#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/03/2220382.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220382_Fobs loop_ _publ_author_name 'Itazaki, Masumi' 'Kamitani, Masahiro' 'Nakazawa, Hiroshi' _publ_section_title ; Carbonyl(\h^5^-cyclopentadienyl)(pyridine)(triethylstannyl)iron(II) ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1578 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.783 _cell_angle_gamma 90.000 _cell_length_a 15.0385 _cell_length_b 7.8271 _cell_length_c 15.7174 _exptl_crystal_F_000 872.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file wm2203Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _saku-kami-070629' _shelx_refln_list_code 4 _shelx_F_calc_maximum 238.88 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 18.40 290.99 131.29 o 5 0 0 17244.92 16951.25 280.05 o 6 0 0 24523.42 24801.58 280.45 o 7 0 0 2605.78 2193.77 145.21 o 8 0 0 21305.42 21822.86 299.41 o 9 0 0 516.90 495.63 122.50 o 10 0 0 4239.94 4279.04 180.19 o 11 0 0 2142.35 2244.51 170.52 o 12 0 0 3056.43 2725.78 180.47 o 13 0 0 3604.02 3326.83 361.11 o 14 0 0 6558.10 6869.59 729.64 o 15 0 0 1339.84 1411.64 332.90 o 16 0 0 2908.80 2809.42 190.59 o 17 0 0 5.70 401.48 270.66 o 18 0 0 204.57 335.01 226.00 o 19 0 0 657.69 674.50 178.47 o 3 1 0 26.35 252.78 45.76 o 4 1 0 23965.27 24040.09 201.17 o 5 1 0 5515.00 5107.47 145.04 o 6 1 0 8087.48 8045.92 126.25 o 7 1 0 21030.65 20455.34 194.86 o 8 1 0 384.87 468.83 100.63 o 9 1 0 12928.89 12295.79 210.00 o 10 1 0 2355.88 2279.67 95.76 o 11 1 0 485.79 606.61 65.90 o 12 1 0 6089.71 6397.65 152.00 o 13 1 0 2185.55 2477.66 140.07 o 14 1 0 1561.58 1412.81 124.70 o 15 1 0 3819.27 3897.55 161.19 o 16 1 0 3.18 136.25 86.51 o 17 1 0 1510.03 1503.94 99.25 o 18 1 0 476.65 439.89 88.78 o 19 1 0 1.93 174.77 103.25 o 0 2 0 140.18 273.58 132.59 o 1 2 0 9731.71 9983.71 115.87 o 2 2 0 4045.50 4178.29 64.56 o 3 2 0 26908.12 27676.54 137.09 o 4 2 0 2160.57 1974.55 43.50 o 5 2 0 17918.33 16920.42 160.21 o 6 2 0 6742.88 6700.33 108.95 o 7 2 0 1732.61 1565.12 62.34 o 8 2 0 8444.27 8479.51 95.19 o 9 2 0 5066.54 4970.58 85.95 o 10 2 0 3982.48 3987.59 81.87 o 11 2 0 12311.85 12057.72 180.15 o 12 2 0 383.25 431.53 54.30 o 13 2 0 4085.40 4165.33 171.66 o 14 2 0 782.00 829.74 74.90 o 15 2 0 7.31 190.81 79.41 o 16 2 0 2447.51 2328.21 105.72 o 17 2 0 779.73 716.18 121.14 o 18 2 0 714.34 629.09 109.62 o 19 2 0 1020.99 778.20 