#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220599.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220599_Fobs loop_ _publ_author_name 'Suwunwong, Thitipone' 'Chantrapromma, Suchada' 'Fun, Hoong-Kun' _publ_section_title ; (E)-1-(4-Bromophenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one ; _journal_coeditor_code PK2134 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o120 _journal_volume 65 _journal_year 2009 _space_group_IT_number 86 _symmetry_space_group_name_Hall '-P 4bc' _symmetry_space_group_name_H-M 'P 42/n :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 26.6517 _cell_length_b 26.6517 _cell_length_c 4.4238 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.5529 _[local]_cod_data_source_file pk2134Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tc25b_0m in P4(2)/n (100K)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 335.57 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-y, x+1/2, z+1/2' 'y+1/2, -x, z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'y, -x-1/2, -z-1/2' '-y-1/2, x, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 15318.13 0.61 0.23 o -1 3 0 6077.50 6376.42 65.58 o 1 3 0 13077.93 13070.34 314.70 o 3 3 0 6844.40 7261.77 68.36 o -2 4 0 20215.11 21036.01 208.72 o 0 4 0 376.95 364.48 6.18 o 2 4 0 27278.86 29423.89 240.18 o 4 4 0 13818.43 13991.45 133.90 o -3 5 0 1253.13 1235.46 16.59 o -1 5 0 7478.83 7783.13 63.65 o 1 5 0 472.10 414.39 7.51 o 3 5 0 32115.42 34296.92 287.38 o 5 5 0 40092.79 40366.98 379.24 o -4 6 0 1222.10 1285.30 18.15 o -2 6 0 1608.92 1641.18 20.11 o 0 6 0 4564.74 5044.21 46.66 o 2 6 0 19617.86 20182.47 182.21 o 4 6 0 71938.38 73335.48 647.07 o 6 6 0 21935.47 22769.27 217.14 o -5 7 0 112607.09 112889.67 992.18 o -3 7 0 5882.29 5905.18 57.62 o -1 7 0 2369.96 2343.90 23.85 o 1 7 0 15.06 21.08 4.49 o 3 7 0 116.30 138.90 7.01 o 5 7 0 28943.59 29313.39 278.34 o 7 7 0 17494.71 17417.03 169.22 o -6 8 0 24275.96 24980.29 226.29 o -4 8 0 13520.67 13178.23 122.58 o -2 8 0 2581.57 2602.81 29.39 o 0 8 0 6434.90 6537.67 60.66 o 2 8 0 518.78 386.26 10.13 o 4 8 0 59931.46 61149.98 725.68 o 6 8 0 23926.01 24559.79 225.26 o 8 8 0 4032.03 4161.50 48.82 o -7 9 0 6045.75 6443.63 63.01 o -5 9 0 5067.35 5012.30 58.10 o -3 9 0 5448.07 5520.25 53.35 o -1 9 0 35955.58 36591.73 298.75 o 1 9 0 8338.54 8657.60 75.97 o 3 9 0 276.93 255.63 8.36 o 5 9 0 17637.64 17631.84 