#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220699.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220699_Fobs loop_ _publ_author_name 'Belandria, Lusbely M.' 'Delgado, Gerzon E.' 'Mora, Asilo\'e J.' 'Seijas, Luis E.' 'Gonz\'alez, Teresa' _publ_section_title ; Redetermination of 1-carboxycyclohexan-1-aminium chloride ; _journal_coeditor_code BH2212 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o245 _journal_volume 65 _journal_year 2009 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.239 _cell_angle_gamma 90.000 _cell_length_a 7.3818 _cell_length_b 6.3568 _cell_length_c 9.3740 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bh2212Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ACC6-Cl en P21/m' _shelx_refln_list_code 4 _shelx_F_calc_maximum 59.40 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 380.14 368.45 1.60 o 2 0 0 523.99 491.84 2.35 o 3 0 0 20.75 22.83 0.68 o 4 0 0 7.64 8.13 0.74 o 5 0 0 97.78 94.57 1.51 o 6 0 0 218.96 216.00 6.02 o 7 0 0 63.76 64.45 3.53 o 8 0 0 49.17 49.30 4.86 o 1 1 0 2470.79 2411.48 14.11 o 2 1 0 1284.96 1269.59 5.01 o 3 1 0 116.19 93.49 0.78 o 4 1 0 92.40 83.33 0.90 o 5 1 0 23.69 22.01 1.13 o 6 1 0 0.25 0.48 0.27 o 7 1 0 66.27 68.00 4.76 o 8 1 0 84.54 89.32 2.38 o 0 2 0 2714.94 2673.08 48.07 o 1 2 0 3528.21 3545.29 11.65 o 2 2 0 136.51 135.22 0.70 o 3 2 0 69.34 79.78 0.72 o 4 2 0 0.12 0.21 0.17 o 5 2 0 48.04 47.09 1.48 o 6 2 0 214.24 227.94 4.39 o 7 2 0 91.47 93.55 2.87 o 8 2 0 0.35 0.84 0.30 o 1 3 0 163.17 161.22 1.30 o 2 3 0 1398.97 1442.41 10.09 o 3 3 0 0.37 0.17 0.09 o 4 3 0 65.33 63.46 1.07 o 5 3 0 15.79 13.29 0.73 o 6 3 0 9.76 7.83 0.57 o 7 3 0 103.34 103.36 2.47 o 8 3 0 20.51 17.50 2.89 o 0 4 0 1408.77 1569.66 28.95 o 1 4 0 294.28 315.37 2.86 o 2 4 0 21.12 20.80 0.54 o 3 4 0 0.25 0.11 0.07 o 4 4 0 15.61 16.97 0.74 o 5 4 0 28.93 26.43 1.46 o 6 4 0 85.66 92.69 2.20 o 7 4 0 24.02 19.69 1.65 o 1 5 0 252.71 269.95 3.96 o 2 5 0 35.40 33.91 1.02 o 3 5 0 68.23 73.20 1.34 o 4 5 0 27.89 25.62 1.22 o 5 5 0 4.67 4.03 0.33 o 6 5 0 1.00 0.60 0.26 o 0 6 0 281.52 309.92 8.77 o 1 6 0 48.48 58.23 3.86 o 2 6 0 9.09 9.31 0.68 o 3 6 0 1.46 