112.83 o 1 3 0 1629.53 1463.99 71.24 o 2 3 0 21506.60 21751.18 222.21 o 3 3 0 4072.73 4051.67 71.51 o 4 3 0 28373.27 28731.53 166.49 o 5 3 0 287.30 371.96 53.63 o 6 3 0 9466.19 9475.79 123.04 o 7 3 0 1949.38 1982.55 107.60 o 8 3 0 2037.06 2025.79 84.35 o 9 3 0 2768.73 2716.22 97.82 o 10 3 0 12579.08 12390.14 163.04 o 11 3 0 1772.58 1581.86 89.12 o 12 3 0 5525.61 5619.50 238.71 o 13 3 0 0.38 220.88 76.05 o 14 3 0 700.27 573.51 76.10 o 15 3 0 1401.15 1377.77 141.39 o 16 3 0 407.82 335.38 86.91 o 17 3 0 1673.64 1674.28 145.56 o 18 3 0 1312.81 910.19 127.23 o 0 4 0 3161.52 2765.07 144.68 o 1 4 0 4317.67 4148.58 140.99 o 2 4 0 4687.29 4462.53 118.08 o 3 4 0 18857.80 19008.06 167.43 o 4 4 0 40.59 157.44 70.95 o 5 4 0 13346.92 13196.23 150.47 o 6 4 0 1594.01 1672.55 130.33 o 7 4 0 1561.06 1773.02 169.64 o 8 4 0 2880.97 2720.75 90.51 o 9 4 0 4271.29 3908.86 103.42 o 10 4 0 1898.45 1757.01 78.97 o 11 4 0 5476.31 5285.42 128.66 o 12 4 0 223.47 248.79 57.40 o 13 4 0 1670.57 1478.66 84.69 o 14 4 0 613.40 504.79 120.50 o 15 4 0 4.61 -27.88 88.25 o 16 4 0 1395.73 1197.00 169.54 o 17 4 0 606.53 491.25 126.80 o 1 5 0 16596.42 17157.85 216.76 o 3 5 0 1524.20 1657.13 90.06 o 4 5 0 2180.33 2145.47 88.56 o 5 5 0 3875.38 3875.53 70.57 o 6 5 0 3564.77 3388.35 81.20 o 7 5 0 7579.35 7542.70 127.58 o 8 5 0 580.23 649.30 95.82 o 9 5 0 2639.86 2830.05 154.51 o 10 5 0 1333.72 1636.39 184.19 o 11 5 0 121.45 243.16 123.16 o 12 5 0 2183.24 1890.23 455.43 o 13 5 0 446.80 280.51 119.93 o 14 5 0 747.02 520.77 130.71 o 15 5 0 1351.03 1450.69 582.65 o 16 5 0 32.43 423.74 179.79 o 0 6 0 14772.87 15216.46 306.08 o 1 6 0 1.67 114.34 113.65 o 2 6 0 4326.85 4356.44 138.27 o 3 6 0 673.22 874.11 88.52 o 4 6 0 457.73 540.86 63.93 o 5 6 0 1211.79 1085.66 88.19 o 6 6 0 5530.57 5386.01 80.54 o 7 6 0 561.81 532.50 92.60 o 8 6 0 7035.30 7319.52 196.71 o 9 6 0 126.41 259.79 276.84 o 10 6 0 1110.59 1107.13 158.55 o 11 6 0 103.87 374.31 163.74 o 12 6 0 276.30 301.31 161.58 o 13 6 0 638.70 1056.92 524.82 o 14 6 0 1724.46 1489.85 311.11 o 15 6 0 628.60 574.07 134.59 o 1 7 0 3570.64 3422.97 203.20 o 2 7 0 401.72 253.07 75.68 o 3 7 0 174.94 301.06 95.80 o 4 7 0 2020.51 2075.74 86.51 o 5 7 0 253.96 353.97 49.81 o 6 7 0 404.48 379.60 45.66 o 7 7 0 2235.26 2241.22 151.79 o 8 7 0 8.60 417.74 94.41 o 9 7 0 1901.29 2103.64 298.90 o 10 7 0 67.13 88.02 163.43 o 11 7 0 57.83 169.33 130.52 o 12 7 0 543.63 633.50 169.48 