#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220698.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220698_Fobs loop_ _publ_author_name 'Zhao, Pei-Zheng' 'Yan, Feng-Mei' 'Wang, Jian-Ge' _publ_section_title ; Aqua(2,9-dimethyl-1,10-phenanthroline-\k^2^N,N')bis(2-hydroxybenzoato-\kO)manganese(II) 2,9-dimethyl-1,10-phenanthroline hemisolvate ; _journal_coeditor_code BH2207 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m194 _journal_page_last m195 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.342 _cell_angle_gamma 90.000 _cell_length_a 23.2250 _cell_length_b 19.6902 _cell_length_c 14.0225 _exptl_crystal_F_000 2736.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file bh2207Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 716.46 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 126304.69 114839.16 1119.25 o 6 0 0 513316.03 526735.31 7581.08 o 8 0 0 3007.97 3537.61 58.53 o 10 0 0 4729.37 5107.02 56.09 o 12 0 0 65893.07 69350.30 775.04 o 14 0 0 591.84 564.40 32.83 o 16 0 0 1209.76 1236.79 46.21 o 18 0 0 3865.11 3941.15 109.59 o 20 0 0 1413.26 1370.15 57.69 o 22 0 0 538.51 583.57 43.54 o 24 0 0 157.96 171.02 32.28 o 26 0 0 8.93 3.71 53.46 o 28 0 0 42.35 51.34 31.42 o 3 1 0 14215.18 16262.96 131.97 o 5 1 0 12830.55 14147.04 107.54 o 7 1 0 390.65 773.84 32.32 o 9 1 0 26357.47 26079.44 172.17 o 11 1 0 2.53 -0.47 4.42 o 13 1 0 5589.22 5953.52 116.71 o 15 1 0 2028.10 1949.71 39.15 o 17 1 0 343.65 421.76 37.89 o 19 1 0 158.52 174.52 19.98 o 21 1 0 844.06 871.56 34.72 o 23 1 0 64.09 53.11 18.33 o 25 1 0 243.90 278.73 26.64 o 27 1 0 72.38 115.03 24.00 o 2 2 0 10986.05 12153.41 126.93 o 4 2 0 6426.14 5686.52 42.40 o 6 2 0 147769.98 150143.63 866.94 o 8 2 0 15593.24 15824.95 98.13 o 10 2 0 1116.78 930.61 20.16 o 12 2 0 16.20 -5.69 12.68 o 14 2 0 81.21 100.48 16.58 o 16 2 0 102.92 125.99 16.62 o 18 2 0 436.42 405.58 23.50 o 20 2 0 696.41 547.30 27.96 o 22 2 0 300.43 293.20 24.54 o 24 2 0 74.75 82.26 19.96 o 26 2 0 77.58 94.87 22.87 o 1 3 0 33788.11 31893.75 196.26 o 3 3 0 16037.29 17904.35 134.40 o 5 3 0 1090.17 1023.80 21.68 o 7 3 0 6360.77 6632.33 47.23 o 9 3 0 1050.91 1129.84 15.85 o 11 3 0 1587.38 1774.55 21.50 o 13 3 0 2688.55 2670.93 28.73 o 15 3 0 145.50 118.91 14.28 o 17 3 0 8.21 17.72 12.83 o 19 3 0 159.40 171.29 19.38 o 21 3 0 93.61 75.42 18.85 o 23 3 0 30.90 24.99 17.36 o 25 3 0 27.69 -11.56 17.45 o 