#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2220722.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220722_Fobs loop_ _publ_author_name 'Prabakaran, K.' 'Maiyalagan, T.' 'Hathwar, Venkatesha R.' 'Kazak, Canan' 'Khan, F. Nawaz' _publ_section_title ; Methyl 1H-1,2,3-triazole-4-carboxylate ; _journal_coeditor_code BT2847 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o300 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.938 _cell_angle_gamma 90.000 _cell_length_a 3.8823 _cell_length_b 17.4989 _cell_length_c 8.8171 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.8257 _[local]_cod_data_source_file bt2847Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vhr2_m in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 102.04 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 569.07 545.90 5.34 o 4 0 0 3.94 4.67 0.87 o 1 1 0 1653.62 1601.99 10.85 o 2 1 0 15.71 22.84 0.41 o 3 1 0 15.60 15.51 0.40 o 4 1 0 0.21 0.24 0.51 o 0 2 0 1793.09 1714.03 11.75 o 1 2 0 1586.65 1621.62 8.45 o 2 2 0 541.66 596.65 4.72 o 3 2 0 11.16 10.31 0.39 o 4 2 0 0.05 0.34 0.67 o 1 3 0 147.14 126.42 0.85 o 2 3 0 254.85 250.16 1.66 o 3 3 0 0.04 0.00 0.20 o 4 3 0 0.26 0.00 0.50 o 0 4 0 1136.69 1116.57 7.58 o 1 4 0 113.66 119.16 0.84 o 2 4 0 283.42 265.43 1.73 o 3 4 0 0.74 0.87 0.24 o 4 4 0 1.10 1.61 0.56 o 1 5 0 129.06 115.47 0.85 o 2 5 0 7.68 8.76 0.26 o 3 5 0 8.84 7.83 0.42 o 4 5 0 0.33 0.83 0.39 o 0 6 0 539.82 527.20 3.92 o 1 6 0 155.45 159.75 1.11 o 2 6 0 54.64 55.29 0.64 o 3 6 0 18.46 18.17 0.78 o 4 6 0 7.55 7.17 0.59 o 1 7 0 1.29 2.49 0.16 o 2 7 0 98.89 84.40 0.98 o 3 7 0 3.09 2.75 0.33 o 4 7 0 2.08 1.60 0.44 o 0 8 0 305.13 335.54 3.56 o 1 8 0 580.56 612.99 3.34 o 2 8 0 264.90 265.36 2.08 o 3 8 0 1.62 3.11 0.41 o 4 8 0 9.35 8.65 0.65 o 1 9 0 97.37 110.42 0.98 o 2 9 0 17.89 21.01 0.61 o 3 9 0 7.25 6.97 0.53 o 4 9 0 1.89 1.55 0.63 o 0 10 0 447.66 428.54 5.11 o 1 10 0 1.55 1.85 0.17 o 2 10 0 2.37 2.00 0.29 o 3 10 0 0.01 0.00 0.30 o 4 10 0 1.48 1.70 0.58 o 1 11 0 0.84 0.79 0.18 o 2 11 0 79.40 71.74 1.19 o 3 11 0 2.24 2.09 0.41 o 0 12 0 120.34 131.05 1.70 o 1 12 0 3.20 2.82 0.22 o 2 12 0 19.60 