 0.24 o 6 2 2 40.26 48.85 1.20 o 7 2 2 20.37 24.17 1.24 o 8 2 2 170.59 177.49 2.66 o 9 2 2 12.71 17.13 0.83 o 10 2 2 59.68 64.01 1.56 o 11 2 2 101.55 110.31 2.51 o 12 2 2 6.90 6.22 0.75 o 13 2 2 74.92 48.27 1.83 o 14 2 2 11.99 14.46 1.26 o 15 2 2 14.24 16.84 1.42 o 16 2 2 5.67 7.28 1.34 o 17 2 2 13.94 15.01 1.82 o 18 2 2 12.29 12.70 1.73 o 19 2 2 1.79 5.03 1.94 o -19 3 2 64.78 76.78 4.73 o -18 3 2 17.78 17.86 2.00 o -17 3 2 13.29 13.23 1.72 o -16 3 2 3.24 4.63 1.13 o -15 3 2 78.06 79.75 3.35 o -14 3 2 6.68 6.59 1.05 o -13 3 2 143.40 140.60 3.56 o -12 3 2 86.17 89.74 2.74 o -11 3 2 29.89 28.48 2.16 o -10 3 2 99.89 101.75 2.79 o -9 3 2 127.17 140.44 3.27 o -8 3 2 121.38 129.27 2.58 o -7 3 2 1.60 1.13 0.47 o -6 3 2 26.84 27.10 1.11 o -5 3 2 0.01 0.55 0.47 o -3 3 2 42.22 31.36 1.56 o -2 3 2 226.40 206.70 3.16 o -1 3 2 161.33 180.01 2.92 o 0 3 2 3.75 4.38 0.52 o 1 3 2 688.89 711.51 8.19 o 2 3 2 0.13 0.42 0.32 o 3 3 2 33.31 28.23 1.11 o 4 3 2 49.55 45.34 2.06 o 5 3 2 31.11 24.87 1.10 o 6 3 2 266.70 261.24 4.07 o 7 3 2 31.89 28.75 1.24 o 8 3 2 20.74 21.66 1.11 o 9 3 2 0.08 0.59 0.45 o 10 3 2 27.84 30.61 1.35 o 11 3 2 122.04 133.16 3.43 o 12 3 2 0.82 0.56 0.58 o 13 3 2 110.45 95.35 3.08 o 14 3 2 9.94 9.45 1.20 o 15 3 2 0.76 1.39 0.88 o 16 3 2 38.69 36.43 2.94 o 17 3 2 1.76 2.50 1.62 o -16 4 2 33.90 41.94 3.89 o -15 4 2 16.01 22.26 2.20 o -14 4 2 26.17 33.01 3.14 o -13 4 2 11.32 16.84 1.91 o -12 4 2 222.10 250.97 12.04 o -11 4 2 3.67 3.95 1.15 o -10 4 2 78.65 91.20 3.73 o -9 4 2 51.10 56.96 2.90 o -8 4 2 127.13 115.16 3.22 o -7 4 2 0.77 0.27 0.57 o -6 4 2 20.74 23.55 1.53 o -5 4 2 68.41 63.54 2.34 o -4 4 2 196.10 191.30 4.35 o -3 4 2 439.33 439.41 7.32 o -2 4 2 8.28 7.97 1.04 o -1 4 2 171.22 168.53 3.98 o 0 4 2 212.82 208.19 4.51 o 1 4 2 315.72 302.58 5.69 o 2 4 2 80.19 76.13 2.56 o 3 4 2 23.48 21.15 1.49 o 5 4 2 4.62 4.15 1.12 o 6 4 2 5.89 7.10 0.87 o 7 4 2 0.97 2.01 0.88 o 8 4 2 107.93 118.45 2.87 o 9 4 2 80.96 87.75 2.48 o 10 4 2 119.31 126.99 3.57 o 11 4 2 13.15 12.44 1.70 o 12 4 2 52.21 54.06 2.98 o 13 4 2 187.69 176.13 5.65 o 14 4 2 48.87 49.96 3.23 o -12 5 2 85.60 99.04 4.38 o -11 5 2 5.49 9.87 1.76 o -10 5 2 48.01 53.06 3.14 o -9 5 2 11.86 12.48 1.82 o -8 5 2 0.03 0.24 1.14 o -7 5 2 162.10 167.53 4.46 o -6 5 2 74.63 78.63 2.96 o -5 5 2 272.21 272.50 6.61 o -4 5 2 1.32 2.25 0.87 o -3 5 2 63.63 62.52 2.86 o -2 5 2 203.93 201.81 4.90 o -1 5 2 416.05 431.53 7.89 o 0 5 2 51.91 50.08 2.37 o 1 5 2 14.65 15.17 1.93 o 2 5 2 257.21 246.23 7.07 o 3 5 2 21.23 20.06 2.15 o 4 5 2 11.33 9.44 1.67 o 5 5 2 140.52 127.83 8.55 o 6 5 2 153.17 160.27 6.48 o 7 5 2 54.94 59.88 3.35 o 8 5 2 137.64 137.12 7.65 o 9 5 2 4.51 7.86 2.32 o 10 5 2 32.98 36.35 4.23 o -22 1 3 23.45 24.25 3.15 o -21 1 3 2.54 2.70 0.83 o -20 1 3 5.15 6.19 1.06 o -19 1 3 8.45 10.26 1.00 o -18 1 3 37.07 33.26 1.48 o -17 1 3 4.11 5.91 0.79 o -16 1 3 34.55 35.20 1.55 o -15 1 3 199.87 189.07 3.54 o -14 1 3 17.94 17.01 1.01 o -13 1 3 55.96 58.81 1.71 o -12 1 3 215.65 222.60 3.00 o -11 1 3 182.85 202.30 2.74 o -10 1 3 384.76 451.94 4.84 o -9 1 3 160.93 197.56 2.54 o -8 1 3 1.83 7.21 0.43 o -7 1 3 138.10 165.26 2.11 o -6 1 3 1083.50 1180.37 11.65 o -5 1 3 196.58 218.48 2.67 o -4 1 3 648.34 812.01 9.62 o -3 1 3 542.02 546.32 8.59 o -2 1 3 60.17 65.12 1.54 o -1 1 3 32.15 18.26 0.60 o 0 1 3 582.63 600.56 6.71 o 3 1 3 4.88 3.81 0.50 o 4 1 3 1473.84 1608.06 18.45 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