#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/05/2220560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220560_Fobs loop_ _publ_author_name 'Arul Jeevan, T. S.' 'Nagaraja, K. S.' _publ_section_title ; 3-[(3-Hydroxypropyl)amino]-1-phenylbut-2-en-1-one ; _journal_coeditor_code IS2371 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o206 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9131 _cell_length_b 8.0101 _cell_length_c 24.9626 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.8416 _[local]_cod_data_source_file is2371Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ORTHO in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 117.28 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 498.98 473.65 5.53 o 4 0 0 9.32 7.12 0.61 o 6 0 0 336.75 347.38 11.40 o 1 1 0 135.67 114.39 0.86 o 2 1 0 1837.11 1854.18 17.25 o 3 1 0 1.05 2.56 0.15 o 4 1 0 8.26 8.17 0.36 o 5 1 0 52.31 48.93 1.31 o 6 1 0 3.90 4.00 0.75 o 0 2 0 2924.56 2787.60 30.92 o 1 2 0 6.93 10.06 0.18 o 2 2 0 110.90 114.29 1.01 o 3 2 0 400.74 457.81 4.83 o 4 2 0 0.55 1.74 0.52 o 5 2 0 6.96 6.16 0.62 o 6 2 0 5.79 4.35 0.58 o 1 3 0 104.01 94.10 0.91 o 2 3 0 229.40 248.51 2.14 o 3 3 0 49.98 57.57 0.65 o 4 3 0 55.68 55.98 0.94 o 5 3 0 1.46 0.87 0.35 o 6 3 0 3.54 6.08 0.60 o 0 4 0 32.82 31.44 0.91 o 1 4 0 1.81 2.43 0.22 o 2 4 0 231.01 202.70 1.87 o 3 4 0 62.08 57.53 0.86 o 4 4 0 89.04 84.69 1.55 o 5 4 0 22.49 23.15 1.11 o 6 4 0 30.90 35.52 1.22 o 1 5 0 2.34 3.74 0.26 o 2 5 0 2.99 4.23 0.24 o 3 5 0 13.07 13.25 0.39 o 4 5 0 85.77 75.17 1.29 o 5 5 0 41.28 37.32 1.49 o 0 6 0 6.91 8.83 0.62 o 1 6 0 6.66 5.80 0.45 o 2 6 0 82.76 86.94 1.76 o 3 6 0 129.11 131.10 1.83 o 4 6 0 9.88 10.48 0.50 o 5 6 0 1.53 2.78 0.76 o 1 7 0 10.37 13.63 0.75 o 2 7 0 27.22 28.58 0.95 o 3 7 0 3.15 2.59 0.47 o 4 7 0 9.67 10.15 0.73 o 0 8 0 8.92 7.22 1.49 o 1 8 0 12.72 13.03 0.96 o 2 8 0 12.20 12.07 0.80 o 3 8 0 35.76 34.17 1.13 o 1 9 0 0.60 0.18 0.80 o 2 9 0 39.80 45.59 2.13 o 1 0 1 1223.13 1120.54 9.92 o 2 0 1 155.82 158.48 1.43 o 3 0 1 139.04 135.07 1.37 o 4 0 1 61.82 62.85 0.84 o 5 0 1 0.39 1.00 0.37 o 6 0 1 197.63 212.11 3.22 o 7 0 1 22.05 21.42 1.30 o 0 1 1 480.15 442.93 14.28 o 1 1 1 362.33 323.21 1.70 o 2 1 1 337.81 334.81 2.07 o 3 1 1 73.28 71.12 0.58 o 4 1 1 78.31 75.74 0.78 o 5 1 1 197.01 202.16 2.28 o 6 1 1 6.94 7.31 0.61 o 0 2 1 5.21 7.49 0.28 o 1 2 1 951.08 922.64 4.68 o 2 2 1 918.84 990.63 5.30 o 3 2 1 1178.91 1294.11 9.33 o 4 2 1 228.04 222.84 2.04 o 5 2 1 0.80 0.06 0.33 o 6 2 1 4.59 4.78 0.40 o 0 3 1 46.81 48.20 0.58 o 1 3 1 25.54 28.05 0.26 o 2 3 1 225.93 237.91 1.41 o 3 3 1 3.86 4.66 0.13 o 4 3 1 72.33 67.73 0.76 o 5 3 1 115.90 120.55 1.49 o 6 3 1 8.62 7.82 0.48 o 0 4 1 984.53 991.05 10.32 o 1 4 1 326.61 323.25 2.15 o 2 4 1 14.79 14.55 0.23 o 3 4 1 107.17 110.09 0.90 o 4 4 