20.32 0.66 o 3 12 0 4.46 4.13 0.49 o 1 13 0 61.82 65.63 0.95 o 2 13 0 28.85 27.11 0.92 o 3 13 0 4.83 4.16 0.53 o 0 14 0 212.41 212.04 2.47 o 1 14 0 4.06 3.97 0.38 o 2 14 0 0.48 1.41 0.39 o 3 14 0 3.00 2.78 0.48 o 1 15 0 0.31 0.26 0.30 o 2 15 0 160.03 148.40 2.35 o 3 15 0 0.96 1.22 0.47 o 0 16 0 24.02 25.02 0.85 o 1 16 0 85.41 83.31 1.40 o 2 16 0 50.45 51.82 1.38 o 3 16 0 7.00 5.64 0.58 o 1 17 0 9.56 11.91 0.57 o 2 17 0 1.31 0.58 0.39 o 0 18 0 0.03 0.18 0.35 o 1 18 0 6.33 9.24 0.62 o 2 18 0 5.92 6.24 0.58 o 1 19 0 6.17 5.45 0.54 o 2 19 0 1.19 1.09 0.52 o 0 20 0 27.47 38.58 2.16 o 1 20 0 1.45 3.11 0.50 o -3 0 1 30.92 26.00 1.79 o -1 0 1 384.69 419.14 3.80 o 1 0 1 6928.43 7078.11 120.58 o 3 0 1 60.19 50.99 1.66 o -4 1 1 2.81 2.90 0.60 o -3 1 1 2.63 2.98 0.30 o -2 1 1 171.45 154.69 1.13 o -1 1 1 2233.92 2321.06 16.85 o 0 1 1 28.48 33.52 0.31 o 1 1 1 10411.79 10310.43 50.30 o 2 1 1 757.54 743.73 4.38 o 3 1 1 71.55 67.83 0.89 o 4 1 1 0.31 0.00 0.74 o -4 2 1 1.34 1.62 0.49 o -3 2 1 1.00 1.07 0.27 o -2 2 1 14.68 13.34 0.28 o -1 2 1 1913.09 1852.01 9.66 o 0 2 1 1843.42 1949.32 10.05 o 1 2 1 26.64 28.06 0.70 o 2 2 1 8.84 9.36 0.71 o 3 2 1 0.14 1.58 0.33 o 4 2 1 3.26 2.60 0.80 o -4 3 1 1.02 1.37 0.46 o -3 3 1 30.35 30.83 0.73 o -2 3 1 10.01 6.66 0.21 o -1 3 1 420.35 458.40 3.04 o 0 3 1 237.48 230.02 1.28 o 1 3 1 347.09 332.26 2.07 o 2 3 1 20.48 21.03 0.58 o 3 3 1 149.39 143.33 1.53 o 4 3 1 2.44 2.37 0.61 o -4 4 1 0.31 0.58 0.43 o -3 4 1 10.25 9.55 0.44 o -2 4 1 14.55 13.57 0.34 o -1 4 1 295.88 287.56 2.13 o 0 4 1 773.81 774.22 3.82 o 1 4 1 40.74 41.14 0.50 o 2 4 1 2.50 2.64 0.22 o 3 4 1 0.11 0.91 0.30 o 4 4 1 1.29 0.75 0.39 o -4 5 1 0.27 0.16 0.64 o -3 5 1 5.78 5.64 0.38 o -2 5 1 38.52 31.66 0.53 o -1 5 1 167.50 141.52 1.23 o 0 5 1 375.38 396.86 2.14 o 1 5 1 273.87 266.94 1.80 o 2 5 1 32.53 32.02 0.51 o 3 5 1 2.62 2.32 0.28 o 4 5 1 5.04 5.84 0.56 o -4 6 1 0.78 0.82 0.38 o -3 6 1 2.04 2.65 0.32 o -2 6 1 168.71 165.76 1.42 o -1 6 1 277.44 298.34 1.78 o 0 6 1 529.78 531.69 2.81 o 1 6 1 76.42 65.72 1.34 o 2 6 1 0.01 0.34 0.15 o 3 6 1 1.29 1.10 0.33 o 4 6 1 1.38 0.69 0.39 o -4 7 1 0.55 0.58 0.38 o -3 7 1 