#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/22/07/2220783.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2220783_Fobs loop_ _publ_author_name 'Aghabozorg, Hossein' 'Attar Gharamaleki, Jafar' 'Olmstead, Marilyn M.' 'Derikvand, Zohreh' 'Hooshmand, Shabnam' _publ_section_title ; Hydroxonium hydrate tris(2,4,6-triamino-1,3,5-triazin-1-ium) bis[bis(pyridine-2,6-dicarboxylato)cuprate(II)] pyridine-2,6-dicarboxylic acid hexahydrate ; _journal_coeditor_code GW2056 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m186 _journal_page_last m187 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.327 _cell_angle_gamma 90.000 _cell_length_a 27.5746 _cell_length_b 22.8142 _cell_length_c 9.8068 _exptl_crystal_F_000 3048.00 _reflns_d_resolution_high 0.8332 _[local]_cod_data_source_file gw2056Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 0.5[H5O2+]1.5[melamineH+][Cu(pydc)2].(0.5pydcH2).3H2O _shelx_refln_list_code 4 _shelx_F_calc_maximum 1393.97 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 53441.56 49683.52 1296.86 o 6 0 0 140553.56 130936.84 2220.06 o 8 0 0 6576.43 6925.44 156.37 o 10 0 0 85.30 89.61 54.35 o 12 0 0 44692.34 41172.69 630.39 o 14 0 0 2901.80 2608.92 143.28 o 16 0 0 58730.62 55540.29 999.05 o 18 0 0 20566.66 19317.84 413.74 o 20 0 0 13027.54 12239.00 315.08 o 22 0 0 9765.14 9868.90 610.13 o 24 0 0 2678.58 2614.86 179.27 o 26 0 0 44.35 17.64 151.50 o 28 0 0 868.80 807.28 181.69 o 30 0 0 1306.55 1057.65 202.00 o 5 1 0 3.11 -23.31 23.31 o 7 1 0 1207.55 1009.90 40.21 o 9 1 0 7364.27 8092.20 127.61 o 11 1 0 4840.83 4382.71 84.71 o 13 1 0 14196.94 13308.87 182.60 o 15 1 0 9722.94 9384.13 165.73 o 17 1 0 6017.46 5650.01 136.30 o 19 1 0 18395.97 17654.36 276.17 o 21 1 0 59.17 69.14 85.67 o 23 1 0 426.39 423.70 100.66 o 25 1 0 2072.86 2124.09 127.61 o 27 1 0 17.54 4.16 112.47 o 29 1 0 1736.95 1979.55 148.61 o 31 1 0 1064.78 981.86 153.38 o 4 2 0 503.59 406.79 54.27 o 6 2 0 17463.37 16397.93 212.58 o 8 2 0 2825.73 2906.82 74.57 o 10 2 0 1612.54 1636.99 50.85 o 12 2 0 5573.56 5325.41 97.98 o 14 2 0 1605.53 1673.35 70.13 o 16 2 0 0.49 -48.44 48.44 o 18 2 0 7743.88 8013.59 165.73 o 20 2 0 3.40 -4.36 80.64 o 22 2 0 16.92 -17.14 88.83 o 24 2 0 763.55 694.79 109.27 o 26 2 0 731.23 735.04 115.28 o 28 2 0 307.08 267.25 125.56 o 30 2 0 196.86 52.08 137.07 o 1 3 0 68.36 105.45 25.10 o 3 3 0 930.08 1095.51 46.20 o 5 3 0 3781.08 3949.08 89.01 o 7 3 0 11192.13 12597.97 192.03 o 9 3 0 3830.67 