162.80 o 7 9 0 36849.57 37774.41 339.52 o 9 9 0 2383.52 2592.01 33.74 o -8 10 0 3964.43 3798.46 44.43 o -6 10 0 1389.25 1434.62 22.58 o -4 10 0 67.59 87.30 8.19 o -2 10 0 29618.29 32310.77 289.76 o 0 10 0 14160.81 14508.88 128.47 o 2 10 0 3783.12 3717.21 37.31 o 4 10 0 766.18 745.10 13.82 o 6 10 0 945.07 948.15 17.71 o 8 10 0 4114.24 4512.63 46.27 o 10 10 0 21747.97 23016.51 203.47 o -9 11 0 9547.58 10050.86 95.67 o -7 11 0 1122.51 1113.77 34.15 o -5 11 0 3770.95 4396.01 46.46 o -3 11 0 7299.33 7534.95 75.32 o -1 11 0 29671.46 29883.82 247.12 o 1 11 0 26533.60 27836.95 230.29 o 3 11 0 23.68 62.38 7.79 o 5 11 0 3081.52 3283.19 35.24 o 7 11 0 9403.08 10043.00 90.30 o 9 11 0 19741.98 20445.52 174.28 o 11 11 0 22754.45 24027.94 204.20 o -10 12 0 6819.98 6976.56 71.41 o -8 12 0 1179.28 1172.47 21.50 o -6 12 0 1756.09 1742.60 26.64 o -4 12 0 44745.37 48900.05 415.56 o -2 12 0 46577.44 47238.09 403.04 o 0 12 0 3378.96 2764.75 34.12 o 2 12 0 48534.60 51864.46 407.00 o 4 12 0 4361.79 4571.42 47.91 o 6 12 0 3637.84 3789.07 40.61 o 8 12 0 16978.78 17737.08 146.94 o 10 12 0 13120.22 12707.79 105.72 o 12 12 0 14667.32 14003.87 116.40 o -11 13 0 7846.93 7992.43 71.81 o -9 13 0 2785.25 2797.72 38.06 o -7 13 0 3431.16 3987.07 43.45 o -5 13 0 1127.41 1167.71 20.94 o -3 13 0 10766.71 10871.67 106.23 o -1 13 0 50607.32 51278.54 403.01 o 1 13 0 8475.55 7835.05 69.50 o 3 13 0 12013.56 13027.62 109.84 o 5 13 0 2017.47 2294.44 28.79 o 7 13 0 1334.69 1496.28 19.98 o 9 13 0 10228.42 10057.69 83.23 o 11 13 0 24575.96 24449.12 193.79 o 13 13 0 15649.54 15616.00 124.29 o -12 14 0 4276.77 4232.74 44.70 o -10 14 0 49.85 55.15 9.70 o -8 14 0 18832.97 20005.36 165.90 o -6 14 0 5231.60 5868.67 58.77 o -4 14 0 2715.06 3314.32 46.07 o -2 14 0 1972.64 1631.70 24.68 o 0 14 0 12747.12 12722.40 112.44 o 2 14 0 1426.80 1394.82 21.47 o 4 14 0 10211.91 12094.07 95.89 o 6 14 0 193.94 222.47 10.48 o 8 14 0 3222.07 3481.82 33.84 o 10 14 0 16375.32 16299.15 120.91 o 12 14 0 27113.94 27361.53 208.81 o 14 14 0 27987.10 28107.36 221.71 o -13 15 0 499.00 486.31 15.60 o -11 15 0 769.56 768.38 18.63 o -9 15 0 4407.18 4748.57 47.51 o -7 15 0 16630.39 16988.39 127.96 o -5 15 0 1859.02 2251.04 28.90 o -3 15 0 1480.88 1472.23 26.52 o -1 15 0 24028.07 24527.37 197.75 o 1 15 0 3202.84 3157.55 32.61 o 3 15 0 2030.50 2214.01 24.51 o 5 15 0 2796.75 2950.29 29.99 o 7 15 0 276.76 388.14 