90.72 86.17 1.36 o -2 7 1 0.36 0.60 0.20 o -1 7 1 434.20 449.37 2.51 o 0 7 1 3.85 2.20 0.14 o 1 7 1 43.13 39.39 0.51 o 2 7 1 52.97 48.53 0.66 o 3 7 1 62.16 57.40 1.29 o 4 7 1 1.27 1.62 0.44 o -4 8 1 0.25 0.43 0.41 o -3 8 1 0.57 1.09 0.31 o -2 8 1 71.00 70.22 1.09 o -1 8 1 697.90 735.33 3.88 o 0 8 1 197.80 217.22 2.11 o 1 8 1 61.09 64.00 0.70 o 2 8 1 57.67 60.60 0.86 o 3 8 1 0.14 0.40 0.32 o 4 8 1 0.06 0.43 0.40 o -4 9 1 6.69 6.54 0.61 o -3 9 1 11.06 11.33 0.55 o -2 9 1 0.22 0.37 0.22 o -1 9 1 68.23 73.62 0.74 o 0 9 1 494.76 550.30 3.08 o 1 9 1 360.19 347.50 2.47 o 2 9 1 12.17 11.64 0.41 o 3 9 1 10.05 9.53 0.59 o 4 9 1 0.98 0.54 0.45 o -4 10 1 0.00 0.27 0.40 o -3 10 1 50.43 48.13 1.07 o -2 10 1 0.02 0.04 0.22 o -1 10 1 31.64 35.24 0.52 o 0 10 1 118.46 141.04 1.17 o 1 10 1 43.69 42.19 0.60 o 2 10 1 2.56 2.55 0.29 o 3 10 1 9.44 10.19 0.62 o -4 11 1 1.60 1.54 0.49 o -3 11 1 0.77 1.34 0.37 o -2 11 1 24.33 23.85 0.70 o -1 11 1 60.87 54.50 0.69 o 0 11 1 16.74 14.29 0.35 o 1 11 1 112.54 116.65 1.11 o 2 11 1 1.65 1.36 0.40 o 3 11 1 6.46 7.68 0.85 o -3 12 1 7.51 6.61 0.56 o -2 12 1 71.72 65.36 1.19 o -1 12 1 147.28 141.47 1.42 o 0 12 1 0.16 0.16 0.15 o 1 12 1 33.27 32.40 0.58 o 2 12 1 3.16 3.32 0.41 o 3 12 1 2.67 2.59 0.43 o -3 13 1 9.99 10.61 0.97 o -2 13 1 2.80 2.41 0.35 o -1 13 1 47.57 46.90 0.96 o 0 13 1 4.20 4.55 0.26 o 1 13 1 1.66 1.82 0.23 o 2 13 1 38.30 36.38 1.06 o 3 13 1 3.87 4.50 0.71 o -3 14 1 15.74 14.97 0.80 o -2 14 1 1.27 1.39 0.34 o -1 14 1 297.91 291.11 2.80 o 0 14 1 89.30 88.53 1.04 o 1 14 1 25.29 26.10 0.63 o 2 14 1 5.89 5.43 0.53 o 3 14 1 25.61 26.35 1.06 o -3 15 1 7.82 7.05 0.62 o -2 15 1 2.91 1.94 0.42 o -1 15 1 250.29 239.53 2.55 o 0 15 1 67.60 68.61 0.95 o 1 15 1 119.26 116.99 1.60 o 2 15 1 7.36 6.61 0.73 o 3 15 1 1.24 1.32 0.47 o -3 16 1 18.18 17.72 0.90 o -2 16 1 2.08 2.21 0.40 o -1 16 1 10.16 8.70 0.54 o 0 16 1 119.31 127.41 1.38 o 1 16 1 0.30 0.00 0.42 o 2 16 1 1.90 1.07 0.40 o -2 17 1 15.25 12.71 0.74 o -1 17 1 33.04 36.72 0.97 o 0 17 1 0.02 1.30 0.25 o 1 17 1 0.06 0.33 0.55 o 2 17 1 8.21 7.14 0.59 o -2 18 1 5.97 6.76 0.59 o -1 18 1 2.51 1.83 0.38 o 0 18 1 8.61 9.90 0.53 