0.72 0.29 o 4 6 0 3.21 3.63 0.60 o 5 6 0 12.96 9.87 1.18 o 1 7 0 6.83 6.30 0.49 o 2 7 0 60.76 57.24 5.53 o 3 7 0 6.78 6.05 0.86 o -8 0 1 7.41 5.05 0.63 o -7 0 1 36.17 39.26 3.73 o -6 0 1 14.69 18.61 2.26 o -5 0 1 133.45 135.44 2.10 o -4 0 1 238.68 241.93 2.74 o -3 0 1 143.02 143.51 1.27 o -2 0 1 0.30 0.76 0.21 o -1 0 1 70.28 53.88 0.49 o 0 0 1 94.28 91.13 0.55 o 1 0 1 908.01 826.96 4.82 o 2 0 1 2650.98 2645.03 9.64 o 3 0 1 7.93 9.72 0.81 o 4 0 1 26.18 27.93 1.49 o 5 0 1 6.09 8.60 0.60 o 6 0 1 35.22 39.12 4.84 o 7 0 1 41.01 45.44 4.27 o 8 0 1 14.62 16.15 1.78 o -8 1 1 12.50 9.68 1.00 o -7 1 1 0.09 0.33 0.27 o -6 1 1 3.85 5.35 0.40 o -5 1 1 3.85 2.98 0.18 o -4 1 1 165.63 176.26 1.72 o -3 1 1 443.97 452.69 3.29 o -2 1 1 46.45 55.74 0.44 o -1 1 1 37.59 48.39 0.31 o 0 1 1 512.94 444.66 1.33 o 1 1 1 667.84 687.13 2.14 o 2 1 1 431.94 423.76 1.64 o 3 1 1 818.20 812.45 4.77 o 4 1 1 502.38 511.43 4.15 o 5 1 1 196.35 193.80 2.43 o 6 1 1 65.85 65.62 4.68 o 7 1 1 18.64 16.99 1.11 o 8 1 1 5.57 6.43 0.55 o -8 2 1 0.09 0.08 0.31 o -7 2 1 5.22 5.55 0.54 o -6 2 1 19.68 16.58 1.30 o -5 2 1 159.11 162.19 2.32 o -4 2 1 199.09 212.63 2.27 o -3 2 1 159.86 155.14 1.06 o -2 2 1 380.08 406.26 1.90 o -1 2 1 534.34 550.12 1.89 o 0 2 1 66.25 66.08 0.67 o 1 2 1 445.24 408.52 1.40 o 2 2 1 17.54 20.09 0.33 o 3 2 1 386.92 397.57 2.53 o 4 2 1 17.86 16.06 0.73 o 5 2 1 19.31 21.46 1.22 o 6 2 1 49.61 50.91 3.11 o 7 2 1 4.64 4.85 0.64 o 8 2 1 28.58 28.26 2.92 o -8 3 1 0.42 0.19 0.44 o -7 3 1 1.28 0.65 0.37 o -6 3 1 2.99 2.45 0.33 o -5 3 1 33.53 27.30 1.60 o -4 3 1 74.81 79.73 1.03 o -3 3 1 287.82 304.44 2.54 o -2 3 1 84.92 82.73 0.62 o -1 3 1 40.67 51.04 0.40 o 0 3 1 138.30 129.42 0.82 o 1 3 1 0.08 0.66 0.10 o 2 3 1 45.75 41.13 0.44 o 3 3 1 76.66 67.30 0.76 o 4 3 1 458.12 467.74 4.44 o 5 3 1 73.09 73.70 2.07 o 6 3 1 21.69 22.73 1.41 o 7 3 1 4.24 4.39 0.46 o -7 4 1 0.55 0.87 0.32 o -6 4 1 0.20 0.84 0.27 o -5 4 1 32.49 37.27 1.50 o -4 4 1 62.69 60.63 1.05 o -3 4 1 31.63 30.13 0.80 o -2 4 1 1.31 1.86 0.13 o -1 4 1 0.02 0.09 0.07 o 0 4 1 4.77 4.86 0.25 o 1 4 1 0.22 0.42 0.09 o 2 4 1 105.65 105.10 1.10 o 3 4 1 42.81 43.55 1.03 o 4 4 1 