1 5.69 6.63 0.32 o 5 4 1 54.93 50.26 0.99 o 6 4 1 9.77 10.06 0.52 o 0 5 1 0.56 0.73 0.20 o 1 5 1 191.36 175.75 1.35 o 2 5 1 98.33 97.01 0.75 o 3 5 1 6.48 5.94 0.20 o 4 5 1 8.74 8.21 0.39 o 5 5 1 1.35 0.03 0.45 o 0 6 1 97.62 102.92 1.58 o 1 6 1 177.28 167.42 1.35 o 2 6 1 16.96 15.88 0.42 o 3 6 1 8.22 9.74 0.34 o 4 6 1 92.70 101.05 1.04 o 5 6 1 36.69 35.94 1.10 o 0 7 1 3.56 3.87 0.56 o 1 7 1 406.26 405.97 4.26 o 2 7 1 82.38 85.97 1.19 o 3 7 1 0.64 0.71 0.30 o 4 7 1 16.21 16.01 0.45 o 0 8 1 3.26 3.04 1.27 o 1 8 1 9.51 10.29 0.63 o 2 8 1 5.47 6.13 0.42 o 3 8 1 7.93 9.30 0.48 o 0 9 1 0.20 0.19 0.80 o 1 9 1 12.17 11.39 1.07 o 2 9 1 2.47 2.77 0.68 o 1 0 2 4965.04 4863.16 45.93 o 2 0 2 325.60 307.17 2.85 o 3 0 2 27.21 31.67 0.45 o 4 0 2 32.24 32.89 0.61 o 5 0 2 713.28 725.69 7.82 o 6 0 2 39.99 42.46 1.67 o 7 0 2 5.55 5.82 0.89 o 0 1 2 417.80 426.56 5.29 o 1 1 2 1014.32 988.63 5.31 o 2 1 2 687.70 719.84 4.59 o 3 1 2 200.47 200.86 1.46 o 4 1 2 25.43 25.94 0.40 o 5 1 2 191.57 184.21 2.35 o 6 1 2 77.37 75.50 1.30 o 0 2 2 7467.50 7538.26 55.41 o 1 2 2 629.08 617.93 3.23 o 2 2 2 24.46 26.71 0.22 o 3 2 2 309.38 338.05 2.61 o 4 2 2 100.77 110.07 1.24 o 5 2 2 24.97 23.85 0.66 o 6 2 2 37.12 34.79 0.82 o 0 3 2 12.38 16.24 0.47 o 1 3 2 113.96 122.04 0.80 o 2 3 2 444.59 479.00 2.92 o 3 3 2 44.83 47.75 0.45 o 4 3 2 50.43 54.28 0.73 o 5 3 2 7.24 6.29 0.33 o 6 3 2 7.59 9.11 0.49 o 0 4 2 0.91 3.41 0.23 o 1 4 2 1176.21 1146.89 6.99 o 2 4 2 53.43 57.12 0.48 o 3 4 2 65.14 72.92 0.60 o 4 4 2 23.02 21.52 0.46 o 5 4 2 13.51 10.48 0.47 o 6 4 2 8.21 6.93 0.48 o 0 5 2 57.53 56.42 1.31 o 1 5 2 63.01 66.23 0.65 o 2 5 2 6.25 6.07 0.19 o 3 5 2 41.84 42.73 0.48 o 4 5 2 40.28 34.84 0.55 o 5 5 2 19.51 17.44 0.76 o 0 6 2 62.85 66.49 1.17 o 1 6 2 207.99 212.97 1.83 o 2 6 2 289.71 276.00 2.62 o 3 6 2 38.75 42.84 0.59 o 4 6 2 60.94 61.59 0.75 o 5 6 2 3.03 2.70 0.51 o 0 7 2 63.51 66.61 1.54 o 1 7 2 56.05 57.80 0.95 o 2 7 2 46.38 46.78 0.84 o 3 7 2 6.39 6.70 0.40 o 4 7 2 44.44 47.39 0.71 o 0 8 2 1.81 1.16 0.85 o 1 8 2 10.51 9.77 0.61 o 2 8 2 25.76 24.26 0.67 o 3 8 2 12.58 16.97 0.58 o 0 9 2 16.88 17.34 1.45 o 1 9 2 2.73 2.26 0.65 o 2 9 2 0.90 1.50 0.65 o 1 0 3 4178.15 4113.92 29.49 o 2 0 3 74.76 68.41 0.59 o 3 0 3 999.95 1014.37 10.52 o 4 0 3 89.70 92.60 1.23 o 5 0 3 1.19 -0.11 0.54 o 6 0 3 0.17 -0.75 1.14 o 0 1 3 1011.56 892.97 6.03 o 1 1 3 6945.80 6976.47 40.44 o 2 1 3 363.91 371.90 2.47 o 3 1 3 406.26 419.28 3.04 o 4 1 3 199.96 192.56 1.53 o 5 1 3 282.59 289.89 2.59 o 6 1 3 5.78 6.22 0.49 o 0 2 3 4.94 5.38 0.15 o 1 2 3 392.64 383.66 1.96 o 2 2 3 243.48 257.62 1.78 o 3 2 3 139.38 145.05 1.37 o 4 2 3 68.42 74.69 0.80 o 5 2 3 27.51 28.78 0.66 o 6 2 3 5.73 5.91 0.43 o 0 3 3 1066.04 1092.82 8.81 o 1 3 3 182.11 180.43 1.16 o 2 3 3 1012.40 1023.13 6.28 o 3 3 3 18.53 18.50 0.32 o 4 3 3 108.91 