27 3 0 1.23 -22.98 20.99 o 0 4 0 581.28 356.46 11.42 o 2 4 0 5030.50 6172.15 41.43 o 4 4 0 5930.47 6470.49 44.69 o 6 4 0 2444.78 2314.85 22.58 o 8 4 0 416.61 391.35 10.20 o 10 4 0 1653.32 1521.79 20.00 o 12 4 0 979.36 967.07 18.69 o 14 4 0 250.89 266.77 12.86 o 16 4 0 229.80 245.96 18.19 o 18 4 0 224.72 265.11 20.58 o 20 4 0 60.28 47.43 21.45 o 22 4 0 2.18 2.87 15.58 o 24 4 0 49.81 81.40 20.18 o 26 4 0 8.08 -26.14 17.43 o 1 5 0 3558.92 2212.16 20.31 o 3 5 0 4993.68 5886.14 42.00 o 5 5 0 172.61 191.28 7.18 o 7 5 0 480.78 378.34 13.53 o 9 5 0 8296.60 8630.67 62.62 o 11 5 0 232.78 151.66 8.37 o 13 5 0 2525.66 2415.72 32.04 o 15 5 0 1867.79 2168.86 41.98 o 17 5 0 404.65 370.83 21.66 o 19 5 0 80.65 82.57 17.74 o 21 5 0 603.65 621.28 31.71 o 23 5 0 12.48 3.71 25.69 o 25 5 0 149.37 208.15 33.72 o 27 5 0 73.02 114.43 23.62 o 0 6 0 70139.57 74357.27 742.56 o 2 6 0 29969.86 31721.40 183.24 o 4 6 0 7.02 26.96 4.67 o 6 6 0 780.84 1183.18 17.14 o 8 6 0 2210.48 2033.30 23.94 o 10 6 0 579.98 556.13 21.68 o 12 6 0 4325.89 4246.65 44.11 o 14 6 0 118.84 180.83 13.22 o 16 6 0 438.78 318.73 20.19 o 18 6 0 2291.92 2392.00 48.84 o 20 6 0 1016.48 877.91 38.86 o 22 6 0 317.21 317.77 25.63 o 24 6 0 278.13 245.07 25.37 o 26 6 0 14.69 23.11 19.64 o 1 7 0 607.44 463.10 11.08 o 3 7 0 595.14 990.76 15.48 o 5 7 0 216.59 204.38 8.38 o 7 7 0 1081.41 1059.18 17.89 o 9 7 0 1254.44 1134.53 19.54 o 11 7 0 82.37 70.77 8.24 o 13 7 0 7802.15 7993.61 65.09 o 15 7 0 403.86 358.90 20.48 o 17 7 0 2.66 -10.74 12.81 o 19 7 0 552.52 584.30 28.70 o 21 7 0 299.73 304.21 28.94 o 23 7 0 29.17 23.19 18.64 o 25 7 0 183.56 173.73 24.38 o 0 8 0 48460.12 52088.75 419.06 o 2 8 0 26.61 107.44 7.69 o 4 8 0 0.17 -7.63 5.09 o 6 8 0 12456.23 13971.56 93.32 o 8 8 0 17.76 -4.96 6.19 o 10 8 0 1394.11 1355.09 37.57 o 12 8 0 712.45 734.88 31.72 o 14 8 0 690.44 742.25 28.26 o 16 8 0 71.14 64.94 15.35 o 18 8 0 5.21 -3.55 13.99 o 20 8 0 229.91 205.81 22.04 o 22 8 0 1.28 -10.48 16.14 o 24 8 0 63.08 50.78 21.99 o 26 8 0 11.72 -16.74 19.06 o 1 9 0 4648.02 5789.18 47.62 o 3 9 0 30121.34 32863.92 195.26 o 5 9 0 1308.08 1691.27 23.14 o 7 9 0 5067.83 5904.06 50.35 o 9 9 0 2866.01 3063.08 34.68 o 11 9 0 45.10 42.32 8.78 o 13 9 0 3704.59 3971.47 43.30 o 15 9 0 1696.92 1772.80 33.80 o 17 9 0 177.63 94.45 17.31 o 19 9 0 661.32 646.39 30.04 o 21 9 0 111.55 95.83 19.42 o 23 9 0 0.31 -2.65 19.75 o 25 9 0 52.08 54.02 