#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220353.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220353_Fobs loop_ _publ_author_name 'Arshad, Muhammad Nadeem' 'Tahir, M. Nawaz' 'Khan, Islam Ullah' 'Shafiq, Muhammad' 'Siddiqui, Waseeq Ahmad' _publ_section_title ; Sodium 2-iodobenzenesulfonate monohydrate ; _journal_coeditor_code SU2075 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1628 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.171 _cell_angle_gamma 90.000 _cell_length_a 13.6141 _cell_length_b 8.8233 _cell_length_c 7.8493 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7497 _[local]_cod_data_source_file su2075Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NT3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 245.87 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9639.71 9910.44 266.21 o 3 0 0 21303.78 22237.17 594.81 o 4 0 0 2893.59 3131.25 61.06 o 5 0 0 50829.33 49394.55 1321.73 o 6 0 0 467.26 394.59 15.24 o 7 0 0 14747.81 14401.67 387.44 o 8 0 0 1365.23 1328.11 41.83 o 9 0 0 4110.80 4077.15 115.56 o 10 0 0 8591.55 8409.87 231.24 o 11 0 0 1415.76 1396.52 46.44 o 12 0 0 1384.44 1375.37 46.61 o 13 0 0 735.58 743.28 30.66 o 14 0 0 138.86 152.48 14.18 o 15 0 0 356.93 311.59 20.74 o 16 0 0 2086.04 2199.18 73.32 o 17 0 0 248.62 276.43 21.50 o 18 0 0 166.10 151.01 17.78 o 1 1 0 13983.24 13943.49 161.19 o 2 1 0 9259.49 9161.28 85.96 o 3 1 0 8112.72 8196.93 104.09 o 4 1 0 22279.13 22415.43 424.29 o 5 1 0 893.05 906.13 20.05 o 6 1 0 9809.12 9654.37 184.50 o 7 1 0 10810.71 10561.61 202.03 o 8 1 0 1398.39 1303.04 36.07 o 9 1 0 7344.95 6993.65 136.42 o 10 1 0 1796.93 1773.92 39.29 o 11 1 0 3702.03 3557.19 73.48 o 12 1 0 1575.58 1575.38 36.87 o 13 1 0 146.85 149.74 9.85 o 14 1 0 2021.30 1912.89 44.68 o 15 1 0 69.24 98.72 9.63 o 16 1 0 270.32 278.55 23.10 o 17 1 0 257.98 258.07 19.91 o 18 1 0 7.55 11.64 11.34 o 0 2 0 685.61 676.54 10.11 o 1 2 0 3693.68 3621.45 33.68 o 2 2 0 5360.33 5269.22 48.23 o 3 2 0 34320.84 34245.37 303.80 o 4 2 0 13084.86 13102.66 137.49 o 5 2 0 291.23 262.69 6.66 o 6 2 0 6076.55 6372.22 82.64 o 7 2 0 732.40 668.73 10.19 o 8 2 0 7125.11 6975.29 100.30 o 9 2 0 1744.91 1694.85 26.44 o 10 2 0 2863.12 2764.51 41.78 o 11 2 0 6.96 9.31 2.56 o 12 2 0 10.50 9.55 2.28 o 13 2 0 3710.53 3724.07 56.24 o 14 2 0 123.74 137.12 5.91 o 15 2 0 681.62 648.05 14.96 o 16 2 0 4.19 8.15 3.32 o 17 2 0 14.18 13.05 6.27 o 1 3 0 7397.14 7350.73 67.52 o 2 3 0 4.73 18.01 