2.95 1.84 0.13 o 5 4 1 2.53 1.16 0.14 o 6 4 1 26.83 26.33 1.06 o 7 4 1 8.68 8.07 0.85 o -6 5 1 3.37 2.97 0.34 o -5 5 1 0.53 0.32 0.14 o -4 5 1 8.46 9.93 0.68 o -3 5 1 25.76 27.38 0.98 o -2 5 1 31.33 31.22 0.66 o -1 5 1 40.30 40.05 1.44 o 0 5 1 46.96 44.11 1.00 o 1 5 1 86.74 87.60 1.44 o 2 5 1 5.44 4.67 0.27 o 3 5 1 96.78 100.01 1.17 o 4 5 1 27.27 23.27 1.44 o 5 5 1 42.55 49.29 2.57 o 6 5 1 13.37 13.79 1.78 o -5 6 1 7.03 7.18 1.26 o -4 6 1 10.58 9.71 1.20 o -3 6 1 8.90 7.11 0.70 o -2 6 1 0.35 0.59 0.59 o -1 6 1 2.43 3.61 0.48 o 0 6 1 0.06 0.18 0.15 o 1 6 1 0.01 0.01 0.27 o 2 6 1 33.37 34.72 1.15 o 3 6 1 8.32 8.13 0.62 o 4 6 1 0.97 1.79 0.40 o 5 6 1 2.64 1.49 0.34 o -3 7 1 15.04 14.47 2.16 o -2 7 1 2.35 4.21 0.66 o -1 7 1 0.05 -0.01 0.27 o 0 7 1 6.31 7.79 0.64 o 1 7 1 0.37 1.14 0.25 o 2 7 1 0.31 0.63 0.28 o 3 7 1 0.17 -0.42 0.96 o -8 0 2 164.41 177.68 4.56 o -7 0 2 25.53 27.68 2.89 o -6 0 2 26.32 30.15 3.38 o -5 0 2 92.77 108.29 1.74 o -4 0 2 73.09 70.09 1.19 o -3 0 2 194.28 170.56 1.72 o -2 0 2 356.23 327.46 1.89 o -1 0 2 35.05 31.41 0.99 o 0 0 2 1109.74 1021.19 3.99 o 1 0 2 1557.53 1586.24 5.98 o 2 0 2 13.97 14.32 0.79 o 3 0 2 85.96 80.84 1.15 o 4 0 2 171.39 161.98 2.57 o 5 0 2 14.86 13.48 1.10 o 6 0 2 15.42 16.14 1.81 o 7 0 2 2.97 4.11 0.63 o 8 0 2 1.02 0.65 0.40 o -8 1 2 0.11 0.32 0.34 o -7 1 2 113.74 116.69 3.18 o -6 1 2 114.89 119.49 2.31 o -5 1 2 254.91 258.18 2.45 o -4 1 2 609.29 620.21 4.03 o -3 1 2 99.05 98.87 0.99 o -2 1 2 0.68 0.63 0.12 o -1 1 2 800.89 831.36 3.33 o 0 1 2 267.48 297.72 0.98 o 1 1 2 1086.16 1100.79 2.74 o 2 1 2 238.50 234.11 1.11 o 3 1 2 175.55 165.78 1.12 o 4 1 2 0.45 0.24 0.11 o 5 1 2 22.08 22.15 1.31 o 6 1 2 5.48 5.08 0.45 o 7 1 2 2.42 2.86 0.28 o 8 1 2 1.34 1.19 0.35 o -8 2 2 36.75 29.89 3.06 o -7 2 2 61.94 66.17 2.25 o -6 2 2 71.38 74.83 1.76 o -5 2 2 11.30 8.94 0.48 o -4 2 2 29.61 27.67 0.88 o -3 2 2 237.22 223.37 2.22 o -2 2 2 220.21 220.51 1.16 o -1 2 2 82.65 85.96 0.53 o 0 2 2 192.08 194.44 1.14 o 1 2 2 0.55 0.49 0.11 o 2 2 2 43.43 44.36 0.41 o 3 2 2 546.51 544.95 3.65 o 4 2 2 4.83 6.02 0.27 o 5 2 2 5.14 6.05 0.37 o 6 2 2 6.37 6.28 0.50 o 7 2 2 2.43 2.34 0.44 