111.72 1.09 o 5 3 3 2.79 2.33 0.26 o 6 3 3 10.80 11.23 0.51 o 0 4 3 762.53 813.12 8.70 o 1 4 3 281.32 283.38 1.85 o 2 4 3 21.78 22.77 0.27 o 3 4 3 17.65 13.49 0.23 o 4 4 3 70.34 67.76 0.88 o 5 4 3 37.02 34.95 0.73 o 6 4 3 7.84 8.20 0.68 o 0 5 3 150.42 153.61 1.85 o 1 5 3 313.69 308.97 2.05 o 2 5 3 35.99 36.11 0.41 o 3 5 3 6.25 5.15 0.21 o 4 5 3 2.17 2.46 0.24 o 5 5 3 12.96 11.73 0.59 o 0 6 3 2.28 1.65 0.34 o 1 6 3 157.78 154.04 1.36 o 2 6 3 232.93 231.98 1.80 o 3 6 3 34.23 32.84 0.59 o 4 6 3 115.58 117.13 1.18 o 5 6 3 11.45 12.54 0.68 o 0 7 3 111.61 112.47 2.16 o 1 7 3 30.63 34.07 0.69 o 2 7 3 42.73 40.45 0.78 o 3 7 3 21.87 20.93 0.74 o 4 7 3 22.80 28.41 0.55 o 0 8 3 0.31 2.10 0.91 o 1 8 3 9.10 8.00 0.60 o 2 8 3 20.47 22.81 0.64 o 3 8 3 1.95 2.71 0.38 o 0 9 3 15.26 19.29 1.48 o 1 9 3 3.87 3.41 0.70 o 2 9 3 10.58 13.22 0.92 o 0 0 4 486.79 521.11 5.86 o 1 0 4 839.02 783.47 8.47 o 2 0 4 666.81 685.70 5.93 o 3 0 4 352.97 350.01 3.50 o 4 0 4 0.63 0.16 0.19 o 5 0 4 19.36 19.20 0.87 o 6 0 4 68.09 66.87 2.47 o 0 1 4 1938.00 1949.52 12.22 o 1 1 4 4509.49 4500.80 22.41 o 2 1 4 520.30 529.01 3.61 o 3 1 4 171.37 186.16 1.42 o 4 1 4 119.18 111.07 1.01 o 5 1 4 328.65 325.72 3.68 o 6 1 4 4.39 5.41 0.45 o 0 2 4 215.40 210.29 1.51 o 1 2 4 915.65 899.69 4.58 o 2 2 4 850.48 912.28 5.61 o 3 2 4 98.02 95.79 1.07 o 4 2 4 26.96 26.23 0.39 o 5 2 4 9.71 9.28 0.39 o 6 2 4 24.91 25.33 0.82 o 0 3 4 55.36 59.42 0.64 o 1 3 4 657.03 675.58 4.00 o 2 3 4 346.32 368.33 2.11 o 3 3 4 76.60 80.01 0.73 o 4 3 4 43.66 43.99 0.61 o 5 3 4 22.61 20.98 0.58 o 6 3 4 4.46 3.64 0.60 o 0 4 4 465.09 481.90 4.55 o 1 4 4 216.55 225.49 1.45 o 2 4 4 41.59 39.75 0.37 o 3 4 4 38.38 37.05 0.39 o 4 4 4 10.98 10.81 0.29 o 5 4 4 28.11 25.05 0.70 o 6 4 4 26.91 29.60 1.08 o 0 5 4 0.16 -0.04 0.19 o 1 5 4 98.82 90.07 0.77 o 2 5 4 11.24 10.81 0.30 o 3 5 4 16.82 14.76 0.32 o 4 5 4 47.70 48.20 0.69 o 5 5 4 2.81 4.62 0.57 o 0 6 4 35.68 37.40 0.73 o 1 6 4 133.29 132.48 1.12 o 2 6 4 182.86 178.14 1.45 o 3 6 4 83.76 84.02 0.89 o 4 6 4 16.53 15.82 0.52 o 5 6 4 1.12 1.49 0.46 o 0 7 4 111.39 108.39 2.09 o 1 7 4 70.44 70.63 0.93 o 2 7 4 38.97 41.50 0.79 o 3 7 4 50.44 58.17 0.79 o 4 7 4 9.76 9.46 0.48 o 0 8 4 130.85 130.77 3.65 o 1 8 4 29.79 31.22 1.06 o 2 8 4 2.76 2.86 0.42 o 3 8 4 6.98 7.78 0.46 o 0 9 4 1.80 1.98 0.92 o 1 9 4 1.01 1.29 0.63 o 2 9 4 15.53 17.53 0.74 o 1 0 5 0.08 0.08 0.08 o 2 0 5 329.94 336.28 2.95 o 3 0 5 97.02 97.55 1.02 o 4 0 5 287.39 298.69 3.07 o 5 0 5 275.66 284.28 3.60 o 6 0 5 41.09 44.37 1.62 o 0 1 5 516.98 520.49 3.20 o 1 1 5 3176.37 3114.20 14.84 o 2 1 5 727.65 737.83 4.59 o 3 1 5 41.39 44.30 0.50 o 4 1 5 378.69 379.72 2.98 o 5 1 5 39.99 38.65 0.84 o 6 1 5 67.99 69.03 1.33 o 0 2 5 12.94 15.71 0.32 o 1 2 5 367.96 353.96 1.82 o 2 2 5 110.62 118.87 0.82 o 3 2 5 18.12 19.29 0.32 o 4 2 5 