2.61 o 3 3 0 93.91 103.37 2.70 o 4 3 0 2258.47 2201.10 24.32 o 5 3 0 138.72 173.95 4.12 o 6 3 0 3882.72 3734.54 46.26 o 7 3 0 252.90 264.91 5.18 o 8 3 0 638.86 666.87 12.34 o 9 3 0 84.63 107.70 3.51 o 10 3 0 533.37 489.06 8.75 o 11 3 0 663.08 614.60 10.45 o 12 3 0 99.58 95.97 3.85 o 13 3 0 221.31 210.00 5.50 o 14 3 0 68.97 69.20 4.30 o 15 3 0 209.65 192.60 6.05 o 16 3 0 21.96 25.94 3.33 o 17 3 0 260.25 230.38 9.22 o 0 4 0 1434.73 1363.66 25.15 o 1 4 0 272.85 233.04 5.39 o 2 4 0 75.46 89.25 3.06 o 3 4 0 120.85 97.86 3.32 o 4 4 0 631.30 628.48 8.07 o 5 4 0 3.80 2.76 1.84 o 6 4 0 310.29 342.40 7.04 o 7 4 0 1535.47 1475.41 20.41 o 8 4 0 1079.37 1052.43 15.46 o 9 4 0 628.42 614.96 10.34 o 10 4 0 88.42 101.28 4.76 o 11 4 0 419.25 397.74 8.77 o 12 4 0 208.02 217.48 6.60 o 13 4 0 260.84 259.77 7.93 o 14 4 0 4.54 3.95 3.32 o 15 4 0 27.30 30.42 4.16 o 16 4 0 105.11 116.32 9.33 o 17 4 0 155.91 173.51 9.73 o 1 5 0 2642.41 2684.37 33.68 o 2 5 0 503.96 546.49 11.47 o 3 5 0 5.98 4.64 1.68 o 4 5 0 457.64 403.87 6.14 o 5 5 0 763.52 769.64 9.50 o 6 5 0 3135.83 3096.84 34.94 o 7 5 0 115.57 104.75 4.55 o 8 5 0 27.24 28.76 3.76 o 9 5 0 2.32 1.45 3.62 o 10 5 0 1328.62 1276.72 27.24 o 11 5 0 784.42 765.82 19.04 o 12 5 0 33.00 41.01 5.74 o 13 5 0 0.78 3.30 4.83 o 14 5 0 0.29 2.00 4.95 o 15 5 0 445.66 447.85 15.11 o 16 5 0 97.79 106.03 8.66 o 0 6 0 10571.47 10643.75 244.88 o 1 6 0 0.87 15.74 3.91 o 2 6 0 1570.52 1616.31 24.21 o 3 6 0 2616.19 2670.89 37.53 o 4 6 0 303.79 288.06 7.13 o 5 6 0 3839.70 3783.63 47.43 o 6 6 0 373.05 391.89 11.92 o 7 6 0 1104.03 1082.33 16.47 o 8 6 0 511.61 508.81 13.29 o 9 6 0 78.91 75.54 6.95 o 10 6 0 1163.66 1134.32 26.16 o 11 6 0 473.11 487.83 15.47 o 12 6 0 176.44 162.91 12.28 o 13 6 0 84.20 80.27 9.99 o 14 6 0 2.05 5.27 5.73 o 15 6 0 25.68 36.03 13.36 o 1 7 0 1069.47 1095.25 18.46 o 2 7 0 5260.06 5296.48 85.17 o 3 7 0 1804.10 1784.50 35.10 o 4 7 0 2387.83 2404.74 36.53 o 5 7 0 25.26 41.29 4.28 o 6 7 0 366.24 354.43 14.05 o 7 7 0 4898.98 4646.38 66.01 o 8 7 0 301.69 297.44 11.26 o 9 7 0 2568.62 2515.55 49.87 o 10 7 0 67.67 78.44 8.61 o 11 7 0 40.65 60.06 8.38 o 12 7 0 704.25 688.80 20.38 o 13 7 0 20.99 28.36 6.83 o 14 7 0 780.19 782.84 23.78 o 0 8 0 2262.24 2512.67 110.01 o 1 8 0 492.40 505.59 12.92 o 2 8 0 2014.10 2050.10 44.20 o 3 8 0 3481.26 3434.34 67.24 o 4 8 0 948.31 886.13 19.13 o 5 8 0 758.75 811.29 16.30 o 6 8 0 1229.27 1163.34 20.57 o 7 8 0 729.86 731.49 15.69 o 8 8 0 535.58 504.25 16.71 o 9 