o 13 7 0 370.61 548.32 154.47 o 14 7 0 562.49 491.08 129.02 o 0 8 0 323.96 282.33 169.26 o 1 8 0 326.50 509.00 118.07 o 2 8 0 246.02 320.34 116.29 o 3 8 0 1928.75 1706.90 147.80 o 4 8 0 106.31 203.34 57.73 o 5 8 0 1419.82 1318.25 82.10 o 6 8 0 65.32 208.39 89.93 o 7 8 0 41.70 75.88 69.37 o 8 8 0 464.57 608.11 168.63 o 9 8 0 198.33 501.98 169.31 o 10 8 0 230.73 262.63 185.57 o 11 8 0 804.13 1357.92 210.27 o 1 9 0 5.18 141.12 121.52 o 2 9 0 1131.70 1239.25 102.91 o 3 9 0 81.82 146.60 82.44 o 4 9 0 1239.36 1537.48 174.57 o 5 9 0 0.43 260.97 139.77 o 6 9 0 384.32 394.18 136.96 o 7 9 0 72.58 316.85 180.21 o 8 9 0 22.70 57.13 141.89 o 9 9 0 166.52 382.52 163.10 o 0 10 0 177.74 134.95 107.08 o 1 10 0 102.93 207.68 86.30 o 2 10 0 97.35 306.20 138.71 o 3 10 0 428.62 474.20 130.21 o -19 1 1 2.78 124.81 100.35 o -18 1 1 48.81 73.10 81.86 o -17 1 1 159.49 221.22 59.90 o -16 1 1 101.03 203.74 119.01 o -15 1 1 238.99 463.06 124.55 o -14 1 1 1221.42 1379.14 121.62 o -13 1 1 32.47 291.36 184.24 o -12 1 1 2940.57 2659.63 181.63 o -11 1 1 619.55 602.27 88.00 o -10 1 1 2.04 246.10 121.40 o -9 1 1 1117.92 945.82 84.95 o -8 1 1 3068.11 2853.90 116.86 o -7 1 1 10.43 211.89 84.88 o -6 1 1 4139.91 3692.69 124.30 o -5 1 1 5566.32 5470.88 112.88 o -4 1 1 231.97 357.76 71.25 o -3 1 1 43030.80 46329.57 316.96 o 2 1 1 250.56 375.79 29.45 o 3 1 1 3901.60 4045.59 46.24 o 4 1 1 135.03 420.01 59.45 o 5 1 1 1075.06 973.31 48.65 o 6 1 1 7299.74 7282.79 90.15 o 7 1 1 2877.98 2713.12 75.10 o 8 1 1 736.92 619.51 62.27 o 9 1 1 3201.19 3270.92 110.14 o 10 1 1 179.88 383.66 82.82 o 11 1 1 32.71 141.72 75.12 o 12 1 1 459.88 427.85 74.93 o 13 1 1 57.85 341.03 101.86 o 14 1 1 875.78 980.19 86.99 o 15 1 1 289.58 331.06 62.89 o 16 1 1 172.35 247.21 62.94 o 17 1 1 242.56 250.94 67.80 o 18 1 1 48.11 180.93 101.86 o 19 1 1 0.00 282.37 102.76 o -19 2 1 187.13 266.47 89.92 o -18 2 1 11.45 231.75 107.90 o -17 2 1 2.14 110.05 92.08 o -16 2 1 82.96 65.44 72.52 o -15 2 1 183.58 290.42 99.14 o -14 2 1 143.55 236.03 84.84 o -13 2 1 1447.09 1395.11 109.90 o -12 2 1 30.05 66.76 72.20 o -11 2 1 1708.79 1476.61 75.00 o -10 2 1 1353.73 1291.14 66.65 o -9 2 1 1017.67 1030.02 93.93 o -8 2 1 1029.68 1025.11 59.09 o -7 2 1 5170.75 5184.27 60.81 o -6 2 1 280.57 111.68 54.00 o -5 2 1 5655.37 4875.48 141.56 o -4 2 1 3857.50 3780.27 84.11 o -3 2 1 261.01 308.80 71.01 o -2 2 1 4617.22 4872.72 88.72 o -1 2 1 140.05 244.76 