#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/06/2220652.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220652_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Kia, Reza' 'Maity, Annada C.' 'Maity, Sibaprasad' 'Goswami, Shyamaprosad' _publ_section_title ; 3,5-Dichloro-6-methylpyridin-2-amine ; _journal_coeditor_code TK2343 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o97 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.990 _cell_angle_gamma 90.000 _cell_length_a 12.7670 _cell_length_b 3.8037 _cell_length_c 15.4129 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.5838 _[local]_cod_data_source_file tk2343Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' spgam473m (fs22m) in P2(1)/n 100K' _shelx_refln_list_code 4 _shelx_F_calc_maximum 155.06 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5567.79 4381.81 56.11 o 4 0 0 24044.73 13943.00 310.51 o 6 0 0 2061.85 2275.93 20.77 o 8 0 0 1564.80 1554.14 13.23 o 10 0 0 2.59 13.69 0.67 o 12 0 0 763.58 699.22 8.83 o 14 0 0 24.82 21.79 1.16 o 16 0 0 32.51 33.66 1.45 o 18 0 0 1.87 1.65 1.35 o 20 0 0 42.77 46.28 2.76 o 1 1 0 449.62 475.37 3.04 o 2 1 0 237.22 283.37 1.85 o 3 1 0 2.21 3.00 0.14 o 4 1 0 1067.68 1103.19 7.05 o 5 1 0 1598.51 1692.85 10.13 o 6 1 0 23.75 21.85 0.36 o 7 1 0 2.65 3.77 0.35 o 8 1 0 1302.35 1327.59 7.55 o 9 1 0 674.17 716.17 4.89 o 10 1 0 103.46 105.09 1.23 o 11 1 0 170.92 148.84 1.49 o 12 1 0 634.44 655.11 5.40 o 13 1 0 834.84 809.42 7.44 o 14 1 0 139.63 143.54 2.18 o 15 1 0 67.09 67.01 1.54 o 16 1 0 168.40 171.71 3.13 o 17 1 0 608.27 615.36 9.08 o 18 1 0 36.37 41.73 1.76 o 19 1 0 17.40 16.97 1.88 o 20 1 0 44.35 48.80 2.26 o 0 2 0 16.73 20.62 0.71 o 1 2 0 2031.61 1991.89 15.12 o 2 2 0 73.51 75.44 0.89 o 3 2 0 1397.25 1359.17 8.82 o 4 2 0 1.74 0.73 0.16 o 5 2 0 1041.50 1032.31 6.18 o 6 2 0 330.69 328.57 2.29 o 7 2 0 513.82 518.86 4.03 o 8 2 0 58.21 59.45 1.06 o 9 2 0 217.87 221.33 2.37 o 10 2 0 147.30 146.57 1.95 o 11 2 0 161.76 165.07 2.30 o 12 2 0 44.55 46.99 1.19 o 13 2 0 1.14 1.84 0.48 o 14 2 0 78.33 72.84 1.57 o 15 2 0 30.91 32.15 1.64 o 16 2 0 14.33 11.70 1.28 o 17 2 0 50.32 48.38 2.58 o 18 2 0 95.82 98.63 3.75 o 19 2 0 9.97 9.34 1.54 o 20 2 0 78.61 72.30 3.47 o 1 3 0 47.34 52.89 0.95 o 2 3 0 892.44 896.32 8.03 o 3 3 0 421.34 448.59 3.92 o 4 3 0 42.88 42.52 0.74 o 5 3 0 129.30 132.38 1.75 o 6 3 0 547.70 551.53 5.02 o 7 3 0 459.72 473.22 4.93 o 8 3 0 26.95 29.04 1.19 o 9 3 0 836.47 832.06 7.73 o 10 3 0 