63.96 58.22 0.99 o 5 2 5 29.68 28.57 0.60 o 6 2 5 1.74 1.29 0.37 o 0 3 5 1607.71 1613.94 12.93 o 1 3 5 682.85 690.96 4.13 o 2 3 5 325.94 342.98 2.10 o 3 3 5 212.74 219.37 1.66 o 4 3 5 154.39 155.25 1.91 o 5 3 5 24.90 25.18 0.92 o 6 3 5 27.39 25.30 0.98 o 0 4 5 9.85 11.14 0.30 o 1 4 5 30.80 27.23 0.32 o 2 4 5 190.02 187.44 1.22 o 3 4 5 56.95 58.35 0.80 o 4 4 5 38.22 45.91 0.54 o 5 4 5 19.34 16.64 0.81 o 6 4 5 22.44 24.51 1.01 o 0 5 5 67.22 71.66 0.95 o 1 5 5 104.62 100.45 0.81 o 2 5 5 151.17 146.02 1.03 o 3 5 5 199.52 200.81 1.67 o 4 5 5 184.15 182.53 1.80 o 5 5 5 1.78 2.00 0.38 o 0 6 5 3.11 3.18 0.31 o 1 6 5 28.74 29.44 0.43 o 2 6 5 195.51 201.00 1.75 o 3 6 5 42.28 41.10 0.58 o 4 6 5 20.68 20.12 0.54 o 5 6 5 0.75 -0.18 0.41 o 0 7 5 44.83 46.63 1.29 o 1 7 5 90.94 86.47 1.16 o 2 7 5 25.54 25.36 0.64 o 3 7 5 6.72 8.14 0.36 o 4 7 5 2.92 3.98 0.29 o 0 8 5 16.34 18.99 1.39 o 1 8 5 29.59 28.54 1.04 o 2 8 5 16.98 17.14 0.74 o 3 8 5 8.55 9.38 0.48 o 0 9 5 6.39 6.67 1.12 o 1 9 5 0.28 -0.38 0.73 o 0 0 6 437.16 422.67 10.52 o 1 0 6 4.46 2.61 0.13 o 2 0 6 16.00 15.49 0.25 o 3 0 6 10.20 10.08 0.27 o 4 0 6 11.68 12.17 0.39 o 5 0 6 154.61 149.56 2.34 o 6 0 6 4.92 4.74 0.76 o 0 1 6 13755.63 14699.30 110.39 o 1 1 6 784.35 786.20 3.77 o 2 1 6 345.99 379.30 2.34 o 3 1 6 7.74 13.27 0.25 o 4 1 6 102.16 102.82 0.83 o 5 1 6 0.57 -0.01 0.40 o 6 1 6 74.52 75.38 1.84 o 0 2 6 124.65 143.52 1.12 o 1 2 6 602.84 575.84 3.08 o 2 2 6 588.57 583.06 3.43 o 3 2 6 148.54 149.44 1.20 o 4 2 6 86.27 83.12 1.26 o 5 2 6 57.61 53.17 1.27 o 6 2 6 1.25 1.04 0.30 o 0 3 6 1075.05 1078.32 7.89 o 1 3 6 242.39 232.23 1.39 o 2 3 6 35.99 34.25 0.38 o 3 3 6 18.10 22.38 0.30 o 4 3 6 19.15 19.12 0.59 o 5 3 6 91.30 85.53 1.76 o 6 3 6 15.59 15.24 0.80 o 0 4 6 58.15 59.15 0.72 o 1 4 6 227.16 222.73 1.49 o 2 4 6 170.59 174.44 1.19 o 3 4 6 17.78 17.32 0.30 o 4 4 6 1.58 1.53 0.18 o 5 4 6 4.19 2.40 0.53 o 6 4 6 18.77 20.82 0.98 o 0 5 6 16.45 21.55 0.44 o 1 5 6 110.66 107.44 0.90 o 2 5 6 94.37 88.50 0.68 o 3 5 6 427.33 428.24 3.04 o 4 5 6 106.85 100.57 1.14 o 5 5 6 27.96 25.97 0.77 o 0 6 6 10.47 9.55 0.37 o 1 6 6 0.78 0.28 0.20 o 2 6 6 8.12 9.25 0.31 o 3 6 6 10.01 9.86 0.34 o 4 6 6 44.76 41.82 0.75 o 5 6 6 21.34 23.11 1.04 o 0 7 6 3.30 1.74 0.62 o 1 7 6 58.17 52.98 0.87 o 2 7 6 14.47 14.96 0.55 o 3 7 6 17.92 16.27 0.48 o 4 7 6 10.02 10.09 0.40 o 0 8 6 3.59 2.60 0.90 o 1 8 6 7.07 9.44 0.70 o 2 8 6 3.82 3.18 0.43 o 3 8 6 5.75 6.67 0.44 o 0 9 6 0.27 -0.22 0.94 o 1 9 6 4.55 3.53 0.72 o 1 0 7 361.44 337.25 2.85 o 2 0 7 53.39 65.86 0.64 o 3 0 7 5.30 5.60 0.26 o 4 0 7 72.38 70.21 0.89 o 5 0 7 2.44 1.42 0.84 o 6 0 7 1.48 -0.21 1.19 o 0 1 7 8014.24 8050.46 51.89 o 1 1 7 2378.66 2345.95 12.08 o 2 1 7 125.91 130.45 1.11 o 3 1 7 514.02 549.42 3.98 o 4 1 7 81.63 82.05 0.77 o 5 1 7 10.48 9.93 0.39 o 6 1 7 9.39 12.07 0.54 