3089.96 60.97 o 11 3 0 323.12 494.60 103.26 o 13 3 0 53647.15 51891.86 560.66 o 15 3 0 4599.14 4135.07 98.14 o 17 3 0 2194.04 2113.34 101.00 o 19 3 0 37467.91 37006.40 558.58 o 21 3 0 5167.25 4983.51 151.66 o 23 3 0 2730.68 3004.65 126.97 o 25 3 0 340.55 353.01 111.78 o 27 3 0 34.38 -56.98 114.73 o 29 3 0 2692.04 2599.28 158.70 o 31 3 0 1049.21 1254.35 177.46 o 0 4 0 9631.01 8889.53 228.57 o 2 4 0 658.56 802.91 39.63 o 4 4 0 6105.49 5946.26 155.18 o 6 4 0 32311.72 32101.60 409.54 o 8 4 0 2017.45 1883.53 51.83 o 10 4 0 21962.59 24411.06 274.26 o 12 4 0 3860.05 4073.44 78.90 o 14 4 0 261.49 237.01 41.63 o 16 4 0 76319.99 72106.84 832.71 o 18 4 0 7841.89 7607.87 144.04 o 20 4 0 760.63 536.30 96.51 o 22 4 0 2978.11 2993.59 125.56 o 24 4 0 422.78 516.76 104.69 o 26 4 0 2092.00 2162.15 132.53 o 28 4 0 1786.31 1655.15 160.24 o 30 4 0 30.90 -38.15 154.51 o 1 5 0 9.13 3.57 53.80 o 3 5 0 7583.34 6578.80 119.72 o 5 5 0 2387.42 2144.99 59.45 o 7 5 0 5607.70 5154.09 85.20 o 9 5 0 58013.05 52076.83 597.14 o 11 5 0 5390.53 6000.65 175.18 o 13 5 0 1023.31 1213.48 51.64 o 15 5 0 5389.82 5714.09 112.37 o 17 5 0 649.74 679.46 55.36 o 19 5 0 346.27 572.09 83.57 o 21 5 0 1481.36 1756.54 122.83 o 23 5 0 697.79 783.34 105.50 o 25 5 0 3227.44 3401.11 197.40 o 27 5 0 197.28 140.10 136.22 o 29 5 0 1617.11 1626.91 168.28 o 0 6 0 5504.86 7071.23 274.65 o 2 6 0 8571.12 8196.85 225.26 o 4 6 0 3857.24 3854.69 118.61 o 6 6 0 23193.54 21423.08 284.45 o 8 6 0 25.39 2.32 33.06 o 10 6 0 3851.08 4234.97 116.85 o 12 6 0 2144.70 2201.61 64.65 o 14 6 0 4773.97 5135.73 99.54 o 16 6 0 10.23 -48.11 48.11 o 18 6 0 6410.41 6369.28 137.02 o 20 6 0 4702.29 4746.45 144.76 o 22 6 0 855.70 938.37 102.77 o 24 6 0 75.07 -38.96 114.81 o 26 6 0 1166.54 892.77 137.22 o 28 6 0 121.50 -102.98 142.84 o 30 6 0 540.11 295.43 237.52 o 1 7 0 4947.01 4398.43 119.95 o 3 7 0 1862.93 2029.56 73.25 o 5 7 0 5664.73 5471.10 118.79 o 7 7 0 16750.63 15710.40 223.57 o 9 7 0 26340.87 28062.46 338.53 o 11 7 0 8329.95 8614.86 124.80 o 13 7 0 6244.89 6077.51 104.80 o 15 7 0 9023.84 9995.06 488.34 o 17 7 0 2547.76 2906.55 85.37 o 19 7 0 14919.94 14666.40 304.43 o 21 7 0 543.99 483.45 92.06 o 23 7 0 6356.30 6383.59 205.94 o 25 7 0 115.16 27.45 128.22 o 27 7 0 332.49 344.40 145.53 o 29 7 0 74.01 89.91 209.96 o 0 8 0 73681.73 71156.11 2344.36 o 2 8 0 16695.27 16439.25 257.16 o 4 8 0 900.03 664.11 47.99 o 6 8 0 3318.51 2535.89 76.23 o 8 8 0 309.44 231.12 45.40 o 10 8 0 19686.26 18913.27 