146.14 146.50 2.40 o 11 3 0 2.14 1.60 0.45 o 12 3 0 42.43 41.58 1.63 o 13 3 0 373.95 384.39 5.91 o 14 3 0 13.33 14.81 1.06 o 15 3 0 19.46 20.10 1.37 o 16 3 0 57.57 56.22 2.11 o 17 3 0 67.51 65.04 3.35 o 18 3 0 0.05 0.81 1.63 o 0 4 0 301.30 310.02 6.25 o 1 4 0 44.98 46.79 1.67 o 2 4 0 154.87 161.78 2.36 o 3 4 0 102.15 109.46 1.93 o 4 4 0 1110.68 1128.77 10.74 o 5 4 0 74.02 76.37 1.49 o 6 4 0 22.90 23.24 0.92 o 7 4 0 463.68 472.91 5.38 o 8 4 0 1021.80 1030.63 9.91 o 9 4 0 1.66 2.43 0.58 o 10 4 0 135.80 130.71 2.83 o 11 4 0 364.69 355.86 5.56 o 12 4 0 36.38 38.56 1.68 o 13 4 0 3.91 2.21 0.74 o 14 4 0 2.07 1.18 0.85 o 15 4 0 177.23 174.90 3.93 o 16 4 0 0.08 0.84 0.86 o 1 5 0 163.45 169.22 8.40 o 2 5 0 85.50 88.40 2.74 o 3 5 0 174.69 177.74 3.39 o 4 5 0 19.03 18.08 1.05 o 5 5 0 43.06 46.32 1.32 o 6 5 0 43.56 40.93 1.35 o 7 5 0 10.58 9.27 1.15 o 8 5 0 34.88 33.77 1.41 o 9 5 0 87.59 90.70 2.34 o 10 5 0 17.79 16.68 1.20 o 11 5 0 7.15 5.51 0.89 o 12 5 0 48.18 47.61 1.95 o 13 5 0 21.81 18.50 1.44 o 2 6 0 11.74 12.27 1.97 o 3 6 0 8.84 6.67 1.06 o 4 6 0 0.23 1.11 0.83 o 5 6 0 6.55 5.72 1.19 o 6 6 0 55.98 59.42 1.61 o 7 6 0 24.38 26.55 1.50 o 8 6 0 4.56 2.96 0.96 o -21 0 1 66.36 69.88 4.09 o -19 0 1 490.08 519.91 11.34 o -17 0 1 0.13 -0.10 0.53 o -15 0 1 545.48 551.85 8.99 o -13 0 1 23.27 18.23 0.95 o -11 0 1 402.06 418.86 5.30 o -9 0 1 14.13 12.74 0.50 o -7 0 1 641.90 654.37 5.65 o -5 0 1 455.81 488.11 4.21 o -3 0 1 16.64 20.40 0.52 o 1 0 1 897.34 873.83 9.55 o 3 0 1 1124.81 1170.28 10.09 o 5 0 1 602.59 504.71 3.96 o 7 0 1 1057.17 961.85 8.39 o 9 0 1 625.01 589.18 6.72 o 11 0 1 1998.11 1809.67 20.55 o 13 0 1 8.48 5.18 0.65 o 15 0 1 865.32 879.85 16.46 o 17 0 1 382.80 388.45 7.67 o 19 0 1 0.07 -0.17 1.00 o -21 1 1 10.72 5.92 2.28 o -20 1 1 0.02 1.18 0.90 o -19 1 1 43.24 42.38 2.19 o -18 1 1 3.46 3.28 0.99 o -17 1 1 287.20 291.36 4.78 o -16 1 1 120.73 127.99 2.61 o -15 1 1 109.27 117.69 2.11 o -14 1 1 83.68 86.47 1.61 o -13 1 1 306.19 285.51 3.25 o -12 1 1 196.33 195.69 2.06 o -11 1 1 946.74 875.10 5.80 o -10 1 1 364.77 358.30 2.75 o -9 1 1 3.64 2.82 0.22 o -8 1 1 321.77 322.28 2.40 o -7 1 1 938.17 850.84 4.96 o -6 1 1 1209.65 1212.98 7.30 o -5 1 1 178.74 196.67 1.68 o -4 1 1 124.59 121.44 0.96 o -3 1 1 2033.97 1999.33 12.45 o -2 1 1 2562.70 2633.99 16.68 o -1 1 1 808.18 932.68 6.21 o 0 1 1 1523.38 1650.88 11.65 o 1 1 1 5814.51 5584.22 35.51 o 2 1 1 8.54 7.30 0.19 o 3 1 1 741.92 720.38 4.38 o 4 1 1 101.17 114.25 1.03 o 5 1 1 