o 0 2 7 186.69 186.94 1.42 o 1 2 7 184.41 191.90 1.11 o 2 2 7 2.01 1.66 0.10 o 3 2 7 189.83 188.75 1.52 o 4 2 7 241.25 243.07 2.38 o 5 2 7 70.59 71.62 2.19 o 6 2 7 17.66 18.59 0.64 o 0 3 7 2128.90 2214.40 16.02 o 1 3 7 644.20 641.96 3.48 o 2 3 7 35.42 37.06 0.34 o 3 3 7 3.77 4.52 0.16 o 4 3 7 1.59 1.34 0.27 o 5 3 7 22.65 20.76 0.88 o 6 3 7 18.62 18.85 0.91 o 0 4 7 227.60 246.33 2.17 o 1 4 7 293.38 294.61 1.80 o 2 4 7 20.91 19.67 0.27 o 3 4 7 1.28 1.05 0.15 o 4 4 7 4.96 5.95 0.24 o 5 4 7 18.00 15.81 0.83 o 6 4 7 4.22 5.49 0.67 o 0 5 7 0.42 0.28 0.18 o 1 5 7 26.10 26.36 0.37 o 2 5 7 344.31 347.10 2.20 o 3 5 7 172.50 175.43 1.40 o 4 5 7 4.45 4.02 0.28 o 5 5 7 1.61 1.00 0.43 o 0 6 7 14.32 14.61 0.50 o 1 6 7 27.42 27.48 0.43 o 2 6 7 15.61 14.90 0.37 o 3 6 7 24.09 20.91 0.47 o 4 6 7 0.69 0.24 0.28 o 5 6 7 0.27 0.36 0.41 o 0 7 7 4.68 3.17 0.50 o 1 7 7 34.36 34.21 0.74 o 2 7 7 11.29 10.74 0.39 o 3 7 7 4.13 3.88 0.30 o 4 7 7 40.27 40.14 0.89 o 0 8 7 4.25 5.52 1.26 o 1 8 7 117.60 119.98 1.70 o 2 8 7 22.04 20.39 0.70 o 3 8 7 0.85 1.30 0.34 o 0 9 7 6.63 8.73 1.19 o 1 9 7 1.23 1.01 0.55 o 0 0 8 1254.04 1220.13 19.35 o 1 0 8 0.33 1.00 0.17 o 2 0 8 533.31 568.56 5.01 o 3 0 8 94.52 104.93 1.21 o 4 0 8 1.32 1.06 0.20 o 5 0 8 121.07 114.27 1.83 o 6 0 8 21.25 19.67 1.93 o 0 1 8 43.82 50.07 0.54 o 1 1 8 1128.36 1064.52 5.51 o 2 1 8 395.82 400.99 2.48 o 3 1 8 458.72 495.32 3.27 o 4 1 8 12.52 11.45 0.31 o 5 1 8 74.18 76.02 0.96 o 6 1 8 46.88 49.98 1.24 o 0 2 8 258.19 256.53 1.99 o 1 2 8 135.38 136.95 0.81 o 2 2 8 156.24 158.10 1.07 o 3 2 8 60.68 63.98 0.57 o 4 2 8 209.06 206.80 1.96 o 5 2 8 69.29 65.75 1.64 o 6 2 8 7.44 8.98 0.91 o 0 3 8 2122.97 2298.04 16.63 o 1 3 8 183.79 176.14 1.05 o 2 3 8 26.87 20.61 0.25 o 3 3 8 105.82 106.19 0.82 o 4 3 8 21.09 23.44 0.45 o 5 3 8 13.59 12.94 0.75 o 6 3 8 27.99 25.78 1.04 o 0 4 8 0.76 0.73 0.16 o 1 4 8 223.02 216.70 1.41 o 2 4 8 9.72 10.33 0.21 o 3 4 8 50.91 50.10 0.53 o 4 4 8 78.54 76.62 0.88 o 5 4 8 14.20 15.06 0.81 o 6 4 8 12.17 15.31 0.90 o 0 5 8 38.52 46.52 0.61 o 1 5 8 202.43 198.93 1.46 o 2 5 8 197.33 191.90 1.32 o 3 5 8 41.67 40.85 0.53 o 4 5 8 33.81 34.88 0.60 o 5 5 8 6.04 5.52 0.65 o 0 6 8 43.54 41.30 0.69 o 1 6 8 101.06 99.03 0.90 o 2 6 8 78.06 73.69 0.75 o 3 6 8 39.78 37.35 0.60 o 4 6 8 16.47 16.07 0.51 o 5 6 8 11.15 9.33 0.42 o 0 7 8 22.23 20.66 0.68 o 1 7 8 17.72 18.70 0.48 o 2 7 8 0.14 -0.23 0.23 o 3 7 8 6.22 6.11 0.33 o 4 7 8 0.27 0.44 0.37 o 0 8 8 50.60 52.57 1.89 o 1 8 8 49.30 53.46 0.99 o 2 8 8 0.75 0.32 0.36 o 3 8 8 1.26 1.27 0.35 o 0 9 8 0.21 -0.45 0.76 o 1 9 8 2.23 1.80 0.52 o 1 0 9 760.52 727.12 5.89 o 2 0 9 22.63 19.15 0.31 o 3 0 9 228.47 251.75 2.66 o 4 0 9 102.14 103.12 1.36 o 5 0 9 13.55 14.03 0.60 o 6 0 9 0.19 0.38 0.60 o 0 1 9 3052.12 2933.17 21.28 o 1 1 9 98.17 103.13 0.73 o 2 1 9 240.11 247.65 