270.13 o 12 8 0 49018.61 46732.72 557.34 o 14 8 0 12.17 14.75 51.44 o 16 8 0 3797.73 3991.14 95.78 o 18 8 0 2529.80 2468.46 151.97 o 20 8 0 6956.23 6911.98 197.56 o 22 8 0 7051.14 7533.90 255.09 o 24 8 0 86.17 -42.52 122.96 o 26 8 0 172.95 208.48 172.83 o 28 8 0 1208.29 1079.75 196.41 o 30 8 0 1.08 -195.03 195.03 o 1 9 0 305.33 214.35 60.91 o 3 9 0 2982.72 3190.97 92.16 o 5 9 0 62.34 7.06 51.22 o 7 9 0 6695.37 6457.06 129.08 o 9 9 0 3463.87 3804.32 104.78 o 11 9 0 6055.85 6163.70 137.51 o 13 9 0 7810.51 7715.53 125.42 o 15 9 0 293.10 304.91 52.79 o 17 9 0 1253.79 1358.97 94.70 o 19 9 0 150.06 82.10 89.62 o 21 9 0 690.48 509.08 117.01 o 23 9 0 63.45 107.59 152.55 o 25 9 0 1594.98 1778.64 187.07 o 27 9 0 0.72 -171.59 171.59 o 29 9 0 26.42 -163.72 191.50 o 0 10 0 8942.33 10232.46 1098.61 o 2 10 0 8787.71 9541.38 215.13 o 4 10 0 2232.73 2510.12 87.73 o 6 10 0 1691.65 1593.15 70.67 o 8 10 0 1134.94 1464.75 101.37 o 10 10 0 913.81 960.44 67.24 o 12 10 0 181.97 293.93 47.46 o 14 10 0 450.45 574.66 54.84 o 16 10 0 576.09 616.84 72.32 o 18 10 0 18.47 89.10 86.15 o 20 10 0 1332.33 1096.96 153.31 o 22 10 0 302.00 74.40 145.52 o 24 10 0 1.32 -157.30 157.30 o 26 10 0 87.95 -65.83 169.55 o 28 10 0 26.70 -187.07 187.07 o 1 11 0 54724.89 53854.06 1007.35 o 3 11 0 73672.59 72142.82 1166.94 o 5 11 0 3229.14 3349.07 85.63 o 7 11 0 9775.62 9725.12 172.10 o 9 11 0 12385.26 12134.75 201.60 o 11 11 0 1290.42 1264.41 83.49 o 13 11 0 14810.06 14704.54 217.80 o 15 11 0 13156.78 13079.28 208.82 o 17 11 0 4542.91 5098.76 153.28 o 19 11 0 19071.26 20081.65 368.45 o 21 11 0 877.79 764.21 157.30 o 23 11 0 1762.93 1599.26 180.83 o 25 11 0 628.30 327.68 173.71 o 27 11 0 40.80 -159.10 181.55 o 0 12 0 64.74 -19.62 117.71 o 2 12 0 12267.30 12076.69 393.08 o 4 12 0 84413.58 88727.86 1234.33 o 6 12 0 21989.40 20881.71 341.11 o 8 12 0 1034.49 1241.81 74.14 o 10 12 0 6257.38 6285.08 143.06 o 12 12 0 5212.27 4960.64 131.53 o 14 12 0 1935.98 2193.10 128.68 o 16 12 0 10706.82 11151.50 218.87 o 18 12 0 4161.16 4269.82 171.00 o 20 12 0 1727.30 1799.37 169.55 o 22 12 0 2511.76 2554.66 195.38 o 24 12 0 1664.56 1579.79 198.21 o 26 12 0 3552.21 3510.76 236.76 o 28 12 0 1082.33 820.77 213.53 o 1 13 0 367.84 210.89 88.28 o 3 13 0 4637.40 5888.58 190.75 o 5 13 0 880.40 908.13 53.81 o 7 13 0 9317.39 9299.62 194.94 o 9 13 0 4333.54 4264.77 125.27 o 11 13 0 186.16 129.30 90.73 o 13 13 0 432.98 416.63 88.21 o 15 13 0 6356.98 7123.94 179.45 o 17 13 0 1370.21 1658.00 