11.66 o 9 15 0 8080.78 8548.00 69.00 o 11 15 0 17693.80 17566.78 134.49 o 13 15 0 5100.10 5063.64 48.40 o 15 15 0 750.97 855.78 17.79 o -14 16 0 912.41 1004.36 20.47 o -12 16 0 1498.91 1405.92 24.13 o -10 16 0 2618.68 2448.40 29.61 o -8 16 0 18375.01 18387.99 143.20 o -6 16 0 5313.09 4775.91 47.43 o -4 16 0 1194.44 1322.48 28.19 o -2 16 0 122.99 95.43 9.99 o 0 16 0 6507.66 6607.29 60.01 o 2 16 0 380.04 507.46 12.46 o 4 16 0 7667.64 8353.08 66.51 o 6 16 0 13305.41 13490.83 105.27 o 8 16 0 5696.00 5856.31 49.74 o 10 16 0 6340.04 5886.37 52.03 o 12 16 0 808.46 823.20 17.85 o 14 16 0 3492.19 3507.68 38.78 o 16 16 0 299.12 357.92 15.67 o -15 17 0 8753.98 8705.55 76.02 o -13 17 0 227.81 267.44 14.79 o -11 17 0 569.76 607.98 16.70 o -9 17 0 7367.17 7197.72 59.25 o -7 17 0 23255.48 23011.20 171.26 o -5 17 0 27067.23 28139.79 212.31 o -3 17 0 1167.76 1181.44 20.69 o -1 17 0 27.66 23.79 8.53 o 1 17 0 1994.39 1961.68 23.15 o 3 17 0 6143.88 6036.17 48.59 o 5 17 0 23527.41 24093.18 168.93 o 7 17 0 17446.36 17939.06 128.86 o 9 17 0 50.95 63.29 9.58 o 11 17 0 11207.13 10818.05 88.49 o 13 17 0 6806.39 6570.88 64.78 o 15 17 0 11424.83 10933.88 91.83 o 17 17 0 554.73 614.68 22.30 o -16 18 0 286.09 351.84 17.26 o -14 18 0 1175.01 1185.20 23.72 o -12 18 0 1887.15 1789.67 26.86 o -10 18 0 3490.39 3372.00 36.28 o -8 18 0 10133.40 10064.52 78.05 o -6 18 0 16135.41 16117.26 123.85 o -4 18 0 4881.67 4546.64 43.66 o -2 18 0 63.75 39.06 9.51 o 0 18 0 299.91 309.85 11.83 o 2 18 0 1217.27 1256.32 21.53 o 4 18 0 21765.88 21730.10 153.75 o 6 18 0 24371.27 24173.01 170.27 o 8 18 0 2247.06 2427.84 28.30 o 10 18 0 2923.16 3007.52 33.97 o 12 18 0 3.27 3.60 8.75 o 14 18 0 344.44 352.65 16.12 o 16 18 0 25187.56 25126.06 204.89 o 18 18 0 5157.42 4983.90 60.95 o -17 19 0 1067.67 1166.24 34.01 o -15 19 0 3288.14 3348.58 42.68 o -13 19 0 2414.83 2379.90 34.52 o -11 19 0 2946.76 2966.20 36.35 o -9 19 0 14817.17 14882.45 110.35 o -7 19 0 17161.62 16994.00 131.06 o -5 19 0 10947.09 10610.35 89.40 o -3 19 0 2900.86 2850.55 33.50 o -1 19 0 1242.23 1257.32 21.09 o 1 19 0 888.03 1006.04 16.49 o 3 19 0 12580.79 12448.37 88.21 o 5 19 0 15140.76 14648.76 105.27 o 7 19 0 10609.64 10482.45 83.90 o 9 19 0 1430.76 1389.48 23.03 o 11 19 0 1913.63 1869.81 26.91 o 13 19 0 6340.47 6196.66 65.82 o 15 19 0 2604.03 2663.06 37.50 o 17 19 0 28326.34 27986.45 239.99 o 19 19 0 4851.13 4911.05 