24.09 o 0 10 0 9270.91 9209.06 95.25 o 2 10 0 205.94 326.85 15.54 o 4 10 0 1295.95 1252.88 20.60 o 6 10 0 1709.66 1374.22 22.02 o 8 10 0 1730.66 1697.33 25.80 o 10 10 0 5957.32 6428.36 56.77 o 12 10 0 2367.55 2370.13 32.89 o 14 10 0 264.48 263.23 16.32 o 16 10 0 4143.43 3922.69 61.80 o 18 10 0 355.20 493.19 26.51 o 20 10 0 191.00 127.32 19.93 o 22 10 0 298.01 233.55 24.53 o 24 10 0 68.58 88.27 25.73 o 1 11 0 14389.67 13955.99 95.58 o 3 11 0 13624.43 13006.63 90.98 o 5 11 0 1144.01 835.29 18.40 o 7 11 0 1836.58 1413.80 23.82 o 9 11 0 5189.11 5211.08 50.26 o 11 11 0 2949.30 2685.59 35.13 o 13 11 0 2750.85 2779.03 38.41 o 15 11 0 4420.17 4310.99 56.83 o 17 11 0 290.87 306.04 21.86 o 19 11 0 221.25 142.83 23.18 o 21 11 0 404.49 435.63 33.20 o 23 11 0 13.30 28.53 21.57 o 0 12 0 5304.67 6337.51 76.91 o 2 12 0 3519.64 3320.17 36.24 o 4 12 0 12.61 25.11 10.36 o 6 12 0 3839.86 3835.15 40.96 o 8 12 0 356.10 330.66 13.82 o 10 12 0 1074.46 1203.00 27.08 o 12 12 0 3499.93 3391.53 42.24 o 14 12 0 431.60 528.80 21.44 o 16 12 0 883.69 800.32 35.76 o 18 12 0 1173.21 978.45 41.93 o 20 12 0 0.72 4.98 19.93 o 22 12 0 71.38 70.98 47.10 o 24 12 0 106.20 144.62 28.31 o 1 13 0 1879.21 1989.98 44.99 o 3 13 0 916.38 953.67 23.39 o 5 13 0 10.09 28.11 8.23 o 7 13 0 141.29 227.14 12.58 o 9 13 0 511.48 452.55 18.49 o 11 13 0 199.73 274.07 18.46 o 13 13 0 195.95 145.15 14.63 o 15 13 0 60.79 74.57 16.02 o 17 13 0 7.51 22.61 18.41 o 19 13 0 0.11 -7.92 18.09 o 21 13 0 33.54 12.06 21.41 o 23 13 0 3.58 -11.95 27.78 o 0 14 0 1.62 -2.58 12.01 o 2 14 0 2929.99 3435.12 39.66 o 4 14 0 1060.33 975.15 21.83 o 6 14 0 16.41 -4.51 9.42 o 8 14 0 101.12 109.18 12.95 o 10 14 0 4.54 15.69 11.33 o 12 14 0 964.20 979.64 27.81 o 14 14 0 49.11 35.08 14.66 o 16 14 0 3.13 13.06 17.52 o 18 14 0 51.45 51.86 20.28 o 20 14 0 63.74 98.01 33.41 o 22 14 0 12.21 -7.90 28.34 o 1 15 0 805.55 1073.35 27.73 o 3 15 0 469.00 330.64 17.05 o 5 15 0 1158.35 1187.62 28.28 o 7 15 0 226.02 281.89 16.76 o 9 15 0 921.88 948.21 26.97 o 11 15 0 370.29 298.38 18.12 o 13 15 0 205.44 357.65 19.51 o 15 15 0 901.81 1109.23 47.24 o 17 15 0 236.90 293.28 48.38 o 19 15 0 67.05 108.76 45.17 o 21 15 0 220.12 212.17 39.12 o 0 16 0 352.23 334.57 27.74 o 2 16 0 484.71 544.63 24.00 o 4 16 0 437.11 501.86 20.24 o 6 16 0 874.86 657.58 24.70 o 8 16 0 1358.52 1301.73 34.00 o 10 16 0 1632.73 1920.03 42.00 o 12 16 0 1203.86 1341.48 