8 0 22.55 15.26 6.31 o 10 8 0 450.00 426.10 15.66 o 11 8 0 138.91 133.91 9.82 o 12 8 0 93.00 95.18 9.09 o 13 8 0 580.91 580.30 19.79 o 1 9 0 2130.98 2087.99 55.04 o 2 9 0 2.08 3.41 5.87 o 3 9 0 90.97 128.08 8.46 o 4 9 0 1594.08 1552.10 26.56 o 5 9 0 48.49 46.59 5.96 o 6 9 0 1446.35 1413.91 26.86 o 7 9 0 134.46 134.78 9.07 o 8 9 0 292.41 303.67 12.50 o 9 9 0 182.55 190.84 11.49 o 10 9 0 200.43 188.38 11.46 o 11 9 0 599.73 616.73 23.30 o 0 10 0 756.07 733.71 38.52 o 1 10 0 73.39 101.66 11.68 o 2 10 0 39.19 58.53 9.60 o 3 10 0 585.54 630.18 26.17 o 4 10 0 38.37 62.87 7.69 o 5 10 0 125.16 137.03 8.86 o 6 10 0 262.30 270.72 10.14 o 7 10 0 391.06 395.49 13.38 o 8 10 0 302.51 269.37 19.60 o 9 10 0 29.51 33.77 9.17 o 1 11 0 179.03 201.62 25.17 o 2 11 0 356.21 355.74 19.41 o 3 11 0 209.32 206.79 15.92 o 4 11 0 336.51 322.88 17.76 o 5 11 0 88.23 109.48 11.28 o 6 11 0 1.54 24.99 14.30 o -18 1 1 0.75 -0.79 3.26 o -17 1 1 276.26 268.46 8.64 o -16 1 1 488.84 504.98 13.32 o -15 1 1 74.98 88.09 5.14 o -14 1 1 710.98 735.00 22.32 o -13 1 1 3.18 1.30 5.35 o -12 1 1 77.50 57.96 6.39 o -11 1 1 2512.64 2361.68 50.90 o -10 1 1 1474.45 1491.51 34.02 o -9 1 1 1394.58 1308.71 29.86 o -8 1 1 862.11 837.45 20.44 o -7 1 1 9.98 5.26 4.14 o -6 1 1 7.15 8.15 1.22 o -5 1 1 3873.88 3797.85 55.10 o -4 1 1 2429.57 2409.52 32.92 o -3 1 1 6970.43 6976.37 61.79 o -2 1 1 2035.27 2203.26 18.49 o -1 1 1 4251.92 4456.50 40.55 o 0 1 1 10262.48 10726.21 86.93 o 1 1 1 5136.80 5430.08 41.92 o 2 1 1 7235.34 7618.14 54.15 o 3 1 1 972.71 1101.73 11.93 o 4 1 1 523.32 593.07 11.29 o 5 1 1 11619.78 12049.27 204.15 o 6 1 1 1242.36 1312.62 28.43 o 7 1 1 4427.97 4448.27 87.71 o 8 1 1 139.25 138.26 7.73 o 9 1 1 0.35 2.69 3.97 o 10 1 1 98.62 91.16 7.30 o 11 1 1 616.96 575.67 22.15 o 12 1 1 847.71 909.05 62.03 o 13 1 1 88.60 70.46 7.37 o 14 1 1 72.03 61.15 10.69 o 15 1 1 43.88 50.69 10.75 o 16 1 1 154.43 153.78 16.13 o 17 1 1 0.57 -0.95 10.34 o -17 2 1 132.90 153.85 9.78 o -16 2 1 49.55 53.34 5.18 o -15 2 1 72.41 80.78 5.04 o -14 2 1 1210.84 1206.90 21.60 o -13 2 1 49.48 57.96 6.96 o -12 2 1 1800.59 1815.99 29.35 o -11 2 1 139.32 138.52 5.13 o -10 2 1 3.64 8.32 2.69 o -9 2 1 6049.85 6001.32 87.06 o -8 2 1 117.41 124.80 2.91 o -7 2 1 5926.46 5933.77 66.09 o -6 2 1 4391.32 4778.58 53.38 o -5 2 1 1897.40 1957.76 22.73 o -4 2 1 13338.66 13768.88 164.42 o -3 2 1 435.89 379.81 4.30 o -2 2 1 21407.80 21713.47 185.75 o -1 2 1 8034.24 8489.43 77.21 o 0 2 1 8968.45 9483.77 