68.10 o -18 20 0 511.74 544.22 23.42 o -16 20 0 4572.12 4285.88 66.89 o -14 20 0 1517.22 1491.24 30.24 o -12 20 0 42.84 41.79 13.08 o -10 20 0 18.58 11.95 11.30 o -8 20 0 20547.21 19856.07 151.86 o -6 20 0 8737.77 8818.85 80.23 o -4 20 0 691.96 603.21 16.24 o -2 20 0 119.81 80.44 10.78 o 0 20 0 177.12 216.64 11.47 o 2 20 0 3274.01 3262.91 30.95 o 4 20 0 10922.90 10974.74 79.81 o 6 20 0 17198.14 16877.75 120.18 o 8 20 0 467.14 460.32 15.22 o 10 20 0 744.92 721.43 18.58 o 12 20 0 86.81 89.59 14.37 o 14 20 0 807.67 856.47 27.10 o 16 20 0 19618.01 19370.48 169.60 o 18 20 0 16216.97 16427.28 154.66 o 20 20 0 5836.34 5686.44 69.55 o -19 21 0 266.73 279.44 21.90 o -17 21 0 534.38 516.59 23.31 o -15 21 0 8121.72 7732.10 83.29 o -13 21 0 15469.16 15043.82 141.52 o -11 21 0 155.13 198.05 15.49 o -9 21 0 1057.42 1059.82 21.46 o -7 21 0 1718.79 1725.29 28.26 o -5 21 0 769.57 625.58 19.89 o -3 21 0 893.00 862.10 24.69 o -1 21 0 4339.62 4245.82 43.10 o 1 21 0 6.89 5.99 9.43 o 3 21 0 7112.26 7304.97 59.16 o 5 21 0 22592.96 22584.69 156.98 o 7 21 0 130.25 141.61 12.87 o 9 21 0 446.45 388.45 15.93 o 11 21 0 40.32 39.33 12.74 o 13 21 0 749.23 677.73 21.84 o 15 21 0 114.16 118.78 16.28 o 17 21 0 6234.16 6271.36 73.09 o 19 21 0 5768.98 5786.27 70.45 o 21 21 0 362.22 340.78 26.40 o -20 22 0 87.10 84.98 22.81 o -18 22 0 15.98 26.42 21.83 o -16 22 0 3733.47 3692.68 52.34 o -14 22 0 2525.04 2592.21 50.16 o -12 22 0 12490.77 12372.35 120.28 o -10 22 0 78.05 60.43 14.97 o -8 22 0 689.47 631.84 29.62 o -6 22 0 145.76 66.84 15.02 o -4 22 0 963.25 998.92 20.79 o -2 22 0 11444.96 10989.04 96.79 o 0 22 0 3533.23 3775.33 40.66 o 2 22 0 915.62 993.88 18.68 o 4 22 0 6992.24 6918.05 60.87 o 6 22 0 119.41 127.37 13.19 o 8 22 0 980.27 1085.22 23.42 o 10 22 0 432.78 484.31 17.76 o 12 22 0 7644.63 7220.12 90.83 o 14 22 0 2.60 -2.92 10.16 o 16 22 0 901.80 998.84 27.41 o 18 22 0 2506.62 2523.13 44.11 o 20 22 0 37.24 64.82 22.14 o 22 22 0 351.09 378.96 28.23 o -21 23 0 506.66 476.57 29.36 o -19 23 0 0.68 -15.82 21.40 o -17 23 0 1601.15 1688.31 44.99 o -15 23 0 4155.48 4379.83 60.37 o -13 23 0 19157.46 18746.31 180.78 o -11 23 0 3018.93 2960.17 46.67 o -9 23 0 209.38 309.18 19.04 o -7 23 0 205.29 133.49 12.91 o -5 23 0 2432.78 2450.00 36.49 o -3 23 0 12917.32 13295.24 123.99 o -1 23 0 12116.02 11704.28 99.38 o 1 23 0 1268.31 1222.63 23.13 o 3 23 0 39.53 15.48 11.28 o 5 23 0 