o 8 2 2 9.82 8.63 1.06 o -8 3 2 4.50 2.57 0.52 o -7 3 2 6.45 5.82 0.58 o -6 3 2 200.77 209.84 5.74 o -5 3 2 89.42 91.83 2.12 o -4 3 2 152.27 158.46 1.82 o -3 3 2 70.63 69.30 0.77 o -2 3 2 5.44 7.49 0.36 o -1 3 2 421.87 441.04 2.36 o 0 3 2 179.85 180.68 1.01 o 1 3 2 136.18 137.04 0.98 o 2 3 2 546.10 552.57 4.80 o 3 3 2 6.02 6.47 0.31 o 4 3 2 1.64 0.72 0.20 o 5 3 2 0.27 0.20 0.15 o 6 3 2 0.03 0.33 0.42 o 7 3 2 5.93 5.99 0.57 o -7 4 2 12.77 9.03 0.81 o -6 4 2 25.24 22.05 1.71 o -5 4 2 0.27 0.60 0.14 o -4 4 2 2.87 2.34 0.15 o -3 4 2 59.94 69.45 0.97 o -2 4 2 57.67 60.97 0.92 o -1 4 2 14.29 15.21 0.60 o 0 4 2 7.86 8.30 0.42 o 1 4 2 62.14 57.24 0.74 o 2 4 2 47.11 47.53 0.78 o 3 4 2 48.44 48.91 0.92 o 4 4 2 17.69 17.30 0.92 o 5 4 2 0.01 0.45 0.25 o 6 4 2 1.99 1.40 0.32 o 7 4 2 0.17 0.09 0.31 o -6 5 2 7.66 6.44 0.66 o -5 5 2 56.67 60.43 3.44 o -4 5 2 70.08 70.00 2.25 o -3 5 2 3.39 4.56 0.30 o -2 5 2 0.88 1.29 0.12 o -1 5 2 18.93 19.46 0.83 o 0 5 2 78.92 80.25 1.44 o 1 5 2 171.93 186.00 3.30 o 2 5 2 0.45 0.52 0.13 o 3 5 2 27.22 28.41 1.39 o 4 5 2 0.50 0.45 0.29 o 5 5 2 9.01 8.98 0.62 o 6 5 2 1.95 1.74 0.43 o -4 6 2 6.41 3.86 0.57 o -3 6 2 12.39 16.17 2.22 o -2 6 2 20.09 20.01 1.33 o -1 6 2 11.69 13.77 1.05 o 0 6 2 8.73 7.67 0.53 o 1 6 2 22.72 18.84 0.92 o 2 6 2 11.42 11.46 0.81 o 3 6 2 11.30 10.57 0.87 o 4 6 2 3.14 3.08 0.32 o -3 7 2 5.18 3.39 0.58 o -2 7 2 0.94 0.65 0.24 o -1 7 2 17.09 15.88 1.39 o 0 7 2 12.63 13.66 1.01 o 1 7 2 8.23 7.66 0.65 o 2 7 2 16.34 14.31 2.92 o -8 0 3 39.88 32.47 4.22 o -7 0 3 0.70 0.60 0.44 o -6 0 3 103.18 111.02 3.64 o -5 0 3 6.78 5.31 0.69 o -4 0 3 40.28 40.80 1.52 o -3 0 3 66.67 70.51 1.10 o -2 0 3 3258.74 3390.98 19.08 o -1 0 3 2164.60 2215.13 8.42 o 0 0 3 2412.06 2410.08 14.70 o 1 0 3 1.30 2.46 0.19 o 2 0 3 1155.80 1173.28 9.15 o 3 0 3 81.54 72.72 0.96 o 4 0 3 200.30 185.82 2.37 o 5 0 3 354.94 373.45 8.49 o 6 0 3 416.10 447.24 5.36 o 7 0 3 3.57 2.90 0.52 o -8 1 3 5.74 5.21 0.63 o -7 1 3 7.59 6.84 0.73 o -6 1 3 3.38 3.41 0.32 o -5 1 3 22.07 21.22 0.75 o -4 1 3 91.64 88.63 0.98 o -3 1 3 501.70 517.03 2.65 o -2 1 3 1067.42 1090.10 4.98 o -1 1 3 57.22 53.60 0.52 o 0 1 3 274.42 