1.63 o 3 1 9 304.09 305.33 2.02 o 4 1 9 47.56 48.25 0.56 o 5 1 9 45.88 44.49 0.69 o 6 1 9 36.35 36.88 1.01 o 0 2 9 193.02 208.36 1.81 o 1 2 9 426.80 398.73 2.16 o 2 2 9 358.31 360.56 2.18 o 3 2 9 2.04 3.07 0.14 o 4 2 9 216.52 197.56 1.90 o 5 2 9 155.74 142.39 2.48 o 6 2 9 8.71 8.83 0.69 o 0 3 9 46.59 62.04 0.67 o 1 3 9 75.46 67.24 0.48 o 2 3 9 68.08 70.26 0.54 o 3 3 9 47.18 48.68 0.48 o 4 3 9 26.44 24.29 0.49 o 5 3 9 56.76 52.24 1.34 o 6 3 9 0.29 0.77 0.52 o 0 4 9 104.31 109.02 1.01 o 1 4 9 168.01 176.94 1.15 o 2 4 9 128.43 130.44 0.96 o 3 4 9 125.73 120.99 0.98 o 4 4 9 18.16 17.35 0.39 o 5 4 9 21.12 21.80 0.97 o 6 4 9 10.78 12.80 0.83 o 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130.22 0.95 o 4 2 10 130.96 131.18 1.72 o 5 2 10 249.25 249.95 3.88 o 6 2 10 3.21 2.64 0.84 o 0 3 10 0.73 0.25 0.14 o 1 3 10 97.01 102.67 0.71 o 2 3 10 28.29 26.07 0.29 o 3 3 10 33.36 32.30 0.43 o 4 3 10 30.35 29.95 0.58 o 5 3 10 5.64 5.89 0.77 o 6 3 10 3.83 3.20 0.61 o 0 4 10 4.54 6.01 0.23 o 1 4 10 106.48 115.94 0.77 o 2 4 10 347.68 345.71 2.17 o 3 4 10 54.06 51.12 0.56 o 4 4 10 17.67 17.87 0.41 o 5 4 10 20.24 22.95 0.98 o 0 5 10 247.19 246.63 2.27 o 1 5 10 14.13 13.63 0.28 o 2 5 10 55.47 55.94 0.57 o 3 5 10 68.74 64.59 0.69 o 4 5 10 3.37 4.00 0.29 o 5 5 10 2.68 2.48 0.60 o 0 6 10 8.57 8.97 0.42 o 1 6 10 58.11 52.86 0.67 o 2 6 10 70.99 67.20 0.75 o 3 6 10 49.10 48.64 0.69 o 4 6 10 12.01 11.56 0.52 o 0 7 10 9.85 10.49 0.65 o 1 7 10 36.52 32.37 0.62 o 2 7 10 22.56 25.16 0.85 o 3 7 10 5.09 4.54 0.32 o 4 7 10 17.73 17.25 0.66 o 0 8 10 23.46 26.30 1.27 o 1 8 10 16.44 18.16 0.62 o 2 8 10 1.55 0.69 0.34 o 1 0 11 106.23 115.67 2.35 o 2 0 11 1399.73 1498.08 14.71 o 3 0 11 37.85 40.62 0.50 o 4 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12 64.82 63.33 0.51 o 2 4 12 20.09 20.78 0.33 o 3 4 12 397.78 405.55 3.17 o 4 4 12 63.89 59.88 0.80 o 5 4 12 18.29 21.80 1.01 o 0 5 12 122.17 122.98 1.28 o 1 5 12 32.62 31.65 0.38 o 2 5 12 49.18 50.32 0.60 o 3 5 12 18.49 19.82 0.60 o 4 5 12 4.21 2.47 0.31 o 5 5 12 10.92 11.56 0.52 o 0 6 12 6.83 4.65 0.38 o 1 6 12 23.67 21.06 0.46 o 2 6 12 5.33 3.87 0.25 o 3 6 12 5.05 4.69 0.31 o 4 6 12 21.19 21.09 0.67 o 0 7 12 0.03 -0.31 0.31 o 1 7 12 16.94 16.99 0.49 o 2 7 12 9.30 10.12 0.44 o 3 7 12 25.34 24.45 0.54 o 0 8 12 6.37 6.69 0.81 o 1 8 12 1.52 1.84 0.33 o 2 8 12 2.45 3.85 0.67 o 1 0 13 877.97 883.25 7.54 o 2 0 13 4.00 3.55 0.25 o 3 0 13 449.66 463.84 4.10 o 4 0 13 30.78 34.95 0.66 o 5 0 13 0.17 -0.06 0.41 o 6 0 13 9.27 10.35 1.99 o 0 1 13 273.58 280.77 2.24 o 1 1 13 122.82 121.49 0.85 o 2 1 13 58.23 52.58 0.49 o 3 1 13 63.48 69.69 0.57 o 4 1 13 20.34 16.45 0.39 o 5 1 13 4.34 4.21 0.55 o 6 1 13 3.80 5.37 0.51 o 0 2 13 0.16 0.14 0.17 o 1 2 13 668.91 646.29 3.61 o 2 2 13 256.29 247.96 1.52 o 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34.80 