1039.24 1076.03 21.48 o 7 23 0 2788.79 2608.78 34.41 o 9 23 0 632.85 680.80 20.07 o 11 23 0 3010.77 3092.89 41.99 o 13 23 0 3687.39 3483.90 49.85 o 15 23 0 724.51 712.76 39.43 o 17 23 0 144.62 100.40 19.87 o 19 23 0 82.94 96.26 22.68 o 21 23 0 931.56 1032.62 39.07 o 23 23 0 4716.15 4822.02 73.91 o -22 24 0 1115.03 1161.85 41.06 o -20 24 0 183.17 155.36 26.91 o -18 24 0 668.24 595.21 29.63 o -16 24 0 6372.98 6316.34 78.63 o -14 24 0 6991.51 6839.83 82.15 o -12 24 0 9814.77 9565.18 109.22 o -10 24 0 2853.19 2643.62 46.56 o -8 24 0 597.36 552.07 22.21 o -6 24 0 28.96 70.07 14.74 o -4 24 0 17736.97 16676.42 140.62 o -2 24 0 6594.63 6942.30 66.35 o 0 24 0 10920.96 11326.69 97.69 o 2 24 0 8253.26 7469.59 65.74 o 4 24 0 62.90 57.74 13.41 o 6 24 0 309.01 331.49 16.45 o 8 24 0 3106.45 3002.44 40.95 o 10 24 0 10000.59 9996.74 90.67 o 12 24 0 12952.63 12801.35 124.79 o 14 24 0 51.25 46.85 13.61 o 16 24 0 414.59 404.58 22.54 o 18 24 0 422.65 422.38 27.62 o 20 24 0 1671.59 1689.91 43.28 o 22 24 0 2152.38 2119.09 49.12 o 24 24 0 4142.91 4358.87 84.90 o -23 25 0 43.43 53.12 29.51 o -21 25 0 643.25 662.61 35.20 o -19 25 0 17.65 14.64 24.52 o -17 25 0 645.02 630.97 31.77 o -15 25 0 5886.61 5819.39 77.94 o -13 25 0 1762.15 1844.32 55.80 o -11 25 0 1853.05 1939.64 41.60 o -9 25 0 1.41 8.23 18.13 o -7 25 0 1960.52 1878.68 38.13 o -5 25 0 2642.12 2678.93 44.48 o -3 25 0 23970.90 23158.19 196.87 o -1 25 0 38476.06 37959.16 297.49 o 1 25 0 3624.62 4098.41 45.34 o 3 25 0 71.49 96.28 14.84 o 5 25 0 1339.59 1257.14 26.04 o 7 25 0 86.13 123.07 15.87 o 9 25 0 3953.55 3995.17 51.14 o 11 25 0 8695.73 8639.51 85.02 o 13 25 0 4897.43 4918.63 65.79 o 15 25 0 1184.11 1097.51 32.65 o 17 25 0 51.20 -12.47 22.38 o 19 25 0 1021.31 1016.50 36.51 o 21 25 0 5822.13 5946.89 88.66 o 23 25 0 4130.05 4139.24 73.92 o 25 25 0 3190.78 3160.04 75.60 o -24 26 0 173.17 187.13 36.64 o -22 26 0 46.28 43.53 30.95 o -20 26 0 843.35 830.32 41.26 o -18 26 0 641.16 628.51 33.70 o -16 26 0 718.66 822.59 40.42 o -14 26 0 1302.78 1357.99 55.02 o -12 26 0 4242.57 4143.85 67.44 o -10 26 0 2335.38 2117.60 45.67 o -8 26 0 1751.60 1629.29 46.16 o -6 26 0 75.90 112.19 19.18 o -4 26 0 961.86 935.53 29.12 o -2 26 0 1004.69 1330.85 28.53 o 0 26 0 4838.74 4576.83 53.20 o 2 26 0 1272.73 1259.44 32.75 o 4 26 0 39.67 80.11 16.92 o 6 26 0 69.55 28.09 15.95 o 8 26 0 4845.46 4962.38 57.55 o 10 26 0 11550.42 