266.10 1.21 o 1 1 3 53.36 42.20 0.43 o 2 1 3 184.65 164.54 1.04 o 3 1 3 245.42 249.89 1.86 o 4 1 3 254.32 264.67 2.26 o 5 1 3 6.79 5.38 0.43 o 6 1 3 78.11 76.55 1.70 o 7 1 3 99.75 105.36 5.02 o 8 1 3 17.09 15.71 2.29 o -8 2 3 11.39 10.23 0.92 o -7 2 3 43.34 43.41 1.89 o -6 2 3 1.35 1.07 0.22 o -5 2 3 24.34 28.42 1.17 o -4 2 3 4.59 4.79 0.26 o -3 2 3 158.82 155.09 1.26 o -2 2 3 581.30 577.39 3.33 o -1 2 3 1333.25 1342.34 6.21 o 0 2 3 1204.88 1194.42 5.22 o 1 2 3 259.44 246.21 1.32 o 2 2 3 0.62 0.36 0.09 o 3 2 3 53.20 56.46 0.83 o 4 2 3 181.30 184.07 2.36 o 5 2 3 523.24 554.09 10.84 o 6 2 3 134.69 140.72 3.98 o 7 2 3 11.82 9.57 0.81 o -7 3 3 1.49 1.83 0.32 o -6 3 3 26.94 22.56 1.78 o -5 3 3 21.90 19.12 1.28 o -4 3 3 283.98 287.59 4.06 o -3 3 3 178.42 179.31 1.56 o -2 3 3 321.20 317.61 2.85 o -1 3 3 35.27 27.77 0.45 o 0 3 3 34.41 29.99 0.43 o 1 3 3 104.03 106.15 1.03 o 2 3 3 78.95 75.92 0.83 o 3 3 3 35.84 36.41 0.85 o 4 3 3 407.77 428.72 5.55 o 5 3 3 14.14 11.48 0.68 o 6 3 3 33.65 33.67 1.82 o 7 3 3 46.52 42.87 3.46 o -7 4 3 1.99 1.90 0.57 o -6 4 3 19.26 20.45 1.56 o -5 4 3 1.08 0.82 0.24 o -4 4 3 2.78 2.49 0.18 o -3 4 3 6.36 8.17 0.43 o -2 4 3 252.04 261.20 2.80 o -1 4 3 356.18 361.02 3.43 o 0 4 3 240.70 260.08 3.05 o 1 4 3 28.01 28.72 1.15 o 2 4 3 46.48 50.97 0.84 o 3 4 3 1.50 1.61 0.13 o 4 4 3 103.21 106.32 1.96 o 5 4 3 123.19 129.57 1.97 o 6 4 3 104.65 112.44 2.30 o -6 5 3 0.38 0.38 0.26 o -5 5 3 31.51 27.93 2.22 o -4 5 3 5.59 6.24 0.43 o -3 5 3 99.57 97.03 1.32 o -2 5 3 108.33 104.09 1.50 o -1 5 3 1.27 0.84 0.17 o 0 5 3 34.40 37.01 1.35 o 1 5 3 1.05 1.27 0.15 o 2 5 3 48.75 48.00 1.11 o 3 5 3 117.53 131.65 4.00 o 4 5 3 8.78 9.62 0.82 o 5 5 3 8.77 9.50 1.88 o -5 6 3 5.85 5.78 1.55 o -4 6 3 0.00 0.46 0.32 o -3 6 3 0.04 0.58 0.39 o -2 6 3 69.21 72.86 1.57 o -1 6 3 66.51 78.17 1.63 o 0 6 3 46.35 47.47 1.46 o 1 6 3 8.86 10.16 0.66 o 2 6 3 21.70 19.26 1.16 o 3 6 3 4.05 2.47 0.26 o 4 6 3 16.27 13.88 1.37 o -2 7 3 7.00 6.91 0.85 o -1 7 3 0.73 0.58 0.78 o 0 7 3 0.48 0.18 0.48 o 1 7 3 12.74 10.45 2.02 o 2 7 3 9.95 7.28 2.00 o -8 0 4 7.00 4.39 1.14 o -7 0 4 26.75 24.64 5.20 o -6 0 4 218.12 238.11 6.74 