112.57 o 19 13 0 864.87 807.72 137.44 o 21 13 0 14.04 102.01 184.06 o 23 13 0 2942.38 2992.50 214.46 o 25 13 0 23.12 -93.41 179.49 o 27 13 0 108.35 -189.29 193.36 o 0 14 0 30577.72 29896.94 2285.50 o 2 14 0 1998.81 1993.79 127.52 o 4 14 0 3889.27 4122.30 120.69 o 6 14 0 2129.43 2032.18 103.27 o 8 14 0 2.42 -72.45 72.45 o 10 14 0 4792.56 4698.84 189.30 o 12 14 0 5506.43 5703.77 184.96 o 14 14 0 1509.17 1735.12 110.01 o 16 14 0 3394.83 3546.14 142.38 o 18 14 0 221.40 301.80 131.75 o 20 14 0 859.23 726.43 147.59 o 22 14 0 49.25 -167.59 167.59 o 24 14 0 411.89 295.62 185.12 o 26 14 0 937.22 614.25 230.90 o 1 15 0 1358.42 1158.48 117.71 o 3 15 0 1381.55 1219.58 122.32 o 5 15 0 83.83 -53.63 90.77 o 7 15 0 17053.76 16859.82 379.44 o 9 15 0 13612.00 13601.48 324.47 o 11 15 0 277.10 314.05 121.79 o 13 15 0 6217.99 6768.75 205.73 o 15 15 0 26867.94 28271.34 431.22 o 17 15 0 1270.29 1446.02 120.34 o 19 15 0 5369.48 5354.70 209.46 o 21 15 0 418.69 534.37 177.49 o 23 15 0 3778.73 4353.37 276.76 o 25 15 0 3810.25 3458.32 357.36 o 0 16 0 3519.66 3726.09 248.54 o 2 16 0 4.36 -105.17 105.17 o 4 16 0 3267.38 3313.11 161.12 o 6 16 0 6331.45 6230.13 229.36 o 8 16 0 65.36 -120.77 120.77 o 10 16 0 9401.32 9094.04 273.24 o 12 16 0 6219.04 6706.80 243.52 o 14 16 0 84.78 140.58 109.80 o 16 16 0 14263.71 14753.49 311.86 o 18 16 0 104.93 66.85 156.65 o 20 16 0 4533.67 4893.03 241.17 o 22 16 0 207.82 197.79 226.96 o 24 16 0 176.88 149.14 227.75 o 1 17 0 204.91 388.44 127.42 o 3 17 0 482.37 406.77 124.84 o 5 17 0 295.69 223.45 123.58 o 7 17 0 9388.57 9730.03 284.34 o 9 17 0 3096.88 3129.88 249.41 o 11 17 0 586.08 621.62 150.08 o 13 17 0 49.37 -112.68 112.68 o 15 17 0 477.46 331.64 122.18 o 17 17 0 9.56 129.43 136.54 o 19 17 0 4067.51 3575.00 246.35 o 21 17 0 777.36 1012.64 221.41 o 23 17 0 154.94 318.37 230.49 o 0 18 0 3549.91 3255.46 353.13 o 2 18 0 47.61 -122.32 122.32 o 4 18 0 5216.47 4851.29 266.17 o 6 18 0 193.71 -29.80 128.73 o 8 18 0 145.36 11.56 137.14 o 10 18 0 2814.13 2737.42 266.05 o 12 18 0 39.24 -155.19 155.19 o 14 18 0 2170.92 1956.49 193.85 o 16 18 0 943.32 718.98 136.58 o 18 18 0 178.42 117.73 171.68 o 20 18 0 2218.86 1854.45 206.56 o 22 18 0 1162.30 1131.64 241.99 o 1 19 0 4942.67 5070.89 217.15 o 3 19 0 73.98 -95.55 178.39 o 5 19 0 2912.15 2651.43 173.95 o 7 19 0 748.06 400.00 148.90 o 9 19 0 8423.93 8286.99 290.59 o 11 19 0 325.55 54.28 153.53 o 13 19 0 1476.93 1456.99 150.23 o 15 19 0 559.88 47.88 177.66 o 17 19 0 