80.81 o 0 2 1 2909.48 2991.18 113.89 o 1 2 1 3133.40 2997.95 107.40 o 2 2 1 512.04 635.73 66.75 o 3 2 1 4523.64 4344.19 60.33 o 4 2 1 2007.43 1926.43 49.56 o 5 2 1 2251.16 1967.91 86.82 o 6 2 1 117.25 266.27 60.66 o 7 2 1 13604.36 13673.00 113.04 o 8 2 1 1474.98 1413.44 80.51 o 9 2 1 864.96 878.73 55.67 o 10 2 1 874.66 823.73 51.78 o 11 2 1 115.73 282.59 64.09 o 12 2 1 13.43 192.10 54.82 o 13 2 1 941.70 818.25 89.13 o 14 2 1 220.18 265.41 93.80 o 15 2 1 406.44 368.44 88.80 o 16 2 1 388.16 310.83 51.26 o 17 2 1 9.02 258.95 98.30 o 18 2 1 26.13 70.54 90.66 o -18 3 1 14.52 -17.02 199.13 o -17 3 1 69.55 174.01 136.48 o -16 3 1 68.06 310.14 107.33 o -15 3 1 1.37 335.36 108.86 o -14 3 1 95.83 387.76 108.20 o -13 3 1 1.63 162.03 173.41 o -12 3 1 122.37 230.53 82.06 o -11 3 1 79.75 174.32 77.97 o -10 3 1 160.90 237.86 65.15 o -9 3 1 573.63 464.04 78.70 o -8 3 1 666.11 685.12 49.09 o -7 3 1 869.61 831.28 50.57 o -6 3 1 706.50 612.11 52.73 o -5 3 1 1351.05 1241.30 65.15 o -4 3 1 0.84 42.82 67.80 o -3 3 1 1080.51 925.65 56.02 o -2 3 1 236.29 187.50 84.09 o -1 3 1 1688.31 1457.78 76.33 o 0 3 1 985.55 951.94 86.87 o 1 3 1 234.62 259.94 72.61 o 2 3 1 893.61 695.10 52.24 o 3 3 1 216.75 227.07 80.98 o 4 3 1 668.35 539.65 47.92 o 5 3 1 866.29 709.62 41.57 o 6 3 1 834.00 816.11 72.52 o 7 3 1 7.56 207.74 72.50 o 8 3 1 846.52 771.12 53.56 o 9 3 1 88.25 160.94 64.24 o 10 3 1 52.38 285.04 77.55 o 11 3 1 290.95 285.99 68.31 o 12 3 1 9.42 70.62 70.42 o 13 3 1 346.84 294.34 59.60 o 14 3 1 12.43 147.30 61.42 o 15 3 1 103.15 216.63 69.04 o 16 3 1 35.49 137.07 123.88 o 17 3 1 26.40 108.10 96.10 o 18 3 1 8.24 232.30 134.54 o -17 4 1 2.88 181.74 173.50 o -16 4 1 442.05 441.21 207.54 o -15 4 1 55.86 116.07 60.69 o -14 4 1 30.85 331.91 124.00 o -13 4 1 1.89 162.00 48.22 o -12 4 1 193.82 362.53 82.57 o -11 4 1 325.19 350.87 83.16 o -10 4 1 3918.94 3799.79 186.50 o -9 4 1 13.62 240.55 71.37 o -8 4 1 3524.80 3357.07 122.98 o -7 4 1 203.19 190.88 69.10 o -6 4 1 893.85 932.80 95.61 o -5 4 1 114.83 185.90 61.12 o -4 4 1 14798.78 14675.08 194.34 o -3 4 1 14.27 133.53 96.09 o -2 4 1 7075.94 6973.58 128.41 o -1 4 1 797.19 641.38 63.90 o 0 4 1 4.93 138.30 95.25 o 1 4 1 525.90 587.27 63.90 o 2 4 1 3589.95 3390.47 118.02 o 3 4 1 239.27 206.78 41.23 o 4 4 1 7701.18 7714.83 106.51 o 5 4 1 2965.82 2593.40 87.92 o 6 4 1 890.29 1030.72 74.91 o 7 4 1 346.38 354.55 60.37 o 8 4 1 745.68 958.39 88.04 o 9 4 1 