82.45 o 1 2 1 18903.51 19749.05 162.90 o 2 2 1 5593.01 5564.60 42.93 o 3 2 1 9097.79 9490.50 86.20 o 4 2 1 4501.79 4314.18 48.89 o 5 2 1 341.27 326.58 5.21 o 6 2 1 3807.92 3690.99 45.35 o 7 2 1 1444.25 1420.17 20.03 o 8 2 1 1357.08 1366.08 25.19 o 9 2 1 2743.31 2672.98 46.98 o 10 2 1 32.86 38.12 3.54 o 11 2 1 879.77 829.81 16.91 o 12 2 1 382.59 433.10 10.40 o 13 2 1 330.84 308.81 8.66 o 14 2 1 476.79 504.33 12.33 o 15 2 1 162.15 184.09 7.32 o 16 2 1 672.36 659.69 16.01 o 17 2 1 39.50 48.49 7.10 o -17 3 1 190.48 208.69 17.77 o -16 3 1 163.22 170.52 6.48 o -15 3 1 254.07 242.71 10.78 o -14 3 1 38.26 47.14 3.58 o -13 3 1 2152.48 2188.93 31.98 o -12 3 1 47.49 47.94 3.30 o -11 3 1 2127.75 2184.12 28.51 o -10 3 1 127.91 120.13 4.12 o -9 3 1 30.17 29.67 2.32 o -8 3 1 14390.00 14666.06 172.03 o -7 3 1 9.20 17.38 2.16 o -6 3 1 5472.04 5392.43 66.34 o -5 3 1 7398.38 7480.36 84.63 o -4 3 1 44.17 71.60 2.10 o -3 3 1 13648.23 13758.74 129.02 o -2 3 1 3166.65 2809.38 35.09 o -1 3 1 9283.76 9310.97 94.70 o 0 3 1 3769.29 3630.21 32.73 o 1 3 1 286.04 309.41 9.37 o 2 3 1 24638.37 24974.74 255.96 o 3 3 1 1738.41 1611.84 15.67 o 4 3 1 490.32 435.06 5.83 o 5 3 1 19901.15 20097.86 223.73 o 6 3 1 309.26 321.10 5.60 o 7 3 1 2933.21 2913.06 36.74 o 8 3 1 5965.38 6023.57 80.64 o 9 3 1 521.30 538.19 11.36 o 10 3 1 8710.74 8601.04 114.03 o 11 3 1 211.31 225.98 5.73 o 12 3 1 1077.82 1052.98 16.54 o 13 3 1 1322.88 1338.72 23.37 o 14 3 1 248.54 247.49 7.44 o 15 3 1 1863.01 1817.61 35.55 o 16 3 1 1.20 5.43 3.38 o 17 3 1 237.54 240.43 8.02 o -17 4 1 234.61 200.75 21.21 o -16 4 1 501.39 476.34 14.73 o -15 4 1 922.10 945.00 22.46 o -14 4 1 518.32 504.51 12.05 o -13 4 1 0.98 5.35 3.40 o -12 4 1 1324.04 1304.81 23.36 o -11 4 1 1611.94 1591.57 24.80 o -10 4 1 1847.17 1900.86 38.65 o -9 4 1 5093.48 5080.67 68.50 o -8 4 1 455.86 454.84 8.66 o -7 4 1 1181.29 1193.36 17.39 o -6 4 1 6266.72 6159.64 70.89 o -5 4 1 4843.44 4973.44 53.86 o -4 4 1 11611.23 11239.06 129.85 o -3 4 1 93.30 107.21 6.17 o -2 4 1 7467.76 7574.06 105.37 o -1 4 1 12862.88 12665.08 135.32 o 0 4 1 1571.03 1582.84 19.36 o 1 4 1 25506.75 25261.18 275.52 o 2 4 1 633.91 702.00 9.71 o 3 4 1 11192.55 11441.60 108.07 o 4 4 1 8888.51 9165.05 86.94 o 5 4 1 23.88 31.01 2.00 o 6 4 1 13384.21 13477.17 162.77 o 7 4 1 842.67 859.27 13.29 o 8 4 1 3340.00 3319.77 46.63 o 9 4 1 1847.62 1864.32 27.66 o 10 4 1 37.38 41.95 3.51 o 11 4 1 2072.17 2159.65 31.78 o 12 4 1 1356.38 1395.12 22.10 o 13 4 1 