35.54 0.55 o 2 3 19 82.53 84.87 0.91 o 3 3 19 76.94 76.65 0.94 o 4 3 19 21.70 23.97 0.58 o 0 4 19 121.91 118.95 1.60 o 1 4 19 32.75 30.32 0.43 o 2 4 19 102.12 101.20 1.05 o 3 4 19 63.19 62.34 1.04 o 4 4 19 30.59 29.81 0.82 o 0 5 19 59.06 51.87 1.13 o 1 5 19 20.81 22.87 0.46 o 2 5 19 2.83 3.76 0.23 o 3 5 19 6.81 7.29 0.46 o 0 6 19 28.47 29.30 0.78 o 1 6 19 4.94 6.17 0.34 o 2 6 19 2.93 3.64 0.33 o 3 6 19 7.58 8.53 0.63 o 0 7 19 1.59 1.16 0.40 o 1 7 19 2.68 2.16 0.36 o 0 0 20 63.00 66.07 1.10 o 1 0 20 17.48 18.69 0.43 o 2 0 20 8.61 9.82 0.46 o 3 0 20 0.40 -0.28 0.28 o 4 0 20 33.55 33.59 0.99 o 5 0 20 7.22 8.57 1.04 o 0 1 20 0.16 0.21 0.15 o 1 1 20 14.68 16.17 0.39 o 2 1 20 3.45 2.29 0.23 o 3 1 20 8.19 8.11 0.34 o 4 1 20 3.91 4.95 0.33 o 5 1 20 7.32 7.57 0.51 o 0 2 20 7.34 10.91 0.37 o 1 2 20 25.95 28.33 0.67 o 2 2 20 7.17 6.97 0.30 o 3 2 20 31.22 32.19 0.63 o 4 2 20 4.07 2.87 0.31 o 0 3 20 0.00 -0.24 0.24 o 1 3 20 114.04 115.68 0.98 o 2 3 20 126.09 120.64 1.22 o 3 3 20 55.71 59.79 0.85 o 4 3 20 34.17 34.78 0.75 o 0 4 20 8.48 9.35 0.55 o 1 4 20 5.40 5.23 0.27 o 2 4 20 15.92 15.60 0.43 o 3 4 20 85.60 82.03 1.24 o 4 4 20 0.64 -0.05 0.35 o 0 5 20 6.07 5.69 0.51 o 1 5 20 17.89 16.00 0.46 o 2 5 20 29.72 29.88 0.47 o 3 5 20 4.94 5.25 0.49 o 0 6 20 54.58 52.77 1.30 o 1 6 20 0.52 0.22 0.27 o 2 6 20 3.67 4.13 0.30 o 0 7 20 1.82 1.43 0.41 o 1 0 21 155.87 149.73 1.61 o 2 0 21 211.82 208.92 2.77 o 3 0 21 35.69 34.52 0.78 o 4 0 21 33.50 32.55 0.67 o 0 1 21 6.24 6.27 0.41 o 1 1 21 88.35 83.97 0.80 o 2 1 21 20.77 18.52 0.46 o 3 1 21 8.94 9.41 0.36 o 4 1 21 26.18 29.13 0.55 o 0 2 21 210.78 209.13 2.27 o 1 2 21 18.28 20.10 0.43 o 2 2 21 72.31 74.66 0.87 o 3 2 21 2.70 2.53 0.29 o 4 2 21 0.42 -0.17 0.28 o 0 3 21 0.01 0.00 0.27 o 1 3 21 9.18 11.22 0.30 o 2 3 21 11.81 14.42 0.42 o 3 3 21 47.34 50.57 0.80 o 4 3 21 1.50 2.11 0.38 o 0 4 21 53.93 52.89 1.14 o 1 4 21 11.73 11.89 0.37 o 2 4 21 7.87 12.14 0.58 o 3 4 21 191.79 185.28 2.16 o 0 5 21 0.17 -0.19 0.31 o 1 5 21 23.00 22.78 0.50 o 2 5 21 6.17 7.08 0.43 o 3 5 21 5.51 5.45 0.63 o 0 6 21 0.66 1.44 0.38 o 1 6 21 1.38 1.54 0.31 o 2 6 21 0.06 -0.18 0.23 o 0 0 22 1.96 2.49 0.31 o 1 0 22 16.23 19.61 0.50 o 2 0 22 2.66 5.69 0.65 o 3 0 22 45.85 48.70 0.96 o 4 0 22 53.46 51.13 0.87 o 0 1 22 1.21 1.23 0.26 o 1 1 22 12.68 14.85 0.35 o 2 1 22 2.30 1.71 0.27 o 3 1 22 19.86 21.51 0.48 o 4 1 22 9.45 10.73 0.33 o 0 2 22 75.85 75.95 1.08 o 1 2 22 104.75 100.94 1.09 o 2 2 22 109.54 107.48 1.13 o 3 2 22 4.62 3.98 0.32 o 4 2 22 26.56 28.37 0.73 o 0 3 22 53.56 52.67 0.95 o 1 3 22 14.27 13.76 0.32 o 2 3 22 3.41 1.98 0.26 o 3 3 22 21.24 21.10 0.55 o 4 3 22 50.42 52.89 1.00 o 0 4 22 0.75 0.33 0.37 o 1 4 22 9.94 11.48 0.37 o 2 4 22 48.79 47.30 0.79 o 3 4 22 11.49 12.67 0.62 o 0 5 22 5.58 7.82 0.48 o 1 5 22 0.53 0.94 