371.31 232.71 53.23 o 10 4 1 493.70 602.43 91.88 o 11 4 1 257.87 227.96 67.07 o 12 4 1 434.91 540.13 107.20 o 13 4 1 102.73 462.53 146.24 o 14 4 1 63.16 179.68 65.55 o 15 4 1 12.34 110.42 93.57 o 16 4 1 166.69 185.32 104.09 o 17 4 1 167.46 210.17 104.07 o -16 5 1 0.07 446.13 185.70 o -15 5 1 137.16 546.03 196.38 o -14 5 1 7.33 221.46 166.46 o -13 5 1 289.70 377.83 195.06 o -12 5 1 14.40 77.22 170.78 o -11 5 1 2034.40 2008.74 213.35 o -10 5 1 44.51 -6.96 149.30 o -9 5 1 2373.85 2385.03 194.51 o -8 5 1 91.05 164.41 171.30 o -7 5 1 48.43 223.29 62.20 o -6 5 1 3.05 153.01 57.94 o -5 5 1 2849.43 2919.56 107.97 o -4 5 1 178.57 257.37 46.76 o -3 5 1 8228.25 8033.37 137.71 o -2 5 1 711.36 717.09 99.42 o -1 5 1 753.38 571.93 74.30 o 0 5 1 2.01 107.32 91.52 o 1 5 1 1094.04 1223.87 99.45 o 2 5 1 613.16 646.91 65.54 o 3 5 1 4709.68 4682.68 100.25 o 4 5 1 981.69 1097.96 66.06 o 5 5 1 3679.12 3824.27 139.20 o 6 5 1 1072.54 1168.03 55.50 o 7 5 1 53.46 177.60 73.93 o 8 5 1 55.67 168.53 107.93 o 9 5 1 1073.70 1232.71 207.30 o 10 5 1 855.40 695.61 116.89 o 11 5 1 833.01 1048.31 114.27 o 12 5 1 368.79 340.87 75.64 o 13 5 1 235.09 267.46 130.07 o 14 5 1 16.06 247.48 219.36 o 15 5 1 78.60 337.16 163.99 o 16 5 1 185.14 302.54 166.02 o -15 6 1 172.02 374.05 156.62 o -14 6 1 8.53 167.34 234.40 o -13 6 1 298.19 236.45 135.49 o -12 6 1 434.22 652.45 138.36 o -11 6 1 194.11 284.80 138.59 o -10 6 1 207.78 257.84 171.43 o -9 6 1 134.96 438.48 180.50 o -8 6 1 59.09 478.24 201.48 o -7 6 1 1382.58 1283.37 112.69 o -6 6 1 220.70 172.16 42.47 o -5 6 1 322.58 262.61 54.49 o -4 6 1 257.18 193.37 40.28 o -3 6 1 0.05 211.31 66.97 o -2 6 1 1921.35 1992.75 112.09 o -1 6 1 324.65 414.90 81.61 o 0 6 1 174.96 327.76 133.39 o 1 6 1 1669.44 1552.29 101.72 o 2 6 1 126.30 191.25 79.05 o 3 6 1 335.44 329.20 67.57 o 4 6 1 1208.80 1030.81 77.89 o 5 6 1 148.41 207.83 72.48 o 6 6 1 904.92 812.37 75.29 o 7 6 1 158.62 97.63 96.16 o 8 6 1 0.35 105.26 108.64 o 9 6 1 676.07 666.06 117.90 o 10 6 1 513.12 425.03 182.37 o 11 6 1 261.41 237.84 113.25 o 12 6 1 520.15 404.36 135.10 o 13 6 1 32.82 492.76 158.19 o 14 6 1 169.76 516.23 160.62 o 15 6 1 196.12 422.03 134.47 o -14 7 1 752.16 1101.83 219.87 o -13 7 1 16.88 358.49 283.76 o -12 7 1 625.90 236.80 149.59 o -11 7 1 19.79 146.02 159.09 o -10 7 1 2.90 121.86 164.14 o -9 7 1 28.53 179.26 125.21 o -8 7 1 2135.06 2476.58 195.66 o -7 7 1 16.41 188.78 59.59 o -6 7 1 