266.70 49.39 277.56 o 19 19 0 2589.49 2285.63 216.94 o 21 19 0 250.57 183.20 231.09 o 0 20 0 262.95 -9.81 284.46 o 2 20 0 2221.24 1720.13 166.32 o 4 20 0 1503.02 1274.61 166.32 o 6 20 0 1552.91 1575.73 171.45 o 8 20 0 250.94 222.27 150.85 o 10 20 0 313.53 360.86 163.72 o 12 20 0 3980.03 4045.94 189.38 o 14 20 0 272.85 -54.00 172.15 o 16 20 0 3129.42 3216.39 181.68 o 18 20 0 84.15 -129.27 184.09 o 20 20 0 293.56 514.65 206.51 o 1 21 0 1327.00 1423.62 181.22 o 3 21 0 15.65 -144.49 144.49 o 5 21 0 21.29 -146.64 146.64 o 7 21 0 2.74 -102.41 152.55 o 9 21 0 4.44 -78.95 156.19 o 11 21 0 318.56 483.08 143.35 o 13 21 0 138.54 -140.24 140.24 o 15 21 0 1176.69 858.79 155.57 o 17 21 0 305.97 185.72 226.53 o 19 21 0 160.40 58.55 201.24 o 0 22 0 1300.12 987.40 242.46 o 2 22 0 27.07 -151.80 151.80 o 4 22 0 441.32 245.07 164.13 o 6 22 0 1899.50 1504.16 236.00 o 8 22 0 173.63 -165.89 165.89 o 10 22 0 2186.87 1915.28 164.70 o 12 22 0 5567.75 5000.65 215.62 o 14 22 0 1033.03 741.83 163.53 o 16 22 0 172.26 -152.50 152.50 o 18 22 0 99.06 20.58 207.12 o 1 23 0 92.30 -239.67 302.98 o 3 23 0 11894.29 10742.30 474.83 o 5 23 0 516.95 115.36 178.44 o 7 23 0 2233.04 2027.80 217.26 o 9 23 0 1502.27 1218.98 160.90 o 11 23 0 30.67 37.86 146.87 o 13 23 0 4382.68 4515.98 414.52 o 15 23 0 1570.13 1134.32 177.68 o 17 23 0 497.45 175.13 209.01 o 0 24 0 2979.08 2408.86 290.32 o 2 24 0 61.56 17.21 192.55 o 4 24 0 102.97 -171.45 171.45 o 6 24 0 235.61 53.62 178.87 o 8 24 0 113.17 -29.16 179.68 o 10 24 0 531.36 340.15 192.16 o 12 24 0 455.29 292.24 159.52 o 14 24 0 495.88 527.82 168.53 o 1 25 0 3.60 -160.03 181.22 o 3 25 0 43.87 -24.38 180.83 o 5 25 0 652.53 353.38 191.09 o 7 25 0 11.63 -179.40 179.40 o 9 25 0 452.71 -142.34 189.08 o 11 25 0 222.17 181.16 240.69 o 0 26 0 233.45 -78.47 270.24 o 2 26 0 32.83 -188.69 188.69 o 4 26 0 61.39 -190.75 190.75 o 6 26 0 4198.62 3565.55 354.89 o 8 26 0 71.21 -98.35 280.33 o 1 27 0 926.85 598.24 213.22 o 3 27 0 463.51 302.13 205.64 o 5 27 0 90.64 70.27 203.06 o -31 1 1 12.10 -164.87 164.87 o -29 1 1 65.31 212.45 129.21 o -27 1 1 1034.63 1130.22 125.56 o -25 1 1 45.49 -1.90 103.72 o -23 1 1 3435.92 3319.75 130.35 o -21 1 1 8579.50 8252.38 179.44 o -19 1 1 931.34 768.32 58.18 o -17 1 1 20565.11 19276.96 238.03 o -15 1 1 21.28 -47.92 47.92 o -13 1 1 1780.87 1642.04 53.96 o -11 1 1 69.18 39.01 35.19 o -9 1 1 5204.04 5187.85 95.79 o -7 1 1 14199.33 14926.75 438.15 o -5 1 1 5195.67 5545.49 109.41 o -3 1 1 1197.90 