0.25 o 2 5 22 2.36 1.98 0.41 o 0 6 22 11.68 13.57 0.60 o 1 6 22 23.12 20.30 0.61 o 1 0 23 20.16 20.04 0.54 o 2 0 23 18.60 16.01 0.58 o 3 0 23 78.49 71.52 1.21 o 4 0 23 12.33 11.73 0.49 o 0 1 23 46.27 45.15 0.87 o 1 1 23 10.23 11.54 0.33 o 2 1 23 1.62 0.97 0.27 o 3 1 23 2.50 2.72 0.27 o 4 1 23 9.61 10.90 0.36 o 0 2 23 0.28 1.10 0.30 o 1 2 23 42.60 46.95 0.68 o 2 2 23 67.68 67.79 0.92 o 3 2 23 6.34 5.45 0.34 o 4 2 23 32.01 34.75 0.80 o 0 3 23 2.00 2.43 0.35 o 1 3 23 10.47 10.53 0.29 o 2 3 23 16.53 17.03 0.48 o 3 3 23 8.82 6.70 0.38 o 0 4 23 3.40 3.10 0.45 o 1 4 23 26.75 26.44 0.52 o 2 4 23 58.06 60.35 1.05 o 3 4 23 3.12 5.12 0.45 o 0 5 23 0.56 0.30 0.36 o 1 5 23 9.08 10.03 0.45 o 2 5 23 11.63 13.09 0.48 o 0 6 23 7.16 7.97 0.53 o 0 0 24 6.45 7.55 0.40 o 1 0 24 30.31 30.10 0.65 o 2 0 24 32.19 27.20 0.75 o 3 0 24 0.00 0.83 0.36 o 4 0 24 30.58 31.49 0.72 o 0 1 24 11.96 13.15 0.55 o 1 1 24 43.37 47.48 0.67 o 2 1 24 11.92 11.55 0.42 o 3 1 24 6.79 7.01 0.34 o 4 1 24 18.23 17.47 0.39 o 0 2 24 47.39 44.48 0.97 o 1 2 24 56.40 57.59 0.81 o 2 2 24 18.22 17.54 0.50 o 3 2 24 10.71 10.96 0.57 o 0 3 24 7.74 8.17 0.50 o 1 3 24 1.32 1.49 0.21 o 2 3 24 15.47 16.20 0.49 o 3 3 24 1.36 0.86 0.31 o 0 4 24 1.03 1.26 0.35 o 1 4 24 9.69 10.07 0.41 o 2 4 24 13.64 12.62 0.46 o 0 5 24 42.88 42.73 1.07 o 1 5 24 2.02 2.82 0.30 o 1 0 25 3.81 4.64 0.39 o 2 0 25 7.97 6.46 0.46 o 3 0 25 17.03 18.29 0.67 o 0 1 25 18.46 17.83 0.48 o 1 1 25 18.27 16.93 0.43 o 2 1 25 4.80 5.60 0.35 o 3 1 25 10.65 10.73 0.39 o 0 2 25 29.35 32.15 0.96 o 1 2 25 113.43 110.96 1.31 o 2 2 25 7.58 6.81 0.41 o 3 2 25 0.54 0.82 0.32 o 0 3 25 1.60 1.28 0.32 o 1 3 25 39.42 37.80 0.83 o 2 3 25 2.76 2.94 0.33 o 3 3 25 10.89 11.55 0.47 o 0 4 25 1.79 2.28 0.45 o 1 4 25 0.78 0.83 0.24 o 2 4 25 8.80 9.67 0.46 o 0 5 25 8.38 9.97 0.54 o 0 0 26 1.98 2.21 0.75 o 1 0 26 30.98 31.36 0.78 o 2 0 26 2.06 3.91 0.43 o 3 0 26 16.11 17.83 0.68 o 0 1 26 22.99 25.25 0.67 o 1 1 26 23.77 25.24 0.57 o 2 1 26 15.89 13.76 0.42 o 3 1 26 19.29 20.60 0.51 o 0 2 26 14.07 15.05 0.53 o 1 2 26 17.66 18.87 0.50 o 2 2 26 11.04 10.72 0.48 o 3 2 26 8.60 12.08 0.47 o 0 3 26 1.85 3.59 0.38 o 1 3 26 15.42 17.22 0.62 o 2 3 26 1.77 1.75 0.32 o 0 4 26 7.53 7.52 0.61 o 1 4 26 7.26 6.94 0.31 o 1 0 27 3.83 3.14 0.40 o 2 0 27 20.80 19.75 0.71 o 0 1 27 68.74 70.32 1.32 o 1 1 27 33.42 32.07 0.60 o 2 1 27 5.75 6.65 0.39 o 0 2 27 8.60 8.36 0.44 o 1 2 27 4.40 4.08 0.31 o 2 2 27 5.32 4.39 0.43 o 0 3 27 0.00 1.09 0.44 o 1 3 27 7.09 7.22 0.49 o 0 0 28 3.29 1.70 0.84 o 1 0 28 0.29 0.15 0.40 o 2 0 28 4.88 5.80 0.52 o 0 1 28 8.06 13.01 0.83 o 1 1 28 21.25 22.59 0.52 o 2 1 28 31.77 35.27 0.74 o 0 2 28 5.34 5.30 0.49 o 1 2 28 2.62 2.48 0.71 o 0 3 28 76.68 73.41 1.25 o 1 0 29 18.56 19.58 0.71 o 0 1 29 18.32 17.45 0.94 o 1 1 29 35.70 37.13 0.73 o 0 2 29 14.81 17.61 0.52 o