1162.85 1157.07 21.53 o 14 4 1 209.55 215.06 7.89 o 15 4 1 152.80 152.98 8.44 o 16 4 1 225.73 237.61 10.47 o -16 5 1 408.04 378.89 14.16 o -15 5 1 163.82 162.44 9.52 o -14 5 1 625.16 621.84 17.79 o -13 5 1 357.20 330.32 12.24 o -12 5 1 402.33 398.61 15.14 o -11 5 1 2156.65 2140.80 48.64 o -10 5 1 1797.58 1771.47 35.20 o -9 5 1 492.87 474.26 14.46 o -8 5 1 4029.42 3971.86 85.15 o -7 5 1 654.55 669.49 11.94 o -6 5 1 1682.29 1707.61 28.82 o -5 5 1 11620.91 11600.63 116.04 o -4 5 1 1153.43 1240.87 21.48 o -3 5 1 3618.28 3556.30 65.24 o -2 5 1 6968.27 7021.84 82.23 o -1 5 1 6115.43 6136.38 72.34 o 0 5 1 5538.91 5445.34 69.91 o 1 5 1 1621.70 1667.56 22.28 o 2 5 1 9316.99 9431.55 130.02 o 3 5 1 1515.19 1542.03 18.37 o 4 5 1 811.05 833.21 9.83 o 5 5 1 6664.83 6627.85 66.97 o 6 5 1 33.94 43.90 2.80 o 7 5 1 3679.08 3696.99 47.80 o 8 5 1 5020.90 5063.80 94.92 o 9 5 1 922.06 909.46 18.15 o 10 5 1 528.41 522.30 14.33 o 11 5 1 1114.31 1105.89 21.43 o 12 5 1 1005.99 1028.31 23.74 o 13 5 1 625.75 624.18 17.23 o 14 5 1 244.89 240.77 10.83 o 15 5 1 267.65 262.85 11.60 o 16 5 1 196.52 182.15 10.66 o -15 6 1 51.74 49.96 7.37 o -14 6 1 194.06 194.21 10.95 o -13 6 1 61.42 79.16 7.50 o -12 6 1 1709.46 1649.00 35.56 o -11 6 1 19.12 22.36 5.72 o -10 6 1 29.00 30.37 8.24 o -9 6 1 1370.79 1329.62 29.27 o -8 6 1 958.37 927.23 19.47 o -7 6 1 3604.86 3586.15 46.64 o -6 6 1 955.92 923.99 16.71 o -5 6 1 1042.74 1046.93 14.30 o -4 6 1 1471.76 1550.43 20.87 o -3 6 1 2756.00 2808.59 38.54 o -2 6 1 7489.36 7503.60 125.91 o -1 6 1 3264.46 3283.58 50.24 o 0 6 1 1049.55 1080.08 19.18 o 1 6 1 1078.58 1048.16 19.01 o 2 6 1 1874.32 1840.56 24.24 o 3 6 1 1778.69 1804.60 31.06 o 4 6 1 4147.62 4240.56 56.36 o 5 6 1 389.16 388.77 6.75 o 6 6 1 771.45 797.18 13.71 o 7 6 1 587.91 580.92 10.29 o 8 6 1 70.10 72.06 5.88 o 9 6 1 3345.24 3239.75 60.44 o 10 6 1 328.83 339.94 12.55 o 11 6 1 228.66 242.80 11.06 o 12 6 1 162.95 169.01 9.89 o 13 6 1 1.21 -2.54 5.26 o 14 6 1 735.54 763.38 23.64 o 15 6 1 5.42 8.75 6.48 o -14 7 1 3.86 12.16 6.42 o -13 7 1 178.66 181.82 11.21 o -12 7 1 92.74 92.78 8.43 o -11 7 1 94.86 92.13 9.42 o -10 7 1 141.65 143.12 9.33 o -9 7 1 1.60 7.48 5.69 o -8 7 1 644.99 615.33 15.80 o -7 7 1 158.14 163.72 8.58 o -6 7 1 93.98 93.62 4.79 o -5 7 1 1435.52 1404.06 23.52 o -4 7 1 158.72 152.69 8.12 o -3 7 1 2.92 3.50 4.13 o -2 7 1 2161.81 2116.60 33.95 o -1 7 1 1338.54 1320.99 26.69 o 0 7 1 328.05 328.91 10.12 o 1 7 1 19.27 18.17 3.92 o 2 7 1 996.99 