1143.26 78.47 o 3 1 1 858.51 781.71 28.55 o 5 1 1 8658.69 8312.53 121.63 o 7 1 1 13927.93 14820.04 199.01 o 9 1 1 1130.70 1230.76 50.33 o 11 1 1 21467.11 19717.31 270.45 o 13 1 1 3517.17 3587.51 101.38 o 15 1 1 4382.14 4017.11 111.86 o 17 1 1 9885.30 9561.53 182.05 o 19 1 1 2267.44 2279.80 105.45 o 21 1 1 4086.79 4397.67 141.26 o 23 1 1 1172.61 1131.05 112.03 o 25 1 1 47.65 51.47 112.03 o 27 1 1 3036.08 3209.96 159.74 o 29 1 1 10259.78 9567.83 323.16 o -32 2 1 632.44 872.84 184.36 o -30 2 1 989.06 1056.61 175.89 o -28 2 1 958.73 1049.39 132.84 o -26 2 1 836.21 917.26 121.86 o -24 2 1 2059.59 2120.59 122.23 o -22 2 1 1842.46 1944.23 111.36 o -20 2 1 12475.85 11844.30 227.39 o -18 2 1 15638.83 15283.08 226.16 o -16 2 1 6093.75 5605.53 124.20 o -14 2 1 23094.77 21616.46 276.03 o -12 2 1 16416.55 15287.12 199.89 o -10 2 1 8579.23 8003.04 115.49 o -8 2 1 27301.70 27154.68 523.48 o -6 2 1 8179.70 8201.04 172.73 o -4 2 1 115561.28 106960.94 1945.32 o -2 2 1 86133.98 83338.88 2726.91 o 0 2 1 32953.98 34390.47 1000.52 o 2 2 1 122926.20 122576.41 1465.74 o 4 2 1 52.74 -30.84 30.84 o 6 2 1 60.81 -2.20 36.56 o 8 2 1 5264.13 4734.41 134.05 o 10 2 1 15184.04 15100.76 254.43 o 12 2 1 15856.93 15642.92 261.37 o 14 2 1 18575.87 18142.47 262.96 o 16 2 1 288.90 425.15 68.30 o 18 2 1 27935.71 27893.82 392.16 o 20 2 1 862.25 876.53 93.01 o 22 2 1 3561.76 3663.76 134.00 o 24 2 1 2745.14 2770.77 136.88 o 26 2 1 319.15 401.29 120.98 o 28 2 1 3548.77 3649.30 169.64 o 30 2 1 2808.68 2988.72 255.89 o -31 3 1 250.70 77.84 174.91 o -29 3 1 893.53 815.07 150.78 o -27 3 1 2469.72 2665.88 141.89 o -25 3 1 728.40 782.06 112.77 o -23 3 1 1051.05 1007.50 128.26 o -21 3 1 846.47 883.17 99.38 o -19 3 1 1055.75 1131.92 64.34 o -17 3 1 6872.10 6761.91 116.16 o -15 3 1 19471.36 19387.70 234.22 o -13 3 1 14826.71 13858.41 187.73 o -11 3 1 18909.83 18197.02 275.09 o -9 3 1 12745.05 12894.78 168.05 o -7 3 1 12390.96 13405.17 221.01 o -5 3 1 128.50 261.12 37.33 o -3 3 1 5471.34 5041.58 90.95 o -1 3 1 4328.43 4052.64 80.62 o 1 3 1 21837.81 21969.32 236.09 o 3 3 1 33550.21 34360.47 391.11 o 5 3 1 67181.75 62328.60 698.48 o 7 3 1 13.49 53.95 29.54 o 9 3 1 1408.20 1938.09 56.18 o 11 3 1 19030.71 19438.87 269.55 o 13 3 1 468.77 507.15 57.36 o 15 3 1 4569.57 4119.46 116.36 o 17 3 1 3004.67 3037.29 105.82 o 19 3 1 11805.07 12512.64 225.75 o 21 3 1 3350.19 3323.28 150.61 o 23 3 1 743.44 770.23 108.81 o 25 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