456.19 506.37 3.59 o 6 1 1 19.92 27.92 0.44 o 7 1 1 411.25 442.40 2.61 o 8 1 1 59.77 70.71 0.76 o 9 1 1 151.32 143.99 1.42 o 10 1 1 5.37 3.31 0.31 o 11 1 1 78.56 66.74 0.93 o 12 1 1 1.86 1.24 0.33 o 13 1 1 21.95 27.01 0.86 o 14 1 1 63.77 61.60 1.69 o 15 1 1 182.67 191.53 3.01 o 16 1 1 8.56 8.86 0.97 o 17 1 1 8.26 5.99 1.07 o 18 1 1 73.57 73.80 4.49 o 19 1 1 44.12 42.51 6.74 o 20 1 1 37.00 37.39 2.08 o -20 2 1 121.30 112.67 4.29 o -19 2 1 3.16 4.39 1.26 o -18 2 1 0.04 1.54 0.99 o -17 2 1 6.22 6.22 1.12 o -16 2 1 292.42 291.46 5.83 o -15 2 1 151.52 159.55 3.58 o -14 2 1 48.86 49.72 1.30 o -13 2 1 70.29 72.26 1.76 o -12 2 1 259.67 253.71 3.22 o -11 2 1 302.93 282.34 3.18 o -10 2 1 75.94 72.55 1.45 o -9 2 1 1096.94 1069.48 8.73 o -8 2 1 72.52 75.81 1.24 o -7 2 1 92.96 100.56 1.20 o -6 2 1 1.71 3.48 0.20 o -5 2 1 565.63 567.69 3.72 o -4 2 1 2.24 1.53 0.18 o -3 2 1 463.53 470.68 3.25 o -2 2 1 282.90 301.75 2.37 o -1 2 1 23.49 11.66 0.33 o 0 2 1 20.93 15.82 0.26 o 1 2 1 65.51 42.52 0.59 o 2 2 1 997.26 978.23 6.27 o 3 2 1 158.28 159.38 1.32 o 4 2 1 1.24 -0.05 0.12 o 5 2 1 275.99 275.17 1.90 o 6 2 1 1509.63 1483.77 8.95 o 7 2 1 0.01 0.87 0.42 o 8 2 1 43.60 40.65 0.90 o 9 2 1 90.53 86.99 1.32 o 10 2 1 989.23 964.97 7.74 o 11 2 1 27.80 29.94 1.01 o 12 2 1 121.35 120.35 2.09 o 13 2 1 0.01 0.10 0.39 o 14 2 1 330.98 338.39 4.28 o 15 2 1 2.25 2.68 0.77 o 16 2 1 90.99 86.70 2.87 o 17 2 1 1.44 1.12 0.97 o 18 2 1 64.24 59.65 3.05 o 19 2 1 1.98 1.32 0.90 o -18 3 1 0.02 0.32 1.23 o -17 3 1 44.30 44.23 2.85 o -16 3 1 22.42 23.22 1.86 o -15 3 1 0.57 -0.17 0.54 o -14 3 1 10.44 8.73 0.82 o -13 3 1 11.04 9.43 0.91 o -12 3 1 169.93 167.95 2.79 o -11 3 1 5.08 4.40 0.58 o -10 3 1 381.77 374.67 4.73 o -9 3 1 129.60 130.86 2.26 o -8 3 1 53.20 52.84 1.23 o -7 3 1 198.75 198.04 2.57 o -6 3 1 773.77 764.11 6.61 o -5 3 1 99.03 106.38 1.50 o -4 3 1 4.52 5.80 0.28 o -3 3 1 447.98 472.08 3.83 o -2 3 1 608.24 586.53 5.55 o -1 3 1 19.46 19.01 0.49 o 0 3 1 0.76 0.46 0.27 o 1 3 1 132.21 128.66 1.87 o 2 3 1 1251.44 1291.85 9.45 o 3 3 1 318.21 332.09 2.85 o 4 3 1 543.12 557.54 4.73 o 5 3 1 392.14 399.97 3.99 o 6 3 1 208.70 212.66 2.47 o 7 3 1 271.81 266.46 3.06 o 8 3 1 1009.51 1009.76 8.62 o 9 3 1 598.37 594.09 5.89 o 10 3 1 296.00 286.60 3.51 o 11 3 1 3.71 1.90 0.52 o 12 3 1 101.13 101.43 2.36 o 13 3 1 126.73 124.78 2.91 o 14 3 1 286.95 294.26 4.51 o 15 3 1 1.08 0.88 0.64 o 16 3 1 0.09 0.01 0.71 o 17 3 1 14.47 12.21 1.85 o 18 3 1 103.99 108.41 4.42 o -16 4 