o 1 18 1 2.57 2.98 0.44 o 2 18 1 0.51 0.68 0.52 o -2 19 1 0.93 0.80 0.44 o -1 19 1 4.00 5.68 0.84 o 0 19 1 0.58 2.21 0.43 o 1 19 1 7.88 9.75 0.66 o -1 20 1 3.26 3.39 0.66 o 0 20 1 5.02 5.93 0.99 o 1 20 1 3.03 3.77 0.51 o 0 21 1 0.01 0.00 0.74 o -4 0 2 4.68 5.99 0.95 o -2 0 2 48.77 50.14 0.84 o 0 0 2 7142.82 7531.44 135.05 o 2 0 2 791.90 773.70 5.95 o 4 0 2 1.49 1.91 0.92 o -4 1 2 29.55 31.21 1.32 o -3 1 2 4.79 4.61 0.36 o -2 1 2 40.07 38.74 0.58 o -1 1 2 278.76 276.66 2.68 o 0 1 2 590.73 596.68 3.28 o 1 1 2 661.89 698.30 3.60 o 2 1 2 1019.85 1068.38 6.11 o 3 1 2 35.82 36.58 0.77 o 4 1 2 8.55 7.75 0.83 o -4 2 2 0.90 1.96 0.53 o -3 2 2 24.48 25.28 0.64 o -2 2 2 156.67 161.45 1.23 o -1 2 2 16.17 11.79 0.24 o 0 2 2 53.72 40.90 0.39 o 1 2 2 111.46 119.18 0.97 o 2 2 2 566.96 596.97 3.80 o 3 2 2 62.13 57.24 1.19 o 4 2 2 17.43 17.51 1.53 o -4 3 2 2.73 2.96 0.54 o -3 3 2 1.65 2.23 0.26 o -2 3 2 177.18 172.20 1.42 o -1 3 2 585.11 626.40 5.70 o 0 3 2 1131.96 1151.01 7.52 o 1 3 2 0.04 0.21 0.17 o 2 3 2 4.28 5.67 0.37 o 3 3 2 1.53 1.52 0.35 o 4 3 2 2.50 2.44 0.65 o -4 4 2 1.56 1.14 0.50 o -3 4 2 0.01 0.00 0.21 o -2 4 2 54.62 53.96 0.85 o -1 4 2 168.72 167.94 1.95 o 0 4 2 292.62 312.15 1.77 o 1 4 2 36.86 34.84 0.52 o 2 4 2 34.41 29.09 0.50 o 3 4 2 1.20 0.54 0.29 o 4 4 2 9.63 7.31 0.81 o -4 5 2 7.78 9.95 0.67 o -3 5 2 10.66 10.74 0.48 o -2 5 2 18.52 18.05 0.50 o -1 5 2 218.64 229.36 1.89 o 0 5 2 119.64 117.37 0.87 o 1 5 2 722.65 737.82 3.87 o 2 5 2 31.84 32.38 0.70 o 3 5 2 1.14 0.36 0.29 o 4 5 2 0.00 0.02 0.89 o -4 6 2 14.43 15.67 0.82 o -3 6 2 1.04 1.17 0.28 o -2 6 2 68.74 75.13 1.07 o -1 6 2 190.78 190.36 1.70 o 0 6 2 9.81 13.08 0.26 o 1 6 2 23.37 22.76 0.46 o 2 6 2 11.30 12.10 0.45 o 3 6 2 2.25 2.83 0.37 o 4 6 2 1.90 1.64 0.48 o -4 7 2 0.81 0.42 0.35 o -3 7 2 12.34 12.26 0.54 o -2 7 2 61.04 57.25 0.96 o -1 7 2 7.32 12.79 0.30 o 0 7 2 1705.81 1887.17 9.07 o 1 7 2 6.03 5.40 0.22 o 2 7 2 5.78 4.41 0.27 o 3 7 2 7.84 7.59 0.55 o 4 7 2 2.07 3.03 0.49 o -4 8 2 23.45 24.28 0.86 o -3 8 2 1.26 1.17 0.30 o -2 8 2 312.95 311.73 2.75 o -1 8 2 151.29 152.45 1.17 o 0 8 2 42.04 44.04 0.55 o 1 8 2 18.60 18.82 0.38 o 2 