32.98 o 14 16 0 73.98 71.72 31.48 o 16 16 0 425.40 425.15 42.50 o 18 16 0 39.41 9.08 26.87 o 20 16 0 57.98 94.05 33.45 o 1 17 0 801.13 659.02 30.86 o 3 17 0 4541.61 4480.59 63.99 o 5 17 0 2299.43 2088.18 43.81 o 7 17 0 67.61 69.39 14.04 o 9 17 0 2394.31 2284.17 47.11 o 11 17 0 264.88 277.92 21.44 o 13 17 0 700.77 689.95 30.03 o 15 17 0 495.35 515.60 33.62 o 17 17 0 23.14 10.52 25.55 o 19 17 0 143.57 126.70 53.99 o 0 18 0 277.44 448.47 51.59 o 2 18 0 0.61 12.73 20.22 o 4 18 0 16.94 -1.01 13.86 o 6 18 0 36.84 55.59 18.81 o 8 18 0 9.74 9.22 16.93 o 10 18 0 44.67 56.12 18.61 o 12 18 0 402.63 540.63 27.73 o 14 18 0 113.42 129.04 23.41 o 16 18 0 195.41 248.02 35.91 o 18 18 0 38.08 63.00 55.87 o 1 19 0 33.08 10.16 18.52 o 3 19 0 0.14 3.61 17.06 o 5 19 0 212.00 279.01 37.92 o 7 19 0 46.66 31.29 19.72 o 9 19 0 53.32 34.36 18.82 o 11 19 0 10.84 12.08 18.46 o 13 19 0 65.55 32.19 24.76 o 15 19 0 54.42 134.66 30.01 o 0 20 0 1424.52 1411.86 79.65 o 2 20 0 162.34 221.37 29.67 o 4 20 0 573.75 668.63 36.58 o 6 20 0 967.70 923.89 40.80 o 8 20 0 186.03 107.87 31.22 o 10 20 0 46.66 41.72 19.55 o 12 20 0 272.40 193.15 31.73 o 14 20 0 130.91 142.36 30.62 o 1 21 0 187.05 248.93 33.27 o 3 21 0 535.39 458.50 38.71 o 5 21 0 71.58 101.04 28.35 o 7 21 0 116.46 86.83 26.55 o 9 21 0 241.74 182.15 25.19 o 11 21 0 28.24 20.65 21.72 o 13 21 0 171.48 160.61 32.70 o 0 22 0 949.09 1025.89 74.84 o 2 22 0 20.23 35.28 25.71 o 4 22 0 459.97 473.90 54.53 o 6 22 0 474.35 477.96 41.39 o 8 22 0 186.92 221.93 35.55 o 10 22 0 155.58 184.52 32.04 o 1 23 0 109.02 152.68 30.34 o 3 23 0 338.22 326.15 39.56 o 5 23 0 45.43 30.96 30.20 o 7 23 0 2.04 -25.07 28.60 o -27 1 1 4.44 33.39 21.51 o -25 1 1 469.48 399.81 29.76 o -23 1 1 4.25 -11.29 20.91 o -21 1 1 29.25 39.89 16.97 o -19 1 1 7270.49 7391.87 92.16 o -17 1 1 48.58 70.41 15.03 o -15 1 1 183.16 168.07 15.98 o -13 1 1 111841.49 118301.23 1193.68 o -11 1 1 137.35 160.66 8.05 o -9 1 1 12782.72 11963.70 78.36 o -7 1 1 493187.53 484926.25 2752.09 o -5 1 1 14926.51 16349.10 97.27 o -3 1 1 2549.53 2072.09 20.40 o 3 1 1 1230.25 898.06 14.35 o 5 1 1 22570.63 26332.20 239.68 o 7 1 1 761.35 764.55 36.43 o 9 1 1 8555.63 8982.94 82.50 o 11 1 1 63.60 112.67 11.45 o 13 1 1 180.34 126.22 13.52 o 15 1 1 648.38 608.98 24.11 o 17 1 1 0.98 -15.82 16.51 o 19 1 1 76.34 39.71 16.32 o 21 1 1 362.79 379.81 25.96 o 23 1 1 10.19 29.22 17.83 o 25 1 1 12.08 -0.27 17.56 o 27 1 1 31.07 22.76 20.20 o -28 2 1 40.09 32.02 21.31 o -26 2 1 2.20 -3.80 19.00 o -24 2 1 423.30 417.69 28.89 o -22 2 1 658.15 701.88 54.63 o -20 2 1 555.47 484.29 39.51 o -18 2 1 4930.74 4832.80 82.72 o -16 2 1 4057.88 3752.05 56.31 o -14 2 1 1.26 14.06 11.53 o -12 2 1 24548.08 24434.66 150.69 o -10 2 1 15253.34 16480.05 109.64 o -8 2 1 22.81 4.41 4.52 o -6 2 1 4168.12 4057.29 38.09 o -4 2 1 7781.16 8575.17 54.20 o -2 2 1 6399.37 6503.64 50.75 o 0 2 1 18468.54 21532.16 152.70 o 2 2 1 35110.84 38755.78 239.67 o 4 2 1 8.63 26.52 5.27 o 6 2 1 1996.71 1893.74 21.14 o 8 2 1 24320.95 24617.09 231.47 o 10 2 1 1989.99 2428.33 28.16 o 12 2 1 2489.24 2380.50 38.98 o 14 2 1 919.97 914.69 27.63 o 16 2 1 1639.84 1534.52 36.37 o 18 2 1 1369.31 1491.72 61.19 o 20 2 1 1029.04 1047.49 48.30 o 22 2 1 102.92 77.75 18.76 o 24 2 1 178.15 157.08 22.55 o 26 2 1 0.26 -6.61 17.69 o -27 3 1 117.42 154.16 24.79 o -25 3 1 167.40 181.99 23.89 o -23 3 1 3.73 -0.29 16.76 o -21 3 1 454.45 479.06 38.43 o -19 3 1 83.95 101.88 19.15 o -17 3 1 426.10 339.10 21.11 o -15 3 1 5825.28 5499.01 69.99 o -13 3 1 30.38 22.06 10.91 o -11 3 1 1820.78 1789.80 22.68 o -9 3 1 15859.51 15653.34 134.27 o -7 3 1 2759.11 3590.64 43.47 o -5 3 1 1025.08 1449.90 17.54 o -3 3 1 1453.06 1125.41 13.92 o -1 3 1 20807.53 24151.87 196.23 o 1 3 1 6341.96 7917.95 61.15 o 3 3 1 97.30 224.21 9.52 o 5 3 1 13013.04 12613.21 78.43 o 7 3 1 19.28 4.38 3.72 o 9 3 1 15182.50 14304.02 91.79 o 11 3 1 3189.14 3156.64 109.22 o 13 3 1 2586.47 2549.08 32.52 o 15 3 1 5384.33 4805.34 64.24 o 17 3 1 708.52 722.78 28.25 o 19 3 1 680.47 818.30 31.75 o 21 3 1 966.73 1030.92 59.97 o 23 3 1 94.76 86.93 19.68 o 25 3 1 51.66 23.02 27.93 o 27 3 1 73.64 53.10 22.22 o -26 4 1 0.48 30.42 24.46 o -24 4 1 59.93 56.28 19.32 o -22 4 1 41.38 60.78 19.18 o -20 4 1 180.12 164.99 25.31 o -18 4 1 332.10 252.72 20.32 o -16 4 1 1498.68 1485.83 36.44 o -14 4 1 10.58 7.32 6.59 o -12 4 1 1498.79 1568.19 22.54 o -10 4 1 1101.46 1167.16 18.13 o -8 4 1 649.72 760.23 16.94 o -6 4 1 104.03 166.52 6.64 o -4 4 1 9343.44 9699.28 62.31 o -2 4 1 64.72 30.10 4.75 o 0 4 1 209056.48 210732.94 1296.20 o 2 4 1 80522.06 88395.20 489.63 o 4 4 1 54.34 81.19 6.56 o 6 4 1 26.82 59.01 4.89 o 8 4 1 9604.34 12093.61 105.35 o 10 4 1 4089.99 4119.88 36.12 o 12 4 1 1131.69 990.15 16.57 o 14 4 1 513.58 552.84 24.23 o 16 4 1 2127.52 1993.77 41.85 o 