1 0.88 0.19 0.80 o -15 4 1 118.92 120.33 3.19 o -14 4 1 105.80 107.83 2.92 o -13 4 1 0.01 -0.49 0.61 o -12 4 1 68.20 66.60 2.12 o -11 4 1 133.06 122.59 3.03 o -10 4 1 125.96 127.44 3.13 o -9 4 1 21.43 19.24 1.01 o -8 4 1 272.86 279.69 4.19 o -7 4 1 0.36 0.37 0.35 o -6 4 1 54.14 51.79 1.67 o -5 4 1 36.72 36.21 0.98 o -4 4 1 480.55 491.05 5.89 o -3 4 1 10.37 11.07 1.25 o -2 4 1 0.64 0.87 0.36 o -1 4 1 111.02 113.65 2.36 o 0 4 1 607.10 619.64 8.91 o 1 4 1 38.52 39.09 1.09 o 2 4 1 88.85 93.07 1.64 o 3 4 1 175.08 180.12 2.90 o 4 4 1 403.02 399.92 4.72 o 5 4 1 81.34 80.22 1.54 o 6 4 1 355.07 356.69 4.02 o 7 4 1 368.63 373.49 4.31 o 8 4 1 25.58 24.74 1.40 o 9 4 1 4.56 4.38 0.67 o 10 4 1 258.95 254.58 4.34 o 11 4 1 46.27 47.45 2.28 o 12 4 1 51.57 52.22 2.22 o 13 4 1 0.04 0.10 0.59 o 14 4 1 19.74 19.97 1.46 o 15 4 1 1.24 0.63 0.80 o 16 4 1 49.72 52.03 2.26 o -13 5 1 26.17 25.22 1.58 o -12 5 1 16.84 15.42 1.29 o -11 5 1 13.99 13.13 1.15 o -10 5 1 11.94 9.83 0.99 o -9 5 1 63.63 61.02 2.18 o -8 5 1 3.93 4.58 0.70 o -7 5 1 279.78 273.02 4.24 o -6 5 1 0.16 -0.05 0.45 o -5 5 1 16.14 16.01 0.84 o -4 5 1 3.42 2.71 0.80 o -3 5 1 223.16 215.98 3.92 o -2 5 1 23.43 22.28 3.61 o -1 5 1 158.62 160.11 8.15 o 0 5 1 147.62 154.73 4.56 o 1 5 1 1.11 1.80 1.15 o 2 5 1 0.00 -0.78 0.51 o 3 5 1 10.04 10.07 0.73 o 4 5 1 164.42 170.27 2.79 o 5 5 1 0.30 0.97 0.69 o 6 5 1 1.16 0.35 0.48 o 7 5 1 1.64 0.44 0.55 o 8 5 1 107.96 112.54 2.56 o 9 5 1 10.39 7.98 0.92 o 10 5 1 1.19 0.89 0.63 o 11 5 1 8.37 7.78 0.99 o 12 5 1 121.17 127.56 3.18 o 13 5 1 8.05 5.11 0.97 o -8 6 1 62.67 61.72 1.89 o -7 6 1 15.53 13.16 0.94 o -6 6 1 1.69 1.31 0.53 o -5 6 1 170.12 173.02 4.63 o -4 6 1 50.36 55.83 3.08 o -3 6 1 2.13 2.10 1.04 o -2 6 1 0.45 -0.03 0.69 o 2 6 1 4.35 4.72 0.97 o 3 6 1 24.13 26.56 2.13 o 4 6 1 4.67 3.67 1.03 o 5 6 1 58.26 58.53 2.16 o 6 6 1 3.66 3.20 0.60 o 7 6 1 0.07 0.81 0.58 o -20 0 2 12.15 9.26 1.54 o -18 0 2 170.09 169.42 4.66 o -16 0 2 144.17 140.15 3.03 o -14 0 2 647.79 669.20 12.15 o -12 0 2 505.08 530.69 6.94 o -10 0 2 1786.05 1845.16 16.68 o -8 0 2 2179.08 2315.41 18.59 o -6 0 2 1069.61 1143.53 10.13 o -4 0 2 2919.94 2974.79 33.07 o -2 0 2 279.85 286.56 5.90 o 0 0 2 2385.72 2219.45 47.61 o 2 0 2 1013.64 982.82 9.45 o 4 0 2 1280.18 1346.92 11.25 o 6 0 2 419.57 475.17 3.88 o 8 0 2 472.25 485.81 4.28 o 10 0 2 135.62 98.87 1.90 o 12 0 2 2247.28 2106.68 23.84 o 14 0 2 8.37 6.82 0.90 o 16 0 2 1511.70 1583.25 45.07 o 18 0 2 239.69 248.14 6.69 o 20 0 