8 2 1.95 2.49 0.24 o 3 8 2 3.60 3.17 0.42 o 4 8 2 4.28 3.43 0.54 o -4 9 2 1.13 1.59 0.52 o -3 9 2 10.29 10.16 0.53 o -2 9 2 62.41 63.91 1.08 o -1 9 2 193.09 210.73 1.47 o 0 9 2 207.81 228.47 1.59 o 1 9 2 59.26 54.41 0.76 o 2 9 2 92.98 88.25 1.19 o 3 9 2 7.01 7.53 0.57 o -4 10 2 0.08 0.00 0.38 o -3 10 2 11.96 10.89 0.56 o -2 10 2 26.61 27.84 0.75 o -1 10 2 2.78 4.18 0.27 o 0 10 2 22.52 23.67 0.44 o 1 10 2 131.94 136.81 1.25 o 2 10 2 41.40 37.97 0.86 o 3 10 2 0.04 0.03 0.46 o -4 11 2 0.27 0.60 0.92 o -3 11 2 1.73 1.80 0.35 o -2 11 2 92.09 89.50 1.39 o -1 11 2 273.21 275.04 2.53 o 0 11 2 4.94 7.46 0.28 o 1 11 2 20.94 21.56 0.53 o 2 11 2 32.11 31.71 0.81 o 3 11 2 0.20 0.58 0.40 o -3 12 2 4.71 5.82 0.47 o -2 12 2 9.58 9.36 0.50 o -1 12 2 0.00 0.30 0.26 o 0 12 2 1.44 1.73 0.20 o 1 12 2 6.11 5.60 0.35 o 2 12 2 0.80 0.75 0.60 o 3 12 2 9.94 8.97 0.69 o -3 13 2 7.14 7.23 0.51 o -2 13 2 0.16 0.58 0.28 o -1 13 2 11.89 12.46 0.65 o 0 13 2 502.23 483.30 3.45 o 1 13 2 22.05 21.86 0.58 o 2 13 2 1.40 0.14 0.36 o 3 13 2 0.26 0.00 0.37 o -3 14 2 11.62 11.18 0.63 o -2 14 2 43.96 38.80 0.99 o -1 14 2 0.00 0.00 0.27 o 0 14 2 215.66 201.17 1.71 o 1 14 2 129.09 121.65 1.43 o 2 14 2 12.23 10.46 0.66 o 3 14 2 5.18 5.48 1.27 o -3 15 2 2.75 3.06 0.49 o -2 15 2 43.79 42.66 1.07 o -1 15 2 0.07 0.11 0.39 o 0 15 2 5.03 7.02 0.36 o 1 15 2 42.19 43.44 0.99 o 2 15 2 30.38 30.55 1.07 o -3 16 2 0.77 1.05 0.41 o -2 16 2 78.51 73.64 1.44 o -1 16 2 15.62 17.79 0.69 o 0 16 2 125.54 116.75 1.47 o 1 16 2 5.64 5.92 0.52 o 2 16 2 7.75 7.93 0.64 o -2 17 2 1.25 1.32 0.59 o -1 17 2 39.10 37.99 1.00 o 0 17 2 0.12 0.84 0.39 o 1 17 2 5.84 6.45 0.53 o 2 17 2 4.67 4.66 0.55 o -2 18 2 3.87 5.08 0.47 o -1 18 2 0.12 0.09 0.32 o 0 18 2 17.41 15.20 0.77 o 1 18 2 0.90 0.83 0.37 o 2 18 2 2.21 2.13 0.89 o -2 19 2 0.17 0.00 0.40 o -1 19 2 1.55 1.92 0.40 o 0 19 2 5.46 5.65 0.56 o 1 19 2 5.04 6.43 0.56 o -1 20 2 0.07 0.95 0.38 o 0 20 2 3.25 3.90 0.63 o 1 20 2 0.17 0.75 0.81 o -3 0 3 260.12 281.20 5.54 o -1 0 3 44.70 28.79 0.52 o 1 0 3 1028.95 1111.93 9.97 o 3 0 3 264.41 247.62 6.42 o -4 1 3 2.59 3.57 0.61 o -3 1 3 12.79 14.52 0.61 o -2 1 3 13.08 15.94 