11352.45 105.84 o 12 26 0 12124.24 11504.29 111.59 o 14 26 0 626.36 651.64 29.43 o 16 26 0 529.18 512.70 30.59 o 18 26 0 328.09 374.63 29.11 o 20 26 0 3456.38 3542.14 76.15 o 22 26 0 8224.97 8338.58 112.46 o 24 26 0 3909.92 3952.26 90.21 o 26 26 0 202.72 251.47 44.57 o -25 27 0 1655.36 1726.57 65.41 o -23 27 0 82.48 75.48 39.21 o -21 27 0 5909.62 5884.22 136.55 o -19 27 0 552.44 536.11 35.89 o -17 27 0 9.85 19.97 27.29 o -15 27 0 2245.99 2083.23 58.89 o -13 27 0 4681.78 4462.80 91.96 o -11 27 0 3.48 4.34 24.07 o -9 27 0 5839.97 5685.03 92.92 o -7 27 0 1560.64 1595.15 50.15 o -5 27 0 2876.07 2854.16 47.77 o -3 27 0 95.92 120.38 19.03 o -1 27 0 1382.21 1534.74 36.08 o 1 27 0 1897.53 2076.27 38.78 o 3 27 0 1333.63 1277.68 38.49 o 5 27 0 1012.98 1109.50 28.38 o 7 27 0 1401.47 1312.84 31.18 o 9 27 0 3936.92 3842.18 54.49 o 11 27 0 4656.69 4714.57 59.55 o 13 27 0 700.84 755.52 28.22 o 15 27 0 509.75 471.74 28.62 o 17 27 0 28.69 30.03 25.25 o 19 27 0 28.53 24.37 26.96 o 21 27 0 2583.19 2733.16 74.73 o 23 27 0 1243.81 1211.43 51.21 o 25 27 0 45.32 68.99 41.00 o 27 27 0 1.14 65.00 43.01 o -26 28 0 67.11 47.39 43.29 o -24 28 0 433.71 476.23 48.46 o -22 28 0 5885.37 5971.85 124.56 o -20 28 0 4976.10 4950.44 86.50 o -18 28 0 3792.98 3622.07 84.94 o -16 28 0 271.41 331.85 42.10 o -14 28 0 120.37 67.27 29.57 o -12 28 0 32.94 5.94 25.53 o -10 28 0 2767.00 2720.68 63.42 o -8 28 0 1608.75 1693.59 48.67 o -6 28 0 797.63 845.19 33.63 o -4 28 0 16.00 1.35 21.45 o -2 28 0 816.04 932.34 31.90 o 0 28 0 4264.43 4153.35 66.26 o 2 28 0 723.43 697.32 33.70 o 4 28 0 9105.76 8961.18 100.51 o 6 28 0 3283.66 3055.05 48.72 o 8 28 0 339.40 314.60 24.43 o 10 28 0 1255.87 1339.34 36.90 o 12 28 0 2614.37 2680.15 52.00 o 14 28 0 159.59 210.93 27.48 o 16 28 0 1247.23 1308.71 45.73 o 18 28 0 44.11 22.28 29.52 o 20 28 0 901.16 931.71 43.77 o 22 28 0 3227.66 3094.56 85.78 o 24 28 0 2293.25 2288.37 73.61 o 26 28 0 365.03 458.53 52.39 o 28 28 0 11.59 -1.94 44.28 o -27 29 0 2.44 -1.12 42.92 o -25 29 0 363.20 405.20 52.56 o -23 29 0 1440.78 1580.73 68.96 o -21 29 0 4083.76 4075.92 101.23 o -19 29 0 3654.11 3692.94 79.65 o -17 29 0 3019.04 2987.41 77.99 o -15 29 0 101.45 66.49 29.45 o -13 29 0 32.49 48.87 27.45 o -11 29 0 2186.22 2245.20 60.23 o -9 29 0 9051.10 8691.78 127.42 o -7 29 0 3134.88 3280.26 64.41 o -5 29 0 170.29 165.99 25.46 o -3 29 0 2.26 -8.65 21.03 o -1 29 