2374.60 2339.79 71.13 o -5 7 1 250.97 277.99 46.60 o -4 7 1 169.13 263.75 49.64 o -3 7 1 63.40 143.71 109.34 o -2 7 1 540.59 549.14 137.03 o -1 7 1 485.10 376.43 130.86 o 0 7 1 1627.50 1852.64 159.83 o 1 7 1 33.20 551.31 182.53 o 2 7 1 1558.17 1185.71 104.58 o 3 7 1 5.30 97.01 93.64 o 4 7 1 22.78 267.01 95.71 o 5 7 1 0.33 71.60 87.59 o 6 7 1 2228.18 2172.64 79.03 o 7 7 1 646.60 663.30 75.19 o 8 7 1 2009.59 1879.96 120.00 o 9 7 1 362.28 729.63 224.52 o 10 7 1 344.45 454.11 304.93 o 11 7 1 21.29 343.30 166.51 o 12 7 1 212.28 275.83 144.95 o 13 7 1 392.08 293.06 111.93 o -12 8 1 26.81 295.45 166.38 o -11 8 1 103.51 281.61 141.91 o -10 8 1 39.83 250.02 272.97 o -9 8 1 338.38 435.51 210.89 o -8 8 1 41.39 -61.06 175.57 o -7 8 1 1245.45 941.77 157.29 o -6 8 1 2.00 200.32 96.60 o -5 8 1 828.00 726.42 80.35 o -4 8 1 1.44 279.45 77.18 o -3 8 1 27.91 197.12 94.80 o -2 8 1 107.49 215.53 113.39 o -1 8 1 1447.50 1416.68 171.43 o 0 8 1 107.87 313.70 173.22 o 1 8 1 1760.16 1830.35 146.31 o 2 8 1 6.12 126.13 114.54 o 3 8 1 771.37 651.33 139.72 o 4 8 1 0.63 145.67 84.99 o 5 8 1 224.44 285.32 82.21 o 6 8 1 97.73 200.29 118.06 o 7 8 1 1472.22 1338.83 115.48 o 8 8 1 394.40 558.36 147.54 o 9 8 1 459.41 519.57 171.36 o 10 8 1 0.72 311.64 132.85 o 11 8 1 1.73 53.72 147.88 o -9 9 1 236.81 584.15 167.38 o -8 9 1 277.23 198.98 164.27 o -7 9 1 69.51 55.83 113.67 o -6 9 1 235.02 273.43 163.74 o -5 9 1 248.46 222.37 134.05 o -4 9 1 82.17 109.11 180.75 o -3 9 1 634.49 740.87 88.29 o -2 9 1 76.17 230.03 83.90 o -1 9 1 380.12 482.55 100.92 o 0 9 1 346.19 272.10 104.55 o 1 9 1 0.00 240.13 122.62 o 2 9 1 307.54 481.65 183.71 o 3 9 1 394.07 378.87 139.31 o 4 9 1 96.15 306.86 120.69 o 5 9 1 427.19 608.09 141.14 o 6 9 1 100.14 406.24 167.06 o 7 9 1 150.43 305.45 138.98 o 8 9 1 320.27 379.25 139.98 o -3 10 1 48.64 135.78 149.06 o -2 10 1 465.13 539.00 161.80 o -1 10 1 17.98 125.36 131.53 o 0 10 1 60.99 81.94 84.21 o 1 10 1 66.64 240.70 81.53 o 2 10 1 157.02 221.51 90.22 o 3 10 1 58.28 151.45 101.59 o -19 0 2 451.96 333.29 158.16 o -18 0 2 83.20 368.06 134.22 o -17 0 2 840.53 1125.07 235.89 o -16 0 2 1769.56 1733.12 275.72 o -15 0 2 4.97 686.25 289.11 o -14 0 2 10040.85 10695.47 434.12 o -13 0 2 231.92 375.78 283.55 o -12 0 2 8942.78 9332.86 866.99 o -11 0 2 2453.28 2714.56 188.13 o -10 0 2 516.68 508.61 128.70 o -9 0 2 7948.21 8529.29 651.86 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