18 4 1 1316.95 1390.78 38.43 o 20 4 1 153.58 183.45 21.40 o 22 4 1 2.60 -22.16 14.78 o 24 4 1 64.20 38.78 19.04 o 26 4 1 1.83 9.83 18.24 o -27 5 1 3.17 -28.59 19.06 o -25 5 1 10.26 16.52 19.34 o -23 5 1 0.58 -18.10 16.05 o -21 5 1 444.80 322.01 24.40 o -19 5 1 27.44 15.07 15.25 o -17 5 1 784.61 760.59 28.89 o -15 5 1 211.85 191.95 12.88 o -13 5 1 15.41 23.78 7.08 o -11 5 1 57.30 37.80 6.61 o -9 5 1 560.83 418.43 14.98 o -7 5 1 376.28 410.72 10.60 o -5 5 1 3374.39 3704.59 34.10 o -3 5 1 4805.75 5288.28 38.48 o -1 5 1 77448.03 82426.23 497.94 o 1 5 1 6659.80 6252.35 43.38 o 3 5 1 29875.54 30455.19 175.95 o 5 5 1 594.07 599.49 11.64 o 7 5 1 795.95 945.31 15.56 o 9 5 1 2119.72 2065.52 23.89 o 11 5 1 3040.34 3086.59 31.50 o 13 5 1 1398.83 1378.81 25.08 o 15 5 1 154.66 142.24 15.29 o 17 5 1 326.86 315.06 23.56 o 19 5 1 612.51 648.37 29.17 o 21 5 1 98.96 68.47 19.54 o 23 5 1 0.02 -21.85 14.57 o 25 5 1 10.10 -14.36 17.82 o 27 5 1 8.88 -16.00 19.27 o -26 6 1 14.03 0.41 31.33 o -24 6 1 83.30 79.36 20.89 o -22 6 1 305.59 304.79 24.92 o -20 6 1 8.34 2.45 15.23 o -18 6 1 88.95 142.11 18.61 o -16 6 1 204.26 178.48 17.34 o -14 6 1 197.89 190.09 13.59 o -12 6 1 51.59 66.25 8.02 o -10 6 1 19.16 6.77 5.86 o -8 6 1 3085.98 3166.85 31.27 o -6 6 1 609.60 1165.96 27.21 o -4 6 1 1426.21 1075.00 16.49 o -2 6 1 4442.02 4961.53 37.45 o 0 6 1 21917.41 24995.47 152.09 o 2 6 1 13273.47 13446.31 84.72 o 4 6 1 1263.34 1330.48 18.57 o 6 6 1 2052.42 2427.15 25.56 o 8 6 1 900.80 1109.43 17.99 o 10 6 1 1791.52 1564.36 22.12 o 12 6 1 12.63 7.25 6.51 o 14 6 1 327.72 287.10 19.14 o 16 6 1 11.32 4.93 12.25 o 18 6 1 379.03 379.47 23.82 o 20 6 1 314.20 363.32 25.53 o 22 6 1 132.63 116.80 26.77 o 24 6 1 55.99 27.23 19.03 o 26 6 1 0.04 -30.68 20.45 o -25 7 1 266.67 304.66 27.49 o -23 7 1 17.35 23.16 17.49 o -21 7 1 1303.23 1391.55 46.45 o -19 7 1 596.28 716.12 31.26 o -17 7 1 102.93 62.01 16.20 o -15 7 1 1424.26 1376.56 29.83 o -13 7 1 2152.35 2248.10 29.99 o -11 7 1 496.80 604.99 16.04 o -9 7 1 12411.45 12622.11 87.27 o -7 7 1 258.65 297.99 11.37 o -5 7 1 5356.38 5495.57 43.57 o -3 7 1 581.89 539.53 18.47 o -1 7 1 63968.11 65681.89 368.00 o 1 7 1 5407.33 5860.43 44.16 o 3 7 1 31530.23 30646.73 180.02 o 5 7 1 2016.21 1891.53 22.56 o 7 7 1 4534.22 5140.76 43.77 o 9 7 1 7960.77 7289.48 57.72 o 11 7 1 10842.35 10947.65 80.07 o 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