1009.94 16.81 o 3 7 1 788.84 760.48 13.95 o 4 7 1 195.32 176.07 7.46 o 5 7 1 1385.26 1394.95 29.96 o 6 7 1 171.95 186.55 9.35 o 7 7 1 30.64 22.20 4.69 o 8 7 1 335.26 306.69 20.85 o 9 7 1 548.83 501.71 15.96 o 10 7 1 244.22 259.74 11.96 o 11 7 1 7.42 4.20 5.66 o 12 7 1 130.74 115.95 9.25 o 13 7 1 8.32 8.96 6.61 o 14 7 1 38.56 53.54 11.41 o -13 8 1 42.31 57.27 8.20 o -12 8 1 31.83 26.26 7.71 o -11 8 1 126.99 137.58 11.89 o -10 8 1 9.78 7.60 5.98 o -9 8 1 0.43 -4.58 5.37 o -8 8 1 171.47 149.10 13.12 o -7 8 1 178.10 179.39 9.88 o -6 8 1 149.16 153.31 7.02 o -5 8 1 101.43 106.36 6.26 o -4 8 1 93.66 92.20 7.12 o -3 8 1 105.93 104.49 8.28 o -2 8 1 253.70 250.65 10.49 o -1 8 1 56.56 59.50 6.33 o 0 8 1 371.71 377.47 12.62 o 1 8 1 797.49 804.92 17.06 o 2 8 1 39.20 36.38 4.73 o 3 8 1 9.94 17.75 4.36 o 4 8 1 103.77 118.96 6.48 o 5 8 1 356.27 351.33 12.39 o 6 8 1 625.36 591.81 18.42 o 7 8 1 4.61 -2.19 5.19 o 8 8 1 264.82 298.63 22.75 o 9 8 1 0.19 2.15 7.15 o 10 8 1 25.56 10.75 7.83 o 11 8 1 14.01 4.44 8.17 o 12 8 1 89.93 111.45 11.96 o 13 8 1 213.11 207.32 15.08 o -11 9 1 52.88 60.36 8.57 o -10 9 1 7.90 4.55 6.86 o -9 9 1 347.09 356.42 15.15 o -8 9 1 15.08 21.17 5.24 o -7 9 1 11.79 12.67 5.54 o -6 9 1 189.76 187.97 8.09 o -5 9 1 8.62 13.17 4.80 o -4 9 1 2.06 -3.36 5.90 o -3 9 1 1.33 12.18 9.34 o -2 9 1 7.63 15.44 6.32 o -1 9 1 3.09 16.77 9.13 o 0 9 1 157.49 206.27 15.54 o 1 9 1 23.09 22.18 5.93 o 2 9 1 20.62 36.98 5.48 o 3 9 1 260.41 252.17 10.05 o 4 9 1 10.54 10.98 5.05 o 5 9 1 88.82 112.39 6.58 o 6 9 1 1.66 3.57 3.86 o 7 9 1 140.34 153.11 9.92 o 8 9 1 25.47 19.67 6.64 o 9 9 1 5.30 4.60 5.87 o 10 9 1 146.09 148.92 10.17 o 11 9 1 3.24 18.03 8.31 o -9 10 1 21.89 38.51 9.60 o -8 10 1 62.13 72.23 8.40 o -7 10 1 5.25 2.39 6.61 o -6 10 1 176.28 192.02 9.25 o -5 10 1 133.25 140.39 8.33 o -4 10 1 416.01 426.16 15.33 o -3 10 1 185.80 175.84 18.11 o -2 10 1 152.29 168.88 13.26 o -1 10 1 52.32 48.91 13.47 o 0 10 1 37.26 33.28 9.15 o 1 10 1 956.08 967.83 32.05 o 2 10 1 20.16 38.37 9.33 o 3 10 1 303.80 352.34 18.34 o 4 10 1 24.59 24.19 8.55 o 5 10 1 22.05 21.76 6.82 o 6 10 1 278.32 256.31 21.63 o 7 10 1 48.57 58.17 8.49 o 8 10 1 256.15 242.43 13.91 o 9 10 1 1.74 12.82 12.88 o -6 11 1 251.38 268.21 16.36 o -5 11 1 118.26 123.26 9.42 o -4 11 1 60.64 55.63 7.97 o -3 11 1 295.22 314.19 16.57 o -2 11 1 337.70 365.77 21.98 o -1 11 1 446.15 504.71 23.08 o 0 11 1 94.86 109.98 12.43 o 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