2 189.77 204.54 7.39 o -21 1 2 18.50 18.41 2.98 o -20 1 2 5.78 4.56 0.93 o -19 1 2 12.35 11.95 1.18 o -18 1 2 154.04 151.58 3.67 o -17 1 2 0.15 0.64 0.60 o -16 1 2 8.29 6.79 0.64 o -15 1 2 101.42 105.09 1.97 o -14 1 2 118.75 118.88 2.46 o -13 1 2 37.31 30.96 0.90 o -12 1 2 0.33 0.66 0.24 o -11 1 2 331.06 304.25 2.52 o -10 1 2 23.22 19.08 0.51 o -9 1 2 44.29 53.37 0.79 o -8 1 2 7.98 7.46 0.30 o -7 1 2 10.63 5.84 0.24 o -6 1 2 579.25 582.36 3.53 o -5 1 2 2630.55 2735.63 15.57 o -4 1 2 1691.28 1620.50 10.17 o -3 1 2 328.83 317.70 2.63 o -2 1 2 3265.49 3255.84 20.70 o -1 1 2 14666.66 12014.26 99.19 o 0 1 2 11088.25 9681.39 85.02 o 1 1 2 4230.49 4176.54 25.58 o 2 1 2 342.90 340.67 2.23 o 3 1 2 5211.09 4969.34 28.05 o 4 1 2 5098.17 5014.06 27.78 o 5 1 2 866.71 925.33 5.20 o 6 1 2 2.62 5.95 0.22 o 7 1 2 1484.95 1488.50 7.90 o 8 1 2 1287.05 1318.64 7.49 o 9 1 2 183.73 202.06 1.72 o 10 1 2 4.82 1.82 0.22 o 11 1 2 449.50 453.73 3.46 o 12 1 2 639.26 631.47 5.10 o 13 1 2 34.25 35.75 1.00 o 14 1 2 41.56 39.12 1.23 o 15 1 2 40.16 41.05 1.29 o 16 1 2 98.81 96.19 3.39 o 17 1 2 37.54 33.84 1.85 o 18 1 2 112.70 121.09 4.64 o 19 1 2 43.52 43.65 2.15 o 20 1 2 29.38 36.70 4.89 o -20 2 2 0.34 -1.20 1.85 o -19 2 2 22.28 22.15 1.81 o -18 2 2 56.57 56.41 2.81 o -17 2 2 295.21 301.78 6.11 o -16 2 2 227.28 232.57 5.01 o -15 2 2 98.95 94.93 2.41 o -14 2 2 31.98 36.70 1.09 o -13 2 2 1237.49 1235.27 10.99 o -12 2 2 97.76 84.44 1.62 o -11 2 2 153.80 154.62 2.36 o -10 2 2 218.69 210.82 2.46 o -9 2 2 3280.97 3177.09 23.92 o -8 2 2 251.39 259.35 2.88 o -7 2 2 5.52 9.24 0.51 o -6 2 2 106.34 112.91 1.08 o -5 2 2 5088.01 5075.44 29.08 o -4 2 2 236.98 243.60 1.81 o -3 2 2 133.72 153.13 1.40 o -2 2 2 554.32 608.93 4.36 o -1 2 2 3319.78 3381.50 21.73 o 0 2 2 126.57 128.73 1.19 o 1 2 2 82.79 108.44 1.09 o 2 2 2 694.26 751.41 5.03 o 3 2 2 359.40 383.18 2.46 o 4 2 2 38.40 35.30 0.42 o 5 2 2 2.11 4.29 0.21 o 6 2 2 718.51 731.10 4.69 o 7 2 2 39.79 46.29 0.77 o 8 2 2 62.88 64.50 0.97 o 9 2 2 48.33 50.26 0.90 o 10 2 2 98.18 97.81 1.52 o 11 2 2 239.52 243.25 3.02 o 12 2 2 33.72 33.56 1.13 o 13 2 2 147.17 149.26 2.30 o 14 2 2 3.01 2.29 0.61 o 15 2 2 187.66 190.98 3.83 o 16 2 2 6.91 6.64 0.92 o 17 2 2 127.77 132.58 3.67 o 18 2 2 0.69 1.48 0.87 o 19 2 2 60.10 61.85 3.11 o -19 3 2 0.00 -0.35 1.33 o -18 3 2 88.62 88.01 3.95 o -17 3 2 107.33 110.64 5.75 o -16 3 2 37.19 35.73 1.52 o -15 3 2 55.24 52.50 1.76 o -14 3 2 68.10 66.54 2.72 o -13 3 2 59.67 57.94 1.79 o -12 