0 218.38 136.46 20.47 o 1 29 0 5106.55 5195.55 82.91 o 3 29 0 7815.66 7955.70 110.37 o 5 29 0 5823.50 5790.35 78.99 o 7 29 0 2659.49 2508.31 47.18 o 9 29 0 418.20 391.92 29.99 o 11 29 0 461.33 423.45 30.43 o 13 29 0 933.73 988.69 42.81 o 15 29 0 1895.66 2002.38 54.17 o 17 29 0 5380.22 5469.38 90.46 o 19 29 0 41.02 66.49 32.15 o 21 29 0 637.97 741.95 46.77 o 23 29 0 910.38 878.18 53.46 o 25 29 0 1102.61 1147.71 77.72 o 27 29 0 693.34 750.36 69.56 o 29 29 0 528.05 545.53 55.35 o -28 30 0 1.58 -18.07 50.04 o -26 30 0 297.03 274.23 52.09 o -24 30 0 249.04 273.90 50.76 o -22 30 0 2650.69 2670.15 86.27 o -20 30 0 1154.17 1105.39 60.73 o -18 30 0 3177.66 2980.33 85.68 o -16 30 0 763.01 660.30 41.85 o -14 30 0 58.84 36.19 30.89 o -12 30 0 224.86 233.03 34.48 o -10 30 0 4037.58 4003.35 91.43 o -8 30 0 10318.81 10627.03 138.79 o -6 30 0 3952.15 3937.85 82.72 o -4 30 0 45.97 85.25 26.57 o -2 30 0 494.75 508.56 47.82 o 0 30 0 7.26 32.26 26.14 o 2 30 0 3741.57 3796.89 70.46 o 4 30 0 7064.90 7037.17 103.00 o 6 30 0 4684.96 4840.91 72.41 o 8 30 0 1297.38 1406.80 38.12 o 10 30 0 1093.22 1223.56 53.46 o 12 30 0 183.60 237.34 31.26 o 14 30 0 2819.65 2662.32 73.41 o 16 30 0 4480.45 4490.79 87.42 o 18 30 0 4101.11 4124.89 79.91 o 20 30 0 54.84 42.01 36.33 o 22 30 0 6.73 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3699.50 54.63 o -8 31 2 52.43 29.90 22.54 o -7 31 2 1900.37 1875.67 40.92 o -6 31 2 2.33 -13.56 21.86 o -5 31 2 1984.66 2011.77 40.91 o -4 31 2 499.98 476.85 25.97 o -3 31 2 354.80 358.67 24.35 o -2 31 2 865.15 822.25 28.24 o -1 31 2 29.99 43.29 20.69 o 0 31 2 32.62 45.88 20.66 o 1 31 2 960.21 908.98 29.23 o 2 31 2 65.95 50.58 20.81 o 3 31 2 2716.00 2639.39 43.50 o 4 31 2 9.08 -8.24 20.32 o 5 31 2 7230.99 7185.43 81.07 o 6 31 2 30.44 1.91 19.65 o 7 31 2 1214.05 1214.59 32.40 o 8 31 2 10.28 -8.22 21.04 o 9 31 2 13.46 6.27 22.30 o 10 31 2 909.82 896.80 31.69 o 11 31 2 158.24 171.24 24.75 o 12 31 2 348.35 361.02 28.28 o 13 31 2 573.04 570.01 32.80 o 14 31 2 430.76 483.96 33.85 o 15 31 2 1323.90 1376.28 48.09 o 16 31 2 283.15 273.46 36.62 o 17 31 2 1725.27 1683.87 57.04 o 18 31 2 8.93 -7.77 32.64 o 19 31 2 1343.54 1333.87 50.59 o 20 31 2 6.56 14.87 34.75 o 21 31 2 3.06 61.34 36.01 o 22 31 2 278.27 220.49 38.69 o 23 31 2 84.54 139.03 38.24 o 24 31 2 105.87 39.64 40.34 o 25 31 2 473.04 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