o -5 0 4 112.83 113.69 3.68 o -4 0 4 239.96 242.82 2.89 o -3 0 4 40.39 53.92 0.98 o -2 0 4 15.57 14.69 0.85 o -1 0 4 376.84 376.10 3.02 o 0 0 4 363.39 339.42 3.24 o 1 0 4 948.47 987.49 6.77 o 2 0 4 34.61 28.44 1.07 o 3 0 4 203.57 230.37 3.50 o 4 0 4 5.05 4.56 0.43 o 5 0 4 9.11 12.26 1.09 o 6 0 4 4.40 4.67 0.74 o 7 0 4 4.36 5.77 0.64 o -8 1 4 0.38 -0.12 0.48 o -7 1 4 63.12 61.46 4.89 o -6 1 4 0.02 0.38 0.39 o -5 1 4 37.97 38.91 1.62 o -4 1 4 122.15 113.53 1.34 o -3 1 4 93.05 90.85 0.97 o -2 1 4 158.83 176.70 1.34 o -1 1 4 48.26 40.35 0.48 o 0 1 4 4.48 3.31 0.17 o 1 1 4 207.67 206.73 1.30 o 2 1 4 1389.71 1473.29 9.78 o 3 1 4 201.29 192.29 2.49 o 4 1 4 44.17 41.69 1.83 o 5 1 4 18.54 18.22 0.86 o 6 1 4 4.15 5.04 0.45 o 7 1 4 5.09 5.40 0.48 o -8 2 4 0.07 -0.02 0.46 o -7 2 4 8.38 6.93 0.69 o -6 2 4 70.24 71.73 1.85 o -5 2 4 463.81 498.73 9.35 o -4 2 4 31.21 30.29 0.94 o -3 2 4 31.62 27.01 0.79 o -2 2 4 8.12 9.27 0.43 o -1 2 4 3.29 2.33 0.14 o 0 2 4 139.56 128.85 1.00 o 1 2 4 295.45 291.69 1.85 o 2 2 4 30.11 27.26 0.61 o 3 2 4 0.78 0.31 0.10 o 4 2 4 175.94 177.84 2.91 o 5 2 4 32.20 33.96 2.01 o 6 2 4 6.43 8.01 0.65 o 7 2 4 26.26 23.37 1.94 o -7 3 4 9.43 9.95 0.97 o -6 3 4 20.16 18.00 1.42 o -5 3 4 44.85 43.83 3.13 o -4 3 4 178.26 187.62 2.64 o -3 3 4 6.20 6.18 0.35 o -2 3 4 12.29 11.87 0.55 o -1 3 4 11.35 10.73 0.58 o 0 3 4 0.02 0.04 0.09 o 1 3 4 79.33 80.96 0.87 o 2 3 4 274.74 272.58 2.48 o 3 3 4 256.91 260.78 3.85 o 4 3 4 8.42 9.06 0.49 o 5 3 4 0.99 0.86 0.21 o 6 3 4 35.42 32.67 2.25 o 7 3 4 0.56 0.63 0.64 o -7 4 4 12.71 11.54 1.21 o -6 4 4 38.18 32.11 2.82 o -5 4 4 64.58 73.28 2.32 o -4 4 4 12.05 10.32 0.59 o -3 4 4 2.18 1.74 0.18 o -2 4 4 0.60 1.25 0.24 o -1 4 4 1.12 1.44 0.13 o 0 4 4 60.14 60.17 0.92 o 1 4 4 149.31 147.33 1.97 o 2 4 4 14.27 13.77 0.58 o 3 4 4 14.31 12.53 0.67 o 4 4 4 7.81 5.49 0.74 o 5 4 4 0.00 0.67 0.21 o 6 4 4 5.88 5.98 0.61 o -6 5 4 5.00 4.58 0.53 o -5 5 4 2.42 2.65 0.25 o -4 5 4 12.04 12.35 0.85 o -3 5 4 58.53 58.32 1.44 o -2 5 4 11.92 8.00 0.53 o -1 5 4 11.58 10.75 0.75 o 0 5 4 4.76 4.12 0.30 o 1 5 4 11.02 8.53 0.68 o 2 5 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