3 2 171.38 175.32 2.86 o -11 3 2 375.38 362.20 4.75 o -10 3 2 9.21 8.04 0.69 o -9 3 2 185.77 183.65 2.79 o -8 3 2 896.32 884.89 9.02 o -7 3 2 120.20 117.54 1.93 o -6 3 2 67.25 67.60 1.11 o -5 3 2 558.23 576.16 5.04 o -4 3 2 1118.85 1132.07 7.86 o -3 3 2 3.01 2.57 0.40 o -2 3 2 53.21 56.37 0.68 o -1 3 2 686.02 675.82 5.50 o 0 3 2 427.44 413.71 4.18 o 1 3 2 1.13 1.77 0.33 o 2 3 2 256.22 273.60 2.65 o 3 3 2 1112.62 1122.84 8.15 o 4 3 2 619.83 626.94 5.01 o 5 3 2 153.43 153.64 1.82 o 6 3 2 514.34 515.30 5.58 o 7 3 2 403.82 403.62 3.95 o 8 3 2 855.00 828.96 8.09 o 9 3 2 182.89 181.97 2.70 o 10 3 2 125.22 129.29 2.47 o 11 3 2 55.67 52.10 1.44 o 12 3 2 219.26 212.68 3.92 o 13 3 2 73.07 66.84 2.13 o 14 3 2 78.17 79.69 2.12 o 15 3 2 0.12 0.40 0.61 o 16 3 2 27.66 23.87 1.55 o 17 3 2 28.33 27.40 2.37 o 18 3 2 79.29 78.77 3.83 o -17 4 2 1.30 0.35 0.89 o -16 4 2 39.79 41.63 2.04 o -15 4 2 46.02 47.76 2.07 o -14 4 2 31.91 28.72 1.62 o -13 4 2 9.87 7.99 1.00 o -12 4 2 95.42 94.87 2.53 o -11 4 2 4.63 3.82 0.75 o -10 4 2 28.04 29.01 1.33 o -9 4 2 72.62 70.53 1.66 o -8 4 2 20.70 19.41 0.91 o -7 4 2 130.30 135.44 2.84 o -6 4 2 138.28 138.02 2.32 o -5 4 2 26.06 24.47 1.05 o -4 4 2 2.28 1.52 0.56 o -3 4 2 535.59 545.71 5.81 o -2 4 2 325.29 334.58 3.37 o -1 4 2 19.61 21.48 1.31 o 0 4 2 61.45 63.85 2.14 o 1 4 2 577.23 590.87 6.60 o 2 4 2 0.34 0.86 0.38 o 3 4 2 75.77 72.61 1.30 o 4 4 2 112.94 121.66 1.92 o 5 4 2 390.83 389.92 4.55 o 6 4 2 4.52 4.49 1.09 o 7 4 2 95.69 93.96 1.99 o 8 4 2 669.36 690.65 7.17 o 9 4 2 171.86 171.54 3.07 o 10 4 2 200.55 202.60 4.16 o 11 4 2 99.34 101.40 2.91 o 12 4 2 125.40 130.76 3.11 o 13 4 2 12.59 11.95 1.17 o 14 4 2 53.55 57.01 2.19 o 15 4 2 29.88 27.31 1.74 o 16 4 2 26.10 23.72 1.73 o -13 5 2 47.06 44.70 1.94 o -12 5 2 66.10 63.17 2.16 o -11 5 2 157.57 160.34 3.43 o -10 5 2 6.87 6.28 0.87 o -9 5 2 189.87 190.69 4.02 o -8 5 2 18.59 19.48 1.30 o -7 5 2 710.75 730.80 9.74 o -6 5 2 23.89 24.36 1.26 o -5 5 2 13.38 12.77 0.93 o -4 5 2 0.15 -0.50 0.45 o -3 5 2 527.32 547.74 8.34 o -2 5 2 17.66 19.93 1.35 o -1 5 2 12.69 12.08 0.98 o 0 5 2 5.52 6.01 1.30 o 1 5 2 20.06 21.13 1.16 o 2 5 2 40.08 37.54 1.51 o 3 5 2 58.98 60.97 1.33 o 4 5 2 91.87 94.60 2.29 o 5 5 2 2.86 2.53 0.55 o 6 5 2 0.07 0.35 0.49 o 7 5 2 72.93 73.35 1.97 o 8 5 2 119.48 119.11 3.32 o 9 5 2 3.53 3.87 0.80 o 10 5 2 95.93 94.09 2.54 o 11 5 2 44.42 44.39 1.85 o 12 5 2 1.21 0.52 0.71 o 13 5 2 42.20 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