0.31 o -1 1 3 1.35 1.12 0.12 o 0 1 3 150.12 134.59 1.04 o 1 1 3 244.31 252.21 1.61 o 2 1 3 130.04 127.92 1.17 o 3 1 3 15.84 18.83 0.75 o 4 1 3 0.94 0.62 0.79 o -4 2 3 3.05 3.54 0.57 o -3 2 3 35.08 35.54 0.91 o -2 2 3 125.63 121.32 1.04 o -1 2 3 576.59 629.21 3.26 o 0 2 3 64.96 77.59 0.66 o 1 2 3 15.32 14.45 0.36 o 2 2 3 5.36 6.35 0.32 o 3 2 3 60.36 59.56 1.16 o 4 2 3 8.81 8.38 0.70 o -4 3 3 4.31 4.54 0.77 o -3 3 3 20.86 19.28 0.68 o -2 3 3 3.22 3.21 0.19 o -1 3 3 77.70 75.88 0.65 o 0 3 3 430.16 416.92 2.31 o 1 3 3 22.63 19.12 0.44 o 2 3 3 1.37 1.89 0.23 o 3 3 3 37.77 38.44 0.93 o 4 3 3 5.16 4.91 1.47 o -4 4 3 0.04 0.37 0.46 o -3 4 3 17.77 19.06 0.60 o -2 4 3 190.80 174.21 1.73 o -1 4 3 625.86 652.98 5.92 o 0 4 3 11.23 13.87 0.27 o 1 4 3 290.04 304.72 2.17 o 2 4 3 28.24 27.09 0.59 o 3 4 3 0.26 0.67 0.29 o 4 4 3 0.08 0.00 0.54 o -4 5 3 4.96 6.30 1.35 o -3 5 3 0.00 0.00 0.35 o -2 5 3 46.22 42.93 0.79 o -1 5 3 81.20 108.45 1.30 o 0 5 3 79.43 74.81 0.69 o 1 5 3 14.85 18.45 0.43 o 2 5 3 12.84 12.93 0.44 o 3 5 3 0.57 0.23 0.31 o 4 5 3 1.77 1.54 0.92 o -4 6 3 6.63 7.66 0.65 o -3 6 3 37.56 36.70 0.88 o -2 6 3 16.22 14.72 0.49 o -1 6 3 7.99 10.23 0.29 o 0 6 3 3.89 3.29 0.16 o 1 6 3 139.99 153.54 1.40 o 2 6 3 94.22 88.02 1.12 o 3 6 3 2.94 3.43 0.38 o -4 7 3 3.09 3.04 0.86 o -3 7 3 155.67 159.28 1.97 o -2 7 3 40.67 36.72 0.78 o -1 7 3 373.92 419.91 2.75 o 0 7 3 21.32 24.98 0.41 o 1 7 3 87.77 92.60 1.05 o 2 7 3 0.41 0.41 0.23 o 3 7 3 0.05 0.38 0.37 o -4 8 3 12.37 14.36 0.96 o -3 8 3 5.57 6.85 0.48 o -2 8 3 0.25 0.65 0.25 o -1 8 3 587.76 643.64 3.52 o 0 8 3 0.42 0.62 0.16 o 1 8 3 408.39 402.58 2.83 o 2 8 3 5.54 4.85 0.32 o 3 8 3 3.97 4.79 0.44 o -4 9 3 4.46 6.27 0.60 o -3 9 3 36.71 36.11 0.94 o -2 9 3 0.32 0.01 0.25 o -1 9 3 41.07 40.67 0.64 o 0 9 3 347.14 374.81 2.34 o 1 9 3 0.32 0.69 0.20 o 2 9 3 6.30 6.51 0.46 o 3 9 3 0.23 0.68 0.41 o -4 10 3 4.12 4.86 0.50 o -3 10 3 7.39 9.75 0.54 o -2 10 3 4.96 5.15 0.40 o -1 10 3 30.86 28.68 0.69 o 0 10 3 1.18 1.00 0.16 o 1 10 3 0.08 0.47 0.20 o 2 10 3 10.51 9.76 0.49 o 3 10 3 24.86 24.16 0.96 o -3 11 3 1.73 2.65 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